CN103451019A - Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume - Google Patents
Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume Download PDFInfo
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- CN103451019A CN103451019A CN2013103980420A CN201310398042A CN103451019A CN 103451019 A CN103451019 A CN 103451019A CN 2013103980420 A CN2013103980420 A CN 2013103980420A CN 201310398042 A CN201310398042 A CN 201310398042A CN 103451019 A CN103451019 A CN 103451019A
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- essence
- microcapsule
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- extract
- perfume
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 57
- 239000003094 microcapsule Substances 0.000 title claims abstract description 56
- 239000002304 perfume Substances 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 54
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000463 material Substances 0.000 claims abstract description 17
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 16
- 239000003205 fragrance Substances 0.000 claims abstract description 16
- 238000003756 stirring Methods 0.000 claims abstract description 13
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- 239000002994 raw material Substances 0.000 claims abstract description 9
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- KWGRBVOPPLSCSI-WPRPVWTQSA-N (-)-ephedrine Chemical compound CN[C@@H](C)[C@H](O)C1=CC=CC=C1 KWGRBVOPPLSCSI-WPRPVWTQSA-N 0.000 claims description 2
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 claims description 2
- 239000001306 (7E,9E,11E,13E)-pentadeca-7,9,11,13-tetraen-1-ol Substances 0.000 claims description 2
- OOCCDEMITAIZTP-QPJJXVBHSA-N (E)-cinnamyl alcohol Chemical compound OC\C=C\C1=CC=CC=C1 OOCCDEMITAIZTP-QPJJXVBHSA-N 0.000 claims description 2
- VPKMGDRERYMTJX-CMDGGOBGSA-N 1-(2,6,6-Trimethyl-2-cyclohexen-1-yl)-1-penten-3-one Chemical compound CCC(=O)\C=C\C1C(C)=CCCC1(C)C VPKMGDRERYMTJX-CMDGGOBGSA-N 0.000 claims description 2
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 2
- 244000144927 Aloe barbadensis Species 0.000 claims description 2
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- 244000003416 Asparagus officinalis Species 0.000 claims description 2
- 235000005340 Asparagus officinalis Nutrition 0.000 claims description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 2
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 claims description 2
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 claims description 2
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- 239000005770 Eugenol Substances 0.000 claims description 2
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- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 claims description 2
- 235000011201 Ginkgo Nutrition 0.000 claims description 2
- 244000194101 Ginkgo biloba Species 0.000 claims description 2
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- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 2
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 claims description 2
- 244000044822 Simmondsia californica Species 0.000 claims description 2
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- 244000273928 Zingiber officinale Species 0.000 claims description 2
- 235000006886 Zingiber officinale Nutrition 0.000 claims description 2
- OOCCDEMITAIZTP-UHFFFAOYSA-N allylic benzylic alcohol Natural products OCC=CC1=CC=CC=C1 OOCCDEMITAIZTP-UHFFFAOYSA-N 0.000 claims description 2
- 235000011399 aloe vera Nutrition 0.000 claims description 2
- 235000021028 berry Nutrition 0.000 claims description 2
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 claims description 2
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- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 claims description 2
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- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 claims description 2
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Landscapes
- Manufacturing Of Micro-Capsules (AREA)
Abstract
The invention discloses a microcapsule essence perfume for cigarettes as well as a preparation method of the microcapsule essence perfume. The microcapsule essence perfume contains the following raw materials in parts by weight: 1-3 parts of essence, 0.05-0.2 part of glycerinum or/and propylene glycol, 1-5 parts of wall materials and 0.01-0.03 part of emulsifier. The preparation method comprises the steps of: mixing essence, glycerinum or/and propylene glycol to obtain a mixture, evenly stirring the mixture, adding 95% ethanol with 1-10 times weight of the mixture, and mixing and evenly mixing to obtain a mixed solution; adding wall materials and emulsifier in the mixed solution and stirring for homogenization; and sealing, standing for 1-2 hours at normal temperature, refrigerating for 15-60 minutes at the temperature of minus 20 DEG C to minus 80 DEG C, drying for 8-24 hours at the vacuum degree of 30-80MPa and the temperature of 40-80 DEG C, grinding dried products, sieving the ground products to prepare microcapsule particles, thereby obtaining the microcapsule essence perfume for cigarettes. The perfume for cigarettes is made to microcapsules, so that perfume is free from being affected by external factors, and loss and fragrance distortion caused by volatile components in the perfume for cigarettes are effectively reduced.
Description
Technical field
The present invention relates to technical field of cigarettes, be specifically related to microcapsule essence spices and preparation method thereof for a kind of cigarette.
Background technology
China is production of cigarettes and consumption big country, and along with the concern of people to smoking and health problem, tobacco industry is faced with when improving the cigarette quality, also faces and reduces the problem of cigarette to the harm of human body.So, for reducing cigarette hazardness, reducing the coal-tar middle oil content of cigarette is a very important approach.For cigarette product, along with the reduction of tar content, can have influence on cigarette fragrance, inhale the quality of all respects such as flavor, the human consumer is difficult for the such cigarette product of acceptance.The quality of the product of cigarette and security are conflicts, and how solving this becomes China's tobacco industry key subjects of research at present to contradiction.
Along with the development of low-coke tar cigarette, after filtration and dilution, it is obviously not enough that fragrance seems the fragrance of tobacco itself, and perfuming can make up these losses, does not increase again the tar generation.The perfuming of cigarette product is an important step of formulating of recipe, it is the effective means that improves the cigarette product quality, the very important means of cigarette industry, it plays a part not replace for the fragrance of augmenting, modify cigarette, it is also one of extremely secret core technology of cigarette enterprise, and the Main Function of perfuming has:
(1) flavouring is fragrant with tax;
(2) improve jealous;
(3) coordinate fragrance;
(4) there is purpose increase or strengthen other fragrance, make smoke plentiful;
(5) perfuming is suitable, can improve the cigarette grade to a certain extent.
Flavouring essence for tobacco is of a great variety, and various component volatilization gender gap are large, and the component volatilization of many essence is strong, and the easy oxidation of some spices or chance photo-thermal easily decompose, and can not apply in tobacco blend well.The volatilization of perfume ingredient not only causes the loss of essence, and causes the distortion of fragrance.A lot of components are lost by volatilization at manufacture and the lay up period of smoking article, thereby cause the cigarette lost of life.
For fear of loss or the volatilization of flavouring essence for tobacco, usually adopt various methods to wrap up perfume ingredient.High volatile volatile, perishable tobacco aromatics using, by microcapsule coated, are improved to stability on the one hand, can discharge aroma component burning and sucking under state on the other hand, play the effect that improves cigarette mainstream flue gas taste and quality, reach the purpose of flavouring.
The method of existing micro encapsulation has Physical, physico-chemical processes and chemical method, and essence microcapsule more extensively adopts spray-drying process, but the high temperature in the spray-drying process process can cause essence volatilization loss larger, and may cause the fragrance distortion.Therefore, spray-drying process prepares high-volatile essence and has the weakness that is difficult to overcome as the flavouring essence for tobacco microcapsule.
Summary of the invention
The present invention is directed to common micro encapsulation in prior art and be not suitable for essence that volatility is high and make the defect of flavouring essence for tobacco microcapsule and studied, provide a kind of lyophilize to prepare the method for cigarette with microcapsule essence.
For solving the problems of the technologies described above, a kind of cigarette microcapsule essence of the present invention, its raw material is counted according to weight part ratio: the essence of 1 ~ 3 part, the glycerine of 0.05 ~ 0.2 part are or/and propylene glycol, the wall material of 1 ~ 5 part and the emulsifying agent of 0.01 ~ 0.03 part.
Further, its raw material is counted according to weight part ratio: the essence of 1 ~ 3 part, the glycerine of 0.05 ~ 0.1 part are or/and propylene glycol, the wall material of 1 ~ 3 part and the emulsifying agent of 0.01 ~ 0.03 part.
Again further, its raw material is counted according to weight part ratio: the essence of 1 part, the glycerine of 0.08 part, the wall material of 3 parts and the emulsifying agent of 0.01 part.
Again further, its raw material is counted according to weight part ratio: the essence of 1 part, the propylene glycol of 0.08 part, the wall material of 3 parts and the emulsifying agent of 0.01 part.
Again further, the particle diameter of these microcapsule is 10 ~ 100nm.
Again further, described essence be in natural extract, mono-isolate and flavouring essence for tobacco any one.
Again further, described natural extract be asparagus juice and aloe vera gel, Radix Panacis Quinquefolii, ?rattletop, Fructus Capsici extract, Echinacea purpurea Moench essence oil from plant, Cacumen Cupressi oil, cocoa extract, extractive of flax seed, ginger and Folium Ginkgo extract, Jojoba oil and Jojoba berry extract, yellow flag extract, lupulus extract, spearmint oil, Alfalfa P.E, green tea extract, racephedrine, Radix Glycyrrhizae extract, Angelica roots, fenugreek extract, peru balm, Fructus Jujubae extract, ginkgo biloba extract, Semen Vitis viniferae extract;
Described mono-isolate is mentha camphor, isoesdragol, borneol, santalol, citral, Geraniol, Eugenol, cinnamic alcohol, Methylionone;
Described tobacco aromatics using is chocolate perfume, milk, fruital, nutty, the banksia rose, the fragrance of a flower, Xin Xiang, honey is fragrant, cream is fragrant, beans are fragrant, bread is fragrant, camerlsed, phenol perfume, sootiness is fragrant or aroma.
Again further, described wall material be in beta-cyclodextrin, methylcellulose gum, ethyl cellulose, polyoxyethylene glycol, chitosan, gelatin, sodium alginate, maltodextrin, soybean protein isolate, gum arabic and casein arbitrarily one or more; Described emulsifying agent be in soybean phospholipid, glycerin fatty acid ester, sucrose ester, hard ester acyl lactylate and calcium, xylitol ester and Nitranitol arbitrarily one or more.
The present invention also provides the preparation method of a kind of cigarette with microcapsule essence, comprises the following steps:
1) by above-mentioned weight part ratio, take: essence, glycerine are or/and propylene glycol, wall material and emulsifying agent;
2) by essence, glycerine or/and mixed with propylene glycol stirs, add 95% ethanol of 1 ~ 10 times of weight, mixing and stirring, obtain mixed solution;
3) to step 2) in mixed solution add wall material and emulsifying agent, stir homogeneous;
4) then seal rear normal temperature after standing 1 ~ 2 hour, be freezing 15-60min under-20 ~-80 ℃ of conditions in temperature, then be 30-80MPa in vacuum tightness, temperature is dry 8 ~ 24h under 40 ~ 80 ℃ of conditions, dried product is pulverized and sieved and makes microcapsule granule, obtain the cigarette microcapsule essence.
As preferred version, when spices is essential oil, in step 3), processing condition: pressure is under 20 ~ 60MPa condition, homogeneous 5 ~ 10min, and homogeneous 2 ~ 4 times.
Beneficial effect of the present invention is:
1, the selected wall material of the present invention is nontoxic, tasteless, harmless, non-environmental-pollution, and chemical property is more stable, under normal temperature, with cores such as essence and flavoring agents, does not react.
2, in the preparation process of flavouring essence for tobacco lyophilize micro encapsulation of the present invention, cryogenic freezing, vacuum-drying, reduced the loss of high volatile volatile fragrance matter and distributed, and effectively guaranteed the quality of flavouring essence for tobacco.
3, the present invention makes microcapsule to flavouring essence for tobacco and can make flavouring essence for tobacco avoid the impact of extraneous factor, has effectively improved the loss that in the flavouring essence for tobacco, volatile component causes and fragrance distortion.
4, the present invention is applied to the microcapsule flavouring essence for tobacco in cigarette stability and the shelf time that is conducive to improve cigarette.
5, that flavouring essence for tobacco is made to the microcapsule production cost is low in the present invention, and technological process is simple, and equipment is simple, and supplementary material is easy to get, easy to utilize.
Embodiment
In order to explain better the present invention, further illustrate main contents of the present invention below in conjunction with specific embodiment, but content of the present invention not only is confined to following examples.
Embodiment 1
The preparation of microcapsule Dendranthema indicum essential oil fragrances for cigarette
Take 1 part of cigarette Dendranthema indicum essential oil fragrances, add the glycerine of 0.05 part, add the propylene glycol of 0.10 part, add 95% edible ethanol of 2 parts, mixing and stirring.The mixed solution stirred is added to 2 parts of soybean protein isolates doubly, add the fatty acid glycerine fat of 0.01 part, under the condition that is 40MPa at homogenization pressure, homogeneous is 8 minutes, homogeneous 2 times.Mixed solution normal temperature after homogeneous is carried out to pre-freeze after standing 2 hours, and the pre-freeze temperature is :-40 ℃, the pre-freeze time is: 30min.The mixed solution that pre-freeze is good is 56MPa in vacuum tightness, and Heating temperature is dry 24h under 45 ℃.Dried product is taken out and pulverizes and sieves, make microcapsule Dendranthema indicum essential oil fragrances for cigarette.
Embodiment 2
The preparation of microcapsule Radix Glycyrrhizae extract essence for cigarette
Take 1 part of cigarette Radix Glycyrrhizae extract essence, the propylene glycol that adds 0.08 part, 95% edible ethanol that adds 1.5 parts, add the beta-cyclodextrin of 3 parts and the soybean phospholipid of 0.01 part, mixing and stirring, mixed solution normal temperature after stirring is carried out to pre-freeze after standing 2 hours, and the pre-freeze temperature is :-60 ℃, the pre-freeze time is: 20min.The mixed solution that pre-freeze is good is 60MPa in vacuum tightness, and Heating temperature is dry 12h under 50 ℃.Dried product is taken out and pulverizes and sieves, make microcapsule Radix Glycyrrhizae extract essence for cigarette.
Embodiment 3
Take 0.5 part of mentha camphor and 0.5 part of isoesdragol essence, add the glycerine of 0.05 part, add 95% edible ethanol of 10 parts, add the beta-cyclodextrin of 1 part, the methylcellulose gum of 2 parts, the ethyl cellulose of 1 part, the soybean protein isolate of 1 part; The sucrose ester that adds again 0.01 part, be under the 20MPa condition at pressure, homogeneous 10min, and homogeneous 4 times; Then the rear normal temperature of sealing is after standing 1 hour, be freezing 40min under-60 ℃ of conditions in temperature, then be 60MPa in vacuum tightness, temperature is dry 12h under 60 ℃ of conditions, dried product is pulverized and sieved and makes microcapsule granule, obtain microcapsule mentha camphor and isoesdragol essence for cigarette
Embodiment 4
Take 1 part of chocolate perfume, add the glycerine of 0.15 part and the propylene glycol of 0.05 part, add 95% edible ethanol of 1 part, then add the chitosan of 2 parts, the gelatin of 1 part, the glycerin fatty acid ester of 0.01 part and the sucrose ester of 0.02 part; Stir homogeneous; Then the rear normal temperature of sealing is after standing 2 hours, be freezing 60min under-80 ℃ of conditions in temperature, then be 80MPa in vacuum tightness, temperature is dry 8h under 80 ℃ of conditions, dried product is pulverized and sieved and makes microcapsule granule, obtain the chocolate essence of microcapsule for cigarette.
Embodiment 5
Take 1 part of banksia rose, add the glycerine of 0.1 part, add 95% edible ethanol of 6 parts, then add the gelatin of 1 part and the soybean phospholipid of 0.01 part; At pressure, be homogeneous 10min under the 20MPa condition, homogeneous 2 times.Then after the sealing, normal temperature, after standing 1 hour, is freezing 15min under-20 ℃ of conditions in temperature, then is 30MPa in vacuum tightness, and temperature is dry 8h under 80 ℃ of conditions, and dried product is pulverized and sieved and makes microcapsule granule, obtains cigarette microcapsule costustoot essence.
Embodiment 6
Take 1 part of cocoa extract, 1 part of Radix Glycyrrhizae extract and 1 part of Angelica roots, the propylene glycol that adds 0.1 part, add 95% edible ethanol of 8 parts, then add the gelatin of 1 part, the gum arabic of 2 parts, the glycerin fatty acid ester of 0.02 part and the xylitol ester of 0.01 part; Stir homogeneous; Then after the sealing, normal temperature, after standing 2 hours, is freezing 40min under-40 ℃ of conditions in temperature, then is 40MPa in vacuum tightness, and temperature is dry 16h under 60 ℃ of conditions, and dried product is pulverized and sieved and makes microcapsule granule, obtains the cigarette microcapsule essence.
Embodiment 7
Take 1 part of Fructus Jujubae extract essence, 1 part of milk and 1 part of fruital, the propylene glycol that adds 0.0.5 part, add 95% edible ethanol of 8 parts, then add the ethyl cellulose of 1 part, the polyoxyethylene glycol of 1 part, the casein of 3 parts and the Nitranitol of 0.01 part; At pressure, be homogeneous 5min under the 60MPa condition, homogeneous 4 times.Then after the sealing, normal temperature, after standing 2 hours, is freezing 15min under-20 degree conditions in temperature, then is 60MPa in vacuum tightness, and temperature is dry 24h under 60 ℃ of conditions, and dried product is pulverized and sieved and makes microcapsule granule, obtains the cigarette microcapsule essence.
Embodiment 8
Take 1 part of fenugreek extract and 1 part of peru balm, the propylene glycol that adds 0.0.8 part, add 95% edible ethanol of 3 parts, then add the beta-cyclodextrin of 2.4 parts and the xylitol ester of 0.01 part; At pressure, be under the 30MPa condition, homogeneous 60min, homogeneous 3 times, then the rear normal temperature of sealing is after standing 2 hours, be freezing 15min under-20 ℃ of conditions in temperature, then be 60MPa in vacuum tightness, temperature is dry 24h under 60 ℃ of conditions, dried product is pulverized and sieved and makes microcapsule granule, obtain the cigarette microcapsule essence.
Embodiment 9
Take 1 part of cocoa extract, the glycerine that adds 0.0.8 part, add 95% edible ethanol of 3 parts, then add the beta-cyclodextrin of 3 parts and the soybean phospholipid of 0.01 part; At pressure, be homogeneous 5min under the 60MPa condition, and homogeneous 4 times.Then after the sealing, normal temperature, after standing 1 hour, is freezing 40min under-60 ℃ of conditions in temperature, then is 40MPa in vacuum tightness, and temperature is dry 10h under 60 ℃ of conditions, and dried product is pulverized and sieved and makes microcapsule granule, obtains the cigarette microcapsule essence.
Embodiment 10
Take 1 part of extractive of flax seed, the glycerine that adds 0.0.8 part, add 95% edible ethanol of 3 parts, then add the beta-cyclodextrin of 3 parts and the soybean phospholipid of 0.01 part; At pressure, be homogeneous 5min under the 60MPa condition, and homogeneous 4 times.Then after the sealing, normal temperature, after standing 1 hour, is freezing 40min under-60 ℃ of conditions in temperature, then is 40MPa in vacuum tightness, and temperature is dry 10h under 60 ℃ of conditions, and dried product is pulverized and sieved and makes microcapsule granule, obtains the cigarette microcapsule essence.
Claims (10)
1. cigarette microcapsule essence, it is characterized in that: its raw material is counted according to weight part ratio: the essence of 1 ~ 3 part, the glycerine of 0.05 ~ 0.2 part are or/and propylene glycol, the wall material of 1 ~ 5 part and the emulsifying agent of 0.01 ~ 0.03 part.
2. cigarette microcapsule essence according to claim 1, it is characterized in that: its raw material is counted according to weight part ratio: the essence of 1 ~ 3 part, the glycerine of 0.05 ~ 0.1 part are or/and propylene glycol, the wall material of 1 ~ 3 part and the emulsifying agent of 0.01 ~ 0.03 part.
3. cigarette microcapsule essence according to claim 2, it is characterized in that: its raw material is counted according to weight part ratio: the essence of 1 part, the glycerine of 0.08 part, the wall material of 3 parts and the emulsifying agent of 0.01 part.
4. cigarette microcapsule essence according to claim 2, it is characterized in that: its raw material is counted according to weight part ratio: the essence of 1 part, the propylene glycol of 0.08 part, the wall material of 3 parts and the emulsifying agent of 0.01 part.
5. cigarette microcapsule essence according to claim 1, it is characterized in that: the particle diameter of these microcapsule is 10 ~ 100nm.
6. cigarette microcapsule essence according to claim 1 is characterized in that: described essence be in natural extract, mono-isolate and flavouring essence for tobacco any one.
7. cigarette microcapsule essence according to claim 1 is characterized in that:
Described natural extract is asparagus juice and aloe vera gel, Radix Panacis Quinquefolii, ?rattletop, Fructus Capsici extract, the Echinacea purpurea Moench essence oil from plant, Cacumen Cupressi oil, cocoa extract, extractive of flax seed, ginger and Folium Ginkgo extract, Jojoba oil and Jojoba berry extract, the yellow flag extract, the lupulus extract, spearmint oil, Alfalfa P.E, green tea extract, racephedrine, Radix Glycyrrhizae extract, Angelica roots, fenugreek extract, peru balm, Fructus Jujubae extract, ginkgo biloba extract, Semen Vitis viniferae extract,
Described mono-isolate is mentha camphor, isoesdragol, borneol, santalol, citral, Geraniol, Eugenol, cinnamic alcohol, Methylionone;
Described tobacco aromatics using is chocolate perfume, milk, fruital, nutty, the banksia rose, the fragrance of a flower, Xin Xiang, honey is fragrant, cream is fragrant, beans are fragrant, bread is fragrant, camerlsed, phenol perfume, sootiness is fragrant or aroma.
8. cigarette microcapsule essence according to claim 1 is characterized in that: described wall material be in beta-cyclodextrin, methylcellulose gum, ethyl cellulose, polyoxyethylene glycol, chitosan, gelatin, sodium alginate, maltodextrin, soybean protein isolate, gum arabic and casein arbitrarily one or more; Described emulsifying agent be in soybean phospholipid, glycerin fatty acid ester, sucrose ester, hard ester acyl lactylate and calcium, xylitol ester and Nitranitol arbitrarily one or more.
9. the preparation method of microcapsule essence for the described cigarette of a claim 1 is characterized in that: comprise the following steps:
1) by above-mentioned weight part ratio, take: essence, glycerine are or/and propylene glycol, wall material and emulsifying agent;
2) by essence, glycerine or/and mixed with propylene glycol stirs, add 95% ethanol of 1 ~ 10 times of weight, mixing and stirring, obtain mixed solution;
3) to step 2) in mixed solution add wall material and emulsifying agent, will stir homogeneous;
4) then seal rear normal temperature after standing 1 ~ 2 hour, be freezing 15-60min under-20 ~-80 ℃ of conditions in temperature, then be 30-80MPa in vacuum tightness, temperature is dry 8 ~ 24h under 40 ~ 80 ℃ of conditions, dried product is pulverized and sieved and makes microcapsule granule, obtain the cigarette microcapsule essence.
10. the preparation method of microcapsule essence for cigarette according to claim 1, it is characterized in that: when described spices is essential oil, in step 3), processing condition: pressure is under 20 ~ 60MPa condition, homogeneous 5 ~ 10min, and homogeneous 2 ~ 4 times.
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