CN110122923A - A kind of cigarette filter rod and preparation method thereof containing novel solid perfume (or spice) pearl - Google Patents

A kind of cigarette filter rod and preparation method thereof containing novel solid perfume (or spice) pearl Download PDF

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Publication number
CN110122923A
CN110122923A CN201910439499.9A CN201910439499A CN110122923A CN 110122923 A CN110122923 A CN 110122923A CN 201910439499 A CN201910439499 A CN 201910439499A CN 110122923 A CN110122923 A CN 110122923A
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China
Prior art keywords
pearl
spice
perfume
solid perfume
porous
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CN201910439499.9A
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Chinese (zh)
Inventor
冯守爱
黄江锋
刘鸿
李志华
韦康
陈义昌
宋凌勇
班强
黄善松
胡超
务文涛
潘连华
黄宇亮
白森
白家峰
施怡
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China Tobacco Guangxi Industrial Co Ltd
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China Tobacco Guangxi Industrial Co Ltd
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Priority to CN201910439499.9A priority Critical patent/CN110122923A/en
Publication of CN110122923A publication Critical patent/CN110122923A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/061Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/18Mouthpieces for cigars or cigarettes; Manufacture thereof

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Fats And Perfumes (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The present invention provides a kind of cigarette filter rods and preparation method thereof containing novel solid perfume (or spice) pearl.The novel solid perfume (or spice) pearl after the one or more potpourris for adsorbing cocoa extract, 2,3- dimethyl pyrazine, furfural and ethylmaltol, is prepared using centrifugation ball blast technology, microwave processes using porous-starch as primary raw material.By in cavity reserved among solid perfume (or spice) pearl merging two-section vinegar fibre filter stick, it is prepared into the Three-element composite filter core of the pearl of perfume (or spice) containing novel solid.Novel solid perfume (or spice) pearl raw material of the invention is ecological, environmentally friendly;Fragrant pearl release fragrance is stablized;Fragrance use scope is wide, can not only load oil soluble flavors, but also can load water soluble fragrance;With the fragrant and sweet style of baking.It does not need to pinch brokenly fragrant pearl when cigarette smoking, cigarette flavouring effect can be played.

Description

A kind of cigarette filter rod and preparation method thereof containing novel solid perfume (or spice) pearl
Technical field
The present invention relates to cigarette filter rod technical field, in particular to a kind of cigarette filter rod containing novel solid perfume (or spice) pearl and its Preparation method.
Background technique
The cigarette of cigarette filter rod is the round bead shape glue made of polymeric shell package oil-based liquid fragrance with flavoring pearl at present Capsule is commonly called as cigarette with quick-fried pearl, is placed in cigarette filter rod tow, and when use, which is pinched brokenly, discharges internal fragrance, as cigarette flavor Compensation technique is promoted the use of in cigarette product in recent years.But there are many defects with quick-fried pearl for cigarette: 1, liquid perfume release exists After rolling up in filter stick, fragrance supply is unstable when will cause cigarette smoking, and fragrance is excessively dense when just starting to aspirate, with cigarette Suction, liquid perfume volatilization, fragrance become very light quickly;2, cigarette filter can also be deformed because of extruding while pinching brokenly quick-fried pearl, Both the appearance of cigarette filter had been influenced, also will affect cigarette smoking experience;3, quick-fried pearl shell is easy the moisture absorption, causes to be difficult to pinch brokenly, shadow Ring its using effect;4, due to the water solubility of polymeric shell in the prior art, cause it that can only wrap up oil soluble flavors, it can not Coated water-soluble or alcohol-soluble fragrance, cause a large amount of flavors and fragrancess not to be available in quick-fried pearl.
To solve the above problems, some enterprise developments solid perfume (or spice) pearl in recent years.Shanghai Juhua Technology Co., Ltd. It has invented cigarette filter tip and cigarette the zeolite perfume (or spice) pearl preparation method (201710990114.9) containing zeolite perfume (or spice) pearl and has contained silicon Cigarette filter tip and cigarette the silica gel perfume (or spice) pearl preparation method (201710990115.3) of glue perfume (or spice) pearl;Cigarette industry Limited Liability in Jiangxi Company has invented a kind of cigarette filter tip containing bulky grain solid-state perfume (or spice) pearl and preparation method thereof (201810886849.1), and solid-state is fragrant Pearl wants raw material based on porous konilite;China Tobacco Jiangxi Industrial LLC has invented a kind of containing single solid-state perfume (or spice) pearl particle Ramuscule cigarette holder stick and preparation method thereof (201810887483.X), the perfume pearl is to activate montmorillonite as primary raw material;In Jiangxi A kind of cigarette filter tip and preparation method thereof containing double solid-state perfume (or spice) pearl particles has been invented by cigarette industry Co., Ltd (201810887493.3), solid-state perfume (or spice) pearl is using white carbon black as primary raw material.But, foregoing invention file is with inorganic chemical industry material Cigarette solid perfume (or spice) pearl is prepared for raw material, inorganic chemical industry material is applied to cigarette filter rod, is difficult to coordinate with cigarette smoke, be easy to produce Miscellaneous gas, and cigarette is based food product, be easy to cause security risks using inorganic chemical industry material.Cigarette industry is limited in Hubei Responsible company has invented a kind of cigarette solid flavoring pearl and preparation method thereof (201510219037.8), substrate be starch, rice flour, Diatomite, cellulose acetate powder, gum arabic, sodium alginate, gelatin, carragheen, dextrin, cyclodextrin, poloxamer, Ka Bo Mother, polyvinyl alcohol, povidone, carboxymethyl cellulose, methylcellulose, hydroxyethyl cellulose, sodium hyaluronate, polyethylene glycol, hydroxyl One of propyl cellulose or a variety of mixtures.This document institute protection materials range is too wide, not according to solid perfume (or spice) pearl Demand selects material, not very practical, and material therefor is greatly most without porous structure, the limited capacity of carried perfume is made It is not high at its flue gas flavouring effect, and make pellet application when need to crumb to be powdered, can just play flavouring effect, not be true The solid perfume (or spice) pearl of positive meaning.
Summary of the invention
In view of the above technical problems, the present invention provides a kind of cigarette filter rod containing novel solid perfume (or spice) pearl and its preparation side Method.
To achieve the above object, the technical solution adopted by the present invention are as follows:
Novel solid perfume (or spice) pearl of the present invention is prepared first.It is main former that the novel solid perfume (or spice) pearl, which is with porous-starch, Expect, after the one or more potpourris for adsorbing cocoa extract, 2,3- dimethyl pyrazine, furfural and ethylmaltol, benefit It is prepared with centrifugation ball blast technology, microwave processes, the solid perfume (or spice) pearl, which has, bakes fragrant and sweet style.
It is that will be consolidated during filter stick formation using fragrant pearl feeder when novel solid perfume (or spice) pearl is applied to cigarette filter rod Body note pearl is placed in cavity reserved among two-section vinegar fibre filter stick, forms the Three-element composite filter core of the pearl of perfume (or spice) containing solid.
The preferred technical solution of the present invention is as follows:
The preparation method of novel solid perfume (or spice) pearl the following steps are included:
1, prepared by cocoa extract: using low fat cocoa powder as raw material, extracting combination alcohol reflux by alcohol percolation method and mentions It takes and is made.
The alcohol percolation method extracts combination alcohol reflux and extracts, it is characterised in that first carries out ethyl alcohol infiltration to low fat cocoa powder Method of filtering is extracted, and obtained solid residue carries out alcohol reflux extraction again, then carries out mixing and dense for two methods are extract obtained Cocoa extract is made in contracting.
During the alcohol percolation method extracts, concentration of alcohol 70%, low fat cocoa powder 1000g flows out 2~3mL infiltration per minute It filters liquid.
During the alcohol reflux extracts, concentration of alcohol 70%, selection water-bath temperature control, 80 DEG C of temperature.
2, prepared by solid perfume (or spice) pearl young bird ball:
(1) using porous-starch as primary raw material, uniformly spray into a certain proportion of cocoa extract, 2,3- dimethyl pyrazine, One or more potpourris of furfural and ethylmaltol, stirring are stood, and fragrance is adsorbed in the duct of porous-starch In;
The ratio that the cocoa extract accounts for porous-starch is 1.0-5.0%;The 2,3- dimethyl pyrazine accounts for porous shallow lake The ratio of powder is 10/5000000ths to million/1000000ths;The ratio that the furfural accounts for porous-starch is 5000000 to million/1000000ths points Ten;The ratio that the ethylmaltol accounts for porous-starch is 6/3rds/100000ths to 100,000;
(2) porous-starch for being adsorbed with fragrance is put into centrifugation shot-blasting machine, carries out centrifugation ball blast, it is young to obtain fragrant pearl Ball, the diameter of the perfume pearl young bird ball is by centrifugation ball blast process parameter control, selectable range 1.0mm-4.0mm.
3, the preparation of novel solid perfume (or spice) pearl: the fragrant pearl young bird ball is subjected to microwave treatment, microwave treatment can make low intensive Fragrant pearl young bird ball becomes high-intensitive novel solid perfume (or spice) pearl;Meanwhile the carbonyls in microwave processing process in porous-starch and Maillard reaction occurs for amino-compound, generates fragrance matter, can further function as the effect of flue gas flavouring;
The fragrance matter purges chromatography through head space, is mainly furfuryl alcohol, 2 (5H)-furanones, in 4 hydroxybutyric acid Ester etc. bakes fragrant, fragrant and sweet, milk flavor component.
The preparation method of cigarette filter rod of the present invention containing above-mentioned novel solid perfume (or spice) pearl: during filter stick formation, You Xiangzhu Solid perfume (or spice) pearl is added in cavity reserved among two-section vinegar fibre filter stick by feeder, forms the tri compound filter of the pearl of perfume (or spice) containing solid Stick;
The additive amount of solid perfume (or spice) pearl is determined by the diameter of fragrant pearl in the Three-element composite filter core, and fragrant pearl diameter is bigger, fragrant pearl Additive amount it is fewer.Solid perfume (or spice) 1-100, pearl is preferably comprised in the Three-element composite filter core of every cigarette;
Unless otherwise specified, ratio described in this document is weight ratio.
Compared with prior art, the invention has the following advantages that
1, after the novel solid perfume (or spice) pearl invented is added to cigarette filter rod, when cigarette smoking, does not need to pinch brokenly fragrant pearl Play cigarette flavouring effect;
2, since porous-starch has duct abundant, fragrance can effectively be adsorbed, when cigarette smoking, due to porous-starch Slow-release function, fragrance uniformly discharge, and are not in the defect unstable with aspiration procedure fragrance when quick-fried pearl using cigarette;
3, due to the existing water imbibition of porous-starch, and have oil absorption, thus its not only can load water soluble fragrance, but also oil can be loaded Soluble flavor, fragrance use scope are greatly expanded;
4, using porous-starch as primary raw material, green, environmental protection, safety are applied in cigarette and do not have security risks;
5, pass through the use of cocoa extract, 2,3- dimethyl pyrazine, furfural and ethylmaltol, made solid perfume (or spice) pearl With the fragrant and sweet style of baking;
6, by specific microwave processes Maillard reaction occurs for porous-starch, and generating has the fragrant and sweet style of baking Fragrance matter.
Detailed description of the invention
Fig. 1 is structural schematic diagram of the invention.
In figure: 1- novel solid perfume (or spice) pearl, 2- cigarette filter rod, 3- pipe tobacco.
Specific embodiment
In conjunction with the structural schematic diagram of Fig. 1 cigarette filter rod of the present invention.Wherein: 1 being novel solid perfume (or spice) pearl, 2 be cigarette filter rod, 3 For pipe tobacco.
Embodiment 1
Step 1: cocoa extract preparation: using low fat cocoa powder as raw material, combination ethyl alcohol is extracted by alcohol percolation method and is returned Stream is extracted and is made.
Alcohol percolation method extracts combination alcohol reflux and extracts: first carrying out alcohol percolation method extraction, ethyl alcohol to low fat cocoa powder Concentration is 70%, and low fat cocoa powder 1000g flows out 2~3mL percolate per minute.Obtained solid residue carries out alcohol reflux again and mentions It takes, in alcohol reflux extraction, concentration of alcohol 70%, selection water-bath temperature control, 80 DEG C of temperature.Then it will be extracted obtained by two methods Object is mixed and is concentrated, and cocoa extract is made.
Step 2: solid perfume (or spice) pearl young bird ball preparation.
(1) 100g cocoa extract, 50mg 2,3- dimethyl pyrazine, 50mg furfural and 300mg ethyl malt are weighed Phenol, it is uniformly mixed, it sufficiently dissolves, forms transparent clear solution, it is uniformly sprayed into 10kg Corn Porous Starch, stirs, is quiet It sets, fragrance is adsorbed in the duct of porous-starch;
(2) porous-starch for being adsorbed with fragrance is put into centrifugation shot-blasting machine, carries out centrifugation ball blast, control centrifugation ball blast Technological parameter sprays into pure water while ball blast, and the fragrant pearl young bird ball that diameter is 4.0mm is made, and the 10kg for adsorbing fragrance is porous Cornstarch need to spray into 6.5kg pure water altogether.
Step 3: novel solid perfume (or spice) pearl preparation.The fragrant pearl young bird ball is subjected to microwave treatment, microwave treatment temperature is no more than 120 DEG C, microwave treatment time according to when ball blast spray into pure water amount and microwave heating equipment used power calculation, specifically with 0.8 kg of water of water lift rate/kilowatt-hour (kg/kwh) is so that low intensive fragrant pearl young bird ball is become high-intensitive solid fragrant according to calculating Pearl;Meanwhile microwave treatment temperature and processing time are controlled, the carbonyls and amino-compound in porous-starch occur beauty and draw Moral reaction, generates fragrance matter.
Step 4: the preparation of the cigarette filter rod of the pearl of perfume (or spice) containing novel solid.During filter stick formation, You Xiangzhu feeder will 1 solid perfume (or spice) pearl is added in 6mm cavity reserved among two-section vinegar fibre filter stick, forms the tri compound filter of the pearl of perfume (or spice) containing solid Stick is named as 1# filter stick.
Embodiment 2
Step 1: cocoa extract preparation.Using low fat cocoa powder as raw material, combination ethyl alcohol is extracted by alcohol percolation method and is returned Stream is extracted and is made.
Alcohol percolation method extracts combination alcohol reflux and extracts: it is first to carry out alcohol percolation method extraction to low fat cocoa powder, Concentration of alcohol is 70%, and low fat cocoa powder 1000g flows out 2~3mL percolate per minute.Obtained solid residue carries out ethyl alcohol again and returns Stream extracts, concentration of alcohol 70%, selection water-bath temperature control, and 80 DEG C of temperature.Then it mixes two methods are extract obtained And concentration, cocoa extract is made.
Step 2: solid perfume (or spice) pearl young bird ball preparation.
(1) 300g cocoa extract, 80mg 2,3- dimethyl pyrazine, 80mg furfural and 500mg ethyl malt are weighed Phenol is uniformly mixed, and is sufficiently dissolved, is formed transparent clear solution, sprayed into 10kg Corn Porous Starch, and stirring is stood, will Fragrance is adsorbed in the duct of porous-starch;
(2) porous-starch for being adsorbed with fragrance is put into centrifugation shot-blasting machine, carries out centrifugation ball blast, control centrifugation ball blast Technological parameter sprays into pure water while ball blast, and the fragrant pearl young bird ball that diameter is 2.0mm is made, and the 10kg for adsorbing fragrance is porous Cornstarch need to spray into 6.2kg pure water altogether.
Step 3: solid perfume (or spice) pearl preparation.The fragrant pearl young bird ball is subjected to microwave treatment, microwave treatment temperature is no more than 120 DEG C, microwave treatment time is according to the amount of pure water and the power calculation of microwave heating equipment used is sprayed into when ball blast, specifically to mention 0.8 kg of water of water rate/kilowatt-hour (kg/kwh) is so that low intensive fragrant pearl young bird ball is become high-intensitive solid fragrant according to calculating Pearl;Meanwhile microwave treatment temperature and processing time are controlled, the carbonyls and amino-compound in porous-starch occur beauty and draw Moral reaction, generates fragrance matter.
Step 4: the preparation of the cigarette filter rod of the pearl of perfume (or spice) containing solid.During filter stick formation, You Xiangzhu feeder is by 15 Left and right solid perfume (or spice) pearl is added in 6mm cavity reserved among two-section vinegar fibre filter stick, forms the tri compound filter of the pearl of perfume (or spice) containing solid Stick is named as 2# filter stick.
Embodiment 3
Step 1: cocoa extract preparation.Using low fat cocoa powder as raw material, combination ethyl alcohol is extracted by alcohol percolation method and is returned Stream is extracted and is made.
Alcohol percolation method extracts combination alcohol reflux and extracts: first carrying out alcohol percolation method extraction, ethyl alcohol to low fat cocoa powder Concentration is 70%, and low fat cocoa powder 1000g flows out 2~3mL percolate per minute.Obtained solid residue carries out alcohol reflux again and mentions It takes, concentration of alcohol 70%, selection water-bath temperature control, 80 DEG C of temperature.Then by two methods it is extract obtained carry out mixing and it is dense Cocoa extract is made in contracting.
Step 2: solid perfume (or spice) pearl young bird ball preparation.
(1) 500g cocoa extract, 100mg 2,3- dimethyl pyrazine, 100mg furfural and 600mg ethyl malt are weighed Phenol is uniformly mixed, and is sufficiently dissolved, is formed transparent clear solution, sprayed into 10kg Corn Porous Starch, and stirring is stood, will Fragrance is adsorbed in the duct of porous-starch;
(2) porous-starch for being adsorbed with fragrance is put into centrifugation shot-blasting machine, carries out centrifugation ball blast, control centrifugation ball blast Technological parameter sprays into pure water while ball blast, and the fragrant pearl young bird ball that diameter is 1.0mm is made, and the 10kg for adsorbing fragrance is porous Cornstarch need to spray into 6.0kg pure water altogether.
Step 3: solid perfume (or spice) pearl preparation.The fragrant pearl young bird ball is subjected to microwave treatment, microwave treatment temperature is no more than 120 DEG C, microwave treatment time is according to the amount of pure water and the power calculation of microwave heating equipment used is sprayed into when ball blast, specifically to mention 0.8 kg of water of water rate/kilowatt-hour (kg/kwh) is so that low intensive fragrant pearl young bird ball is become high-intensitive solid fragrant according to calculating Pearl;Meanwhile microwave treatment temperature and processing time are controlled, the carbonyls and amino-compound in porous-starch occur beauty and draw Moral reaction, generates fragrance matter.
Step 4: the preparation of the cigarette filter rod of the pearl of perfume (or spice) containing solid.During filter stick formation, You Xiangzhu feeder is by 80 Left and right solid perfume (or spice) pearl is added in 6mm cavity reserved among two-section vinegar fibre filter stick, forms the tri compound filter of the pearl of perfume (or spice) containing solid Stick is named as 3# filter stick.
Embodiment 4
Step 1: cocoa extract preparation.Using low fat cocoa powder as raw material, combination ethyl alcohol is extracted by alcohol percolation method and is returned Stream is extracted and is made.
Alcohol percolation method extracts combination alcohol reflux and extracts: first carrying out alcohol percolation method extraction, ethyl alcohol to low fat cocoa powder Concentration is 70%, and low fat cocoa powder 1000g flows out 2~3mL percolate per minute.Obtained solid residue carries out alcohol reflux again and mentions It takes, concentration of alcohol 70%, selection water-bath temperature control, 80 DEG C of temperature.Then by two methods it is extract obtained carry out mixing and it is dense Cocoa extract is made in contracting.
Step 2: solid perfume (or spice) pearl young bird ball preparation.
(1) 300g cocoa extract solution is weighed, is sprayed into 10kg Corn Porous Starch, stirring is stood, by fragrance It is adsorbed in the duct of porous-starch;
(2) porous-starch for being adsorbed with fragrance is put into centrifugation shot-blasting machine, carries out centrifugation ball blast, control centrifugation ball blast Technological parameter sprays into pure water while ball blast, and the fragrant pearl young bird ball that diameter is 1.5mm is made, and the 10kg for adsorbing fragrance is porous Cornstarch need to spray into 6.1kg pure water altogether.
Step 3: novel solid perfume (or spice) pearl preparation.The fragrant pearl young bird ball is subjected to microwave treatment, microwave treatment temperature is no more than 120 DEG C, microwave treatment time according to when ball blast spray into pure water amount and microwave heating equipment used power calculation, specifically with 0.8 kg of water of water lift rate/kilowatt-hour (kg/kwh) is so that low intensive fragrant pearl young bird ball is become high-intensitive solid fragrant according to calculating Pearl;Meanwhile microwave treatment temperature and processing time are controlled, the carbonyls and amino-compound in porous-starch occur beauty and draw Moral reaction, generates fragrance matter.
Step 4: the preparation of the cigarette filter rod of the pearl of perfume (or spice) containing novel solid.During filter stick formation, You Xiangzhu feeder will 40 or so solid perfume (or spice) pearls are added in 6mm cavity reserved among two-section vinegar fibre filter stick, and the ternary for forming the pearl of perfume (or spice) containing solid is multiple Filter stick is closed, 4# filter stick is named as.
Embodiment 5
Step 1: cocoa extract preparation.Using low fat cocoa powder as raw material, combination ethyl alcohol is extracted by alcohol percolation method and is returned Stream is extracted and is made.
Alcohol percolation method extracts combination alcohol reflux and extracts: first carrying out alcohol percolation method extraction, ethyl alcohol to low fat cocoa powder Concentration is 70%, and low fat cocoa powder 1000g flows out 2~3mL percolate per minute.Obtained solid residue carries out alcohol reflux again and mentions It takes, concentration of alcohol 70%, selection water-bath temperature control, 80 DEG C of temperature.Then by two methods it is extract obtained carry out mixing and it is dense Cocoa extract is made in contracting.
Step 2: solid perfume (or spice) pearl young bird ball preparation.
(1) 300g cocoa extract and 100mg 2 are weighed, 3- dimethyl pyrazine is uniformly mixed, and forms clear solution, will It is sprayed into 10kg Corn Porous Starch, and stirring is stood, and fragrance is adsorbed in the duct of porous-starch;
(2) porous-starch for being adsorbed with fragrance is put into centrifugation shot-blasting machine, carries out centrifugation ball blast, control centrifugation ball blast Technological parameter sprays into pure water while ball blast, and the fragrant pearl young bird ball that diameter is 4.0mm is made, and the 10kg for adsorbing fragrance is porous Cornstarch need to spray into 6.5kg pure water altogether.
Step 3: novel solid perfume (or spice) pearl preparation.The fragrant pearl young bird ball is subjected to microwave treatment, microwave treatment temperature is no more than 120 DEG C, microwave treatment time according to when ball blast spray into pure water amount and microwave heating equipment used power calculation, specifically with 0.8 kg of water of water lift rate/kilowatt-hour (kg/kwh) is so that low intensive fragrant pearl young bird ball is become high-intensitive solid fragrant according to calculating Pearl;Meanwhile microwave treatment temperature and processing time are controlled, the carbonyls and amino-compound in porous-starch occur beauty and draw Moral reaction, generates fragrance matter.
Step 4: the preparation of the cigarette filter rod of the pearl of perfume (or spice) containing novel solid.During filter stick formation, You Xiangzhu feeder will 1 solid perfume (or spice) pearl is added in 6mm cavity reserved among two-section vinegar fibre filter stick, forms the tri compound filter of the pearl of perfume (or spice) containing solid Stick is named as 5# filter stick.
Application Example
Using identical pipe tobacco and cigarette supplementary, it is utilized respectively above-mentioned 1# filter stick, 2# filter stick, 3# filter stick, 4# filter stick, 5# filter stick Cigarette is rolled, 1# cigarette, 2# cigarette, 3# cigarette, 4# cigarette, 5# cigarette are made respectively;Meanwhile it being rolled using common vinegar fibre filter stick Cigarette is compareed, 0# cigarette is named as, above-mentioned carry out Sensory Quality of Cigarette is smoked panel test, as a result see the table below.
Kinds of cigarettes sample Analyses Methods for Sensory Evaluation Results
After adding solid perfume (or spice) pearl of the present invention in filter stick it can be seen from upper table cigarette sample Analyses Methods for Sensory Evaluation Results, flue gas sense Official's mass gets a promotion, and cigarette bakes fragrant and sweet style and shown.

Claims (11)

1. a kind of novel solid perfume (or spice) pearl, which is characterized in that the solid perfume (or spice) pearl is to adsorb cocoa using porous-starch as primary raw material Extract, 2,3- dimethyl pyrazine, furfural and ethylmaltol one or more potpourris be prepared.
2. novel solid perfume (or spice) pearl according to claim 1, it is characterised in that: the cocoa extract accounts for the ratio of porous-starch Example is 1 percent to 5 percent;The ratio that the 2,3- dimethyl pyrazine accounts for porous-starch is 5000000 to million/1000000ths points Ten;The ratio that the furfural accounts for porous-starch is 10/5000000ths to million/1000000ths;The ethylmaltol accounts for porous shallow lake The ratio of powder is 6/3rds/100000ths to 100,000.
3. novel solid perfume (or spice) pearl according to claim 2, it is characterised in that: the cocoa extract accounts for the ratio of porous-starch Example is 1.0-5.0%;The ratio that the 2,3- dimethyl pyrazine accounts for porous-starch is 0.0005%-0.001%;The furfural accounts for The ratio of porous-starch is 0.0005%-0.001%;The ratio that the ethylmaltol accounts for porous-starch is 0.003%- 0.006%.
4. the preparation method of novel solid perfume (or spice) pearl according to claim 1 to 3, object sign is:
The following steps are included:
(1) prepared by cocoa extract: using low fat cocoa powder as raw material, extracting combination alcohol reflux by alcohol percolation method and extracts It is made;
The alcohol percolation method extracts combination alcohol reflux and extracts: first carrying out alcohol percolation method extraction, gained to low fat cocoa powder Solid residue carries out alcohol reflux extraction again, is then mixed two methods are extract obtained and are concentrated, be made it is described can Extractable;
(2) prepared by solid perfume (or spice) pearl young bird ball: using porous-starch as primary raw material, a certain proportion of cocoa extract, 2 are uniformly sprayed into, One or more potpourris of 3- dimethyl pyrazine, furfural and ethylmaltol, stirring are stood, and fragrance are adsorbed in more In the duct of hole starch;The porous-starch for being adsorbed with fragrance is put into centrifugation shot-blasting machine, centrifugation ball blast is carried out, obtains fragrant pearl Young ball;
(3) prepared by solid perfume (or spice) pearl: the fragrant pearl young bird ball being carried out microwave treatment, microwave treatment can be such that low intensive fragrant pearl young bird ball becomes For high-intensitive solid perfume (or spice) pearl;Meanwhile carbonyls and amino-compound generation beauty in microwave processing process in porous-starch Maillard reaction generates fragrance matter, can further function as the effect of flue gas flavouring.
5. a kind of preparation method of novel solid perfume (or spice) pearl according to claim 4, which is characterized in that
Alcohol percolation method in the cocoa extract preparation step extracts, concentration of alcohol 70%, and low fat cocoa powder 1000g is every Minute outflow 2~3mL percolate;Alcohol reflux in the cocoa extract preparation step extracts, concentration of alcohol 70%, choosing Select water-bath temperature control, 80 DEG C of temperature.
6. a kind of preparation method containing novel solid perfume (or spice) pearl according to claim 4, it is characterised in that: the solid perfume (or spice) pearl In young ball preparation step, the diameter of fragrant pearl young bird ball is by centrifugation ball blast process parameter control, selectable range 1.0mm-4.0mm.
7. a kind of preparation method containing novel solid perfume (or spice) pearl according to claim 4, it is characterised in that:
In the novel solid perfume (or spice) pearl preparation step, temperature is no more than 120 DEG C when microwave treatment, and microwave treatment time is according to ball blast When spray into pure water amount and microwave heating equipment used power calculation, specifically with 0.8 kg of water of water lift rate/kilowatt-hour (kg/kwh) for according to calculating;
The fragrance matter includes furfuryl alcohol, 2 (5H)-furanones, fragrant, fragrant and sweet, the milk flavor component of 4 hydroxybutyric acid lactone baking.
8. a kind of cigarette filter rod containing novel solid perfume (or spice) pearl, it is characterised in that: novel solid perfume (or spice) pearl is added to the filter of two-section vinegar fibre Among stick in reserved cavity, the Three-element composite filter core of the pearl of perfume (or spice) containing novel solid is formed.
9. a kind of cigarette filter rod containing novel solid perfume (or spice) pearl according to claim 8, it is characterised in that: the tri compound The additive amount of novel solid perfume (or spice) pearl is determined by the diameter of fragrant pearl in filter stick, and fragrant pearl diameter is bigger, and the additive amount of fragrant pearl is fewer.
10. a kind of cigarette filter rod containing novel solid perfume (or spice) pearl according to claim 9, it is characterised in that: every cigarette Contain solid perfume (or spice) 1-100, pearl in the Three-element composite filter core.
11. special according to a kind of any preparation method of the cigarette filter rod containing novel solid perfume (or spice) pearl of claim 8-10 Sign is: during filter stick formation, solid perfume (or spice) pearl is added to sky reserved among two-section vinegar fibre filter stick by You Xiangzhu feeder In chamber, the Three-element composite filter core of the pearl of perfume (or spice) containing solid is formed;Contain solid perfume (or spice) pearl 1- in the Three-element composite filter core of every cigarette 100.
CN201910439499.9A 2019-05-24 2019-05-24 A kind of cigarette filter rod and preparation method thereof containing novel solid perfume (or spice) pearl Pending CN110122923A (en)

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Application publication date: 20190816