CN105237358B - Natural borneol extraction system and method capable of increasing yield - Google Patents
Natural borneol extraction system and method capable of increasing yield Download PDFInfo
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- CN105237358B CN105237358B CN201510761989.2A CN201510761989A CN105237358B CN 105237358 B CN105237358 B CN 105237358B CN 201510761989 A CN201510761989 A CN 201510761989A CN 105237358 B CN105237358 B CN 105237358B
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
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Abstract
The invention provides a natural borneol extraction system capable of increasing the yield. The natural borneol extraction system aims to solve the technical problem that an existing extraction system is low in yield at present. The system comprises a distillatory kettle and a condenser, wherein a steam distributor is arranged in the bottom of the distillatory kettle, and the condenser is correspondingly communicated with a steam outlet of the distillatory kettle. A steam inlet of the steam distributor in the distillatory kettle is correspondingly communicated with a saturated steam generator through a saturated steam pipeline. The natural borneol extraction system further comprises a condensate water temporary storage barrel used for recycling condensate water condensed by the condenser. The condensate water temporary storage barrel is further communicated with the interior of the distillatory kettle through a water pump, so that the condensate water collected in the condensate water temporary storage barrel is conveyed into the distillatory kettle through the water pump. By the adoption of the system and method, there is no need to improve an existing cooling system any more in implementation, automatic improvement of a steam flow control system and method is not needed either, and therefore the improvement cost of enterprises is reduced.
Description
Technical field
The present invention relates to natural Broneolum Syntheticum extractive technique field, more particularly to a kind of natural Broneolum Syntheticum extraction for improving recovery rate
System.
Background technology
Used as a kind of Chinese medicine, which is white crystalline powder or flaky crystal body to natural Broneolum Syntheticum, gas delicate fragrance, acrid in the mouth, cool, is
The fresh branch of canella Borneolum Syntheticum Camphor tree, leaf is extracted is processed into；Which is distributed mainly on south and southwestern each provinces and regions, with having one's ideas straightened out
The effect of refreshment, clearing away heat to alleviate pain, it is usually used in calentura coma, faints from fear, apoplexy syncope due to accumulation of phlegm, bstruction of the circulation of vital energy is fainted cruelly, middle evil is gone into a coma, obstruction of qi in the chest and cardialgia,
Conjunctival congestion, aphtha, laryngopharynx swelling and pain, auditory meatus are suppurated.The found Borneolum Syntheticum Lignum cinnamomi camphorae of Ji'an City woods section in last century the eighties Jiangxi Province
Containing 0.5%～3% natural Broneolum Syntheticum and Borneolum Syntheticum oil in branch and leaf, and propose natural Broneolum Syntheticum and Borneolum Syntheticum oil from Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf
The extracting method of the method for middle extraction, the natural Broneolum Syntheticum and Borneolum Syntheticum oil is mainly at ambient pressure, using the method for steam distillation.
Specially：
1st, the Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf of felling are uniformly mated formation in air-distillation pot, cover pot cover, and by boiler and
Condenser is communicated as one.
2nd, lead to cooling water cooling in condenser chuck.
3rd, the steam in boiler is passed through the bottom of boiler, and Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf are distilled.
In aforesaid operations, which passes through manually to control steam pressure（Standard does not leak vapour, water seal height 20 for boiler water seal
Centimetre）And steam flow（Gone out by observing the exhaust gas conditions and condensed water of the air vent on natural Broneolum Syntheticum and Borneolum Syntheticum oil collecting vessel
Mouthful condensate flow controlling.Using the size of the steam pressure on the jet chimney behind control and regulation valve come controlling stream
Amount, completely with control vapour personnel experience controlling.Through actual measure, steam flow is controlled in 120～200 ㎏/hour
In the range of）.After air in distilling apparatus are drained, distillation time is kept for 1 hour, and distillation terminates.In whole still-process,
Steam control valve is adjusted at any time, steam pressure and steam flow in boiler is maintained at and oneself is thought suitable scope
It is interior.
4th, after distillation terminates, the Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf in boiler are taken out, new Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf is reloaded, is entered
The distillation of next pot of row.
5th, after 4～8 pots of continuous still, condenser cover is opened, the natural ice on condenser inner wall will be condensed in scoop
Under slice bar, allow it to fall in natural Broneolum Syntheticum collecting vessel, the natural Broneolum Syntheticum in collecting vessel and Borneolum Syntheticum oil are pulled out with strainer.This all one's life
Produce batch to terminate, then proceed to the production of next batch.
6th, the natural Broneolum Syntheticum and Borneolum Syntheticum oil pulled out is centrifuged in being put into centrifuge, is come natural Broneolum Syntheticum and Borneolum Syntheticum separating of oil.
They are each entered into rear operation and are processed.
And found by aforesaid operations, in the case where the Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf to same weight are extracted, using existing
Its total output of system is little, and the recovery rate that every kilogram of Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf extract natural Broneolum Syntheticum is low, and in its production operation it is artificial because
Impact of the element to natural Broneolum Syntheticum recovery rate is very big, meanwhile, the condensed condensed water of condensed device is drained directly as waste water, causes
The problem of environmental pollution.
The content of the invention
It is an object of the invention to overcome the deficiencies in the prior art, reality need is adapted to, there is provided one kind can improve recovery rate
Natural Broneolum Syntheticum extraction system, to solve that currently existing extraction system recovery rate is low, yield is little, anthropic factor affect big, pollution
The technical problem of environment.
In order to realize the purpose of the present invention, the technical solution adopted in the present invention is：
A kind of natural Broneolum Syntheticum extraction system for improving recovery rate of design, it includes being provided with steam distributor in its bottom
Boiler and the condenser of connection corresponding with the steam (vapor) outlet of the boiler, the steam distributor in the boiler enter vapour
Mouth is by the connection corresponding with saturated vapor producer of saturated vapor pipeline；It is also including one for condensed by condenser
The condensed water temporary storage barrel reclaimed by condensed water；The condensed water temporary storage barrel is also connected with the inside of the boiler by water pump
It is logical, the condensed water collected in condensed water temporary storage barrel is delivered in boiler by the water pump.
Further, also including the product collecting vessel which is provided with bung, the outlet of the condenser is collected with the product
The inlet communication of bucket；Be additionally provided with the middle part of the product collecting vessel one for by the product collecting vessel condensed water discharge
Outlet, and a vertically disposed pipeline is provided with the product collecting vessel, the upper end of the pipeline is connected with the outlet, should
The lower end of pipeline is arranged at drum head；The outlet connected with the pipeline upper end is via a drainage element and the condensed water temporary storage barrel
Correspondence is connected；The drainage element is without blocking guiding gutter；The lower U-lag for including that without blocking guiding gutter its section takes the shape of the letter U
Main body and upper U-lag groove lid, the upper U-lag groove lid are buckled in the lower U-lag main body, by the passage for being formed between the two
Constitute condensation flow circulation passage.
Further, it is further opened with condensing water inlet in the bottom of the boiler；The condensed water temporary storage barrel passes through water
Pump connection corresponding with the condensation water inlet.
Further, saturated vapor pipeline connection also corresponding with the condensation water inlet, and in the saturation water
The second steam control valve is additionally provided with pipeline between jet chimney and the condensation water inlet.
Further, the saturated vapor pipeline that the steam distributor in the boiler is connected with steam generating stove
On be additionally provided with the first steam control valve.
Further, the first pressure tap is additionally provided with the inwall of the boiler middle and lower part, first pressure tap passes through
First surveys pressure control valve connection corresponding with minute-pressure manometer.
Further, the second pressure measurement is offered on the saturated vapor pipeline of the first steam control valve steam output end
Mouthful, second pressure tap surveys pressure control valve also connection corresponding with the minute-pressure manometer by second.
Further, pressure gauge is additionally provided with the saturated vapor pipeline of the first steam control valve admission end.
Further, the minute-pressure manometer include filling in which liquid, and the setting that takes the shape of the letter U transparent tube, and will
The fixed plate that the transparent tube is fixed；And scale is additionally provided with the vertical direction of the transparent tube in the fixed plate
Line；One end of the transparent tube pass through tee pipe fitting and described first survey pressure control valve and second survey pressure control valve it is corresponding connect,
Its another end opening.
Further, it is additionally provided with the liquid in by the boiler in the condensed water entrance of the distillation pot bottom to discharge
Discharging tube, and be additionally provided with discharge opeing control valve on the discharging tube.
Further, by the method for the system extraction natural Broneolum Syntheticum it is：
The first step, Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf is put in boiler and is distilled, and is distilled the steam for producing and is entered condensation in condenser,
Collect the condensed water that condensed device is produced；
The condensed water of collection is carried out distillation process by second step, and the natural Broneolum Syntheticum in condensed water is separated out with steam；
3rd step：The steam that generation is distilled in second step is entered in condenser and is condensed.
Further, it is specifically that above-mentioned to state in the first step, it is temporary that the condensed water produced by condenser is into condensed water
Deposit what is be collected in bucket；
After in the first step be collected condensed water in condensed water temporary storage barrel, also include to distill in boiler
Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf afterwards take out, the step of the liquid in boiler is discharged；
The second step is specially：New Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf are put in boiler, will be cold in condensed water temporary storage barrel
Solidifying water is sent in boiler by water pump, continues to distill the condensed water in boiler and the new Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf for loading
Process；
3rd step is specially：The steam that generation is distilled in pot condensation in condenser will evaporated in second step；
Also include the 4th step：The first step, second step, the 3rd step described in repetitive operation；
5th step：Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf after distilling in boiler are taken out, and the liquid in boiler is discharged；Simultaneously
The natural Broneolum Syntheticum formed on condenser inner wall is collected.
Further, after sent in boiler by the condensed water in condensed water temporary storage barrel, described second steams
Vapour control valve is opened, and now, steam is entered in the boiler via condensation water inlet.
The beneficial effects of the present invention is：
1. the present invention carry out in boiler distillation process by sending into as the condensed water of waste water originally, reclaims therein
Natural Broneolum Syntheticum, and then the recovery rate of natural Broneolum Syntheticum can be improved（Extraction ratio）And productivity effect.
2. the present invention avoids natural Broneolum Syntheticum from condensing in cause on conveying pipeline inner wall pipe without blocking guiding gutter in use
The generation of road clogging, to ensure the normal operation of the system.
3. the present invention also has other beneficial effects, will propose in the lump in embodiment.
Description of the drawings
Primary structure schematic diagrams of the Fig. 1 for the system；
Fig. 2 be the system in without blocking guiding gutter primary structure schematic diagram；
Fig. 3 is the minute-pressure manometer primary structure schematic diagram in the system；
In figure：1. saturated vapor producer;2. pressure gauge;3. saturated vapor pipeline;4. tee pipe fitting;5. first steams
Vapour controls valve;6. second pressure control valve is surveyed;7. first pressure control valve is surveyed;8. minute-pressure manometer;9. the first pressure tap;10. second
Pressure tap;11. second steam control valves;12. condensation water inlets;13. boilers;14. water pumps;15. condensed water temporary storage barrels;16.
Without blocking guiding gutter;17. condensers;Pipeline between 18. boilers and condenser;19. cover plates;20.U shape groove bodies;21. is saturating
Bright pipe;22. fixed plates;23. graduation marks;24. discharge opeing control valves;25. discharging tubes；26. product collecting vessels；27. pipelines.
Specific embodiment
The present invention is further described with reference to the accompanying drawings and examples：
The present inventor is having found that in long-term production practices and repeatedly experimental demonstration existing system and method are main
There is problems with：
In the prior art, condensed water is treated as waste water and drains, and as natural Broneolum Syntheticum and Borneolum Syntheticum oil have unique gas
Taste, and its abnormal smells from the patient is very heavy, and certain pollution will be caused to working environment after its discharge；And inventor is in long-term production practices
The middle water vapour for finding that condensed water is separated out can be condensed on wall after being contacted with wall repeatedly and have crystal, meanwhile, discharge condensation
The pipeline of water is also often blocked；Inventor this will tamper in the crystal and pipeline that condense on wall take out after and it is right
Which is analyzed；Inventor is natural Broneolum Syntheticum the crystal is found after long-term analysis unexpectedly, and this discovery is to the present invention
Very shock for people, because before this, expert in the art is free from natural Broneolum Syntheticum in unanimously thinking condensed water,
Even if or being also micro containing which；For this purpose, the present inventor by being further analyzed discovery to condensed water, its condensed water
In be not without the presence of natural Broneolum Syntheticum, but contain substantial amounts of natural Broneolum Syntheticum, therefore, the crystalline substance of condensation is just had on wall
Body.Therefore, condensed water is drained very unfortunately as waste water in prior art, also result in serious waste, while also causing
The recovery rate of existing system is low.
For this purpose, inventor is had found after the condensed water to reclaiming in the lab experimental analysiss：When water temperature is 53 DEG C,
Natural Broneolum Syntheticum recovery rate 0.126% in condensed water；When water temperature is 55 DEG C, natural Broneolum Syntheticum recovery rate 0.128% in condensed water；Work as water
When temperature is 58 DEG C, natural Broneolum Syntheticum recovery rate 0.130% in condensed water；When water temperature is 65 DEG C, natural Broneolum Syntheticum recovery rate in condensed water
0.135%.This explanation：1. water temperature is higher, and the natural Broneolum Syntheticum being dissolved in water is more.2. condensation water quantity is more, and water temperature is higher, its
The natural Broneolum Syntheticum wasted in distillation is more, therefore the natural Broneolum Syntheticum in condensed water is more.And in the document about natural Broneolum Syntheticum
In say in this way：Natural Broneolum Syntheticum is slightly soluble in water.Found by analysis, above-mentioned conclusion should more refer to that natural Broneolum Syntheticum is slightly soluble in cold water,
And practical situation should be：Natural Broneolum Syntheticum can be dissolved in water, and the higher meltage of water temperature is more.In the side using vapor distillation
When method extracts natural Broneolum Syntheticum, the temperature of condensed water is necessarily higher than the temperature of cooling water, and condenser cooling effect is poorer, then condensed water
Temperature it is higher than the temperature of cooling water must be more.In actual production process, in the condensed water after distillation, necessarily contain natural ice
Piece, and condensate temperature is higher, and natural Broneolum Syntheticum amount therein is more.
Inventor can draw to draw a conclusion in the analysis to more than and after testing：Natural Broneolum Syntheticum in Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf and
On the premise of Borneolum Syntheticum oil is all distilled, how many decision natural Broneolum Syntheticums and Borneolum Syntheticum of the amount of the natural Broneolum Syntheticum being lost in condensed water
The size of the recovery rate of oil；Therefore reduce the content of natural Broneolum Syntheticum in condensed water（The temperature of condensed water is reduced）Or in condensed water
Natural Broneolum Syntheticum carry out reclaiming and can significantly increase the production efficiency and product recovery rate of enterprise；But if specially purchase new
Good cooling results condensing plant reducing the temperature of condensed water, reach the purpose for reducing natural Broneolum Syntheticum loss, then enterprise
Input is too big, can not thoroughly solve the problems, such as that natural Broneolum Syntheticum is lost in condensed water and loses.Therefore, inventor is to existing water
Steam distillation device is transformed, and in the case where its existing apparatus and equipment is made full use of, be increased with a small amount of investment
A set of condensate water recovery device, the natural Broneolum Syntheticum in condensed water is reclaimed completely, has reached maximum raising output, is reduced
The purpose of cost.
For this current inventor provides a kind of natural Broneolum Syntheticum extraction system and method for improving recovery rate；Which passes through following
Embodiment is realized：
Embodiment 1：A kind of natural Broneolum Syntheticum extraction system for improving recovery rate, referring to Fig. 1 to Fig. 3；It includes its bottom
Inside be provided with steam distributor boiler 13, and connection corresponding with the steam (vapor) outlet of the boiler 13 condenser 17, should
The steam (vapor) outlet of condenser 17 and boiler 13 is connected by the pipeline 18 between boiler and condenser；Meanwhile, the boiler
Steam distributor air intake in 13 connects by saturated vapor pipeline 3 is corresponding with the steam (vapor) outlet of saturated vapor producer 1
It is logical；Further, in place of the key Design of the system it also including one for by 17 condensed condensing hot air furnace of condenser
Condensed water temporary storage barrel 15.
It also includes the product collecting vessel 26 which is provided with bung, the outlet of the condenser 17 and the product collecting vessel 26
Import is directly connected；One is additionally provided with for the condensed water in the product collecting vessel is discharged at the middle part of the product collecting vessel 26
Outlet, and be provided with a vertically disposed pipeline 27, the upper end of the pipeline 27 and the water outlet in the product collecting vessel 26
Mouth connection, the lower end of the pipeline is arranged at drum head；The outlet connected with the pipeline upper end is cold with described via a drainage element
The solidifying correspondence of water temporary storage barrel 15 is connected；And above-described drainage element is without blocking guiding gutter 16；Without blocking guiding gutter, it includes for this
Lower U-lag main body 20 and upper U-lag groove lid 19 that its section takes the shape of the letter U, the upper U-lag groove lid 19 are buckled in the lower U-lag
In main body 20, the passage for being formed between the two is constituted into condensation flow circulation passage.This in use may be used without blocking guiding gutter 16
To avoid the crystal that condensed water is separated out from blocking the generation of condensation flow circulation passage phenomenon, meanwhile, even if without blocking guiding gutter 16
Inwall on separate out crystal, after only need to take out upper U-lag groove lid 19, is removed, while from without blocking guiding gutter 16
The crystal of an interior removing part also for product.
In the application, the steam containing natural Broneolum Syntheticum and Borneolum Syntheticum oil that Jing boilers are steamed is entered in condenser and is condensed,
During this, its most of natural Broneolum Syntheticum is condensed on the inwall of condenser, the crystal of its Borneolum Syntheticum oil and part natural Broneolum Syntheticum with
Condensed water containing natural Broneolum Syntheticum is flowed in product collecting vessel together；Condensed water, natural Broneolum Syntheticum in inflow product collecting vessel 26
With Borneolum Syntheticum oil due to the difference of density, its natural Broneolum Syntheticum, Borneolum Syntheticum oil density it is little and be located at the top of condensed water, and condensed water level
In natural Broneolum Syntheticum and the lower section of Borneolum Syntheticum oil, therefore the product collecting vessel by the design, its condensed water can be from product collecting vessel
Bottom be expelled in condensed water temporary storage barrel 15 by pipeline 27 and stored, again will not be by the natural ice on the condensed water water surface
Piece, Borneolum Syntheticum oil discharge product collecting vessel.
The condensed water temporary storage barrel 15 of the design is also connected with inside the boiler 13 by water pump 14, with by institute
State water pump 14 condensed water collected in condensed water temporary storage barrel 15 is delivered in boiler 13；Specifically, in the boiler 13
Bottom offer condensation water inlet 12；Water inlet 12 is corresponding connects with the condensation by water pump 14 for the condensed water temporary storage barrel 15
It is logical.Meanwhile, the discharge opeing that the liquid in by the boiler is discharged is additionally provided with the condensed water entrance 12 of the distillation pot bottom
Pipe 25, and discharge opeing control valve 24 is additionally provided with the discharging tube, the discharging tube 25 constitutes blow-off pipe, with by this discharging tube 25
Waste water in boiler is discharged.
Further, the saturated vapor pipeline 3 is connected by tee pipe fitting is also corresponding with the condensation water inlet 12,
And the second steam control valve is additionally provided with the pipeline between the saturated vapor pipeline 3 and the condensation water inlet 12
11.The first steam control valve 5 is additionally provided with the saturated vapor pipeline 3 that boiler 13 is connected with steam generating stove 1.Institute
Pressure gauge 2 is additionally provided with the saturated vapor pipeline 3 for stating 5 admission end of the first steam control valve.
And the pressure change and scope in order to control and observe in boiler, the design is also in 13 middle and lower part of boiler
The first pressure tap 9 is additionally provided with wall, first pressure tap 9 surveys the connection corresponding with minute-pressure manometer 8 of pressure control valve 7 by first.
The second pressure tap 10 is offered on the saturated vapor pipeline 3 of 5 steam output end of the first steam control valve, second pressure tap
10 survey the also connection corresponding with the minute-pressure manometer 8 of pressure control valve 6 by second.Further, the minute-pressure used by the design is surveyed
Pressure meter 8 it include filling in which liquid, and the setting that takes the shape of the letter U transparent tube 21, and the fixation that the transparent tube 21 is fixed
Plate 22；And graduation mark 23 is additionally provided with the vertical direction of the transparent tube in the fixed plate 22；The transparent tube 21
One end survey pressure control valve and second also through tee pipe fitting and described first and survey that pressure control valve is corresponding to be connected, and its other end is opened
Mouth is arranged.The open and close that pressure control valve and the second survey pressure control valve are surveyed by control first in use can monitor saturation
Pressure size in water vapour pipeline 3 and boiler 13, and then control the pressure size in boiler 13 and enter boiler 13
Steam flow.
Further, the method by the system extraction natural Broneolum Syntheticum is as follows：
The first step, Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf is put in boiler and is distilled, and distills the steam for producing with natural Broneolum Syntheticum and dragon
Cerebrol is entered in condenser and is condensed, and during this, natural Broneolum Syntheticum major part is condensed on condenser inner wall, and small part is entered into
In product collecting vessel, meanwhile, steam is condensed into condensed water, and the Borneolum Syntheticum oil cooling liquid that congeals into together is flowed into product collection with condensed water
In bucket, hereafter, product is stayed in product collecting vessel, and it is temporary that condensed water exits into condensed water by pipeline from product collection bottom of the barrel
Deposit in bucket；
Second step, after the completion of the distillation of Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf, is drawn off, the liquid in boiler is discharged, and in distillation
New Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf are reentered in pot；
3rd step：The condensed water that first step condensed water temporary storage barrel is collected is pumped into into boiler bottom, then, switch off the pump place
Ball valve, to prevent the condensation water back flow in boiler from temporarily storing in bucket to condensed water；Second steam control valve is opened then, to entering
Entering the condensed water in boiler carries out heating, distills, and the natural Broneolum Syntheticum and Borneolum Syntheticum that script is dissolved and is suspended in condensed water is oily
It is distilled off, the Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf layer of the natural Broneolum Syntheticum for distilling out and Borneolum Syntheticum oil with steam by new loading, and with from new clothes
Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf in the natural Broneolum Syntheticum that distills and Borneolum Syntheticum oil enter in condenser with steam and condensed, so
Reclaim in product collecting vessel afterwards and be again introduced into natural Broneolum Syntheticum therein and Borneolum Syntheticum oil.
4th step：Condensed water in boiler is through a period of time（Distillation time general control was at 20 to 30 minutes）'s
After distillation, so that it may finish the natural Broneolum Syntheticum distillation dissolved and be suspended in condensed water.And condensed water was distilled in boiler
The steam produced in journey is while also just complete to the heating of new clothes Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf and to excluding air in distilling apparatus
Process, just enter directly into the process distilled to new clothes Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf.
5th step：After above-mentioned 4th step process terminates, the blowoff valve of distillation pot bottom is opened（Namely discharging tube）, can be by
In boiler, the condensed water without natural Broneolum Syntheticum is discharged, and after condensed water of the emptying without natural Broneolum Syntheticum, closes blowoff valve.Then,
The first steam control valve of the second steam control valve of slowly closing and opening, closes the second steam control valve and opens the first steam control
Valve processed will be carried out simultaneously, during above-mentioned two valve is changed, to be kept the pressure in boiler to be basically unchanged, be prevented in pot
Steam sprays from its boiler water seal or the water in water seal is sucked in pot, after the conversion of two valves is finished, by the first steam
Control valve is passed through steam to the steam distributor in boiler, and steam distributor is evenly distributed on steam in boiler, to new
Dress Borneolum Syntheticum Camphor tree branch and leaf are distilled.
6th step：Other Organic substances that can by the natural Broneolum Syntheticum on condenser inner wall and thereon every 4 to 8 pots time are shoveled
It is collected into product collecting vessel, so far, the production of this batch terminates.The production of next batch starts to the 6th from second step
EOS.Circulate successively.
Originally the condensed water drained as waste water is sent in boiler by the present invention carries out distillation process, reclaims day therein
So Borneolum Syntheticum, improves the recovery rate of natural Broneolum Syntheticum.
The system is in 2014 year of the Jiangxi Ji'an company whole production cycle（January 24 days to 2015 November in 2014
15 days）Middle extraction system and method using the present invention carries out the extraction work of natural Broneolum Syntheticum, and the creation data of the said firm is abundant
Demonstrate the ideal effect of the present invention.
12014 annual Borneolum Syntheticum output statistics table of table（Unit：㎏）
Table 1 is 2014 annual Borneolum Syntheticum output statistics tables, be can be seen that from upper table data：Natural Broneolum Syntheticum is reclaimed from condensed water
Forward and backward equal pot Borneolum Syntheticum yield is significantly different.On big level ground, hill does not reclaim the natural Broneolum Syntheticum in condensed water, and equal pot Borneolum Syntheticum yield is
1.456kg, the pheasant pool, Lao Wushan, Yi Jialing, my humble abode hill have reclaimed the natural Broneolum Syntheticum in condensed water, and equal pot Borneolum Syntheticum yield is
1.754kg, after natural Broneolum Syntheticum in condensed water is reclaimed, equal pot natural Broneolum Syntheticum output increased 20.47%.
By the system, in the case where existing equipment, production time, production cost are constant, a small amount of fund is spent to increase
Plus a set of condensate water recovery device, by the natural Broneolum Syntheticum in condensed water and some other Organic substances（Such as Borneolum Syntheticum oil）All return
Receive, do not produce and a little waste, and thoroughly solve environmental issue.Meanwhile, the U-shaped pressure gauge for micropressure used by the system replaces spring
Pressure in formula pressure gauge direct measurement boiler, so as to can it is more directly perceived, be more convenient, the pressure precisely controlled in boiler
And steam flow.All problems present in existing system and method are made fundamentally to obtain after system and method using the present invention
Solution is arrived, while its investment is little, has been had high repayment.The present invention is except for extraction natural Broneolum Syntheticum and Borneolum Syntheticum from Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf
It is oily outer, can be used for all in principle and extracted in the production technology of product using steam distillation.
Meanwhile, the system and method for the present invention are not required to transform existing cooling system again, it is not required that to steam
Flow control system and control method carry out automatic improving, have saved many improvement expenseses.
What embodiments of the invention were announced is preferred embodiment, but is not limited thereto, the ordinary skill people of this area
Member, easily according to above-described embodiment, understands the spirit of the present invention, and makes different amplifications and change, but as long as without departing from this
The spirit of invention, all within the scope of the present invention.
Claims (7)
1. a kind of natural Broneolum Syntheticum extraction system for improving recovery rate, it includes the distillation that steam distributor is provided with its bottom
Pot, and connection corresponding with the steam (vapor) outlet of the boiler condenser, the air intake of the steam distributor in the boiler
By the connection corresponding with saturated vapor producer of saturated vapor pipeline；It is characterized in that：It is also used for including one will condensation
The condensed water temporary storage barrel reclaimed by the condensed condensed water of device；The condensed water temporary storage barrel by water pump also with the boiler
Inside connection, the condensed water collected in condensed water temporary storage barrel is delivered in boiler by the water pump；Also include which
It is provided with the product collecting vessel of bung, the outlet of the condenser and the inlet communication of the product collecting vessel；Receive in the product
One is additionally provided with the middle part of collection bucket for the outlet of discharging the condensed water in the product collecting vessel, and in the product collecting vessel
A vertically disposed pipeline is provided with, the upper end of the pipeline is connected with the outlet, and the lower end of the pipeline is arranged at drum head；With institute
The outlet of pipeline upper end connection is stated via drainage element connection corresponding with the condensed water temporary storage barrel；The drainage element is without stifled
Plug guiding gutter；The lower U-lag main body and upper U-lag groove lid for including that without blocking guiding gutter its section takes the shape of the letter U, the upper U
Shape groove groove lid is buckled in the lower U-lag main body, and the passage for being formed between the two is constituted condensation flow circulation passage；Described
The bottom of boiler is further opened with condensing water inlet；Water inlet is corresponding connects with the condensation by water pump for the condensed water temporary storage barrel
It is logical；The discharging tube that liquid in by the boiler is discharged is additionally provided with the condensed water entrance of the distillation pot bottom, and
Discharge opeing control valve is additionally provided with the discharging tube；Saturated vapor pipeline connection also corresponding with the condensation water inlet, and
The second steam control valve is additionally provided with pipeline between the saturated vapor pipeline and the condensation water inlet.
2. the natural Broneolum Syntheticum extraction system of recovery rate can be improved as claimed in claim 1, it is characterised in that：In the boiler
The first steam control valve is additionally provided with the saturated vapor pipeline that interior steam distributor is connected with steam generating stove；Described
Pressure gauge is additionally provided with the saturated vapor pipeline of the first steam control valve admission end.
3. the natural Broneolum Syntheticum extraction system of recovery rate can be improved as claimed in claim 2, it is characterised in that：In the boiler
The first pressure tap is additionally provided with the inwall of middle and lower part, it is corresponding with minute-pressure manometer that first pressure tap surveys pressure control valve by first
Connection；The second pressure tap is offered on the saturated vapor pipeline of the first steam control valve steam output end, second pressure measurement
Mouth surveys pressure control valve also connection corresponding with the minute-pressure manometer by second.
4. the natural Broneolum Syntheticum extraction system of recovery rate can be improved as claimed in claim 3, it is characterised in that：The minute-pressure pressure measurement
Meter include filling in which liquid, and the setting that takes the shape of the letter U transparent tube, and by the fixed plate of transparent tube fixation；And institute
State graduation mark is additionally provided with the vertical direction of the transparent tube in fixed plate；One end of the transparent tube passes through tee pipe fitting
Connection corresponding with the described first survey pressure control valve and the second survey pressure control valve, its another end opening.
5. it is a kind of to realize extracting natural Broneolum Syntheticum using the natural Broneolum Syntheticum extraction system that can improve recovery rate as claimed in claim 1
Method, it is characterised in that：The first step, Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf is put in boiler and is distilled, and is distilled the steam for producing and is entered cold
Condensation in condenser, collects the condensed water that condensed device is produced；
The condensed water of collection is carried out distillation process by second step, and the natural Broneolum Syntheticum in condensed water is separated out with steam；
3rd step：The steam that generation is distilled in second step is entered in condenser and is condensed, collect product.
6. method as claimed in claim 5, it is characterised in that：In the first step, the condensed water produced by condenser be into
Enter in condensed water temporary storage barrel what is be collected；
After in the first step be collected condensed water in condensed water temporary storage barrel, after also including to distill in boiler
Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf take out, the step of the liquid in boiler is discharged；
The second step is specially：New Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf are put in boiler, by the condensed water in condensed water temporary storage barrel
Sent in boiler by water pump, continue to carry out at distillation the condensed water in boiler and the new Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf for loading
Reason；
3rd step is specially：The steam that generation is distilled in pot condensation in condenser will evaporated in second step；
Also include the 4th step：The first step, second step, the 3rd step described in repetitive operation；
5th step：Borneolum Syntheticum Lignum cinnamomi camphorae branch and leaf after distilling in boiler are taken out, and the liquid in boiler is discharged；Simultaneously will be cold
The natural Broneolum Syntheticum formed on condenser inwall is collected.
7. method as claimed in claim 6, it is characterised in that：The condensed water in condensed water temporary storage barrel is being sent into by water pump
After in boiler, second steam control valve is opened, and now, steam is entered in the boiler via condensation water inlet.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510761989.2A CN105237358B (en) | 2015-11-11 | 2015-11-11 | Natural borneol extraction system and method capable of increasing yield |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510761989.2A CN105237358B (en) | 2015-11-11 | 2015-11-11 | Natural borneol extraction system and method capable of increasing yield |
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| CN105237358A CN105237358A (en) | 2016-01-13 |
| CN105237358B true CN105237358B (en) | 2017-04-12 |
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| CN201510761989.2A Active CN105237358B (en) | 2015-11-11 | 2015-11-11 | Natural borneol extraction system and method capable of increasing yield |
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| CN113149815A (en) * | 2021-05-13 | 2021-07-23 | 安徽右旋龙脑生物科技有限公司 | Extraction system and extraction method of high-purity borneol |
| CN113527056B (en) * | 2021-08-20 | 2023-05-02 | 福建南平青松化工有限公司 | Separation equipment for borneol |
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| CN102512839B (en) * | 2011-12-24 | 2015-06-17 | 吉安市林业科学研究所 | Natural d-borneol extraction equipment |
| CN205088156U (en) * | 2015-11-11 | 2016-03-16 | 江西玉霞山农业开发有限公司 | Can improve natural borneol extraction system who receives yield |
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Effective date of registration: 20160608 Address after: West Industrial Park 331600 Ji'an city of Jiangxi province Jishui county two Ji Chang Lu Applicant after: Jiangxi Jinggang Natural Medicine Co., Ltd. Address before: 343000 Ji'an province Jiangxi City Qingyuan Road on the eastern side Everising spring No. 51 1-201 Applicant before: JIANGXI YUXIASHAN AGRICULTURE DEVELOPMENT CO., LTD. |
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