CN107616929A - One kind removes oil type face cleaning cream and preparation method thereof - Google Patents

One kind removes oil type face cleaning cream and preparation method thereof Download PDF

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Publication number
CN107616929A
CN107616929A CN201710972235.0A CN201710972235A CN107616929A CN 107616929 A CN107616929 A CN 107616929A CN 201710972235 A CN201710972235 A CN 201710972235A CN 107616929 A CN107616929 A CN 107616929A
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CN
China
Prior art keywords
face cleaning
type face
cleaning cream
oil type
acid
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Pending
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CN201710972235.0A
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Chinese (zh)
Inventor
欧阳彬洁
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Zhongshan Laixiang Cosmetics Co Ltd
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Zhongshan Laixiang Cosmetics Co Ltd
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Priority to CN201710972235.0A priority Critical patent/CN107616929A/en
Publication of CN107616929A publication Critical patent/CN107616929A/en
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Abstract

The invention discloses one kind to remove oil type face cleaning cream, is made up of the raw material of following percentage by weight:Aliphatic acid 20 35%, surfactant 5 12%, emulsifying agent 1 3%, alkaline agent 4.5 6%, glycerine 8 10%, butanediol 2 6%, Sweet Almond Oil 1 3%, preservative 0.2 0.5%, surplus is distilled water, and this goes oil type face cleaning cream not only can carry out deep layer cleaning to skin, and have and deoil and oil-control effect well, rich in nutrient, softening skin is moistened, and to no skin irritation.

Description

One kind removes oil type face cleaning cream and preparation method thereof
Technical field
The present invention relates to cosmetic field, and in particular to good face cleaning cream of a kind of effect of deoiling and preparation method thereof.
Background technology
Face cleaning cream is a kind of cosmetics for cleaning facial skin, as the improvement of people's living standards, face cleaning cream has been enter into The life of people, turn into the indispensable commodity of family.As the improvement of people's living standards, people are remarkable for face cleaning Stay in dirt, it is also desirable to which it has oil-control and other effects.However, the face cleaning cream for declaring oil-control at present on the market is more with clear Based on clean skin surface grease, solves its fundamental issue not in terms of skin oil and fat secretion.Oily is 2 small in face cleaning When after can usually be formed again and have one's face covered with glossy, as the vigorous crowd of sebum secretion, such as clean not in time, easily block hair follicle hole, easily Trigger a series of skin problem.Face cleaning cream cleaning effect of the fatty acid containing alkaline agent is pretty good mostly at present, but washes rear tight thorn It is sharp to feel to give people to leave very bad impression;, can not further opposite and existing face cleaning cream only has face cleaning effect The skin in portion is nourished and protected;The moon larger to human body skin excitant is typically used in other existing face cleaning skin care item Cinnamic acid, skin is preferably damaged after being used for multiple times for a long time.
The content of the invention
For overcome the deficiencies in the prior art, present invention offer is a kind of gentle non-stimulated, and not tight after washing, regulation sebum is put down Weighing apparatus removes oil type face cleaning cream.
The technical solution adopted for the present invention to solve the technical problems is:
One kind removes oil type face cleaning cream, is made up of the raw material of following percentage by weight:Aliphatic acid 20-35%, surfactant 5-12%, Emulsifying agent 1-3%, alkaline agent 4.5-6%, glycerine 8-10%, butanediol 2-6%, Sweet Almond Oil 1-3%, preservative 0.2-0.5%, surplus are Distilled water.
In above-mentioned formula, the aliphatic acid is the mixture of myristic acid, palmitic acid and stearic acid arbitrary proportion.
In above-mentioned formula, the surfactant is cocoyl glycine potassium and coconut oleoyl amine DEA arbitrary proportions Mixture.
In above-mentioned formula, the emulsifying agent is single stearic acid glycerine lipoprotein and polyoxyethylene(100)Stearate arbitrarily compares The mixture of example.
In above-mentioned formula, the alkaline agent is the potassium hydroxide that purity is 91%.
In above-mentioned formula, the preservative is the mixture of the fat of oxybenzene third and oxybenzene formicester arbitrary proportion.
It is further optimal, oil type face cleaning cream is gone with one kind that above-mentioned formula manufactures, by the raw material of following percentage by weight It is made:Aliphatic acid 28%, surfactant 8%, emulsifying agent 2%, alkaline agent 4.77%, glycerine 10%, butanediol 4%, Sweet Almond Oil 3%, steam Distilled water 39.93%, preservative 0.3%.
It is further optimal, oil type face cleaning cream is gone with one kind that above-mentioned formula manufactures, by the raw material of following percentage by weight It is made:Myristic acid 4%, palmitic acid 6%, stearic acid 18%, single stearic acid glycerine lipoprotein 1%, polyoxyethylene(100)Stearate 1%, Cocoyl glycine potassium 6.5%, coconut oleoyl amine DEA1.5%, purity are 91% potassium hydroxide 4.77%, glycerine 10%, butanediol 4%, Sweet Almond Oil 3%, distilled water 39.93%, the third fat of oxybenzene 0.1%, oxybenzene formicester 0.2%.
Another technical scheme provided by the invention is the above-mentioned preparation method for removing oil type face cleaning cream of manufacture:
A kind of method for preparing above-mentioned formula and removing oil type face cleaning cream, comprises the following steps:
(1)The aliphatic acid, emulsifying agent, preservative of above-mentioned parts by weight are added and is heated to 70-80 DEG C in oil phase pot and persistently stirs Mix, it is standby as oil phase;
(2)Glycerine, alkaline agent, distilled water the addition aqueous phase pot of above-mentioned parts by weight are heated to 75 DEG C and continue to stir, as water It is mutually standby;
(3)Aqueous phase is first pumped into emulsification pot, then oil phase is pumped into emulsification pot, insulation by preheating emulsification pot to 70-80 DEG C of temperature Stirring 40 minutes;
(4)70 DEG C and constant temperature are cooled to, it is equal that the surfactant of above-mentioned parts by weight and butanediol are added into stirring in emulsification pot It is even;
(5)55 DEG C and constant temperature are cooled to, the Sweet Almond Oil of above-mentioned parts by weight is added in emulsification pot and persistently stirred 30 minutes;
(6)Being cooled to 40 DEG C and continuing stirring until when lotion has the precipitation of pearly-lustre color to discharge.
The beneficial effects of the invention are as follows:
1st, face cleaning cream of the invention be soap base type, has good stability, surface-active and an antibacterial ability, its foam exquisiteness, It is gentle non-stimulated.
2nd, in the selection of aliphatic acid, the big bay of excitant in the prior art is replaced using bland palmitic acid Acid, it ensure that the mildness of product.
3rd, the addition of alkaline agent, it is the accurate amount calculated needed for the aliphatic acid for neutralizing 75%, it is excessive not by fat avoids alkaline agent Fat acid neutralizes, and producing excessive free alkali stimulates skin.
4th, it have selected two anion surfactant:Cocoyl glycine potassium and coconut oleoyl amine DEA, its advantage are It is dirty strong and gentle, it is not tight to wash rear skin.
5th, Sweet Almond Oil is neutral and non-greasy, and be rich in nutrient, moistens and softens skin.
6th, butanediol has moisturizing and bacteriostasis.
Embodiment
With reference to embodiment, the invention will be further described.
One kind removes oil type face cleaning cream, is made up of the raw material of following percentage by weight:Aliphatic acid 20-35%, surfactant 5- 12%, emulsifying agent 1-3%, alkaline agent 4.5-6%, glycerine 8-10%, butanediol 2-6%, Sweet Almond Oil 1-3%, preservative 0.2-0.5% are remaining Measure as distilled water, provided by the invention to remove oil type face cleaning cream, it can not only carry out deep layer cleaning to skin, and with good Oil-control effect.
Inventor implements and has tested various embodiments to be respectively provided with good effect, in above-mentioned formula material, the fat Fat acid is the mixture of myristic acid, palmitic acid and stearic acid arbitrary proportion, and in the selection of aliphatic acid, use is bland Palmitic acid replaces the big laurate of excitant in the prior art, ensure that the mildness of product;The surfactant is cocounut oil The mixture of acylglycine potassium and coconut oleoyl amine DEA arbitrary proportions, wherein coconut oleoyl amine DEA are also known as fatty acid distribution of coconut oil diacetyl Amine, belong to nonionic surfactant, compatibility thickening effect is particularly evident therewith when anion surfactant is in acid, energy With a variety of surfactant compatibilities, cocoyl glycine potassium and coconut oleoyl amine DEA advantages used at the same time are that decontamination is strong and warm With it is not tight to wash rear skin;The emulsifying agent is single stearic acid glycerine lipoprotein and polyoxyethylene(100)Stearate arbitrary proportion Mixture, wherein polyoxyethylene(100)Stearate is also known as PEG-100 stearates, and both of which is conventional emulsifying agent, but There are some differences and difference, more preferable with the use of effect in the present invention, cooperation optimal in the present invention is described single stearic Percentage by weight of the acid glyceride in the emulsifying agent is 30-50%, and remaining is polyoxyethylene(100)Stearate;It is described Alkaline agent is the potassium hydroxide that purity is 91%, and it is the accurate amount calculated needed for the aliphatic acid for neutralizing 75%, avoids alkaline agent excess Do not neutralized by aliphatic acid, and producing excessive free alkali stimulates skin;Aliphatic acid and potassium hydroxide reaction generation fatty acid potassium salt (Soap base)So as to play cleaning action, glycerine can be with disperse fat acid potassium salt;The preservative is the fat of oxybenzene third and oxybenzene formicester The mixture of arbitrary proportion, it plays corrosion-resistant effect in the basic conditions;Sweet Almond Oil is neutral and non-greasy, and is rich in nutrition Element, moisten softening skin;Butanediol has moisturizing and bacteriostasis.
In the present invention, above-mentioned formula goes the oil type face cleaning cream to make in accordance with the following methods, and it comprises the following steps:
(1)The aliphatic acid, emulsifying agent, preservative of above-mentioned parts by weight are added and is heated to 70-80 DEG C in oil phase pot and persistently stirs Mix, it is standby as oil phase;
(2)Glycerine, alkaline agent, distilled water the addition aqueous phase pot of above-mentioned parts by weight are heated to 75 DEG C and continue to stir, as water It is mutually standby;
(3)Aqueous phase is first pumped into emulsification pot, then oil phase is pumped into emulsification pot, insulation by preheating emulsification pot to 70-80 DEG C of temperature Stirring 40 minutes;
(4)70 DEG C and constant temperature are cooled to, it is equal that the surfactant of above-mentioned parts by weight and butanediol are added into stirring in emulsification pot It is even, in step(3)In due to it is lasting stirring thus emulsification pot in temperature can be higher than 70 DEG C, so in step(4)In need to be by it Temperature is down to 70 DEG C;
(5)55 DEG C and constant temperature are cooled to, the Sweet Almond Oil of above-mentioned parts by weight is added in emulsification pot and persistently stirred 30 minutes;
(6)Being cooled to 40 DEG C and continuing stirring until when lotion has the precipitation of pearly-lustre color to discharge.
For above-mentioned formula remove oil type face cleaning cream, the multiple embodiments of inventor's design experiment are simultaneously made according to the method described above Make:
Embodiment 1, one kind are removed oil type face cleaning cream, are made up of the raw material of following percentage by weight:Myristic acid 4%, palmitic acid 6%, Stearic acid 18%, single stearic acid glycerine lipoprotein 1%, polyoxyethylene(100)Stearate 1%, cocoyl glycine potassium 6.5%, cocounut oil Acid amides DEA1.5%, purity are 91% potassium hydroxide 4.77%, glycerine 10%, butanediol 4%, Sweet Almond Oil 3%, the fat of oxybenzene third 0.1%, oxybenzene formicester 0.2%, distilled water 39.93%.
Embodiment 2, one kind are removed oil type face cleaning cream, are made up of the raw material of following percentage by weight:Myristic acid 5%, palmitic acid 5%, stearic acid 17.3%, single stearic acid glycerine lipoprotein 0.5%, polyoxyethylene(100)Stearate 0.5%, cocoyl glycine potassium 2.5%, coconut oleoyl amine DEA2.5%, purity are 91% potassium hydroxide 4.68%, glycerine 10%, butanediol 6%, Sweet Almond Oil 3%, hydroxyl Phenylpropyl alcohol fat 0.2%, oxybenzene formicester 0.3%, surplus are distilled water.
Embodiment 3, one kind are removed oil type face cleaning cream, are made up of the raw material of following percentage by weight:Myristic acid 8%, palmitic acid 6%, stearic acid 21%, single stearic acid glycerine lipoprotein 1.2%, polyoxyethylene(100)Stearate 1.8%, cocoyl glycine potassium 6%, Coconut oleoyl amine DEA6%, purity are 91% potassium hydroxide 6%, glycerine 8%, butanediol 2%, Sweet Almond Oil 1%, the third fat of oxybenzene 0.3%, Oxybenzene formicester 0.2%, surplus are distilled water.
Embodiment 4, one kind are removed oil type face cleaning cream, are made up of the raw material of following percentage by weight:Myristic acid 8%, palmitic acid 6%, stearic acid 16%, single stearic acid glycerine lipoprotein 0.9%, polyoxyethylene(100)Stearate 2.1%, cocoyl glycine potassium 6.5%, coconut oleoyl amine DEA1.5%, purity are 91% potassium hydroxide 4.8%, glycerine 10%, butanediol 6%, Sweet Almond Oil 3%, oxybenzene Third fat 0.1%, oxybenzene formicester 0.2%, surplus are distilled water.
Embodiment 5, one kind are removed oil type face cleaning cream, are made up of the raw material of following percentage by weight:Myristic acid 8%, palmitic acid 6%, stearic acid 16%, single stearic acid glycerine lipoprotein 0.6%, polyoxyethylene(100)Stearate 1.4%, cocoyl glycine potassium 6.5%, coconut oleoyl amine DEA1.5%, purity are 91% potassium hydroxide 4.5%, glycerine 10%, butanediol 4%, Sweet Almond Oil 2%, oxybenzene Third fat 0.1%, oxybenzene formicester 0.2%, surplus are distilled water.
In order to illustrate the using effect for removing oil type face cleaning cream of the present invention, 5 equal extent Oily volunteers have been looked for, The face cleaning cream that deoils that production is formulated with embodiment 1-5 respectively cleans face, right under the conditions of 25 DEG C of air-conditioned room normal office works of room temperature Tested after raw facial skin and cleaning in 3 hours every half an hour with German CK (MPA9) skinanalysis apparatus, facial skin oil Part value test result is as shown in the table:
Tester and embodiment Original value It is worth after cleaning 0.5 hour 1.0 hour 1.5 hour 2.0 hour 2.5 hour 3.0 hour
Tester 1 and embodiment 1 195 79 86 109 132 146 155 169
Tester 2 and embodiment 2 195 82 96 113 134 152 167 174
Tester 3 and embodiment 3 195 83 95 116 136 160 167 178
Tester 4 and embodiment 4 195 84 95 118 137 163 171 182
Tester 5 and embodiment 5 195 82 93 114 138 161 172 182
Make discovery from observation and experimental data is seen, go oil type face cleaning cream effect best manufactured by the formula of embodiment 1, not only most First cleaning skin effect is good, and has preferable oil-control effect, so provided by the invention remove oil type face cleaning cream, it not only can be right Skin carries out deep layer cleaning, and has and deoil and oil-control effect well.

Claims (9)

1. one kind removes oil type face cleaning cream, it is characterised in that is made up of the raw material of following percentage by weight:Aliphatic acid 20-35%, table Face activating agent 5-12%, emulsifying agent 1-3%, alkaline agent 4.5-6%, glycerine 8-10%, butanediol 2-6%, Sweet Almond Oil 1-3%, preservative 0.2-0.5%, surplus are distilled water.
2. according to claim 1 remove oil type face cleaning cream, it is characterised in that the aliphatic acid be myristic acid, palmitic acid and The mixture of stearic acid arbitrary proportion.
3. according to claim 1 remove oil type face cleaning cream, it is characterised in that the surfactant is the sweet ammonia of cocoyl The mixture of sour potassium and coconut oleoyl amine DEA arbitrary proportions.
4. according to claim 1 remove oil type face cleaning cream, it is characterised in that the emulsifying agent be single stearic acid glycerine lipoprotein and Polyoxyethylene(100)The mixture of stearate arbitrary proportion.
5. according to claim 1 remove oil type face cleaning cream, it is characterised in that the alkaline agent is the hydroxide that purity is 91% Potassium.
6. according to claim 1 remove oil type face cleaning cream, it is characterised in that the preservative is the fat of oxybenzene third and oxybenzene first The mixture of fat arbitrary proportion.
7. described oil type face cleaning cream is removed according to claim 1-6 is any, it is characterised in that by following components in percentage by weight Raw material be made:Aliphatic acid 28%, surfactant 8%, emulsifying agent 2%, alkaline agent 4.77%, glycerine 10%, butanediol 4%, dessert almond Oil 3%, distilled water 39.93%, preservative 0.3%.
8. described oil type face cleaning cream is removed according to claim 1-6 is any, it is characterised in that by following components in percentage by weight Raw material be made:Myristic acid 4%, palmitic acid 6%, stearic acid 18%, single stearic acid glycerine lipoprotein 1%, polyoxyethylene(100)Stearic acid Fat 1%, cocoyl glycine potassium 6.5%, coconut oleoyl amine DEA1.5%, purity are 91% potassium hydroxide 4.77%, glycerine 10%, fourth Glycol 4%, Sweet Almond Oil 3%, distilled water 39.93%, the third fat of oxybenzene 0.1%, oxybenzene formicester 0.2%.
9. a kind of prepare the method that oil type face cleaning cream is removed as described in claim 1-8 is any, it is characterised in that comprises the following steps:
(1)The aliphatic acid, emulsifying agent, preservative of above-mentioned parts by weight are added and is heated to 70-80 DEG C in oil phase pot and persistently stirs Mix, it is standby as oil phase;
(2)Glycerine, alkaline agent, distilled water the addition aqueous phase pot of above-mentioned parts by weight are heated to 75 DEG C and continue to stir, as water It is mutually standby;
(3)Aqueous phase is first pumped into emulsification pot, then oil phase is pumped into emulsification pot, insulation by preheating emulsification pot to 70-80 DEG C of temperature Stirring 40 minutes;
(4)70 DEG C and constant temperature are cooled to, it is equal that the surfactant of above-mentioned parts by weight and butanediol are added into stirring in emulsification pot It is even;
(5)55 DEG C and constant temperature are cooled to, the Sweet Almond Oil of above-mentioned parts by weight is added in emulsification pot and persistently stirred 30 minutes;
(6)Being cooled to 40 DEG C and continuing stirring until when lotion has the precipitation of pearly-lustre color to discharge.
CN201710972235.0A 2017-10-18 2017-10-18 One kind removes oil type face cleaning cream and preparation method thereof Pending CN107616929A (en)

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Application Number Priority Date Filing Date Title
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CN107616929A true CN107616929A (en) 2018-01-23

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102178611A (en) * 2011-04-22 2011-09-14 杭州珀莱雅控股股份有限公司 High-pearly-lustre high-foam soap base cleansing cream and preparation method thereof
CN103505382A (en) * 2013-09-17 2014-01-15 广州环亚化妆品科技有限公司 Cleanser composition with stable wire drawing effect and preparation method thereof
CN104257567A (en) * 2014-10-22 2015-01-07 广东幸美化妆品股份有限公司 Oil-controlling facial cleanser and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102178611A (en) * 2011-04-22 2011-09-14 杭州珀莱雅控股股份有限公司 High-pearly-lustre high-foam soap base cleansing cream and preparation method thereof
CN103505382A (en) * 2013-09-17 2014-01-15 广州环亚化妆品科技有限公司 Cleanser composition with stable wire drawing effect and preparation method thereof
CN104257567A (en) * 2014-10-22 2015-01-07 广东幸美化妆品股份有限公司 Oil-controlling facial cleanser and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
李小迪: "浅淡乳化型皂基洁面膏的配方与工艺特点", 《中国洗涤用品工业》 *

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Application publication date: 20180123

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