CN103666068B - A kind of energy-conserving and environment-protective UV curing inks and preparation method thereof - Google Patents
A kind of energy-conserving and environment-protective UV curing inks and preparation method thereof Download PDFInfo
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- CN103666068B CN103666068B CN201310602412.8A CN201310602412A CN103666068B CN 103666068 B CN103666068 B CN 103666068B CN 201310602412 A CN201310602412 A CN 201310602412A CN 103666068 B CN103666068 B CN 103666068B
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- energy
- conserving
- protective
- environment
- curing inks
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- 239000000976 ink Substances 0.000 title claims abstract description 27
- 238000003848 UV Light-Curing Methods 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title claims description 8
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 21
- PQLMXFQTAMDXIZ-UHFFFAOYSA-N isoamyl butyrate Chemical compound CCCC(=O)OCCC(C)C PQLMXFQTAMDXIZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims abstract description 7
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910021536 Zeolite Inorganic materials 0.000 claims abstract description 7
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims abstract description 7
- 229920003180 amino resin Polymers 0.000 claims abstract description 7
- 235000012538 ammonium bicarbonate Nutrition 0.000 claims abstract description 7
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 7
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000975 dye Substances 0.000 claims abstract description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229940094941 isoamyl butyrate Drugs 0.000 claims abstract description 7
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000049 pigment Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000010457 zeolite Substances 0.000 claims abstract description 7
- LJRSZGKUUZPHEB-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxypropoxy)propoxy]propyl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COC(C)COC(=O)C=C LJRSZGKUUZPHEB-UHFFFAOYSA-N 0.000 claims abstract description 4
- OOJBEQBXIJTMIN-UHFFFAOYSA-N europium 1,1,1-trifluoropentane-2,4-dione Chemical compound FC(C(=O)CC(C)=O)(F)F.[Eu] OOJBEQBXIJTMIN-UHFFFAOYSA-N 0.000 claims abstract description 4
- KCTAWXVAICEBSD-UHFFFAOYSA-N prop-2-enoyloxy prop-2-eneperoxoate Chemical compound C=CC(=O)OOOC(=O)C=C KCTAWXVAICEBSD-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 10
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 9
- 239000012467 final product Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- KDVYCTOWXSLNNI-UHFFFAOYSA-N 4-t-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 claims description 3
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- 229920002367 Polyisobutene Polymers 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- APZPSKFMSWZPKL-UHFFFAOYSA-N [3-hydroxy-2,2-bis(hydroxymethyl)propyl] 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCC(CO)(CO)CO APZPSKFMSWZPKL-UHFFFAOYSA-N 0.000 claims description 3
- 229940022663 acetate Drugs 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 239000002904 solvent Substances 0.000 abstract description 5
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 abstract description 2
- 238000003912 environmental pollution Methods 0.000 abstract description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052737 gold Inorganic materials 0.000 abstract description 2
- 239000010931 gold Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000010422 painting Methods 0.000 abstract description 2
- 239000011087 paperboard Substances 0.000 abstract description 2
- 229910052709 silver Inorganic materials 0.000 abstract description 2
- 239000004332 silver Substances 0.000 abstract description 2
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 206010034972 Photosensitivity reaction Diseases 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 230000036211 photosensitivity Effects 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000002211 ultraviolet spectrum Methods 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of energy-conserving and environment-protective UV curing inks, it is characterized in that, be made up of the raw material of following weight part: pigment dyestuff 1-3, aminoresin 20-23, bicarbonate of ammonia 1-2, zeolite 1-2, ethylene glycol ether acetate 13-15, isoamyl butyrate 11-13, Viscoat 295 12-14, cobalt naphthenate 1-1.1, dibutyl tin laurate 1-2, tri (propylene glycol) diacrylate 10-12, ethyl acetate 5-8, UV epoxy acrylate 10-12, 1173 light trigger 4-8, trifluoroacetylacetone europium 4-5, vulcabond 5-6, auxiliary agent 4-5, it once can be imprinted in gold and silver paperboard or PVC card by screen painting mode by ink of the present invention, improves production efficiency, has saved the energy, and not containing solvent, alleviates the infringement to human body and environmental pollution.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly a kind of energy-conserving and environment-protective UV curing inks and preparation method thereof.
Background technology
Ultraviolet light polymerization (UV) ink refers under uviolizing, utilizes the UV-light of different wave length and energy to make ink film forming and dry ink.Utilize different UV spectrum, can different-energy be produced, the monomer polymerization in different ink vehicle is become polymkeric substance, so the look film of UV ink has good machinery and chemical property.The major advantage of UV ink has: (1) is without solvent; (2) rate of drying is fast, and power consumption is few; (3) good luster, bright in luster; (4) water-fast, solvent resistant, wear resisting property is good.In UV ink, light trigger is that one is subject to light activated compound, after absorb light is shone, be excited into free radical, and energy trasfer, to photosensitivity molecule or photocrosslinking agent, makes UV ink that photocuring reaction occur.Current UV ink has become a kind of more ripe ink technology, and its pollutant emission is almost nil.UV curable ink due in system not containing solvent, there is efficient, wide adaptability, economy, energy-conservation, environmental friendliness, become tool novel ink with broad prospects for development.
Summary of the invention
The object of this invention is to provide a kind of energy-conserving and environment-protective UV curing inks and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of energy-conserving and environment-protective UV curing inks, is made up of the raw material of following weight part: pigment dyestuff 1-3, aminoresin 20-23, bicarbonate of ammonia 1-2, zeolite 1-2, ethylene glycol ether acetate 13-15, isoamyl butyrate 11-13, Viscoat 295 12-14, cobalt naphthenate 1-1.1, dibutyl tin laurate 1-2, tri (propylene glycol) diacrylate 10-12, ethyl acetate 5-8, UV epoxy acrylate 10-12,1173 light trigger 4-8, trifluoroacetylacetone europium 4-5, vulcabond 5-6, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, double pentaerythritol methacrylate 10-12, neopentyl glycol 5-7, p-tert-butyl benzoic acid 1-2, linking agent TAC2-3, polyisobutene 2-3, silane coupling agent KH5601-2, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
Energy-conserving and environment-protective UV curing inks of the present invention, be made up of following concrete steps: first add pigment dyestuff, aminoresin, bicarbonate of ammonia, zeolite, ethylene glycol ether acetate, isoamyl butyrate, Viscoat 295, cobalt naphthenate, dibutyl tin laurate stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except 1173 light triggers are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 1173 light triggers, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
The invention has the beneficial effects as follows: it once can be imprinted in gold and silver paperboard or PVC card by screen painting mode by ink of the present invention, improves production efficiency, has saved the energy, and not containing solvent, alleviate the infringement to human body and environmental pollution.
Specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of energy-conserving and environment-protective UV curing inks, is made up of the raw material of following weight part (kilogram): pigment dyestuff 1, aminoresin 20, bicarbonate of ammonia 1, zeolite 1, ethylene glycol ether acetate 13, isoamyl butyrate 11, Viscoat 295 12, cobalt naphthenate 1, dibutyl tin laurate 1, tri (propylene glycol) diacrylate 10, ethyl acetate 5, UV epoxy acrylate 10,1173 light trigger 4, trifluoroacetylacetone europium 4, vulcabond 5, auxiliary agent 4;
Described auxiliary agent is prepared from by the raw material of following weight part (kilogram): nano diatomite powder 0.2, nano mica powder 0.2, double pentaerythritol methacrylate 10, neopentyl glycol 5, p-tert-butyl benzoic acid 1, linking agent TAC2, polyisobutene 2, silane coupling agent KH5601, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
Energy-conserving and environment-protective UV curing inks of the present invention, be made up of following concrete steps: first add pigment dyestuff, aminoresin, bicarbonate of ammonia, zeolite, ethylene glycol ether acetate, isoamyl butyrate, Viscoat 295, cobalt naphthenate, dibutyl tin laurate stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except 1173 light triggers are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 1173 light triggers, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
The ink of gained, uses cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, 100% attachment; Use the spirituous cotton balls of leaching, 300 grams of pressure wipings 50 times, are as good as shape; To be soaked in salad oil (normal temperature) 8 hours, to be as good as shape; Use and be soaked with the cotton balls of salt solution, 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. an energy-conserving and environment-protective UV curing inks, it is characterized in that, be prepared from by the raw material of following weight part: pigment dyestuff 1-3, aminoresin 20-23, bicarbonate of ammonia 1-2, zeolite 1-2, ethylene glycol ether acetate 13-15, isoamyl butyrate 11-13, Viscoat 295 12-14, cobalt naphthenate 1-1.1, dibutyl tin laurate 1-2, tri (propylene glycol) diacrylate 10-12, ethyl acetate 5-8, UV epoxy acrylate 10-12,1173 light trigger 4-8, trifluoroacetylacetone europium 4-5, vulcabond 5-6, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, double pentaerythritol methacrylate 10-12, neopentyl glycol 5-7, p-tert-butyl benzoic acid 1-2, linking agent TAC2-3, polyisobutene 2-3, silane coupling agent KH5601-2, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
2. energy-conserving and environment-protective UV curing inks according to claim 1, it is characterized in that, be made up of following concrete steps: first add pigment dyestuff, aminoresin, bicarbonate of ammonia, zeolite, ethylene glycol ether acetate, isoamyl butyrate, Viscoat 295, cobalt naphthenate, dibutyl tin laurate stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except 1173 light triggers are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 1173 light triggers, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310602412.8A CN103666068B (en) | 2013-11-25 | 2013-11-25 | A kind of energy-conserving and environment-protective UV curing inks and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310602412.8A CN103666068B (en) | 2013-11-25 | 2013-11-25 | A kind of energy-conserving and environment-protective UV curing inks and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666068A CN103666068A (en) | 2014-03-26 |
| CN103666068B true CN103666068B (en) | 2016-03-23 |
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| CN201310602412.8A Active CN103666068B (en) | 2013-11-25 | 2013-11-25 | A kind of energy-conserving and environment-protective UV curing inks and preparation method thereof |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104804522A (en) * | 2015-04-13 | 2015-07-29 | 郭小曼 | Environment-friendly ultraviolet-curing pad-printing ink |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1970656A (en) * | 2006-11-23 | 2007-05-30 | 北京印刷学院 | Thermoforming plastic printing ink adopting ultraviolet-infra red drying technology |
| CN103342921A (en) * | 2013-07-29 | 2013-10-09 | 中国科学院化学研究所 | Ink with high hiding rate for ink-jet printing and application thereof to preparation of flexible plate |
-
2013
- 2013-11-25 CN CN201310602412.8A patent/CN103666068B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1970656A (en) * | 2006-11-23 | 2007-05-30 | 北京印刷学院 | Thermoforming plastic printing ink adopting ultraviolet-infra red drying technology |
| CN103342921A (en) * | 2013-07-29 | 2013-10-09 | 中国科学院化学研究所 | Ink with high hiding rate for ink-jet printing and application thereof to preparation of flexible plate |
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| Publication number | Publication date |
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| CN103666068A (en) | 2014-03-26 |
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| PB01 | Publication | ||
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: An energy-saving and environmentally friendly UV curing ink and its preparation method Effective date of registration: 20231113 Granted publication date: 20160323 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980065339 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20231219 Granted publication date: 20160323 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980065339 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240103 Address after: Room 101, No. 165 Qiaoli Nanmen Road, Changping Town, Dongguan City, Guangdong Province, 523575 Patentee after: DONGGUAN HAOCAI INK TECHNOLOGY CO.,LTD. Address before: 244000 No. 3201, Cuihu Fourth Road, Tongling Economic Development Zone, Anhui Province Patentee before: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. |
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