CN201208517Y - Natural herbals light-oil heavy-oil extraction device - Google Patents
Natural herbals light-oil heavy-oil extraction device Download PDFInfo
- Publication number
- CN201208517Y CN201208517Y CNU2008200670709U CN200820067070U CN201208517Y CN 201208517 Y CN201208517 Y CN 201208517Y CN U2008200670709 U CNU2008200670709 U CN U2008200670709U CN 200820067070 U CN200820067070 U CN 200820067070U CN 201208517 Y CN201208517 Y CN 201208517Y
- Authority
- CN
- China
- Prior art keywords
- oil
- natural herbal
- water
- light
- extraction device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000003921 oil Substances 0.000 title claims abstract description 46
- 238000000605 extraction Methods 0.000 title claims abstract description 27
- 239000000295 fuel oil Substances 0.000 title claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 48
- 238000010992 reflux Methods 0.000 claims description 16
- WYTGDNHDOZPMIW-RCBQFDQVSA-N alstonine Natural products C1=CC2=C3C=CC=CC3=NC2=C2N1C[C@H]1[C@H](C)OC=C(C(=O)OC)[C@H]1C2 WYTGDNHDOZPMIW-RCBQFDQVSA-N 0.000 claims description 4
- 239000000341 volatile oil Substances 0.000 abstract description 38
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 2
- 239000006049 herbal material Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000006200 vaporizer Substances 0.000 abstract 1
- 235000019198 oils Nutrition 0.000 description 28
- 238000000034 method Methods 0.000 description 19
- 239000000284 extract Substances 0.000 description 9
- 241000196324 Embryophyta Species 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 238000009835 boiling Methods 0.000 description 3
- 239000001902 eugenia caryophyllata l. bud oil Substances 0.000 description 3
- 238000001256 steam distillation Methods 0.000 description 3
- 235000005979 Citrus limon Nutrition 0.000 description 2
- 244000131522 Citrus pyriformis Species 0.000 description 2
- 240000006927 Foeniculum vulgare Species 0.000 description 2
- 235000004204 Foeniculum vulgare Nutrition 0.000 description 2
- 244000178870 Lavandula angustifolia Species 0.000 description 2
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 2
- 244000062730 Melissa officinalis Species 0.000 description 2
- 235000010654 Melissa officinalis Nutrition 0.000 description 2
- 244000223014 Syzygium aromaticum Species 0.000 description 2
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000001102 lavandula vera Substances 0.000 description 2
- 235000018219 lavender Nutrition 0.000 description 2
- 239000000865 liniment Substances 0.000 description 2
- 241000220317 Rosa Species 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 238000001802 infusion Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 229920001206 natural gum Polymers 0.000 description 1
- 235000019476 oil-water mixture Nutrition 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003815 supercritical carbon dioxide extraction Methods 0.000 description 1
Images
Landscapes
- Fats And Perfumes (AREA)
Abstract
The utility model discloses a natural herbal light oil and heavy oil extractor, which belongs to the extracting technology field of natural herbal materials and comprises a condensing tube, a steam collection tube, a water cycle return conduit, a vaporizer and an oil-water separator. A control valve is arranged in the water cycle return conduit; an included angle A between the steam collection tube and the oil-water separator ranges from 65 to 120 degrees; an included angle B between the steam collection tube and the water cycle return conduit ranges from 15 to 75 degrees. The natural herbal light oil and heavy oil extractor has reasonable design, simple structure and convenient operation, blends a light oil extracting device and a heavy oil extracting device together, is suitable for the extraction of the natural herbal light oil and heavy oil which are the volatile oil in two densities, not only meets the needs of experimental study, but also satisfies the large-scale production request, and also satisfies the extraction of the volatile oil in different densities.
Description
Technical field
The utility model belongs to the extractive technique field of natural herbal class material, is specifically related to a kind of device that adapts to natural herbal light oil and two kinds of density volatile oil extractions of heavy oil.
Background technology
Extraction volatile oil is pretty troublesome process from natural herbal, because the volatile oil content of plant is considerably less.So, need a large amount of plants just can extract a spot of volatile oil, finally cause volatile oil very expensive.For example: about 3～5 tons roseleaf could extract 1kg rose volatile oil; The fresh lavender of about 200kg could extract 1kg lavender volatile oil; About 1 ton of flores aurantii petal could extract 1kg flores aurantii volatile oil; About 3000 lemons, the 1kg lemon volatile oil of just squeezing out; About 6～7 tons of balms could be extracted 1kg balm volatile oil, are the medicinal herbs volatile oil of difficult extraction.
At present, the method for extraction volatile oil is a lot of from natural herbal, generally has following several:
1, steam distillation: the method is simple to operate, and cost is low, is the most frequently used extracting process.Fragrant plant raw material fresh or that drying is handled is put in the distiller heats, allow endophytic volatile oil follow evaporation of vapours to come out.After the steam that contains volatile oil was collected cooling via conduit, steam can be cooled to liquid, separated according to the difference of the proportion of water and volatile oil, density again.In the middle of the left moisture, more or less all some volatile oil is dissolved in the inside, Here it is so-called colored water, and most of volatile oil extract with the method.2, freezing compression method (milling process): the method is used for extracting the volatile oil that is housed in the pericarp part specially.3, chemical solvent extraction: the method is the extracting process commonly used of natural gum, resin and flower class volatile oil.4, grease partition method (fat suction method): the method is the extracting process of the costliness of flower volatile oil.5, supercritical carbon dioxide extraction method: the method is a kind of very expensive method.6, infusion method (for soaking oil): the method is immersed in flower in the deep fat, and the volatile oil in the plant is discharged, and gets final product with the filtration method extraction again.
These six kinds of methods comparatively speaking, at present the most frequently used, simple to operate, the essential oil extraction method that cost is low is a steam distillation.Be evaporated together by resulting volatile oil of steam distillation and water vapour, after the steam that contains volatile oil is collected cooling via conduit, steam can be cooled to liquid, again according to the difference of the proportion of water and volatile oil, density and separate, thereby obtains pure volatile oil.According to the comparison of volatile oil and water density, volatile oil is divided into two kinds in light oil and heavy oil.That is: than water light be light oil, than water heavy is heavy oil.At present, for the extraction of these two kinds of volatile oil, employing be the different devices of two covers.This will rooting according to the density characteristics of volatile oil, adopt different devices.For large-scale production, the dismounting of instrument is very inconvenient, and serious potential safety hazard is arranged.
The utility model content
Above-mentioned deficiency at prior art, the technical problems to be solved in the utility model provides a kind of natural herbal light oil heavy oil extraction device, it merges light oil extraction element and heavy oil extraction device, adapts to the extraction of natural herbal light oil and two kinds of density volatile oil of heavy oil.
The technical solution of the utility model is: natural herbal light oil heavy oil extraction device contains condenser pipe, steam collecting pipe, water circulating reflux pipe, distiller, oil water separator, a control valve is set in the water circulating reflux pipe, included angle A between steam collecting pipe and the oil water separator is 65～120 degree, and the included angle B between steam collecting pipe and the water circulating reflux pipe is 15～75 degree.
The volume of described distiller is 500-50,000ml.Described vapor collection external diameter of pipe is 10-30mm, and internal diameter is 5-20mm.Described condenser pipe is 15-50cm serpentine condenser.The volume of described oil water separator is 10-500mL.The external diameter of described water circulating reflux pipe is 10-30mm, and internal diameter is 5-20mm.
The utility model is reasonable in design, and is simple in structure, easy to operate, light oil extraction element and heavy oil extraction device are merged, adapt to the extraction of natural herbal light oil and two kinds of density volatile oil of heavy oil, both satisfied the experimental study needs, satisfy requirement of massive production again; Satisfy the extraction of different densities volatile oil.
Description of drawings
Accompanying drawing acceptance of the bid keep the score state as follows: 1-distiller; 2-steam collecting pipe; 3-condenser pipe; 4-oil water separator; 5-water circulating reflux pipe; 6-drain valve; 7-control valve.
The specific embodiment
Below in conjunction with accompanying drawing the specific embodiment of the present utility model is described in further detail.As shown in Figure 1, be provided with control valve 7 in water circulating reflux pipe 5, the included angle A between steam collecting pipe 2 and the oil water separator 4 is 75 degree, and steam collecting pipe 2 and the included angle B of returning between the circulating reflux pipe 5 are 65 degree.When using the utility model to carry out work, natural herbal and water are put into distiller 1, the volume of natural herbal and water is between 1/2-3/4 of distiller 1 volume.When extracting, natural herbal and water are heated to boiling in distiller 1, and the steam that carries volatile oil is collected through vapor collection pipeline 2, rises to condenser pipe 3.Be dropped in the oil water separator 4 through condensed oil-water mixture, and finish water-oil separating.For light oil, volatile oil is positioned at the upper strata after the water-oil separating, and water level is in lower floor; At this moment, the valve 6 on the water circulating reflux pipeline 5 is opened, the water of lower floor flows back to distiller 1 through reflux line 5, recycles.For heavy oil, volatile oil is positioned at lower floor after the water-oil separating, and water level at this moment, is closed the valve 6 on the water circulating reflux pipeline in the upper strata, and the water on upper strata flows back to distiller 1 through vapor collection pipe 2, recycles.
Be to adopt diagram extractor of the present utility model to carry out the example of natural herbal light oil heavy oil extraction below:
Example 1, ennel oil (light oil) extract:
Select 2 for use, in the 000mL distiller, external diameter is 10mm, and internal diameter is the vapor collection pipeline of 5mm, and the serpentine condenser of 25cm, the oil water separator of 20mL and external diameter are 10mm, and internal diameter is that the water circulating reflux pipeline of 5mm constitutes, in order to extract fennel seeds light oil.
Get the 200g fennel seeds, 1,000g water is put into distiller, leave standstill 24 hours after, be heated to little boiling.Extract after 5 hours, left standstill 12 hours, collect the ennel oil in the oil water separator.Resulting ennel oil is the yellow green oily liquids, and productive rate is 2.1%, and density is 0.92, and refractive power is 1.48.
2, clove bud oil (heavy oil) extracts:
Select 5 for use, in the 000mL distiller, external diameter is 20mm, and internal diameter is the vapor collection pipeline of 10mm, and the serpentine condenser of 50cm, the oil water separator of 50mL and external diameter are 20mm, and internal diameter is that the water circulating reflux pipeline of 10mm constitutes, in order to extract cloves bud heavy oil.
Get 500g cloves bud, 3,000g water is put into distiller, leave standstill 24 hours after, be heated to little boiling.Extract after 5 hours, left standstill 12 hours, collect the clove bud oil in the oil water separator.Resulting clove bud oil is a colourless oil liquid, and productive rate is 1.8%, and density is 1.05, and refractive power is 1.53.
Claims (6)
1, a kind of natural herbal light oil heavy oil extraction device, contain condenser pipe, steam collecting pipe, water circulating reflux pipe, distiller, oil water separator, it is characterized in that: a control valve (7) is set in the water circulating reflux pipe (5), included angle A between steam collecting pipe (2) and the oil water separator (4) is 65～120 degree, and the included angle B between steam collecting pipe (2) and the water circulating reflux pipe (5) is 15～75 degree.
2, natural herbal light oil heavy oil extraction device according to claim 1, it is characterized in that: the volume of described distiller (1) is 500-50,000ml.
3, natural herbal light oil heavy oil extraction device according to claim 1, it is characterized in that: described vapor collection pipe (2) external diameter is 10-30mm, and internal diameter is 5-20mm.
4, natural herbal light oil heavy oil extraction device according to claim 1, it is characterized in that: described condenser pipe (3) is 15-50cm serpentine condenser.
5, natural herbal light oil heavy oil extraction device according to claim 1, it is characterized in that: the volume of described oil water separator (4) is 10-500mL.
6, natural herbal light oil heavy oil extraction device according to claim 1, it is characterized in that: the external diameter of described water circulating reflux pipe (5) is 10-30mm, internal diameter is 5-20mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008200670709U CN201208517Y (en) | 2008-05-12 | 2008-05-12 | Natural herbals light-oil heavy-oil extraction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008200670709U CN201208517Y (en) | 2008-05-12 | 2008-05-12 | Natural herbals light-oil heavy-oil extraction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201208517Y true CN201208517Y (en) | 2009-03-18 |
Family
ID=40479242
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2008200670709U Expired - Fee Related CN201208517Y (en) | 2008-05-12 | 2008-05-12 | Natural herbals light-oil heavy-oil extraction device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201208517Y (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101732893B (en) * | 2010-01-18 | 2014-03-05 | 湖南大学 | Continuous oil-water separating and solvent reclaiming device for chemical synthesis or azeotropic rectification |
| CN103992880A (en) * | 2014-05-15 | 2014-08-20 | 河北中烟工业有限责任公司 | Volatile oil high-efficiency extraction separator |
| CN106281701A (en) * | 2016-08-17 | 2017-01-04 | 上海清轩生物科技有限公司 | Essential oil extraction device and plants essential oil extracting method |
-
2008
- 2008-05-12 CN CNU2008200670709U patent/CN201208517Y/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101732893B (en) * | 2010-01-18 | 2014-03-05 | 湖南大学 | Continuous oil-water separating and solvent reclaiming device for chemical synthesis or azeotropic rectification |
| CN103992880A (en) * | 2014-05-15 | 2014-08-20 | 河北中烟工业有限责任公司 | Volatile oil high-efficiency extraction separator |
| CN103992880B (en) * | 2014-05-15 | 2015-12-09 | 河北中烟工业有限责任公司 | A kind of volatile oil high efficiency extraction separator |
| CN106281701A (en) * | 2016-08-17 | 2017-01-04 | 上海清轩生物科技有限公司 | Essential oil extraction device and plants essential oil extracting method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105296163A (en) | Extraction equipment for fragrant plant essential oil and headspace volatile | |
| CN202658146U (en) | Extraction separation device for volatile oil of traditional Chinese medicinal material | |
| CN107057857A (en) | Agilawood essential oil equipment and process are extracted in a kind of efficiently distillation | |
| CN206580794U (en) | A kind of plants essential oil distills extraction equipment | |
| CN201299980Y (en) | Novel volatile oil distiller | |
| CN103923748A (en) | Volatile oil extracting, collecting and separating device | |
| CN201208517Y (en) | Natural herbals light-oil heavy-oil extraction device | |
| CN201353436Y (en) | Volatile oil extraction device with multi-layer of separation plates | |
| CN205412299U (en) | Multi -functional steam distillation and soxhlet extraction integration experimental apparatus | |
| CN2869023Y (en) | Plant volatile oil extractor | |
| CN206127245U (en) | Distillation edulcoration device of raw oil | |
| CN205965118U (en) | Can draw oil -water separator of light volatile oil and heavy volatile oil simultaneously | |
| CN207862305U (en) | A kind of agilawood essential oil distilling and extracting device | |
| CN201292354Y (en) | Natural medicinal herbs scent component drip catcher | |
| CN203096030U (en) | Volatile oil extraction separator | |
| CN206266534U (en) | Essence spice for cigarette volatile oil extractor | |
| CN205556604U (en) | Rose essential oil extractor | |
| CN215250700U (en) | Volatile oil separation extractor and volatile oil collecting device comprising same | |
| CN205659431U (en) | Device capable of simultaneously distilling and extracting | |
| CN212560170U (en) | Volatile oil extraction equipment | |
| CN101200672A (en) | Volatile oil extraction separator and method of use thereof | |
| CN201940071U (en) | Separation and collection device for traditional Chinese medicinevolatile oil | |
| CN208292961U (en) | A kind of novel plant essential oil extracting device | |
| CN201692682U (en) | Novel volatile oil extraction equipment | |
| CN206955995U (en) | A kind of efficiently distillation extraction agilawood essential oil equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: WUHAN HUANGHELOU ESSENCE AND SPICE CO., LTD. Free format text: FORMER OWNER: CHINA TOBACCO HUNAN INDUSTRIAL CO., LTD. Effective date: 20100920 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20100920 Address after: 430040 Wuhan, East and West Lake District, Jinshan Road, No. 1355, Hubei Patentee after: Wuhan Huanghelou Flavors Co., Ltd. Address before: 430040 Wuhan, East and West Lake District, Jinshan Road, No. 1355, Hubei Patentee before: China Tobacco Hunan Industrial Co., Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090318 Termination date: 20170512 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |