CN103505382A - Cleanser composition with stable wire drawing effect and preparation method thereof - Google Patents
Cleanser composition with stable wire drawing effect and preparation method thereof Download PDFInfo
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- CN103505382A CN103505382A CN201310422917.6A CN201310422917A CN103505382A CN 103505382 A CN103505382 A CN 103505382A CN 201310422917 A CN201310422917 A CN 201310422917A CN 103505382 A CN103505382 A CN 103505382A
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Abstract
The invention discloses cleanser composition with a stable wire drawing effect and a preparation method thereof. The cleanser composition is characterized in that the composition has a wire drawing appearance, the wire drawing effect is long and thin like silk, foams are exquisite, dense, lasting and rich in a using process, and the skin is fresh and moist after the use of the composition; common components such as fatty acid, an amino acid surfactant and phytosterol are selected and used in the composition; when the temperature of a cleanser body of the cleanser composition prepared by an optimal proportional mixing process and an optimized preparation process reaches up to 50 DEG C, the cleanser body is taken out and smeared by hand, the long and thin wire drawing effect can be observed, water is added for rubbing to generate foams, and the foams are exquisite, dense, lasting and rich; after the circulation of high and low temperature from 50 DEG C to 25 DEG C, from 25 DEG C to -15 DEG C and from -15 DEG C to 25 DEG C, the cleanser body is smeared by hand, the long and thin wire drawing effect still can be observed, the water is added for rubbing to generate the foams, and the foams are exquisite, dense, lasting and rich; the usage and high and low-temperature environment transportation conditions are fully met; a test shows that the foams of the cleanser composition are more exquisite, dense, lasting and rich in comparison with a general cleanser; the skin after the use of the cleanser composition is softer and moister. Therefore, the cleanser composition has a good development prospect.
Description
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of facial cleaning cream composition and method of making the same with stable wire-drawing effect.
Background technology
Raising along with people's living standard, and the impact of living environment, consumer is more and more thinner to the requirement of cleaning product, the effect that cleaning product is had more and more receives publicity, and has good spreadability, peculiar outward appearance, enrich very much careful foam, easily rinse, wash rear skinfeel clearly not tight, preferably can have certain moisturizing effect.
On market, common clean product of foam type pressed different surfaces activating agent kind difference at present, and the outward appearance of clean the product obtaining and serviceability are also different, and respectively have pluses and minuses; Outward appearance and the serviceability thereof of product are as shown in table 1:
Table 1
Current clean product of market, leading or soap base system product is on the high side, be more easily subject to the favor of consumer, its market share can reach 60% left and right of market cleaning product.
Although clean product of soap base system accounts for the leading position of cleaning product in city's field energy, clean product of soap base of market is main or take traditional soap base facial cleaning cream as main, and merits and demerits is wherein all very outstanding.The major advantage of this product is: (1) mastic is paste, in flexible pipe, can extrude strip, packs light; (2) product can provide very glittering tempting pearlescent appearance; (3) spreading property of product is good, convenient use; (4) lather quickness is fast, and foam is abundant fine and smooth; (5) easily rinse, wash rear skin very salubrious.The shortcoming of product is: the skin after (1) use is very dry, tight, easily causes the stimulations such as skin pruritus; (2) product appearance is all common white strip, without wire-drawing effect; (3) restorability of high low-temperature stability is poor, easily occurs high temperature layering, and low temperature recovers the hardening of room temperature mastic.
A facial cleaning cream with stable wire-drawing effect, composite and obtain with optimal proportion through many experiments.Mastic has good pearlescent appearance, takes out mastic and smears instigation with hands, can observe elongated wire-drawing effect, adds water and rubs foaming, fine and smooth careful and abundant lastingly, the more soft and moist moistening effect of skinfeel after use.From 50 ℃, return to 25 ℃, from 25 ℃ to-15 ℃, again recover 25 ℃ again, with hands, smear instigation mastic, still can observe elongated wire-drawing effect, add water and rub foaming, fine and smooth careful and abundant lastingly, fully meet and use and high and low temperature environment traffic condition, finer and smoother more careful, abundant lastingly than the bubble of common facial cleaning cream after tested, the more soft and moist moistening effect of skinfeel after use, has good development prospect.
Summary of the invention
The object of the present invention is to provide a kind of have stable wire-drawing effect, finer and smoother more careful, abundant lastingly than the bubble of common facial cleaning cream, the more soft and moist moistening effect facial cleaning cream of the skinfeel composition and method of making the same after use.
In order to reach object of the present invention, the present invention has adopted following technical scheme: a kind of have a stable wire-drawing effect, finer and smoother more careful, abundant lastingly than the bubble of common facial cleaning cream, the facial cleaning cream combination of the more soft and moist moistening effect of skinfeel after use, is characterized in that comprising following percentage by weight component:
Above-mentioned compositions, wherein said fatty acid is any one or the multiple combination in dodecoic acid, tetradecylic acid, hexadecylic acid, stearic acid.
Above-mentioned compositions, wherein said co-emulsifier is any one or the multiple combination in glyceryl stearate, PEG-100 stearate, PEG-80 castor oil hydrogenated.
Above-mentioned compositions, wherein said aminoacid table is lived as any one or multiple combination in sodium N-lauroyl sarcosinate, sodium methyl cocoyl taurate, myristoyl sodium glutamate, sodium lauroyl glutamate.
Above-mentioned compositions, wherein said plant sterol is designated as the 0.1-2% of total consumption with mass percent.
Above-mentioned compositions, wherein said foam stabilizer is any one or the multiple combination in sodium laureth sulfate, cocamido propyl betaine, lauryl hydroxyl sulfo betaine, coconut oleoyl amine DEA.
Above-mentioned compositions, wherein said thickening agent is any one or the multiple combination in acrylic acid (ester) analog copolymer, acrylic acid (ester) class/vinyl neodecanoate cross linked polymer, glycol distearate, acrylic acid (ester) class/stearyl alcohol polyethers-20 methacrylate copolymer, Polyethylene Glycol-45M.
Above-mentioned compositions, wherein said polyhydric alcohol is any one or the multiple combination in glycerol, propylene glycol, butanediol, dipropylene glycol, 1,3-PD, sorbitol, Polyethylene Glycol.
Above-mentioned compositions, wherein said skin conditioning agent is any one or the multiple combination in Polyquaternium-67, olive oil PEG-7 esters, C12-13 alcohol lactate.
Above-mentioned compositions, wherein said nertralizer is one or more combinations in sodium hydroxide, potassium hydroxide, triethanolamine, aminomethyl propanol, arginine.
The facial cleaning cream compositions of wire-drawing effect of the present invention, except above component, can also suitably be added as required and be applicable to the conventional composition that cosmetics are used, as compositions such as chelating agen, antiseptic, essence.
A kind of preparation method with the facial cleaning cream compositions of stable wire-drawing effect of the present invention, is characterized in that concrete steps are::
(1) the oily molten component such as fatty acid, co-emulsifier being dropped into oil cauldron and be heated to 80 ℃, be uniformly mixed, it is dissolved completely transparent, is oil phase, stand-by.
(2) components such as water, polyhydric alcohol, nertralizer being put into emulsifying pot and be heated to 80 ℃, be uniformly mixed, it is dissolved completely transparent, is water, stand-by.
(3) water is controlled to mixing speed at the still state of vacuum of 300r/min, suction oil phase slowly, after exhausting, be incubated 80 ℃ and continue saponification 1h, during keep vacuum state, and every 15min homogenizing once, speed is at 3000r/min, each homogenizing 3-5min.
(4) stop homogenizing and stirring, maintain the temperature at 80 ℃, aminoacid table class alive, plant sterol, foam stabilizer, thickening agent, skin conditioning agent component are dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 30min;
(5) keep mixing speed at 400r/min, cooling;
(6) cool to 40 ℃ thermally sensitive composition is added to emulsifying pot, vacuum state, keeps mixing speed at 400r/min, stirs;
(7) stir, cool to 38 ℃ of dischargings, fill is sealed up for safekeeping.
Beneficial effect of the present invention: a kind of have a stable wire-drawing effect, finer and smoother more careful, abundant lastingly than the bubble of common facial cleaning cream, and the more soft and moist moisturizing of skinfeel after use, does not stimulate.
The specific embodiment
By specific embodiment, come below that the present invention is further illustrated, but these embodiment are just in order to illustrate, the present invention do not done to any type of restriction.
Embodiment 1 wire drawing facial cleaning cream
Formula is in Table 2.
Table 2
Preparation method is as follows:
1. the F phase that is uniformly dispersed in advance, stand-by.
2. A is dropped into oil phase pot mutually and be heated to 80 ℃, be uniformly mixed, it is dissolved completely transparent, stand-by.
3. B is dropped into emulsifying pot mutually, stirring and dissolving is completely transparent, is heated to 80 ℃, stand-by.
4. the insulation of emulsifying pot is 80 ℃, controls mixing speed in the still state of vacuum of 300r/min, slowly suction A phase, after exhausting, be incubated 80 ℃ and continue saponification 1h, during keep vacuum state, and every 15min homogenizing once, speed is at 3000r/min, each homogenizing 3-5min.
5. stop homogenizing and stirring, maintain the temperature at 80 ℃, C phase component is dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 10min, mix homogeneously.
6. stop homogenizing and stirring, maintain the temperature at 80 ℃, D phase component is dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 10min, mix homogeneously.
7. stop homogenizing and stirring, maintain the temperature at 80 ℃, F phase component is dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 10mi n, mix homogeneously.
8. keep mixing speed at 400r/min, cooling.
9. cool to 40 ℃ thermally sensitive composition G phase and F are added to emulsifying pot mutually successively, vacuum state, keeps mixing speed at 400r/min, stirs.
10. stir, cool to 38 ℃ of dischargings, fill is sealed up for safekeeping.
Embodiment 2 wire drawing facial cleaning cream
Formula is in Table 3.
Table 3
Preparation method is as follows:
1. the F phase that is uniformly dispersed in advance, stand-by.
2. A is dropped into oil phase pot mutually and be heated to 80 ℃, be uniformly mixed, it is dissolved completely transparent, stand-by.
3. B is dropped into emulsifying pot mutually, stirring and dissolving is completely transparent, is heated to 80 ℃, stand-by.
4. the insulation of emulsifying pot is 80 ℃, controls mixing speed in the still state of vacuum of 300r/min, slowly suction A phase, after exhausting, be incubated 80 ℃ and continue saponification 1h, during keep vacuum state, and every 15min homogenizing once, speed is at 3000r/min, each homogenizing 3-5min.
5. stop homogenizing and stirring, maintain the temperature at 80 ℃, C phase component is dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 10min, mix homogeneously.
6. stop homogenizing and stirring, maintain the temperature at 80 ℃, D phase component is dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 10min, mix homogeneously.
7. stop homogenizing and stirring, maintain the temperature at 80 ℃, F phase component is dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 10min, mix homogeneously.
8. keep mixing speed at 400r/min, cooling.
9. cool to 40 ℃ thermally sensitive composition G phase and F are added to emulsifying pot mutually successively, vacuum state, keeps mixing speed at 400r/min, stirs.
10. stir, cool to 38 ℃ of dischargings, fill is sealed up for safekeeping.
Embodiment 3 wire drawing facial cleaning cream
Formula is in Table 4.
Table 4
Preparation method is as follows:
1. the F phase that is uniformly dispersed in advance, stand-by.
2. A is dropped into oil phase pot mutually and be heated to 80 ℃, be uniformly mixed, it is dissolved completely transparent, stand-by.
3. B is dropped into emulsifying pot mutually, stirring and dissolving is completely transparent, is heated to 80 ℃, stand-by.
4. the insulation of emulsifying pot is 80 ℃, controls mixing speed in the still state of vacuum of 300r/min, slowly suction A phase, after exhausting, be incubated 80 ℃ and continue saponification 1h, during keep vacuum state, and every 15min homogenizing once, speed is at 3000r/min, each homogenizing 3-5min.
5. stop homogenizing and stirring, maintain the temperature at 80 ℃, C phase component is dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 10min, mix homogeneously.
6. stop homogenizing and stirring, maintain the temperature at 80 ℃, D phase component is dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 10min, mix homogeneously.
7. stop homogenizing and stirring, maintain the temperature at 80 ℃, F phase component is dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 10min, mix homogeneously.
8. keep mixing speed at 400r/min, cooling.
9. cool to 40 ℃ thermally sensitive composition G phase and F are added to emulsifying pot mutually successively, vacuum state, keeps mixing speed at 400r/min, stirs.
10. stir, cool to 38 ℃ of dischargings, fill is sealed up for safekeeping.
The common facial cleaning cream of comparative example 1
Formula is shown in Table 5.
Table 5
Preparation method is as follows:
1. the F phase that is uniformly dispersed in advance, stand-by.
2. A is dropped into oil phase pot mutually and be heated to 80 ℃, be uniformly mixed, it is dissolved completely transparent, stand-by.
3. B is dropped into emulsifying pot mutually, stirring and dissolving is completely transparent, is heated to 80 ℃, stand-by.
4. the insulation of emulsifying pot is 80 ℃, controls mixing speed in the still state of vacuum of 300r/min, slowly suction A phase, after exhausting, be incubated 80 ℃ and continue saponification 1h, during keep vacuum state, and every 15min homogenizing once, speed is at 3000r/min, each homogenizing 3-5min.
5. stop homogenizing and stirring, maintain the temperature at 80 ℃, C phase component is dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 10min, mix homogeneously.
6. keep mixing speed at 400r/min, cooling.
7. cool to 55 ℃ thermally sensitive composition D is added to emulsifying pot, vacuum state, keeps mixing speed to stir at 400r/min.
8. cool to 40 ℃ thermally sensitive composition E phase and F are added to emulsifying pot mutually successively, vacuum state, keeps mixing speed at 400r/min, stirs.
9. stir, cool to 38 ℃ of dischargings, fill is sealed up for safekeeping.
Experimental example 1 skin irritation test
60 women of take are object, with syringe, get in the coyote hole that 0.03ml sample is placed in speckle examination adhesive tape, immediately the speckle examination adhesive tape that is equipped with sample is started to be longitudinally affixed on from bottom the normal skin of left forearm, light pressing chamber, to drive away air, and is uniformly distributed trier one by one simultaneously.Labelling is carried out at test position, to observe.Every 24 hours, paste skin once, open half an hour after paster, according to the term of CTFA guide (1981), check.Carried out altogether the experiment of 6 patch, after pasting skin and finishing the 6th day, in order to observe late response, has carried out appending inspection.Data are utilized last check result, compare.Identify that take table 6 carries out as standard.Substances is respectively the wire drawing facial cleaning cream of embodiment 1, embodiment 2, embodiment 3 and the common facial cleaning cream of comparative example 1, and result is as shown in table 7.
Table 6 standard of perfection
| Grade | Symbol | Standard of perfection |
| 0 | - | Negative reaction: non-stimulated, without erythema |
| 1 | ± | Suspicious reaction: slight erythema |
| 2 | + | Weak positive reaction: erythema |
| 3 | ++ | Strong positive reaction: erythema, pimple, vesicle |
| 4 | +++ | Extremely strong positive reaction: serious edema, bulla |
The irritant test result of table 7 wire drawing facial cleaning cream and common facial cleaning cream
Experimental example 2 result of use experiments
In order to compare clean effect of the embodiment of the present invention 1, example 2, example 3 wire drawing facial cleaning cream and comparative example 1 common facial cleaning cream and to use sensation, with mean age Wei29Sui consumer 60 object by name, assess.Appraisal procedure is to divide middle selection to projects degree of preference (whether liking) at 1-9, as follows:
1----2----3----4----5----6----7----8----9
Very poor generally fine
By each side is marked, at table 8, demonstrate its result.
Table 8 is bought clean effect of face product and is used perceptual result
| Classification | Comparative example 1 | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Wire-drawing effect | 1.0 | 8.5 | 8.5 | 8.5 |
| Pearlescent appearance | 8.0 | 8.5 | 8.5 | 8.5 |
| Spreadability | 8.0 | 8.0 | 8.0 | 8.0 |
| Foam richness | 7.5 | 9.0 | 9.0 | 9.0 |
| Foam sophistication | 7.5 | 9.0 | 9.0 | 9.0 |
| Washability | 8.0 | 8.5 | 8.5 | 8.5 |
| Skinfeel after rinsing | 3.0 | 8.0 | 8.0 | 8.0 |
As shown in table 8, wire drawing facial cleaning cream embodiment 1, embodiment 2, embodiment 3 are different from common facial cleaning cream comparative example 1, product appearance is peculiar, has wire-drawing effect, and after the foam richness in the time of clean, foam sophistication, flushing, skinfeel moisturizing effect is all better than common facial cleaning cream.
Experimental example 3 stability experiments
In order to assess the stability of product wire drawing facial cleaning cream of the present invention, in the variations in temperature of-15-48 ℃, the stability of test wire drawing facial cleaning cream embodiment 1, embodiment 2, embodiment 3 and common facial cleaning cream comparative example 1, and demonstrate its result at table 9.
The stability result of clean product of table 9
As shown in table 9, the good stability of wire drawing facial cleaning cream embodiment 1, embodiment 2, embodiment 3 and common facial cleaning cream comparative example 1.
Claims (11)
1. a facial cleaning cream composition and method of making the same with stable wire-drawing effect, is characterized in that being comprised of according to certain mass percent following component:
2. compositions according to claim 1, wherein said fatty acid is any one or the multiple combination in dodecoic acid, tetradecylic acid, hexadecylic acid, stearic acid.
3. compositions according to claim 1, wherein said co-emulsifier is any one or the multiple combination in glyceryl stearate, PEG-100 stearate, PEG-80 castor oil hydrogenated.
4. compositions according to claim 1, wherein said aminoacid table is lived as any one or multiple combination in sodium N-lauroyl sarcosinate, sodium methyl cocoyl taurate, myristoyl sodium glutamate, sodium lauroyl glutamate.
5. compositions according to claim 1, wherein said plant sterol is designated as the 0.1-2% of total consumption with mass percent.
6. compositions according to claim 1, wherein said foam stabilizer is any one or the multiple combination in sodium laureth sulfate, cocamido propyl betaine, lauryl hydroxyl sulfo betaine, coconut oleoyl amine DEA.
7. compositions according to claim 1, wherein said thickening agent is any one or the multiple combination in acrylic acid (ester) analog copolymer, acrylic acid (ester) class/vinyl neodecanoate cross linked polymer, glycol distearate, acrylic acid (ester) class/stearyl alcohol polyethers-20 methacrylate copolymer, Polyethylene Glycol-45M.
8. compositions according to claim 1, wherein said polyhydric alcohol is any one or the multiple combination in glycerol, propylene glycol, butanediol, dipropylene glycol, 1,3-PD, sorbitol, Polyethylene Glycol.
9. compositions according to claim 1, wherein said skin conditioning agent is any one or the multiple combination in Polyquaternium-67, olive oil PEG-7 esters, C12-13 alcohol lactate.
10. compositions according to claim 1, wherein said nertralizer is one or more combinations in sodium hydroxide, potassium hydroxide, triethanolamine, aminomethyl propanol, arginine.
11. a kind of preparation methoies with the facial cleaning cream compositions of stable wire-drawing effect claimed in claim 1, it is characterized in that concrete steps are: (1) is dropped into oil cauldron by the oily molten component such as fatty acid, co-emulsifier and is heated to 80 ℃, be uniformly mixed, it is dissolved completely transparent, for oil phase, stand-by.(2) components such as water, polyhydric alcohol, nertralizer being put into emulsifying pot and be heated to 80 ℃, be uniformly mixed, it is dissolved completely transparent, is water, stand-by.(3) water is controlled to mixing speed at the still state of vacuum of 300r/min, suction oil phase slowly, after exhausting, be incubated 80 ℃ and continue saponification 1h, during keep vacuum state, and every 15min homogenizing once, speed is at 3000r/min, each homogenizing 3-5min.(4) stop homogenizing and stirring, maintain the temperature at 80 ℃, aminoacid table class alive, plant sterol, foam stabilizer, thickening agent, skin conditioning agent component are dropped into emulsifying pot, keep vacuum state, mixing speed is controlled at 400r/min, stirs 30min; (5) keep mixing speed at 400r/min, cooling; (6) cool to 40 ℃ thermally sensitive composition is added to emulsifying pot, vacuum state, keeps mixing speed at 400r/min, stirs; (7) stir, cool to 38 ℃ of dischargings, fill is sealed up for safekeeping.
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| CN103800253A (en) * | 2014-03-07 | 2014-05-21 | 澳宝化妆品（惠州）有限公司 | Moisturizing refreshing cleansing cream |
| CN103966037A (en) * | 2014-04-11 | 2014-08-06 | 上海梦之队国际贸易有限公司 | Production method of sea-buckthorn transparency liquid facial soap |
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