CN103553717A - Crystal mirror surface Linglong glaze and application method thereof - Google Patents
Crystal mirror surface Linglong glaze and application method thereof Download PDFInfo
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- CN103553717A CN103553717A CN201310508924.8A CN201310508924A CN103553717A CN 103553717 A CN103553717 A CN 103553717A CN 201310508924 A CN201310508924 A CN 201310508924A CN 103553717 A CN103553717 A CN 103553717A
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Abstract
The invention relates to a crystal mirror surface Linglong glaze and an application method thereof. The Linglong glaze comprises the following components by weight percent: 13% to 16% of Suzhou kaolin, 15% to 22% of albite, 12% to 21% of soapstone, 18% to 25% of calcium carbonate, 8% to 15% of quartz, 8% to 10% of chinastone, 5% to 10% of borax, 1% to 3% of zinc oxide, 1% to 3% of lithium oxide, 1% to 3% of cerium oxide and 10% to 15% of frit. On the premise that the traditional Linglong porcelain production process is not changed, the Linglong glaze which is exquisite as well as glittering and translucent in appearance is prepared by designing the formulas and the process parameters of the novel Linglong glaze and the glaze materials of the inner surface and the outer surface of the novel Linglong glaze, so that the quality of JDZ (Jingdezhen) Linglong porcelains is greatly improved; and the ornamental effects of the traditional Linglong porcelains are broken through. In addition, the raw materials of the Linglong glaze are mainly natural minerals, so that the raw materials are abundant and low in cost and have no side effect on a human body. Thus, the Linglong glaze provided by the invention has a broad market space.
Description
Technical field
The present invention relates to ceramic technology field, particularly a kind of crystal minute surface small-size glaze and using method thereof.
Background technology
Ling-lung ware is by piercing technique on porcelain base substrate, chase out many well-regulated " exquisite eye " then with glaze, burn till after these eyes become translucent bright hole, very attractive in appearance, be called " glazing porcelain " however due to the in the past restriction of production technique and raw material treatment technology, glaze body after the traditional ling-lung ware in Jing Dezhen burns till in its eye is not completely transparent, really do not reach " exquisite " definition requirement, that is: dexterous, bright thorough, exquisitely carved technique effect.Therefore the ling-lung ware in Jing Dezhen can not meet the requirement of people to high-quality life at present.
Summary of the invention
The technical problem to be solved in the present invention is to provide crystal minute surface small-size glaze and the using method thereof that a kind of preparation technology is simple, with low cost, health environment-friendly is reaching exquisite technique effect.
Technical scheme of the present invention is: a kind of crystal minute surface small-size glaze, is characterized in that: the weight percent of described glaze consists of:
Kaolin of Suzhou 13-16%, albite 15-22%, talcum 12-21%, calcium carbonate 18-25%, quartzy 8-15%, glaze fruit 8-10%, borax 5-10%, zinc oxide 1-3%, Lithium Oxide 98min 1-3%, cerium oxide 1-3%, frit 10-15%;
The chemical weight percentage composition of above-mentioned frit is: Na
2o 1-3%, CaO 6-10%, ZnO 6-8%, BaO7-9%, SiO
210-20%, B
2o
336-45%, Li
2o 10-15%.
The glaze glossiness 100-120 of described crystal minute surface small-size glaze.
The glaze specific surface area of described crystal minute surface small-size glaze is 100-150m
2/ g.
The using method of above-mentioned crystal minute surface small-size glaze, is characterized in that according to following steps:
(1) choose the excellent base substrate after 760 ℃ of biscuitings;
(2) on base substrate, paste pierced decoration decorative pattern, through sandblast carving eye, wash, put small-size glaze, wash after glaze, in 900 ℃ warm biscuiting, kiln discharge, obtain biscuit;
(3) cover-coat enamel and outer cover-coat enamel in respectively on inside and outside the executing of above-mentioned biscuit, the porcelain body of decorating through 1320 ℃ of grand feus, kiln discharge, acquisition crystal minute surface small-size glaze.
The using method of described crystal minute surface small-size glaze, is characterized in that: the chemical weight percentage composition of described interior cover-coat enamel is: Na
2o 12-20%, CaO 14-18%, Li
2o 5-8%, Al
2o
37-10%, SiO
26-15%, B
2o
345-55%.
The using method of described crystal minute surface small-size glaze, is characterized in that: the chemical weight percentage composition of described outer cover-coat enamel is: Na
2o 12-20%, CaO 14-18%, ZnO 5-8%, Al
2o
315-20%, SiO
210-15%, B
2o
335-40%.
The using method of described crystal minute surface small-size glaze, it is characterized in that: the calcining system of described grand feu is: room temperature-650 ℃ are oxidation period, temperature rise rate is 7 degree/min, and the temperature rise rate of 650-1000 ℃ is 4 degree/min, 1000 ℃ for oxidation soak, be incubated 60 minutes, the 1000-1200 ℃ of reduction period of attaching most importance to, temperature rise rate is 1 degree/min, 1200-1320 ℃ is weak reduction period, temperature rise rate is 0.8 degree/min, is incubated 60 minutes and becomes porcelain in the time of 1320 ℃.
The using method of described crystal minute surface small-size glaze, is characterized in that: described interior cover-coat enamel thickness is 0.5-0.8mm.
The using method of described crystal minute surface small-size glaze, is characterized in that: described outer cover-coat enamel thickness is 0.6-1mm.
The using method of described crystal minute surface small-size glaze, is characterized in that: the porcelain body surface that described crystal minute surface small-size glaze is decorated adopts Freehandhand-drawing mode blue and white or decal paper to decorate.
The present invention is not changing under the prerequisite of traditional ling-lung ware production technique, by designing new glaze formula and processing parameter, obtain just like noble crystal minute surface small-size glaze as penetrating as glass, crystal, not only significantly promoted the quality of Jing Dezhen ling-lung ware, also broken through the decorative effect of traditional ling-lung ware, and the raw materials used major part of the present invention be natural mineral raw not only originate enrich cheap, and without any side effects to human body, therefore there is the wide market space.
Embodiment
embodiment 1-6:
By table, 1-4 forms preparation raw material, table 5 processing parameter, through selecting base, paste pierced decoration decorative pattern, sandblast carving eye, wash, put small-size glaze, wash glaze, middle temperature biscuiting, execute inside and outside cover-coat enamel, grand feu obtains the ling-lung ware that crystal minute surface small-size glaze is decorated.
Table 1 small-size glaze material formula forms (massfraction %)
The chemical constitution of table 2 frit (massfraction %)
The chemical constitution of the interior cover-coat enamel of table 3 (massfraction %)
The chemical constitution of the outer cover-coat enamel of table 4 (massfraction %)
Table 5 preparation condition and the performance test results
Claims (10)
1. a crystal minute surface small-size glaze, is characterized in that: the weight percent of described glaze consists of:
Kaolin of Suzhou 13-16%, albite 15-22%, talcum 12-21%, calcium carbonate 18-25%, quartzy 8-15%, glaze fruit 8-10%, borax 5-10%, zinc oxide 1-3%, Lithium Oxide 98min 1-3%, cerium oxide 1-3%, frit 10-15%;
The chemical weight percentage composition of above-mentioned frit is: Na
2o 1-3%, CaO 6-10%, ZnO 6-8%, BaO7-9%, SiO
210-20%, B
2o
336-45%, Li
2o 10-15%.
2. crystal minute surface small-size glaze according to claim 1, is characterized in that: the glaze glossiness of described crystal minute surface small-size glaze is 100-120.
3. crystal minute surface small-size glaze according to claim 1, is characterized in that: the glaze specific surface area of described crystal minute surface small-size glaze is 100-120m
2/ g.
4. the using method of crystal minute surface small-size glaze according to claim 1, is characterized in that according to following steps:
(1) choose the excellent base substrate after 760 ℃ of biscuitings;
(2) on base substrate, paste pierced decoration decorative pattern, through sandblast carving eye, wash, put small-size glaze, wash after glaze, in 900 ℃ warm biscuiting, kiln discharge, obtain biscuit;
(3) cover-coat enamel and outer cover-coat enamel in respectively on inside and outside the executing of above-mentioned biscuit, the porcelain body of decorating through 1320 ℃ of grand feus, kiln discharge, acquisition crystal minute surface small-size glaze.
5. the using method of crystal minute surface small-size glaze according to claim 4, is characterized in that: the chemical weight percentage composition of described interior cover-coat enamel is: Na
2o 12-20%, CaO 14-18%, Li
2o 5-8%, Al
2o
37-10%, SiO
26-15%, B
2o
345-55%.
6. the using method of crystal minute surface small-size glaze according to claim 4, is characterized in that: the chemical weight percentage composition of described outer cover-coat enamel is: Na
2o 12-20%, CaO 14-18%, ZnO 5-8%, Al
2o
315-20%, SiO
210-15%, B
2o
335-40%.
7. the using method of crystal minute surface small-size glaze according to claim 4, it is characterized in that: the calcining system of described grand feu is: room temperature-650 ℃ are oxidation period, temperature rise rate is 7 degree/min, and the temperature rise rate of 650-1000 ℃ is 4 degree/min, 1000 ℃ for oxidation soak, be incubated 60 minutes, the 1000-1200 ℃ of reduction period of attaching most importance to, temperature rise rate is 1 degree/min, 1200-1320 ℃ is weak reduction period, temperature rise rate is 0.8 degree/min, is incubated 60 minutes and becomes porcelain in the time of 1320 ℃.
8. the using method of crystal minute surface small-size glaze according to claim 4, is characterized in that: described interior cover-coat enamel thickness is 0.5-0.8mm.
9. the using method of crystal minute surface small-size glaze according to claim 4, is characterized in that: described outer cover-coat enamel thickness is 0.6-1mm.
10. the using method of crystal minute surface small-size glaze according to claim 4, is characterized in that: the porcelain body surface that described crystal minute surface small-size glaze is decorated adopts Freehandhand-drawing mode blue and white or decal paper to decorate.
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|---|---|---|---|
| CN201310508924.8A CN103553717B (en) | 2013-10-25 | 2013-10-25 | Crystal mirror surface Linglong glaze and application method thereof |
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|---|---|---|---|
| CN201310508924.8A CN103553717B (en) | 2013-10-25 | 2013-10-25 | Crystal mirror surface Linglong glaze and application method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103553717A true CN103553717A (en) | 2014-02-05 |
| CN103553717B CN103553717B (en) | 2014-08-13 |
Family
ID=50008136
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103964825A (en) * | 2014-04-10 | 2014-08-06 | 安徽青花坊瓷业股份有限公司 | Preparation method of heat-resisting solid solution blue and white porcelain |
| CN104649720A (en) * | 2015-02-10 | 2015-05-27 | 山东建筑大学 | Ceramic glaze prepared from waste concrete powder and preparation method of ceramic glaze |
| CN104844151A (en) * | 2015-04-15 | 2015-08-19 | 江苏省宜兴彩陶工艺厂 | Method used for preparing ceramic products with intermediate layer spraying slurry |
| CN104891809A (en) * | 2015-06-02 | 2015-09-09 | 景德镇市亚星特种陶瓷有限公司 | Flaky exquisite glaze |
| CN105800932A (en) * | 2016-03-30 | 2016-07-27 | 安徽青花坊瓷业股份有限公司 | Ground glaze for high-temperature in-glaze decoration manufacturing |
| CN107352799A (en) * | 2017-07-27 | 2017-11-17 | 景德镇富玉青花玲珑陶瓷有限公司 | A kind of crystallite emerald small-size glaze and its application process |
| CN107935392A (en) * | 2017-11-30 | 2018-04-20 | 南宁市生润科技有限公司 | A kind of celeste glaze with anti-pollution function |
| CN107954600A (en) * | 2017-12-05 | 2018-04-24 | 湖南陶润会文化传播有限公司 | Crackle crystal glaze and preparation method thereof |
| CN109265000A (en) * | 2018-11-19 | 2019-01-25 | 惠州学院 | A kind of black pigment used by women in ancient times to paint their eyebrows color medium temperature ceramics glaze and preparation method thereof |
| CN110981418A (en) * | 2019-12-30 | 2020-04-10 | 景德镇市望龙陶瓷有限公司 | Preparation method of colored glaze exquisite porcelain |
| CN110981417A (en) * | 2019-12-30 | 2020-04-10 | 景德镇市望龙陶瓷有限公司 | Preparation method of five-color exquisite porcelain |
| CN112266170A (en) * | 2020-11-20 | 2021-01-26 | 冯琪茗 | Preparation process of high-temperature reduction flame under-glaze color glaze |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101602594A (en) * | 2009-07-06 | 2009-12-16 | 景德镇陶瓷协会 | Process technique for producing blue and white delicate porcelain |
| CN101875567A (en) * | 2010-06-04 | 2010-11-03 | 深圳市永丰源实业有限公司 | Exquisite glaze, exquisite ceramic and preparation process of exquisite ceramic |
| CN101913870A (en) * | 2010-07-14 | 2010-12-15 | 景德镇国韵青瓷股份有限公司 | Blue-and-white bone jewelry delicate porcelain |
| CN102020419A (en) * | 2009-09-23 | 2011-04-20 | 曾庆春 | Oxidizing flame high-temperature exquisite glaze and method for applying same to bone porcelain ornaments |
| CN103232268A (en) * | 2013-05-13 | 2013-08-07 | 景德镇市宁封窑陶瓷文化发展有限公司 | Five-color exquisite glaze and five-color exquisite porcelain |
| CN103253865A (en) * | 2013-05-03 | 2013-08-21 | 深圳市永丰源瓷业有限公司 | Manufacturing process of crystal frit-containing exquisite glazes and exquisite products |
-
2013
- 2013-10-25 CN CN201310508924.8A patent/CN103553717B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101602594A (en) * | 2009-07-06 | 2009-12-16 | 景德镇陶瓷协会 | Process technique for producing blue and white delicate porcelain |
| CN102020419A (en) * | 2009-09-23 | 2011-04-20 | 曾庆春 | Oxidizing flame high-temperature exquisite glaze and method for applying same to bone porcelain ornaments |
| CN101875567A (en) * | 2010-06-04 | 2010-11-03 | 深圳市永丰源实业有限公司 | Exquisite glaze, exquisite ceramic and preparation process of exquisite ceramic |
| CN101913870A (en) * | 2010-07-14 | 2010-12-15 | 景德镇国韵青瓷股份有限公司 | Blue-and-white bone jewelry delicate porcelain |
| CN103253865A (en) * | 2013-05-03 | 2013-08-21 | 深圳市永丰源瓷业有限公司 | Manufacturing process of crystal frit-containing exquisite glazes and exquisite products |
| CN103232268A (en) * | 2013-05-13 | 2013-08-07 | 景德镇市宁封窑陶瓷文化发展有限公司 | Five-color exquisite glaze and five-color exquisite porcelain |
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103964825A (en) * | 2014-04-10 | 2014-08-06 | 安徽青花坊瓷业股份有限公司 | Preparation method of heat-resisting solid solution blue and white porcelain |
| CN104649720A (en) * | 2015-02-10 | 2015-05-27 | 山东建筑大学 | Ceramic glaze prepared from waste concrete powder and preparation method of ceramic glaze |
| CN104844151A (en) * | 2015-04-15 | 2015-08-19 | 江苏省宜兴彩陶工艺厂 | Method used for preparing ceramic products with intermediate layer spraying slurry |
| CN104891809A (en) * | 2015-06-02 | 2015-09-09 | 景德镇市亚星特种陶瓷有限公司 | Flaky exquisite glaze |
| CN104891809B (en) * | 2015-06-02 | 2016-08-24 | 景德镇市亚星特种陶瓷有限公司 | A kind of sheet small-size glaze |
| CN105800932A (en) * | 2016-03-30 | 2016-07-27 | 安徽青花坊瓷业股份有限公司 | Ground glaze for high-temperature in-glaze decoration manufacturing |
| CN107352799B (en) * | 2017-07-27 | 2019-09-20 | 景德镇富玉青花玲珑陶瓷有限公司 | A kind of crystallite emerald small-size glaze and its application method |
| CN107352799A (en) * | 2017-07-27 | 2017-11-17 | 景德镇富玉青花玲珑陶瓷有限公司 | A kind of crystallite emerald small-size glaze and its application process |
| CN107935392A (en) * | 2017-11-30 | 2018-04-20 | 南宁市生润科技有限公司 | A kind of celeste glaze with anti-pollution function |
| CN107954600A (en) * | 2017-12-05 | 2018-04-24 | 湖南陶润会文化传播有限公司 | Crackle crystal glaze and preparation method thereof |
| CN109265000A (en) * | 2018-11-19 | 2019-01-25 | 惠州学院 | A kind of black pigment used by women in ancient times to paint their eyebrows color medium temperature ceramics glaze and preparation method thereof |
| CN110981418A (en) * | 2019-12-30 | 2020-04-10 | 景德镇市望龙陶瓷有限公司 | Preparation method of colored glaze exquisite porcelain |
| CN110981417A (en) * | 2019-12-30 | 2020-04-10 | 景德镇市望龙陶瓷有限公司 | Preparation method of five-color exquisite porcelain |
| CN110981418B (en) * | 2019-12-30 | 2021-12-14 | 景德镇市望龙陶瓷有限公司 | Preparation method of colored glaze exquisite porcelain |
| CN110981417B (en) * | 2019-12-30 | 2022-04-22 | 景德镇市望龙陶瓷有限公司 | Preparation method of five-color exquisite porcelain |
| CN112266170A (en) * | 2020-11-20 | 2021-01-26 | 冯琪茗 | Preparation process of high-temperature reduction flame under-glaze color glaze |
| CN112266170B (en) * | 2020-11-20 | 2022-04-22 | 冯琪茗 | Preparation process of high-temperature reduction flame under-glaze color glaze |
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