CN103666045B - UV curing inks of the little strong adhesion of a kind of granularity and preparation method thereof - Google Patents
UV curing inks of the little strong adhesion of a kind of granularity and preparation method thereof Download PDFInfo
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- CN103666045B CN103666045B CN201310600487.2A CN201310600487A CN103666045B CN 103666045 B CN103666045 B CN 103666045B CN 201310600487 A CN201310600487 A CN 201310600487A CN 103666045 B CN103666045 B CN 103666045B
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- ink
- strong adhesion
- nano
- diacrylate
- granularity
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- 239000000976 ink Substances 0.000 title claims abstract description 32
- 238000003848 UV Light-Curing Methods 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title claims description 8
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 14
- LJRSZGKUUZPHEB-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxypropoxy)propoxy]propyl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COC(C)COC(=O)C=C LJRSZGKUUZPHEB-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 9
- -1 hexanediyl ester Chemical class 0.000 claims abstract description 9
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims abstract description 7
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims abstract description 7
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims abstract description 7
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000005642 Oleic acid Substances 0.000 claims abstract description 7
- FQYUMYWMJTYZTK-UHFFFAOYSA-N Phenyl glycidyl ether Chemical compound C1OC1COC1=CC=CC=C1 FQYUMYWMJTYZTK-UHFFFAOYSA-N 0.000 claims abstract description 7
- 230000002745 absorbent Effects 0.000 claims abstract description 7
- 239000002250 absorbent Substances 0.000 claims abstract description 7
- 239000000975 dye Substances 0.000 claims abstract description 7
- UHESRSKEBRADOO-UHFFFAOYSA-N ethyl carbamate;prop-2-enoic acid Chemical compound OC(=O)C=C.CCOC(N)=O UHESRSKEBRADOO-UHFFFAOYSA-N 0.000 claims abstract description 7
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims abstract description 7
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims abstract description 7
- 239000000049 pigment Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000001071 citrus reticulata blanco var. mandarin Substances 0.000 claims abstract description 4
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 235000019353 potassium silicate Nutrition 0.000 claims abstract description 4
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 10
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000003112 inhibitor Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims description 3
- 239000011347 resin Substances 0.000 claims description 3
- 229920005989 resin Polymers 0.000 claims description 3
- 229910000077 silane Inorganic materials 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 claims 1
- 239000002245 particle Substances 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 206010034972 Photosensitivity reaction Diseases 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 230000036211 photosensitivity Effects 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000002211 ultraviolet spectrum Methods 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses the UV curing inks of the little strong adhesion of a kind of granularity, it is characterized in that, be made up of the raw material of following weight part: pigment dyestuff 1-3, urethane acrylate 24-26,1,6 hexanediyl ester 12-15, nano-aluminium oxide 2-4, gac 1-2, oleic acid 4-5, tri (propylene glycol) diacrylate 10-12, phenyl glycidyl ether 1-2, ultraviolet absorbent UV-531? 1-2, light trigger 2959? 4-7, cobalt naphthenate 1-2, water glass 2-3, mandarin oil 2-3, auxiliary agent 4-5; Auxiliary agent of the present invention improves the toughness of ink, makes distributes ink even, and maintains the stability of ink; Ink of the present invention has the advantages such as particle diameter is little, viscosity is low, it is excellent to soak, strong adhesion, and energy-conserving and environment-protective.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly the UV curing inks and preparation method thereof of the little strong adhesion of a kind of granularity.
Background technology
Ultraviolet light polymerization (UV) ink refers under uviolizing, utilizes the UV-light of different wave length and energy to make ink film forming and dry ink.Utilize different UV spectrum, can different-energy be produced, the monomer polymerization in different ink vehicle is become polymkeric substance, so the look film of UV ink has good machinery and chemical property.The major advantage of UV ink has: (1) is without solvent; (2) rate of drying is fast, and power consumption is few; (3) good luster, bright in luster; (4) water-fast, solvent resistant, wear resisting property is good.In UV ink, light trigger is that one is subject to light activated compound, after absorb light is shone, be excited into free radical, and energy trasfer, to photosensitivity molecule or photocrosslinking agent, makes UV ink that photocuring reaction occur.Current UV ink has become a kind of more ripe ink technology, and its pollutant emission is almost nil.Except not containing solvent, UV ink also just like not easily scumming, the advantages such as site is clear, the bright-coloured light of mass colour, and chemical resistance is excellent, low-consuming.
Summary of the invention
The object of this invention is to provide UV curing inks of the little strong adhesion of a kind of granularity and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
The UV curing inks of the little strong adhesion of a kind of granularity, be made up of the raw material of following weight part: pigment dyestuff 1-3, urethane acrylate 24-26,1,6 hexanediyl ester 12-15, nano-aluminium oxide 2-4, gac 1-2, oleic acid 4-5, tri (propylene glycol) diacrylate 10-12, phenyl glycidyl ether 1-2, ultraviolet absorbent UV-531 1-2, light trigger 29594-7, cobalt naphthenate 1-2, water glass 2-3, mandarin oil 2-3, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, silane resin acceptor kh-550 2-3, morpholine 1-2, neopentyl glycol 3-4, oxidation inhibitor 10351-2, linking agent TAC2-3, tri (propylene glycol) diacrylate 10-12,1-Methoxy-2-propyl acetate 5-10, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
The UV curing inks of the little strong adhesion of granularity of the present invention, be made up of following concrete steps: first add pigment dyestuff, urethane acrylate, 1,6 hexanediyl esters, nano-aluminium oxide, gac, oleic acid, tri (propylene glycol) diacrylate, phenyl glycidyl ether, ultraviolet absorbent UV-531 stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except light trigger 2959 are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add light trigger 2959, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
The invention has the beneficial effects as follows: auxiliary agent of the present invention improves the toughness of ink, make distributes ink even, and maintain the stability of ink; Ink of the present invention has the advantages such as particle diameter is little, viscosity is low, it is excellent to soak, strong adhesion, and energy-conserving and environment-protective.
Specific embodiments
Below by specific examples, the present invention is described in detail.
The UV curing inks of the little strong adhesion of a kind of granularity, be made up of the raw material of following weight part (kilogram): pigment dyestuff 1, urethane acrylate 24,1,6 hexanediyl ester 12, nano-aluminium oxide 2, gac 1, oleic acid 4, tri (propylene glycol) diacrylate 10, phenyl glycidyl ether 1, ultraviolet absorbent UV-531 1, light trigger 29594, cobalt naphthenate 1, water glass 2, mandarin oil 2, auxiliary agent 4;
Described auxiliary agent is prepared from by the raw material of following weight part (kilogram): nano diatomite powder 0.2 nano mica powder 0.2, silane resin acceptor kh-550 2, morpholine 1, neopentyl glycol 3, oxidation inhibitor 10351, linking agent TAC2, tri (propylene glycol) diacrylate 10,1-Methoxy-2-propyl acetate 5, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
The UV curing inks of the little strong adhesion of granularity of the present invention, be made up of following concrete steps: first add pigment dyestuff, urethane acrylate, 1,6 hexanediyl esters, nano-aluminium oxide, gac, oleic acid, tri (propylene glycol) diacrylate, phenyl glycidyl ether, ultraviolet absorbent UV-531 stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except light trigger 2959 are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add light trigger 2959, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
The ink of gained, uses cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, 100% attachment; Use the spirituous cotton balls of leaching, 300 grams of pressure wipings 50 times, are as good as shape; To be soaked in salad oil (normal temperature) 8 hours, to be as good as shape; Use and be soaked with the cotton balls of salt solution, 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. the UV curing inks of the little strong adhesion of granularity, it is characterized in that, be prepared from by the raw material of following weight part: pigment dyestuff 1-3, urethane acrylate 24-26,1,6 hexanediol diacrylate 12-15, nano-aluminium oxide 2-4, gac 1-2, oleic acid 4-5, tri (propylene glycol) diacrylate 10-12, phenyl glycidyl ether 1-2, ultraviolet absorbent UV-531 1-2, light trigger 29594-7, cobalt naphthenate 1-2, water glass 2-3, mandarin oil 2-3, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, silane resin acceptor kh-550 2-3, morpholine 1-2, neopentyl glycol 3-4, oxidation inhibitor 10351-2, linking agent TAC2-3, tri (propylene glycol) diacrylate 10-12,1-Methoxy-2-propyl acetate 5-10, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
2. the UV curing inks of the little strong adhesion of granularity according to claim 1, it is characterized in that, be made up of following concrete steps: first add pigment dyestuff, urethane acrylate, 1,6-hexanediyl ester, nano-aluminium oxide, gac, oleic acid, tri (propylene glycol) diacrylate, phenyl glycidyl ether, ultraviolet absorbent UV-531 stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except light trigger 2959 are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add light trigger 2959, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310600487.2A CN103666045B (en) | 2013-11-25 | 2013-11-25 | UV curing inks of the little strong adhesion of a kind of granularity and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310600487.2A CN103666045B (en) | 2013-11-25 | 2013-11-25 | UV curing inks of the little strong adhesion of a kind of granularity and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666045A CN103666045A (en) | 2014-03-26 |
| CN103666045B true CN103666045B (en) | 2016-04-13 |
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| CN201310600487.2A Active CN103666045B (en) | 2013-11-25 | 2013-11-25 | UV curing inks of the little strong adhesion of a kind of granularity and preparation method thereof |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104263062B (en) * | 2014-09-03 | 2016-04-27 | 安徽雅美油墨有限公司 | A kind of high absorption abrasion-resistance water environmental protection photocuring tin printing ink |
| CN104312265B (en) * | 2014-11-11 | 2016-04-27 | 合肥皖为电气设备工程有限责任公司 | Molten color inhibition plastic printing ink of a kind of environment-friendly type alcohol and preparation method thereof |
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|---|---|---|---|---|
| CN101560348A (en) * | 2009-05-25 | 2009-10-21 | 王景泉 | Ultraviolet light curing offset printing ink and preparation method thereof |
| CN102558580A (en) * | 2012-01-13 | 2012-07-11 | 中国印刷科学技术研究所 | Dissoluble light-cured resin and dissoluble ultraviolet (UV) printing ink and preparing method thereof |
| CN102653650A (en) * | 2012-04-24 | 2012-09-05 | 东莞上海大学纳米技术研究院 | Ultraviolet-curable white character jet-ink and preparation method thereof |
| CN102964913A (en) * | 2012-11-23 | 2013-03-13 | 东莞市佳烨化工科技有限公司 | Environment-friendly UV (ultraviolet) silk-screen printing anti-counterfeiting ink and preparation method thereof |
| CN102964916A (en) * | 2012-11-23 | 2013-03-13 | 东莞市佳烨化工科技有限公司 | Ultraviolet (UV) offset tin printing ink and method for preparing same |
| CN102964915A (en) * | 2012-11-23 | 2013-03-13 | 东莞市佳烨化工科技有限公司 | Ultraviolet (UV) screen plastic film printing ink and method for preparing same |
| CN103232751A (en) * | 2013-04-25 | 2013-08-07 | 深圳市美丽华油墨涂料有限公司 | UV (ultraviolet) curing ink and application thereof |
-
2013
- 2013-11-25 CN CN201310600487.2A patent/CN103666045B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101560348A (en) * | 2009-05-25 | 2009-10-21 | 王景泉 | Ultraviolet light curing offset printing ink and preparation method thereof |
| CN102558580A (en) * | 2012-01-13 | 2012-07-11 | 中国印刷科学技术研究所 | Dissoluble light-cured resin and dissoluble ultraviolet (UV) printing ink and preparing method thereof |
| CN102653650A (en) * | 2012-04-24 | 2012-09-05 | 东莞上海大学纳米技术研究院 | Ultraviolet-curable white character jet-ink and preparation method thereof |
| CN102964913A (en) * | 2012-11-23 | 2013-03-13 | 东莞市佳烨化工科技有限公司 | Environment-friendly UV (ultraviolet) silk-screen printing anti-counterfeiting ink and preparation method thereof |
| CN102964916A (en) * | 2012-11-23 | 2013-03-13 | 东莞市佳烨化工科技有限公司 | Ultraviolet (UV) offset tin printing ink and method for preparing same |
| CN102964915A (en) * | 2012-11-23 | 2013-03-13 | 东莞市佳烨化工科技有限公司 | Ultraviolet (UV) screen plastic film printing ink and method for preparing same |
| CN103232751A (en) * | 2013-04-25 | 2013-08-07 | 深圳市美丽华油墨涂料有限公司 | UV (ultraviolet) curing ink and application thereof |
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| CN103666045A (en) | 2014-03-26 |
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Effective date of registration: 20240103 Address after: 516121 Yide Industrial Park, Xiaopeng Gang Village, Longxi Street, Boluo County, Huizhou City, Guangdong Province Patentee after: Huizhou Zhimeide Technology Co.,Ltd. Address before: 244000 No. 3201, Cuihu Fourth Road, Tongling Economic Development Zone, Anhui Province Patentee before: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. |
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