CN103525552A - Dendrobium nobile cigarette flavor and application thereof - Google Patents
Dendrobium nobile cigarette flavor and application thereof Download PDFInfo
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- CN103525552A CN103525552A CN201310502730.7A CN201310502730A CN103525552A CN 103525552 A CN103525552 A CN 103525552A CN 201310502730 A CN201310502730 A CN 201310502730A CN 103525552 A CN103525552 A CN 103525552A
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- stem
- noble dendrobium
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- filtrate
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- 240000004638 Dendrobium nobile Species 0.000 title claims abstract description 32
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 27
- 239000000796 flavoring agent Substances 0.000 title abstract 4
- 235000019634 flavors Nutrition 0.000 title abstract 4
- 241000208125 Nicotiana Species 0.000 claims abstract description 43
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 43
- 239000000284 extract Substances 0.000 claims abstract description 37
- 239000002994 raw material Substances 0.000 claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 11
- 239000000706 filtrate Substances 0.000 claims description 32
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- 238000007599 discharging Methods 0.000 claims description 16
- 238000000967 suction filtration Methods 0.000 claims description 16
- 230000008014 freezing Effects 0.000 claims description 8
- 238000007710 freezing Methods 0.000 claims description 8
- 230000000717 retained effect Effects 0.000 claims description 8
- 239000002904 solvent Substances 0.000 claims description 6
- 102000035101 Aspartic proteases Human genes 0.000 claims description 5
- 108091005502 Aspartic proteases Proteins 0.000 claims description 5
- 108090000145 Bacillolysin Proteins 0.000 claims description 5
- 102000035092 Neutral proteases Human genes 0.000 claims description 5
- 108091005507 Neutral proteases Proteins 0.000 claims description 5
- 108091005804 Peptidases Proteins 0.000 claims description 4
- 102000035195 Peptidases Human genes 0.000 claims description 4
- 238000004090 dissolution Methods 0.000 claims description 2
- 238000000605 extraction Methods 0.000 abstract description 7
- 235000009508 confectionery Nutrition 0.000 abstract description 3
- 239000003205 fragrance Substances 0.000 abstract description 3
- 239000002304 perfume Substances 0.000 abstract description 3
- 238000002156 mixing Methods 0.000 abstract description 2
- 210000002345 respiratory system Anatomy 0.000 abstract description 2
- 241001523681 Dendrobium Species 0.000 abstract 3
- 230000007794 irritation Effects 0.000 abstract 3
- 239000000779 smoke Substances 0.000 abstract 3
- 239000000126 substance Substances 0.000 abstract 2
- 206010013911 Dysgeusia Diseases 0.000 abstract 1
- 150000001720 carbohydrates Chemical class 0.000 abstract 1
- 239000008399 tap water Substances 0.000 description 12
- 235000020679 tap water Nutrition 0.000 description 12
- 230000000391 smoking effect Effects 0.000 description 8
- 235000013599 spices Nutrition 0.000 description 7
- 239000012153 distilled water Substances 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 241000411851 herbal medicine Species 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 235000012055 fruits and vegetables Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
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- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a dendrobium nobile cigarette flavor and application thereof. The method comprises the steps of taking dendrobium as a raw material, obtaining a dendrobium micromolecular substance extract through a natural extraction process, obtaining a dendrobium carbohydrate substance extract through an enzymolysis process, and mixing the two extracts according to a ratio to obtain the required tobacco flavor. The cigarette perfume can make cigarette smoke have fresh and sweet flavor, make smoke exquisite, clean aftertaste, and simultaneously alleviate irritation of smoke to respiratory tract of smoker, and has functions of increasing sweet feeling and reducing irritation. It features fine fragrance and less irritation.
Description
Technical field
The invention belongs to essence spice for cigarette technical field, specifically relate to a kind of tobacco aromatics using that can promote cigarette smoking quality that the stem of noble dendrobium prepared as raw material of take.Meanwhile, the invention still further relates to the concrete application of this tobacco aromatics using in production of cigarettes.
Background technology
Essence spice for cigarette is as the basic raw material of cigarette blending, and its exploitation innovation receives much attention.From raw material angle, existing essence spice for cigarette classified and can be divided into tealeaves class, fruits and vegetables class, fragrant flower class, plant subclass, herbal medicine, tobacco etc.
Current, along with scientific and technical progress, people more and more pay close attention to the harm problem that smoking brings, and smoker is more and more higher to the specification of quality of cigarette, produce low evil, high-quality cigarette is imperative.The exploitation of the herbal medicine class tobacco aromatics using that therefore pharmaceutical use is higher is trend.The core technology flavoring and casing of tobacco industry is also stricter to the requirement of spices, need to make up by the spices adding the insufficient fragrance on cigarette tobacco leaf formulation, eliminates assorted gas, reduces the effects such as stimulation.Make cigarette product suction comfortableness better, cigarette perfume (or spice) is more abundant, sufficient, thereby inhaling taste, smell on perfume (or spice) and have individual style, strengthens the feature of cigarette product.
The stem of the stem of noble dendrobium can clearing heat and promoting fluid, and clear and rich throat has a good curative effect to treatment voice is hoarse.Although at present more to the research of the stem of noble dendrobium, the research of preparing stem of noble dendrobium class tobacco aromatics using aspect there is not yet report.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of tobacco aromatics using that the stem of noble dendrobium prepared as raw material of take is provided, this tobacco aromatics using can promote the suction quality of cigarette.
The present invention also aims to provide the concrete application of described tobacco aromatics using in cigarette.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage ratio adopting in the present invention is mass percent.
A tobacco aromatics using, is prepared by following method:
(1) stem of noble dendrobium raw material is packed in round-bottomed flask, add 10～20 times of solvents, under 60～90 ℃ of conditions, 1～3h is extracted in thermal backflow, filter, 10～20 times of same solvent that add filter residue continue thermal backflow and extract 1～3h, filter, 2 times filtrate merges, under vacuum tightness 0.02～0.08MPa, 50～80 ℃ of conditions of temperature, concentrated filtrate is to 3～6 times of raw material weight, add 5～8 times of 95% freezing back dissolving 24～48h of ethanol, suction filtration, filter residue is retained, it is 1.0244+0.008 that filtrate is concentrated to density, and discharging obtains 1# extract;
(2) 10～20 times of dissolution with solvents for filter residue of retaining, add 0.5%～2% proteolytic enzyme, enzymolysis 12～24h under the condition of 30～45 ℃, add activated carbon decolorizing 2～6h of 0.5%～2%, suction filtration, it is 1.0261+0.008 that filtrate is concentrated to density, discharging obtains 2# extract;
(3) after 1# extract and 2# extract are mixed by the mass ratio of 1～5:1 stem of noble dendrobium tobacco aromatics using.
The preferred Herba Dendrobii of the described stem of noble dendrobium.
Described proteolytic enzyme is aspartic protease or neutral protease.
The application of stem of noble dendrobium tobacco aromatics using in cigarette: described stem of noble dendrobium tobacco aromatics using is pressed to the consumption of the mono-case of the mono-case～30g/ of 10g/, made an addition on pipe tobacco in the mode of feeding in raw material.
Compared with prior art, the present invention has following beneficial effect:
1, the interpolation of this tobacco aromatics using in cigarette, is characterized in that fragrance is fine and smooth, has the sweet sense of increasing, and alleviates the stimulation of flue gas to smoker's respiratory tract.
2, production technique operability of the present invention and standardization are strong, can realize suitability for industrialized production, have good development prospect.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein is only in order to explain the present invention, the protection domain being not intended to limit the present invention.
Embodiment 1
1. 800g Herba Dendrobii raw material is packed in round-bottomed flask, add 15 times of tap water, under 60～90 ℃ of conditions, 2h is extracted in thermal backflow, filter, filter residue adds 15 times of tap water to continue thermal backflow extraction 2h, filters, and 2 times filtrate merges, under vacuum tightness 0.02～0.08MPa, 50～80 ℃ of conditions of temperature, concentrated filtrate is to 5 times of raw material weight, add 6 times of 95% freezing back dissolving 24h of ethanol, suction filtration, filter residue is retained, it is 1.0244+0.008 that filtrate is concentrated to density, and discharging obtains 1# extract.
2. the filter residue of retaining dissolves with 15 times of distilled water, adds 0.5% aspartic protease, and enzymolysis 12h under the condition of 30～45 ℃ adds 0.5% activated carbon decolorizing 6h, suction filtration, and it is 1.0261+0.008 that filtrate is concentrated to density, discharging obtains 2# extract.
3. after 1# extract and 2# extract being mixed in 1:1 ratio stem of noble dendrobium tobacco aromatics using.
4. the application in pipe tobacco: according to the consumption of the mono-case of 10g/, add in pipe tobacco with feed way, and press same method preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
Embodiment 2:
1. 800g stem of noble dendrobium raw material is packed in round-bottomed flask, add 10 times of tap water, under 60～90 ℃ of conditions, 3h is extracted in thermal backflow, filter, filter residue adds 10 times of tap water to continue thermal backflow extraction 3h, filters, and 2 times filtrate merges, under vacuum tightness 0.02～0.08MPa, 50～80 ℃ of conditions of temperature, concentrated filtrate is to 3 times of raw material weight, add 8 times of 95% freezing back dissolving 24h of ethanol, suction filtration, filter residue is retained, it is 1.0244+0.008 that filtrate is concentrated to density, and discharging obtains 1# extract.
2. the filter residue of retaining dissolves with 10 times of distilled water, adds 1% neutral protease, and enzymolysis 12h under the condition of 30～45 ℃ adds 1% activated carbon decolorizing 4h, suction filtration, and it is 1.0261+0.008 that filtrate is concentrated to density, discharging obtains 2# extract.
3. after 1# extract and 2# extract being mixed in 2:1 ratio stem of noble dendrobium tobacco aromatics using.
4. the application in pipe tobacco: according to the consumption of the mono-case of 10g/, add in pipe tobacco with feed way, and press same method preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
Embodiment 3:
1. 800g stem of noble dendrobium raw material is packed in round-bottomed flask, add 20 times of tap water, under 60～90 ℃ of conditions, 1h is extracted in thermal backflow, filter, filter residue adds 10 times of tap water to continue thermal backflow extraction 1h, filters, and 2 times filtrate merges, under vacuum tightness 0.02～0.08MPa, 50～80 ℃ of conditions of temperature, concentrated filtrate is to 4 times of raw material weight, add 5 times of 95% freezing back dissolving 48h of ethanol, suction filtration, filter residue is retained, it is 1.0244+0.008 that filtrate is concentrated to density, and discharging obtains 1# extract.
2. the filter residue of retaining dissolves with 15 times of distilled water, adds 2% neutral protease, and enzymolysis 24h under the condition of 30～45 ℃ adds 2% activated carbon decolorizing 2h, suction filtration, and it is 1.0261+0.008 that filtrate is concentrated to density, discharging obtains 2# extract.
3. after 1# extract and 2# extract being mixed in 3:1 ratio stem of noble dendrobium tobacco aromatics using.
4. the application in pipe tobacco: according to the consumption of the mono-case of 20g/, add in pipe tobacco with feed way, and press same method preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
Embodiment 4:
1. 800g stem of noble dendrobium raw material is packed in round-bottomed flask, add 15 times of tap water, under 60～90 ℃ of conditions, 1h is extracted in thermal backflow, filter, filter residue adds 15 times of tap water to continue thermal backflow extraction 1h, filters, and 2 times filtrate merges, under vacuum tightness 0.02～0.08MPa, 50～80 ℃ of conditions of temperature, concentrated filtrate is to 5 times of raw material weight, add 8 times of 95% freezing back dissolving 24h of ethanol, suction filtration, filter residue is retained, it is 1.0244+0.008 that filtrate is concentrated to density, and discharging obtains 1# extract.
2. the filter residue of retaining dissolves with 15 times of distilled water, adds 2% neutral protease, and enzymolysis 16h under the condition of 30～45 ℃ adds 1% activated carbon decolorizing 4h, suction filtration, and it is 1.0261+0.008 that filtrate is concentrated to density, discharging obtains 2# extract.
3. after 1# extract and 2# extract being mixed in 4:1 ratio stem of noble dendrobium tobacco aromatics using.
4. the application in pipe tobacco: according to the consumption of the mono-case of 20g/, add in pipe tobacco with feed way, and press same method preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
Embodiment 5:
1. 800g stem of noble dendrobium raw material is packed in round-bottomed flask, add 20 times of tap water, under 60～90 ℃ of conditions, 1h is extracted in thermal backflow, filter, filter residue adds 20 times of tap water to continue thermal backflow extraction 1h, filters, and 2 times filtrate merges, under vacuum tightness 0.02～0.08MPa, 50～80 ℃ of conditions of temperature, concentrated filtrate is to 6 times of raw material weight, add 5 times of 95% freezing back dissolving 24h of ethanol, suction filtration, filter residue is retained, it is 1.0244+0.008 that filtrate is concentrated to density, and discharging obtains 1# extract.
2. the filter residue of retaining dissolves with 20 times of distilled water, adds 1% aspartic protease, and enzymolysis 20h under the condition of 30～45 ℃ adds 2% activated carbon decolorizing 3h, suction filtration, and it is 1.0261+0.008 that filtrate is concentrated to density, discharging obtains 2# extract.
3. after 1# extract and 2# extract being mixed in 5:1 ratio stem of noble dendrobium tobacco aromatics using.
4. the application in pipe tobacco: according to the consumption of the mono-case of 20g/, add in pipe tobacco with feed way, and press same method preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
Embodiment 6:
1. 800g stem of noble dendrobium raw material is packed in round-bottomed flask, add 10 times of tap water, under 60～90 ℃ of conditions, 2h is extracted in thermal backflow, filter, filter residue adds 10 times of tap water to continue thermal backflow extraction 2h, filters, and 2 times filtrate merges, under vacuum tightness 0.02～0.08MPa, 50～80 ℃ of conditions of temperature, concentrated filtrate is to 4 times of raw material weight, add 6 times of 95% freezing back dissolving 48h of ethanol, suction filtration, filter residue is retained, it is 1.0244+0.008 that filtrate is concentrated to density, and discharging obtains 1# extract.
2. the filter residue of retaining dissolves with 10 times of distilled water, adds 0.5% aspartic protease, and enzymolysis 12h under the condition of 30～45 ℃ adds 2% activated carbon decolorizing 2h, suction filtration, and it is 1.0261+0.008 that filtrate is concentrated to density, discharging obtains 2# extract.
3. after 1# extract and 2# extract being mixed in 2:1 ratio stem of noble dendrobium tobacco aromatics using.
4. the application in pipe tobacco: according to the consumption of the mono-case of 30g/, add in pipe tobacco with feed way, and press same method preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any modifications of doing within the spirit and principles in the present invention, be equal to and replace and improvement etc., within all should being included in protection scope of the present invention.
Claims (4)
1. a stem of noble dendrobium tobacco aromatics using, is prepared by following method:
(1) stem of noble dendrobium raw material is packed in round-bottomed flask, add 10～20 times of solvents, under 60～90 ℃ of conditions, 1～3h is extracted in thermal backflow, filter, 10～20 times of same solvent that add filter residue continue thermal backflow and extract 1～3h, filter, 2 times filtrate merges, under vacuum tightness 0.02～0.08MPa, 50～80 ℃ of conditions of temperature, concentrated filtrate is to 3～6 times of raw material weight, add 5～8 times of 95% freezing back dissolving 24～48h of ethanol, suction filtration, filter residue is retained, it is 1.0244+0.008 that filtrate is concentrated to density, and discharging obtains 1# extract;
(2) 10～20 times of dissolution with solvents for filter residue of retaining, add 0.5%～2% proteolytic enzyme, enzymolysis 12～24h under the condition of 30～45 ℃, add activated carbon decolorizing 2～6h of 0.5%～2%, suction filtration, it is 1.0261+0.008 that filtrate is concentrated to density, discharging obtains 2# extract;
(3) after 1# extract and 2# extract are mixed in the ratio of 1～5:1 stem of noble dendrobium tobacco aromatics using.
2. stem of noble dendrobium tobacco aromatics using according to claim 1, is characterized in that: the preferred Herba Dendrobii of the described stem of noble dendrobium.
3. stem of noble dendrobium tobacco aromatics using according to claim 1, is characterized in that: described proteolytic enzyme is aspartic protease or neutral protease.
4. the application of stem of noble dendrobium tobacco aromatics using claimed in claim 1 in cigarette, is specially: described stem of noble dendrobium tobacco aromatics using is pressed to the consumption of the mono-case of 10g～30g/, in the mode of feeding in raw material, made an addition on pipe tobacco.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310502730.7A CN103525552A (en) | 2013-10-23 | 2013-10-23 | Dendrobium nobile cigarette flavor and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310502730.7A CN103525552A (en) | 2013-10-23 | 2013-10-23 | Dendrobium nobile cigarette flavor and application thereof |
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| CN103525552A true CN103525552A (en) | 2014-01-22 |
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| CN201310502730.7A Pending CN103525552A (en) | 2013-10-23 | 2013-10-23 | Dendrobium nobile cigarette flavor and application thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105273841A (en) * | 2015-08-06 | 2016-01-27 | 云南中烟工业有限责任公司 | Phoebe spp. spice preparation method and application |
| CN105733994A (en) * | 2016-04-18 | 2016-07-06 | 云南中烟工业有限责任公司 | Trichoderma aureoviride strain and method for preparing dendrobium candidum tobacco flavor from same |
| CN106148007A (en) * | 2016-08-11 | 2016-11-23 | 江西中烟工业有限责任公司 | A kind of method preparing cigarette Herba Dendrobii spice for Extraction solvent with jowar wine |
| CN108112949A (en) * | 2017-12-06 | 2018-06-05 | 成都新柯力化工科技有限公司 | A kind of preparation method of natural flavor |
| CN108851179A (en) * | 2018-08-07 | 2018-11-23 | 武汉纺织大学 | One kind containing Herba Dendrobii extract additive in cigarette and preparation method thereof |
| CN113308301A (en) * | 2021-06-04 | 2021-08-27 | 安徽中烟工业有限责任公司 | Dendrobium polysaccharide Amadori latent aroma spice, preparation method thereof and application thereof in cigarettes |
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| CN101496638A (en) * | 2009-03-11 | 2009-08-05 | 云南天宏香精香料有限公司 | Additive agent for Chinese herbal medicine tobacco as well as preparation method and application |
| CN102743598A (en) * | 2012-06-29 | 2012-10-24 | 四川万安石斛产业开发有限公司 | var. Denneanum extract and formula particles thereof |
| CN102928373A (en) * | 2012-11-26 | 2013-02-13 | 广东省农业科学院花卉研究所 | Method for testing content of dendrobe polysaccharide and application thereof |
| CN102964461A (en) * | 2012-11-20 | 2013-03-13 | 六安同济生生物科技有限公司 | Auxiliary extraction method of biological enzyme for improving dissolution rate of dendrobe bioactive polysaccharide |
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2013
- 2013-10-23 CN CN201310502730.7A patent/CN103525552A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101496638A (en) * | 2009-03-11 | 2009-08-05 | 云南天宏香精香料有限公司 | Additive agent for Chinese herbal medicine tobacco as well as preparation method and application |
| CN102743598A (en) * | 2012-06-29 | 2012-10-24 | 四川万安石斛产业开发有限公司 | var. Denneanum extract and formula particles thereof |
| CN102964461A (en) * | 2012-11-20 | 2013-03-13 | 六安同济生生物科技有限公司 | Auxiliary extraction method of biological enzyme for improving dissolution rate of dendrobe bioactive polysaccharide |
| CN102928373A (en) * | 2012-11-26 | 2013-02-13 | 广东省农业科学院花卉研究所 | Method for testing content of dendrobe polysaccharide and application thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105273841A (en) * | 2015-08-06 | 2016-01-27 | 云南中烟工业有限责任公司 | Phoebe spp. spice preparation method and application |
| CN105733994A (en) * | 2016-04-18 | 2016-07-06 | 云南中烟工业有限责任公司 | Trichoderma aureoviride strain and method for preparing dendrobium candidum tobacco flavor from same |
| CN106148007A (en) * | 2016-08-11 | 2016-11-23 | 江西中烟工业有限责任公司 | A kind of method preparing cigarette Herba Dendrobii spice for Extraction solvent with jowar wine |
| CN108112949A (en) * | 2017-12-06 | 2018-06-05 | 成都新柯力化工科技有限公司 | A kind of preparation method of natural flavor |
| CN108851179A (en) * | 2018-08-07 | 2018-11-23 | 武汉纺织大学 | One kind containing Herba Dendrobii extract additive in cigarette and preparation method thereof |
| CN113308301A (en) * | 2021-06-04 | 2021-08-27 | 安徽中烟工业有限责任公司 | Dendrobium polysaccharide Amadori latent aroma spice, preparation method thereof and application thereof in cigarettes |
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Application publication date: 20140122 |