CN103706142A - Extracting and collecting device and application thereof - Google Patents
Extracting and collecting device and application thereof Download PDFInfo
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- CN103706142A CN103706142A CN201210370550.3A CN201210370550A CN103706142A CN 103706142 A CN103706142 A CN 103706142A CN 201210370550 A CN201210370550 A CN 201210370550A CN 103706142 A CN103706142 A CN 103706142A
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Abstract
The invention discloses an extracting and collecting device, and specifically relates to an extracting and collecting device for volatile components. The extracting and collecting device comprises an extracting tank (1), an extracting tank outlet (2), a safety valve (3), a pipeline (4), a liquid storage tank (6), an interlayer (11), an exhaust outlet (7), a condensate water inlet (8) and a condensate water outlet (5) and a liquid draining device (8). The extracting and collecting device has the beneficial effects that the structure is simple; operations are convenient; the liquid storage tank has the collecting and condensing functions; use amount of the condensate water is significantly reduced; and collection efficiency of the volatile components can be increased.
Description
Technical field
The invention discloses a kind of extraction gathering-device, be specifically related to a kind of volatile ingredient and extract gathering-device and application thereof.
Background technology
Volatile ingredient extracting method has decocting method, steam distillation, CO
2supercritical fluid extraction, organic solvent extraction method etc., wherein the extraction effect of steam distillation is best.During hydrodistillation volatile ingredient, because of steam, to carry energy high, the volatile ingredient that condensation in time distills out as condenser, and part volatile ingredient is discharged with tail gas, causes extracting yield not high.
Summary of the invention
It is not enough that the present invention has overcome existing volatile ingredient extraction and separation technology, simplify device, by traditional device for extracting volatility component, condensing plant, collecting device optimum organization, change on the one hand heat exchange method, by the gas-solid heat exchange directly being contacted with cryosurface by retort gas, after the water and the heat exchange of subsequent condensation liquid that becomes retort gas first and in receiver, water in receiver and subsequent condensation liquid contact with cryosurface again, heat exchange method is gas-liquid-solid heat exchange, be conducive to retort gas condensation and collection, improve heat exchanger effectiveness, reduce condensed water consumption.Solved on the other hand volatile ingredient and with tail gas, discharged because of the timely condensation in end the loss causing, improved volatile ingredient and extract yield.
For solving the problems of the technologies described above, the present invention by the following technical solutions:
An extraction gathering-device, comprises extraction element, condensation gathering-device.Extraction element comprises extractor 1, safety valve 3, pipeline 4, and condensation gathering-device comprises receiver 6, interlayer 11, condensing water inlet 8, condensation-water drain 5, tail gas outlet 7, pumping equipment 9.
At extractor 1 top, safety valve 3 is housed, when extraction is complete, opens the safety-valve 3, gas is discharged by safety valve, prevents that the distillate suck-back of collecting in receiver 6 is to extractor 1.
The entrance of pipeline 4 is connected with extractor outlet 2, and the outlet 10 of pipeline 4 passes into the bottom of receiver 6.The outlet 10 of pipeline 4, is 0 ~ 90 degree angle, preferably 45 ~ 90 degree with horizontal line down.
Before extraction, in receiver 6, add certain water gaging, water level is for exceeding pipe outlet 10 level height 5-10cm, and the outer wall of receiver 6 is with the interlayer 11 that can lead to condensed water, and condensed water enters from condensing water inlet 8, from condensation-water drain 5.
To better implement the present invention, 2-10 receiver 6 can be through being connected in series 2-10 with pipeline 15, and the entrance of pipeline 15 is connected with previous receiver outlet, and the outlet of pipeline 15 passes into the bottom of Next receiver, is connected in series successively.Each of pipeline 15 goes out mouth down, is 0 ~ 90 degree angle, preferably 45 ~ 90 degree angles with horizontal line.Before extracting, in each receiver, tank enters suitable quantity of water, exceeds the level height 5-10cm of pipe outlet, can further reduce the loss of volatile ingredient, improves and extracts yield.
Another object of the present invention is to provide a kind of extracting method of volatile ingredient, and the extracting method of volatile ingredient provided by the present invention is to utilize device of the present invention to decoct volatile component of plant or steam distillation extraction; The method that described decoction or steam distillation extract is to add suitable quantity of water in device receiver of the present invention, and water level exceeds pipe outlet 10 level height 5-10cm and opens condensed water, decocts or distills extraction.
The invention has the beneficial effects as follows: simple in structure, easy to operate, receiver possesses condensation and collecting function, significantly reduces condensed water consumption, improve volatile ingredient collection rate.
Accompanying drawing explanation
Fig. 1 is the structural representation of the embodiment of the present invention one
Fig. 2 is the structural representation of the embodiment of the present invention two
Fig. 3 is extraction, condensation, the gathering-device schematic diagram of traditional handicraft
The specific embodiment
Below in conjunction with accompanying drawing, the present invention is further elaborated:
Embodiment mono-: as shown in Figure 1,
Figure 1 shows that a kind of extraction gathering-device provided by the invention, comprise extraction element, condensation gathering-device.Extraction element comprises extractor 1, safety valve 3, pipeline 4, and condensation gathering-device comprises receiver 6, interlayer 11, condensing water inlet 8, condensation-water drain 5, tail gas outlet 7, pumping equipment 9.
At extractor 1 top, safety valve 3 is housed, when extraction is complete, opens the safety-valve 3, gas is discharged by safety valve, to prevent that the distillate suck-back of collecting in receiver 6 is to extractor 1.
The entrance of pipeline 4 is connected with extractor outlet 2, and the outlet 10 of pipeline 4 passes into the bottom of receiver 6.The outlet 10 of pipeline 4, is 75 degree angles with horizontal line down.
Before extraction, in receiver 6, add certain water gaging, water level is for exceeding pipe outlet 10 level height 5-10cm, and the outer wall of receiver 6 is with the interlayer 11 that can lead to condensed water, and condensed water enters from condensing water inlet 8, from condensation-water drain 5, discharges.
Embodiment bis-: as shown in Figure 2,
Figure 2 shows that a kind of extraction gathering-device provided by the invention, comprise extraction element, condensation gathering-device.Extraction element comprises extractor 1, safety valve 3, pipeline 4, pipeline 15, and condensation gathering-device comprises receiver 6, receiver 16, receiver 17, interlayer 11, condensing water inlet 8, condensation-water drain 5, tail gas outlet 7, pumping equipment 9, pumping equipment 91, pumping equipment 92.
The outlet 102 of the outlet 10 of pipeline 4, the outlet 101 of pipeline 15, pipeline 15, is 80 degree angles with horizontal line down.
Embodiment tri-: with the extraction of paeonol in Cortex Moutan, collect to illustrate apparatus of the present invention and using method and effect
By moutan bark 20.0kg, be placed on described in embodiment 2 and extract in the extractor 1 of gathering-device, receiver 6,16,17 add suitable quantity of water, and water level exceeds pipe outlet 10,101,102 level height 5cm, opens water vapour and condensed water, and distillation is extracted, and collects.Steam pressure 0.10-0.12Mpa, condensate flow is 1.0 tons/hour.
Distillation finishes rear collection distillate 200kg.
Distillate is placed 4 ℃ of refrigerating chambers and is carried out Paeonol crystallization, obtain altogether Paeonol crystal 0.42kg, calculate Paeonol yield, formula is Paeonol yield=(Paeonol crystal/moutan bark weight) * 100%, with device in embodiment 2, extract paeonol in Cortex Moutan, its yield is 2.10%
Adopt traditional volatile ingredient to extract gathering-device and moutan bark is carried out to the contrast experiment of steam distillation.
Get moutan bark 20.0kg and put into the extractor 1 shown in Fig. 3, open water vapour, the condensed water of open cold condenser 5, distillation, extracts, and collects.Steam pressure 0.10-0.12Mpa, condensate flow is 1.5 tons/hour.
Distillation finishes rear collection distillate 200.0kg
Distillate is placed 4 ℃ of refrigerating chambers and is carried out Paeonol crystallization, obtain altogether Paeonol crystal 0.35kg, calculate Paeonol yield, formula is Paeonol yield=(Paeonol crystal/moutan bark weight) * 100%, with device in embodiment 2, extract paeonol in Cortex Moutan, its yield is 1.75%.
Claims (7)
1. an extraction gathering-device, comprises extraction element, condensation gathering-device; It is characterized in that: described extraction element comprises extractor (1), safety valve (3), pipeline (4), described condensation gathering-device comprises receiver (6), interlayer (11), condensing water inlet (8), condensation-water drain (5), tail gas outlet (7), pumping equipment (9), extractor (1) is connected by pipeline (4) with receiver (6), the entrance of pipeline (4) is connected with extractor outlet (2), and the outlet (10) of pipeline (4) passes into the bottom of receiver (6).
2. extraction gathering-device according to claim 1, is characterized in that: the outlet (10) of pipeline (4), is 0 ~ 90 degree angle with horizontal line down.
3. extraction gathering-device according to claim 2, is characterized in that: the outlet (10) of pipeline (4), is 45 ~ 90 degree angles with horizontal line down.
4. according to the arbitrary described extraction gathering-device of claim 1-3, it is characterized in that: 2-10 receiver (6) can be connected in series through pipeline (15).
5. extraction gathering-device according to claim 4, is characterized in that: pipeline (15) go out mouth down, be 0 ~ 90 degree angle with horizontal line.
6. extraction gathering-device according to claim 5, is characterized in that: pipeline (15) go out mouth down, be 45 ~ 90 degree angles with horizontal line.
7. extracting a method of collecting volatile ingredient, is to utilize device described in claim 1-6 any one to decoct volatile component of plant or steam distillation extracts; The method that described decoction or steam distillation extract is in the device receiver described in any one in claim 1-6, to add suitable quantity of water, and water level exceeds pipe outlet (10) level height 5-10cm and opens condensed water, decocts or distills extraction.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210370550.3A CN103706142B (en) | 2012-09-29 | 2012-09-29 | A kind of extraction collection device and application thereof |
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| CN201210370550.3A CN103706142B (en) | 2012-09-29 | 2012-09-29 | A kind of extraction collection device and application thereof |
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| CN103706142B CN103706142B (en) | 2016-12-21 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107625437A (en) * | 2017-11-03 | 2018-01-26 | 珠海格力电器股份有限公司 | Electric cooker and distillation method thereof |
| CN108261797A (en) * | 2016-12-31 | 2018-07-10 | 九芝堂股份有限公司 | A kind of distillation automaton and its application |
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| US5178734A (en) * | 1990-02-16 | 1993-01-12 | International Water Technologies, Inc. | Water distilling apparatus with vertically stacked components |
| CN2869023Y (en) * | 2005-12-29 | 2007-02-14 | 华南师范大学 | Plant volatile oil extractor |
| CN201692682U (en) * | 2010-06-08 | 2011-01-05 | 湖北中烟工业有限责任公司 | Novel volatile oil extraction equipment |
| CN102512839A (en) * | 2011-12-24 | 2012-06-27 | 吉安市林业科学研究所 | Natural d-borneol extraction equipment |
| CN202892957U (en) * | 2012-09-29 | 2013-04-24 | 九芝堂股份有限公司 | Extraction and collection device |
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Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US4334962A (en) * | 1977-12-28 | 1982-06-15 | Fmc Corporation | Apparatus for stripping immiscible materials |
| US5178734A (en) * | 1990-02-16 | 1993-01-12 | International Water Technologies, Inc. | Water distilling apparatus with vertically stacked components |
| CN2869023Y (en) * | 2005-12-29 | 2007-02-14 | 华南师范大学 | Plant volatile oil extractor |
| CN201692682U (en) * | 2010-06-08 | 2011-01-05 | 湖北中烟工业有限责任公司 | Novel volatile oil extraction equipment |
| CN102512839A (en) * | 2011-12-24 | 2012-06-27 | 吉安市林业科学研究所 | Natural d-borneol extraction equipment |
| CN202892957U (en) * | 2012-09-29 | 2013-04-24 | 九芝堂股份有限公司 | Extraction and collection device |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108261797A (en) * | 2016-12-31 | 2018-07-10 | 九芝堂股份有限公司 | A kind of distillation automaton and its application |
| CN107625437A (en) * | 2017-11-03 | 2018-01-26 | 珠海格力电器股份有限公司 | Electric cooker and distillation method thereof |
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| CN103706142B (en) | 2016-12-21 |
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Address after: 410205 Changsha high tech Zone, Tongzi, west slope road, No. 339, No. Applicant after: Jiuzhitang Co., Ltd. Address before: 410008 Hunan province Changsha Kaifu District, Furong Road No. 129 Applicant before: Jiuzhitang Co., Ltd. |
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