CN111840099A - Facial cleanser with soap base compounded with amino acid surfactant - Google Patents
Facial cleanser with soap base compounded with amino acid surfactant Download PDFInfo
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- CN111840099A CN111840099A CN202010736493.0A CN202010736493A CN111840099A CN 111840099 A CN111840099 A CN 111840099A CN 202010736493 A CN202010736493 A CN 202010736493A CN 111840099 A CN111840099 A CN 111840099A
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- percent
- amino acid
- facial cleanser
- skin
- soap
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- 239000000344 soap Substances 0.000 title claims abstract description 37
- 150000001413 amino acids Chemical class 0.000 title claims abstract description 34
- 230000001815 facial effect Effects 0.000 title claims abstract description 33
- 239000004094 surface-active agent Substances 0.000 title claims abstract description 31
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims abstract description 23
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000005639 Lauric acid Substances 0.000 claims abstract description 11
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 11
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000008117 stearic acid Substances 0.000 claims abstract description 11
- TUNFSRHWOTWDNC-UHFFFAOYSA-N Myristic acid Natural products CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 10
- TWJNQYPJQDRXPH-UHFFFAOYSA-N 2-cyanobenzohydrazide Chemical compound NNC(=O)C1=CC=CC=C1C#N TWJNQYPJQDRXPH-UHFFFAOYSA-N 0.000 claims abstract description 9
- 235000021360 Myristic acid Nutrition 0.000 claims abstract description 9
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 9
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 9
- 230000003472 neutralizing effect Effects 0.000 claims abstract description 6
- 239000008367 deionised water Substances 0.000 claims abstract description 5
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 5
- 239000003906 humectant Substances 0.000 claims abstract description 5
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 5
- 239000002562 thickening agent Substances 0.000 claims abstract description 5
- 150000005846 sugar alcohols Polymers 0.000 claims abstract description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical group [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 24
- JOLYVEWZEPKDIJ-UTLKBRERSA-L dipotassium;(2s)-2-(dodecanoylamino)pentanedioate Chemical compound [K+].[K+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC([O-])=O JOLYVEWZEPKDIJ-UTLKBRERSA-L 0.000 claims description 9
- 229940048109 sodium methyl cocoyl taurate Drugs 0.000 claims description 9
- 229940099874 potassium lauroyl glutamate Drugs 0.000 claims description 8
- IKGKWKGYFJBGQJ-UHFFFAOYSA-M sodium;2-(dodecanoylamino)acetate Chemical compound [Na+].CCCCCCCCCCCC(=O)NCC([O-])=O IKGKWKGYFJBGQJ-UHFFFAOYSA-M 0.000 claims description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 7
- 229940065859 sodium cocoyl glycinate Drugs 0.000 claims description 7
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 6
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims description 5
- 241001135917 Vitellaria paradoxa Species 0.000 claims description 5
- 235000013871 bee wax Nutrition 0.000 claims description 5
- 239000012166 beeswax Substances 0.000 claims description 5
- 229940057910 shea butter Drugs 0.000 claims description 5
- RZRNAYUHWVFMIP-KTKRTIGZSA-N 1-oleoylglycerol Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(O)CO RZRNAYUHWVFMIP-KTKRTIGZSA-N 0.000 claims description 4
- PHYFQTYBJUILEZ-UHFFFAOYSA-N Trioleoylglycerol Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC(OC(=O)CCCCCCCC=CCCCCCCCC)COC(=O)CCCCCCCC=CCCCCCCCC PHYFQTYBJUILEZ-UHFFFAOYSA-N 0.000 claims description 4
- 229940080421 coco glucoside Drugs 0.000 claims description 4
- 229920001577 copolymer Polymers 0.000 claims description 4
- 150000002148 esters Chemical class 0.000 claims description 4
- 229940049294 glyceryl stearate se Drugs 0.000 claims description 4
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 239000003755 preservative agent Substances 0.000 claims description 3
- 230000002335 preservative effect Effects 0.000 claims description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 2
- -1 compound amino acid Chemical class 0.000 claims description 2
- GPLRAVKSCUXZTP-UHFFFAOYSA-N diglycerol Chemical compound OCC(O)COCC(O)CO GPLRAVKSCUXZTP-UHFFFAOYSA-N 0.000 claims description 2
- 229940105990 diglycerin Drugs 0.000 claims 1
- 229920005862 polyol Polymers 0.000 claims 1
- 150000003077 polyols Chemical class 0.000 claims 1
- 239000006260 foam Substances 0.000 abstract description 20
- 206010020751 Hypersensitivity Diseases 0.000 abstract description 7
- 208000026935 allergic disease Diseases 0.000 abstract description 7
- 230000007815 allergy Effects 0.000 abstract description 7
- 230000014759 maintenance of location Effects 0.000 abstract description 4
- 230000003750 conditioning effect Effects 0.000 abstract description 3
- 230000008961 swelling Effects 0.000 abstract description 3
- 239000002585 base Substances 0.000 description 24
- 238000004140 cleaning Methods 0.000 description 21
- 235000001014 amino acid Nutrition 0.000 description 20
- 230000007794 irritation Effects 0.000 description 12
- 230000000694 effects Effects 0.000 description 8
- 235000014113 dietary fatty acids Nutrition 0.000 description 6
- 229930195729 fatty acid Natural products 0.000 description 6
- 239000000194 fatty acid Substances 0.000 description 6
- 150000004665 fatty acids Chemical class 0.000 description 6
- 239000000203 mixture Substances 0.000 description 4
- 239000011148 porous material Substances 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 238000007127 saponification reaction Methods 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 230000000172 allergic effect Effects 0.000 description 3
- 208000010668 atopic eczema Diseases 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000006386 neutralization reaction Methods 0.000 description 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 2
- 235000019864 coconut oil Nutrition 0.000 description 2
- 239000003240 coconut oil Substances 0.000 description 2
- 230000002354 daily effect Effects 0.000 description 2
- 239000003599 detergent Substances 0.000 description 2
- 230000003203 everyday effect Effects 0.000 description 2
- 238000005187 foaming Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- KKDONKAYVYTWGY-UHFFFAOYSA-M sodium;2-(methylamino)ethanesulfonate Chemical compound [Na+].CNCCS([O-])(=O)=O KKDONKAYVYTWGY-UHFFFAOYSA-M 0.000 description 2
- WUWHFEHKUQVYLF-UHFFFAOYSA-M sodium;2-aminoacetate Chemical compound [Na+].NCC([O-])=O WUWHFEHKUQVYLF-UHFFFAOYSA-M 0.000 description 2
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- KEQXNNJHMWSZHK-UHFFFAOYSA-L 1,3,2,4$l^{2}-dioxathiaplumbetane 2,2-dioxide Chemical compound [Pb+2].[O-]S([O-])(=O)=O KEQXNNJHMWSZHK-UHFFFAOYSA-L 0.000 description 1
- IXOCGRPBILEGOX-UHFFFAOYSA-N 3-[3-(dodecanoylamino)propyl-dimethylazaniumyl]-2-hydroxypropane-1-sulfonate Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC(O)CS([O-])(=O)=O IXOCGRPBILEGOX-UHFFFAOYSA-N 0.000 description 1
- 239000004471 Glycine Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000004088 foaming agent Substances 0.000 description 1
- 235000013905 glycine and its sodium salt Nutrition 0.000 description 1
- 239000004247 glycine and its sodium salt Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 229960003444 immunosuppressant agent Drugs 0.000 description 1
- 230000001861 immunosuppressant effect Effects 0.000 description 1
- 239000003018 immunosuppressive agent Substances 0.000 description 1
- 229940033355 lauric acid Drugs 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 235000011118 potassium hydroxide Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 230000005808 skin problem Effects 0.000 description 1
- 229940029258 sodium glycinate Drugs 0.000 description 1
- 229960004274 stearic acid Drugs 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/75—Anti-irritant
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Emergency Medicine (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dermatology (AREA)
- Insects & Arthropods (AREA)
- Zoology (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a facial cleanser with soap base compounded with amino acid surfactant, which is calculated according to the mass percentage; the method comprises the following steps: phase A: lauric acid: 1 to 5 percent; myristic acid: 4 to 15 percent; stearic acid: 3 to 16 percent; amino acid surfactant: 3% -25%; polyhydric alcohol humectant: 15 to 20 percent; emulsifier: 1 to 2 percent; neutralizing agent: adding to 80-85%; phase B: thickening agent: 4 to 7 percent; and C phase: nonionic surfactant: 0.3 to 0.6 percent; auxiliary components: 0.01 to 0.1 percent; deionized water: and (4) the balance. The facial cleanser disclosed by the invention is prepared by matching the soap base component and the amino acid surfactant, realizes rich foam, can mildly clean skin dirt, and has the advantages of comfort, tightness, moisture retention, skin conditioning, no skin cuticle drop caused by dryness and water shortage, no red swelling, no allergy, skin smoothness and the like of the washed skin.
Description
Technical Field
The invention relates to the technical field of daily cosmetics, in particular to a facial cleanser with soap base compounded with an amino acid surfactant.
Background
With the development of economy and the improvement of living standard, the demand of skin care products is increasing. The skin care process starts from skin cleaning, and the facial cleaning link is particularly important.
In the current popular face cleaning products in the market, soap-based face cleaning products are used, although the face cleaning products have strong cleaning power and generate abundant foams, the degreasing power is strong, the cuticle of the skin can fall off after being frequently used, the skin is tight, the skin is dry and lack of water, and severe people can cause the skin to be red and swollen, even allergic.
While the amino acid facial cleansing product is mild, the generated foam is less, and the cleaning power of the amino acid facial cleansing product is limited; although various types of face cleaning products exist in the market at present, the pursuit of the face cleaning products by people not only requires rich foam and strong cleaning power, but also requires mild use, moisture retention and moistening, and the skin after washing is comfortable and not tight, and can not cause skin problems such as allergy and the like.
Disclosure of Invention
In order to solve the problems, the invention aims to provide a facial cleanser with a soap base compounded with an amino acid surfactant, which is formed by combining a soap base component and the amino acid surfactant, wherein the soap base component can provide abundant foams and a good washing effect and can effectively clean skin dirt; the amino acid surfactant can keep moisture, moisten and condition skin, and has the characteristics of comfort, no allergy, smooth skin and the like, and the skin is not tight after being cleaned.
The purpose of the invention is realized by the following technical scheme: a facial cleanser with soap base compounded with amino acid surfactant, which is calculated according to the mass percentage; the method comprises the following steps:
phase A: lauric acid: 1 to 5 percent; myristic acid: 4 to 15 percent; stearic acid: 3 to 16 percent; amino acid surfactant: 3% -25%; polyhydric alcohol humectant: 15 to 20 percent; emulsifier: 1 to 2 percent; neutralizing agent: adding to 80-85%;
phase B: thickening agent: 4 to 7 percent;
and C phase: nonionic surfactant: 0.3 to 0.6 percent; auxiliary components: 0.01 to 0.1 percent; deionized water: and (4) the balance.
Further, the C phase also comprises shea butter with the mass percent of 0.3-0.5%.
Further, the amino acid surfactant comprises the following components: sodium methyl cocoyl taurate: 1 to 10 percent; sodium cocoyl glycinate: 1 to 12 percent; potassium lauroyl glutamate: 1 to 5 percent.
Further, the polyhydric alcohol humectant is at least one of glycerin, propylene glycol, butylene glycol and diglycerol.
Further, the nonionic surfactant is at least one of coco glucoside and glyceryl oleate.
Further, the thickening agent is an acrylic acid (ester) copolymer.
Further, the emulsifier is at least one of glyceryl stearate SE and beeswax.
Further, the neutralizing agent is potassium hydroxide.
Furthermore, the auxiliary component is at least one of a fat-liquoring agent, an aromatizing agent and a preservative.
The main components of the invention are introduced:
lauric acid in the invention is also called lauric acid: (CAS number: 143-07-7), which is one of the components forming the soap base, is used as an emulsifier and a detergent after being neutralized with a base in the present invention.
Myristic acid in the invention, also called myristic acid: (CAS number: 544-63-8) is one of the soap-base-forming ingredients and is used as an emulsifier and a cleanser after neutralization with a base in the present invention.
Stearic acid in the present invention is also called stearic acid: (CAS number: 57-11-4) naturally occurs in various plant and animal derivatives, is one of the commonly used higher fatty acids, soap-base forming ingredients, and is used as an emulsifier and detergent after neutralization with alkali in the present invention.
Potassium hydroxide in the invention: (CAS number 1310-58-3) belongs to strong base, forms soap base after being neutralized with fatty acid, and has strong stimulation to skin at higher concentration.
Sodium methyl cocoyl taurate in the present invention: (CAS number: 12765-39-8) is prepared by condensing natural fatty acid and sodium methyl taurate, has mild performance as amino acid surfactant, can reduce irritation of soap base component to skin when being compatible with soap base component, and is used as cleanser, foaming agent and surfactant in the invention.
Sodium cocoyl glycinate in the invention: (CAS number: 90387-74-9) amino acid surfactant produced by glycine in amino acid and coconut oil fatty acid extracted from plant is used as cleanser and skin conditioner in the invention, which can produce smooth and elastic foam, improve foam fineness of product when being compatible with soap base component, reduce irritation of product to skin, and make skin smooth and not tight after use.
Potassium lauroyl glutamate in the present invention: (CAS number: 29923-31-7) is an amino acid type surfactant with an amino acid skeleton in a molecule, has excellent foaming performance and very mild performance, can improve the foam fineness of a product by being matched with a soap base component, can reduce the irritation to the skin and soften and moisten the skin, and is used as a surfactant and an emulsifier.
The invention has the beneficial effects that:
1. the facial cleanser disclosed by the invention is composed of a soap base component formed by saponification and neutralization of lauric acid, myristic acid, stearic acid and potassium hydroxide; an amino acid surfactant component is formed by matching sodium methyl cocoyl taurate, sodium cocoyl glycinate and potassium lauroyl glutamate; the paste body generated by saponification of lauric acid is soft and semitransparent, and has large and abundant foam; the paste generated by the saponification of the myristic acid is hard, has fine pearlescence and is semitransparent, and has large and rich foam; the paste generated by the saponification of the stearic acid is soft in later period, is pearly-luster milk white, and has rich and fine foam; the sodium methyl cocoyl taurate is prepared by condensing natural fatty acid and sodium methyl taurate, has mild performance, and can reduce the irritation to the skin when being compatible with soap base; when the cocoyl sodium glycinate is compatible with the soap base, the foam fineness of the product can be improved, the irritation of the product to the skin can be reduced, and the skin is smooth and not tight after the product is used; the potassium lauroyl glutamate has excellent foaming performance and very mild performance, can improve the foam fineness of the product by being matched with soap base, can reduce the irritation to the skin, and enables the skin to be soft and moist.
2. The facial cleanser disclosed by the invention is prepared by matching the soap base component and the amino acid surfactant, realizes rich foam, can mildly clean skin dirt, and has the advantages of comfort, tightness, moisture retention, skin conditioning, no skin cuticle falling caused by dryness and water shortage, no red swelling, no allergy, skin smoothness and the like of the washed skin.
3. According to the facial cleanser disclosed by the invention, the glyceryl stearate SE and the beeswax are easy to emulsify after being reacted with the neutralizer, and the beeswax can be mutually dissolved with shea butter and combined with other components, so that the formed facial cleanser cream body is relatively stable and can be stored for a long time.
4. The coco glucoside and the glyceryl oleate have weak cleaning capability, but have small irritation to skin and eyes, and can be compounded with a soap base component and an amino acid surfactant for use, so that the cleaning performance of the facial cleanser can be further improved, and the effects of thickening and reducing irritation can be achieved.
5. The shea butter is natural plant essence, does not generate irritation or cause skin sensitivity to skin, can mildly care the skin, further reduces the irritation of the face cleanser, can recover and maintain the natural elasticity of the skin, and has good deep moisturizing effect.
Detailed Description
In order to make the objects, technical solutions and advantages of the present application more apparent, the present application is further described in detail below with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the present application and are not intended to limit the present application.
Example 1:
the facial cleanser with the soap base compounded with the amino acid surfactant comprises the following components in percentage by mass:
phase A: lauric acid: 3 percent;
myristic acid: 5 percent;
stearic acid: 14 percent;
glyceryl stearate SE: 1 percent;
pearling agent: 2 percent;
beeswax: 0.5 percent;
lauramidopropyl hydroxysultaine: 4 percent;
sodium methyl cocoyl taurate: 4.7 percent;
sodium cocoyl glycinate: 10 percent;
potassium lauroyl glutamate: 1.3 percent;
glycerol: 18 percent;
coconut oil fatty acid monoethanolamide: 0.5 percent;
potassium hydroxide: adding to 85%;
phase B: acrylic acid (ester) copolymer: 6 percent of
And C phase: coco glucoside and glyceryl oleate: 0.5 percent;
shea butter: 0.5 percent;
essence: 0.01;
preservative: 0.01
Water: and (4) the balance.
The preparation method comprises the following steps:
1. accurately weighing the components of the phase A, mixing, and heating to 75-80 ℃ until the components are uniformly dissolved to obtain a mixture A;
2. dissolving and diluting potassium hydroxide by using part of deionized water to obtain a potassium hydroxide solution;
3. dissolving the acrylic acid (ester) copolymer of the phase B by using partial deionized water to obtain a mixture B;
4. firstly, pumping a potassium hydroxide solution into the mixture A, mixing and saponifying for 30 minutes, then adding the mixture B, homogenizing for 3 minutes, cooling to 45 ℃, then sequentially adding the components in the phase C, and uniformly stirring; after each component is added, the next component is added after the components are uniformly stirred, and the temperature is reduced to 37-38 ℃ for discharging, thus obtaining the product 1.
The using method comprises the following steps: moistening face with water, applying appropriate amount of the product to palm, gently rubbing to obtain rich foam, cleaning face, and cleaning with water
The effect is as follows: the skin care product has the advantages of rich foam, mild skin dirt cleaning effect, comfort, tightness and no allergy of the washed skin, and can effectively moisturize and moisten the skin.
Example 2 to example 5:
the method of experimental example 1 was repeated according to the contents of lauric acid, myristic acid, stearic acid, sodium methylcocoyl taurate, sodium cocoyl glycinate and potassium lauroyl glutamate in table 1 below, and the kinds and contents of other ingredients not listed were completely the same as those in example 1, and soap-based compound amino acid surfactant facial cleanser products with different components were obtained.
Table 1:
| components | Example 2 | Example 3 | Example 4 | Example 5 |
| Lauric acid | 5％ | 4％ | 4％ | 6％ |
| Myristic acid | 5％ | 6％ | 12％ | 10％ |
| Stearic acid | 11％ | 10％ | 4％ | 5％ |
| Sodium methyl cocoyl taurate | 2％ | 4％ | 5％ | 3％ |
| Cocoyl glycine sodium salt | 8％ | 9％ | 12％ | 7％ |
| Lauroyl glutamic acid potassium salt | 5％ | 2％ | 3％ | 4％ |
| To obtain | Product 2 | Product 3 | Product 4 | Product 5 |
Clinical trials were conducted comparing the facial cleanser products from examples 1-5 with the pure soap based facial cleanser product.
1. Test environmental conditions
And (3) trial environment: a daily life environment;
2. the number of volunteers:
the patients are 18-35 years old (male-female ratio: 1:1), healthy, have no skin treatment on the tested part, have no hormone medicine and immunosuppressant in the last month and have no participation in other clinical testers in the last three months.
3. Test procedure
(1) The compliance of volunteers is checked firstly, and then the volunteers are randomly and evenly divided into 6 groups, wherein each group uses one of the face cleansers; skin data were collected from each volunteer prior to use.
(2) After cleaning the face in the same time period in the morning and evening every day, using corresponding essence liquid of each group according to the use requirement, using for 1 time in the morning and evening every day, continuously using for 28 days, and collecting the skin data of each volunteer after use, wherein the method and time for collecting the data are the same as the step (1).
(3) According to the skin data of all volunteers before and after use, including the foam height, the cleaning ability, the fine pore condition before and after use, the improvement degree of skin smoothness and skin comfort, the allergic rate and the mild performance (whether tight feeling exists) in the use process, the lifting proportion is counted; wherein the cleansing ability and mildness are scored according to the volunteer's feeling of use. The scoring standard is divided into 10 points, 1 point is the worst, and 10 points are the best. The evaluation result is the average score of all volunteers, and the higher the average score is, the better the effect is.
Testing an instrument:
visia skin tester (USA), and skin oil tester SM815-MPA (Germany).
The results of the tests are shown in Table 2 below.
Table 2:
as can be seen from the test data in table 2, the soap-based facial cleanser product had excessive irritation, had an allergic phenomenon during use, and had no significant improvement before and after use, in terms of fine pores, skin smoothness, and moderate skin comfort. The facial cleansers of the examples 1 to 5 have no allergy phenomenon in the using process and less irritation to the skin, and the heights of the generated foams are not obviously different from those of soap-based facial cleanser products and have stronger cleaning capability, so that the facial cleansers of the examples 1 to 5 have rich foam amount and excellent cleaning effect; in the face cleaning process, pores can be further refined, and the smoothness and comfort of the skin can be improved; the face cleanser of example 4, in terms of lauric acid: 4 percent; myristic acid: 10 percent; stearic acid: 5 percent; potassium hydroxide: neutralizing to 80%; sodium methyl cocoyl taurate: 5 percent; sodium cocoyl glycinate: 12 percent; potassium lauroyl glutamate: the proportion of 3 percent not only has better face cleaning effect, but also has better effects on refining pores, improving skin smoothness and skin comfort.
In conclusion, the facial cleanser disclosed by the invention is prepared by matching the soap base component and the amino acid surfactant, realizes rich foam, can mildly clean skin dirt, and has the advantages of comfort, tightness, moisture retention and moistening of the washed skin, conditioning of the skin, no dryness and water shortage to cause skin cuticle shedding, no redness and swelling, no allergy, skin smoothness and the like.
The above-mentioned embodiments are merely preferred embodiments of the present invention, and the scope of the present invention should not be limited thereby, and those skilled in the art should not make any insubstantial changes and substitutions based on the scope of the present invention.
Claims (9)
1. The facial cleanser with the soap base compounded with the amino acid surfactant is characterized by comprising the following components in percentage by mass; the method comprises the following steps:
phase A: lauric acid: 1 to 5 percent; myristic acid: 4 to 15 percent; stearic acid: 3 to 16 percent; amino acid surfactant: 3% -25%; polyhydric alcohol humectant: 15 to 20 percent; emulsifier: 1 to 2 percent; neutralizing agent: adding to 80-85%;
phase B: thickening agent: 4 to 7 percent;
and C phase: nonionic surfactant: 0.3 to 0.6 percent; auxiliary components: 0.01 to 0.1 percent; deionized water: and (4) the balance.
2. The soap-based amino acid surfactant-compounded facial cleanser according to claim 1, wherein the phase C further comprises shea butter in an amount of 0.3-0.5% by mass.
3. The soap-based amino acid surfactant facial cleanser according to claim 1, wherein the amino acid surfactant comprises the following components: sodium methyl cocoyl taurate: 1 to 10 percent; sodium cocoyl glycinate: 1 to 12 percent; potassium lauroyl glutamate: 1 to 5 percent.
4. The soap-based amino acid surfactant-compounded facial cleanser according to claim 1, wherein the polyol humectant is at least one of glycerin, propylene glycol, butylene glycol and diglycerin.
5. The soap-based amino acid surfactant complex facial cleanser of claim 1, wherein the nonionic surfactant is at least one of coco glucoside and glyceryl oleate.
6. The soap-based amino acid surfactant facial cleanser according to claim 1, wherein the thickener is an acrylic acid (ester) copolymer.
7. The soap base compound amino acid surfactant facial cleanser according to claim 1, wherein the emulsifier is at least one of glyceryl stearate SE and beeswax.
8. The soap-based amino acid surfactant complex facial cleanser of claim 1, wherein the neutralizing agent is potassium hydroxide.
9. The soap-based amino acid surfactant-compounded facial cleanser according to claim 1, wherein the auxiliary component is at least one of a fatting agent, an aromatizer and a preservative.
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