CN111849633A - Essential oil composition and preparation method and application thereof - Google Patents
Essential oil composition and preparation method and application thereof Download PDFInfo
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- CN111849633A CN111849633A CN202010759512.1A CN202010759512A CN111849633A CN 111849633 A CN111849633 A CN 111849633A CN 202010759512 A CN202010759512 A CN 202010759512A CN 111849633 A CN111849633 A CN 111849633A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
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Abstract
The invention relates to an essential oil composition and a preparation method and application thereof. The essential oil composition is mainly prepared from the following raw materials in percentage by mass: 0.5 to 40 percent of exocarpium citri grandis essential oil, 0.5 to 50 percent of mint essential oil, 0.01 to 20 percent of cypress essential oil, 0.01 to 20 percent of cedar essential oil, 0.01 to 20 percent of frankincense essential oil, 0 to 0.5 percent of emulsifier and 0 to 98 percent of grease solvent. Through blending of different types of essential oil, the problem that the fragrance of the pummelo peel essential oil is not fused and coordinated with the fragrance of cigarettes is solved, the fragrance of the cigarettes is enriched, the effect of smoking comfort is enhanced, and the throat discomfort symptom caused by smoking is effectively relieved.
Description
Technical Field
The invention relates to the technical field of cigarettes, in particular to an essential oil composition containing pummelo peel essential oil and a preparation method and application thereof.
Background
Smoking affects human health, and in order to reduce the harm of cigarettes to human bodies, China clearly limits the content of tar in cigarettes, so that tar reduction and harm reduction are development trends of the tobacco industry, and tar reduction refers to reduction of the content of tar in cigarettes. However, the reduction of tar content in cigarettes results in insufficient cigarette aroma and poor smoking taste. In order to make up for the insufficient aroma of cigarettes, a common method is to add spices into the cigarettes.
The popping beads, also called as flavor pills, brittle capsules and beads, are flavor beads with core materials with different types of flavors wrapped by polymer capsule walls, are mainly used in filter tips of cigarettes, can be squeezed and broken, have popping feeling when being squeezed, release the core materials with flavor after being squeezed and realize flavor supplement in the smoking process. Compared with the traditional method of adding spices into tobacco shreds, the bead blasting wraps the essential oil composition in the capsule wall, so that the fragrance loss is effectively delayed, the essential oil is prevented from being oxidized, and the bead blasting is added in the non-combustion section of the cigarette, so that the burning deterioration of the essential oil composition is avoided.
With the development of the bead-exploded cigarette market, the bead-exploded cigarettes with various flavors such as wine flavor, herbal flavor, fruit flavor, flower flavor and the like are available on the market, but most of the bead-exploded cigarettes are made of artificial essence at present, the original flavor characteristics of the cigarettes are greatly changed, the flavor is unnatural, the smoking comfort is influenced, and the health-care effect on the throat is not achieved.
Exocarpium Citri Grandis is dry young fruit, immature or near mature dry epicarp of Citrus grandis (Citrus grandis) of Rutaceae; or the immature or near mature dried outer pericarp of Osbeck of Citrus grandis (L.). Pummelo peel is known as one of ten broad medicines, has the effects of regulating qi, relieving epigastric distention, eliminating dampness and resolving phlegm, is classified as a court tribute in the Mingqing period, is called southern ginseng and is also called a 'one-piece worth with great value'. Modern pharmacological research shows that the pummelo peel essential oil has the functions of reducing phlegm and relieving cough. The pummelo peel essential oil is applied to the cigarette blasting beads, and can play a health care role in the throat of smokers. However, the fragrance of pummelo peel is greatly different from that of cigarettes, and when the pummelo peel is used for cigarette blasting, the problem that the fragrance of blasting is not fused with that of cigarettes easily occurs.
Therefore, the research is carried out to develop new fragrance type exploded bead cigarettes with health care function aiming at the problem that the fragrance of the pummelo peel essential oil is not fused and coordinated with the fragrance of the cigarettes.
Disclosure of Invention
The invention aims to provide an essential oil composition containing pummelo peel essential oil, which is prepared with other essential oil, so that the problem that the fragrance of the pummelo peel essential oil is not fused with and inconsistent with the fragrance of cigarettes is solved, the overall fragrance of the prepared essential oil composition does not influence the original fragrance of smoke, and the situation of bustling is avoided. The cigarette fragrance enhancer can be used in cigarettes with low tar content, supplement of insufficient cigarette fragrance is realized, the cigarette fragrance style is enriched, the smoking comfort is enhanced, and throat discomfort symptoms such as dry throat, cough, excessive phlegm and the like caused by smoking can be effectively relieved.
The specific technical scheme is as follows:
an essential oil composition is mainly prepared from the following raw materials in percentage by mass:
0.5 to 40 percent of exocarpium citri grandis essential oil, 0.5 to 50 percent of mint essential oil, 0.01 to 20 percent of cypress essential oil, 0.01 to 20 percent of cedar essential oil, 0.01 to 20 percent of frankincense essential oil, 0 to 0.3 percent of emulsifier and 0 to 98 percent of grease solvent.
In one preferred embodiment, the essential oil composition is mainly prepared from the following raw materials in percentage by mass:
2 to 20 percent of pummelo peel essential oil, 2 to 40 percent of mint essential oil, 0.1 to 10 percent of cypress essential oil, 0.1 to 10 percent of cedar essential oil, 0.1 to 10 percent of frankincense essential oil, 0.01 to 0.3 percent of emulsifier and 10 to 95 percent of grease solvent.
In one preferred embodiment, the essential oil composition is mainly prepared from the following raw materials in percentage by mass:
3 to 15 percent of exocarpium citri grandis essential oil, 3 to 20 percent of mint essential oil, 1 to 5 percent of cypress essential oil, 1 to 5 percent of cedar essential oil, 1 to 5 percent of frankincense essential oil, 0.05 to 0.3 percent of emulsifier and 50 to 90 percent of grease solvent.
In one preferred embodiment, the oil solvent is selected from one or more of caprylic capric acid glyceride, palm oil, olive oil, corn oil, sunflower oil, peanut oil, wheat germ oil, sweet almond oil, persic oil, jojoba oil, sesame oil, and coconut oil.
In one preferred embodiment, the emulsifier is selected from one or both of span and tween.
The invention also provides a preparation method of the essential oil composition.
The specific technical scheme is as follows:
a method for preparing an essential oil composition, comprising the steps of:
mixing the exocarpium Citri Grandis essential oil, herba Menthae essential oil, Cupressus Sempervirens essential oil, Cedar essential oil and Olibanum essential oil, and stirring well to obtain mixed essential oil;
and adding or not adding the grease solvent and the emulsifier into the mixed essential oil, stirring for 0.5-2 h, and then carrying out vacuum degassing treatment for 10-20 min.
The invention also provides an essential oil popping bead. The blasting bead is round, the diameter is 3-4 mm, the mass is 17-23 mg, the content of the essential oil composition is 20-25 mul, and the crushing pressure is 1.0-1.5 kg.
The specific technical scheme is as follows:
an essential oil bead comprises a core material and a capsule wall wrapping the core material;
the core material comprises the essential oil composition or the essential oil composition prepared by the preparation method.
In one preferred embodiment, the capsule wall is mainly prepared from the following raw materials in percentage by mass:
1-12% of sodium alginate, 0.1-2% of Arabic gum, 0.05-0.5% of glycerol, 0.5-3% of carrageenan and 83-98% of water.
The invention also provides a preparation method of the essential oil popple. The bead prepared by the method has the advantages of round appearance, less broken particles, moderate brittleness and strength, uniform capsule wall and good hand feeling when being pinched broken.
The specific technical scheme is as follows:
a preparation method of essential oil popping beads comprises the steps of mixing sodium alginate, Arabic gum, glycerol, carrageenan and water, heating to melt, stirring uniformly, standing for 1-2 h, and filtering to obtain a capsule wall solution;
and curing and molding the essential oil composition serving as a raw material of a core material and the capsule wall solution serving as a raw material of a capsule wall.
In one preferred embodiment, the curing agent for curing and forming is selected from one or more of a calcium chloride aqueous solution with the mass fraction of 2-10%, a calcium carbonate aqueous solution with the mass fraction of 2-10% and a dicalcium phosphate aqueous solution with the mass fraction of 2-10%.
Compared with the prior art, the invention has the following beneficial effects:
the essential oil composition is prepared by blending pummelo peel essential oil, mint essential oil, cypress essential oil, cedar essential oil and frankincense essential oil, the essential oil composition is obtained by blending different types of essential oil according to a certain proportion, the problems that the fragrance of the pummelo peel essential oil and the fragrance of cigarettes are not fused and coordinated are solved, the integral fragrance of the blended essential oil composition does not influence the original fragrance of smoke, and the situation of bustling is avoided. The cigarette fragrance enhancer can be used in cigarettes with low tar content, supplement of insufficient cigarette fragrance is realized, the cigarette fragrance style is enriched, the smoking comfort is enhanced, and throat discomfort symptoms such as dry throat, cough, excessive phlegm and the like caused by smoking can be effectively relieved.
Detailed Description
The present invention will be described in further detail with reference to specific examples. The present invention may be embodied in many different forms and is not limited to the embodiments described herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
Although the pummelo peel essential oil has the effects of relieving cough and reducing phlegm, the fragrance of pummelo peel is different from that of cigarettes, and the problem that the fragrance of popping beads is not fused with that of cigarettes easily occurs when the pummelo peel essential oil is used for popping the beads of cigarettes.
The invention provides an essential oil composition which is mainly prepared from the following raw materials in percentage by mass:
0.5 to 40 percent of exocarpium citri grandis essential oil, 0.5 to 50 percent of mint essential oil, 0.01 to 20 percent of cypress essential oil, 0.01 to 20 percent of cedar essential oil, 0.01 to 20 percent of frankincense essential oil, 0 to 0.5 percent of emulsifier and 0 to 98 percent of grease solvent.
According to the invention, through blending of different types of essential oils, the problem that the fragrance of the pummelo peel essential oil is not fused with and coordinated with the fragrance of cigarettes is solved, the overall fragrance of the blended essential oil composition does not influence the original taste of smoke, and the situation of bustling is avoided. The cigarette fragrance enhancer can be used in cigarettes with low tar content, supplement of insufficient cigarette fragrance is realized, the cigarette fragrance style is enriched, the smoking comfort is enhanced, and throat discomfort symptoms such as dry throat, cough, excessive phlegm and the like caused by smoking can be effectively relieved.
Preferably, the essential oil composition is mainly prepared from the following raw materials in percentage by mass:
2 to 20 percent of exocarpium citri grandis essential oil, 2 to 40 percent of mint essential oil, 0.1 to 10 percent of cypress essential oil, 0.1 to 10 percent of cedar essential oil, 0.1 to 10 percent of frankincense essential oil, 0.01 to 0.3 percent of emulsifier and 10 to 95 percent of grease solvent.
More preferably, the essential oil composition is mainly prepared from the following raw materials in percentage by mass:
3 to 15 percent of exocarpium citri grandis essential oil, 3 to 20 percent of mint essential oil, 1 to 5 percent of cypress essential oil, 1 to 5 percent of cedar essential oil, 1 to 5 percent of frankincense essential oil, 0.05 to 0.3 percent of emulsifier and 50 to 90 percent of grease solvent.
The proportion of the raw materials is adjusted, so that the fragrance of the pummelo peel and the fragrance of the cigarettes are more coordinated.
Preferably, the oil solvent is selected from one or more of caprylic capric acid glyceride, palm oil, olive oil, corn oil, sunflower seed oil, peanut oil, wheat germ oil, sweet almond oil, peach kernel oil, jojoba oil, sesame oil and coconut oil.
Preferably, the emulsifier is selected from one or two of span and tween.
More preferably, the emulsifier is selected from one or two of span-80 and tween-80.
A method for preparing an essential oil composition, comprising the steps of:
mixing the exocarpium Citri Grandis essential oil, herba Menthae essential oil, Cupressus Sempervirens essential oil, Cedar essential oil, and Olibanum essential oil, and stirring to obtain mixed essential oil;
and adding or not adding the grease solvent and the emulsifier into the mixed essential oil, stirring for 0.5-2 h, and then carrying out vacuum degassing treatment for 10-20 min.
It is understood that the essential oil composition may be prepared by directly mixing the essential oils with stirring; or adding a fat solvent and/or an emulsifier into the mixed essential oil, and then stirring; or mixing the oil solvent and the emulsifier, then mixing with the mixed essential oil, and stirring.
The invention also provides an essential oil bead, which structurally comprises a core material and a capsule wall wrapping the core material;
the core material comprises the essential oil composition or the essential oil composition prepared by the preparation method.
The essential oil composition is wrapped in the wall capsule to isolate the wall capsule from the external environment, so that the essential oil is more stable.
The blasting bead is round, the diameter is 3-4 mm, the mass is 17-23 mg, the content of the essential oil composition is 20-25 mul, and the crushing pressure is 1.0-1.5 kg. The cigarette bead is applied to a cigarette filter stick in a positioning manner to prepare the essential oil bead-exploded cigarette containing pummelo peel essential oil, so that throat discomfort symptoms such as dry throat, cough, excessive phlegm and the like caused by smoking can be effectively relieved.
Preferably, the capsule wall is mainly prepared from the following raw materials in percentage by mass:
1 to 12 percent of sodium alginate, 0.1 to 2 percent of Arabic gum, 0.05 to 0.5 percent of glycerol, 0.5 to 3 percent of carrageenan and 83 to 98 percent of water.
A preparation method of essential oil popping beads comprises the steps of mixing sodium alginate, Arabic gum, glycerol, carrageenan and water, heating to melt, stirring uniformly, standing for 1-2 h, and filtering to obtain a capsule wall solution;
and curing and molding the essential oil composition serving as a raw material of a core material and the capsule wall solution serving as a raw material of a capsule wall.
Preferably, the temperature for heating and melting is 65-75 ℃.
Preferably, the curing agent for curing and forming is selected from one or more of a calcium chloride aqueous solution with the mass fraction of 2% -10%, a calcium carbonate aqueous solution with the mass fraction of 2% -10% and a dicalcium phosphate aqueous solution with the mass fraction of 2% -10%.
The bead prepared by the method has the advantages of round appearance, less broken particles, moderate brittleness and strength, uniform capsule wall, good hand feeling when being pinched broken, wide application range, contribution to improving the fragrance of cigarettes of various large brands on the market, particularly the fragrance of cigarettes with low tar content, rich cigarette fragrance style, enhancement of the suction comfort, and effective relief of throat discomfort symptoms such as dry throat, cough, excessive phlegm and the like caused by smoking.
The puffed beads prepared by the method can be applied to cigarettes, and can also be applied to other fields such as food, medicines, daily chemical products and the like.
The following examples and comparative examples are further described below, and the starting materials used in the following examples can be commercially available, unless otherwise specified, and the equipment used therein can be commercially available, unless otherwise specified.
Example 1
The embodiment provides an essential oil composition and a preparation method thereof, and an essential oil popping bead and a preparation method thereof. The method comprises the following specific steps:
(1) preparation of essential oil composition
S1, weighing the following raw materials in percentage by mass:
0.5% of exocarpium Citri Grandis essential oil, 0.5% of peppermint essential oil, 20% of cypress essential oil, 0.01% of cedar essential oil, 0.01% of frankincense essential oil, 67.7% of caprylic/capric glyceride and 11.28% of palm oil.
S2, mixing the pummelo peel essential oil, the mint essential oil, the cypress essential oil, the cedar essential oil and the frankincense essential oil at normal temperature, and stirring uniformly to obtain mixed essential oil;
s3, mixing the caprylic capric glyceride and the palm oil at normal temperature, stirring uniformly, adding the mixed essential oil, stirring for 2h, and carrying out vacuum degassing treatment for 20min to obtain the essential oil composition.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
12% of sodium alginate, 2% of Arabic gum, 0.05% of glycerol, 0.5% of carrageenan and 85.45% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing 10% calcium dihydrogen phosphate water solution as curing agent.
S4, placing the prepared essential oil composition into a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the essential oil composition and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the essential oil composition in the capsule wall material, solidifying and forming by using a curing agent, collecting the exploded beads, drying, cleaning by using water, removing the damaged exploded beads, and performing secondary drying to obtain the essential oil exploded beads containing the pummelo peel essential oil.
The essential oil bead obtained in the embodiment is round, the diameter is 3 mm-4 mm, the mass is 17 mg-23 mg, the content of the essential oil composition is 20 mul-25 mul, and the crushing pressure is 1.0 kg-1.5 kg.
Example 2
This example provides an essential oil composition and a method for preparing the same, and an essential oil popping bead and a method for preparing the same, which are substantially the same as example 1 except that: the essential oil composition has different raw material formula proportions, and comprises the following specific steps:
(1) preparation of essential oil composition
S1, weighing the following raw materials in percentage by mass:
40% of pummelo peel essential oil, 50% of mint essential oil, 0.01% of cypress essential oil, 0.01% of cedar essential oil, 0.01% of frankincense essential oil, span-800.5%, 7% of caprylic capric glyceride and 2.47% of olive oil.
S2, mixing the pummelo peel essential oil, the mint essential oil, the cypress essential oil, the cedar essential oil and the frankincense essential oil at normal temperature, and stirring uniformly to obtain mixed essential oil;
s3, mixing the caprylic/capric glyceride and the olive oil at normal temperature, adding span-80, stirring uniformly, adding the mixed essential oil, stirring for 2h, and performing vacuum degassing treatment for 20min to obtain the essential oil composition.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
12% of sodium alginate, 2% of Arabic gum, 0.05% of glycerol, 0.5% of carrageenan and 85.45% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing 10% calcium dihydrogen phosphate water solution as curing agent.
S4, placing the prepared essential oil composition into a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the essential oil composition and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the essential oil composition in the capsule wall material, solidifying and forming by using a curing agent, collecting the exploded beads, drying, cleaning by using water, removing the damaged exploded beads, and performing secondary drying to obtain the essential oil exploded beads containing the pummelo peel essential oil.
Example 3
This example provides an essential oil composition and a method for preparing the same, and an essential oil popping bead and a method for preparing the same, which are substantially the same as example 1 except that: the essential oil composition has different raw material formula proportions, and comprises the following specific steps:
(1) preparation of essential oil composition
S1, weighing the following raw materials in percentage by mass:
10% of pummelo peel essential oil, 8% of mint essential oil, 1% of cypress essential oil, 20% of cedar essential oil, 20% of frankincense essential oil, span-800.3% and 40.7% of olive oil.
S2, mixing the pummelo peel essential oil, the mint essential oil, the cypress essential oil, the cedar essential oil and the frankincense essential oil at normal temperature, and stirring uniformly to obtain mixed essential oil;
s3, stirring the olive oil at normal temperature, adding span-80, stirring uniformly, adding the mixed essential oil, stirring for 2h, and performing vacuum degassing treatment for 20min to obtain the essential oil composition.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
12% of sodium alginate, 2% of Arabic gum, 0.05% of glycerol, 0.5% of carrageenan and 85.45% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing 10% calcium dihydrogen phosphate water solution as curing agent.
S4, placing the prepared essential oil composition into a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the essential oil composition and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the essential oil composition in the capsule wall material, solidifying and forming by using a curing agent, collecting the exploded beads, drying, cleaning by using water, removing the damaged exploded beads, and performing secondary drying to obtain the essential oil exploded beads containing the pummelo peel essential oil.
Example 4
This example provides an essential oil composition and a method for preparing the same, and an essential oil popping bead and a method for preparing the same, which are substantially the same as example 1 except that: the essential oil composition has different raw material formula proportions, and comprises the following specific steps:
(1) preparation of essential oil composition
S1, weighing the following raw materials in percentage by mass:
pummelo peel essential oil 10%, mint essential oil 8%, cypress essential oil 1%, cedar essential oil 10%, frankincense essential oil 10%, span-800.3%, caprylic capric glyceride 54% and wheat germ oil 6.7%.
S2, mixing the pummelo peel essential oil, the mint essential oil, the cypress essential oil, the cedar essential oil and the frankincense essential oil at normal temperature, and stirring uniformly to obtain mixed essential oil;
s3, mixing the caprylic/capric glyceride and the wheat germ oil at normal temperature, adding span-80, stirring uniformly, adding the mixed essential oil, stirring for 2h, and performing vacuum degassing treatment for 20min to obtain the essential oil composition.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
12% of sodium alginate, 2% of Arabic gum, 0.05% of glycerol, 0.5% of carrageenan and 85.45% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing 10% calcium dihydrogen phosphate water solution as curing agent.
S4, placing the prepared essential oil composition into a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the essential oil composition and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the essential oil composition in the capsule wall material, solidifying and forming by using a curing agent, collecting the exploded beads, drying, cleaning by using water, removing the damaged exploded beads, and performing secondary drying to obtain the essential oil exploded beads containing the pummelo peel essential oil.
Example 5
This example provides an essential oil composition and a method for preparing the same, and an essential oil popping bead and a method for preparing the same, which are substantially the same as example 1 except that: the essential oil composition has different raw material formula proportions, and comprises the following specific steps:
(1) preparation of essential oil composition
S1, weighing the following raw materials in percentage by mass:
8% of pummelo peel essential oil, 18% of mint essential oil, 2% of cypress essential oil, 2% of cedar essential oil, 2% of frankincense essential oil, span-800.2% and 67.8% of caprylic capric glyceride.
S2, mixing the pummelo peel essential oil, the mint essential oil, the cypress essential oil, the cedar essential oil and the frankincense essential oil at normal temperature, and stirring uniformly to obtain mixed essential oil;
s3, stirring the caprylic capric glyceride at normal temperature, adding span-80, stirring uniformly, adding the mixed essential oil, stirring for 2h, and performing vacuum degassing treatment for 20min to obtain the essential oil composition.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
12% of sodium alginate, 2% of Arabic gum, 0.05% of glycerol, 0.5% of carrageenan and 85.45% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing 10% calcium dihydrogen phosphate water solution as curing agent.
S4, placing the prepared essential oil composition into a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the essential oil composition and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the essential oil composition in the capsule wall material, solidifying and forming by using a curing agent, collecting the exploded beads, drying, cleaning by using water, removing the damaged exploded beads, and performing secondary drying to obtain the essential oil exploded beads containing the pummelo peel essential oil.
Example 6
This example provides an essential oil composition and a method for preparing the same, and an essential oil popping bead and a method for preparing the same, which are substantially the same as example 5 except that: the essential oil composition has different grease solvents, and meanwhile, in the preparation process, the stirring and vacuum defoaming time is different, and the preparation method comprises the following specific steps:
(1) preparation of essential oil composition
S1, weighing the following raw materials in percentage by mass:
8% of pummelo peel essential oil, 18% of mint essential oil, 2% of cypress essential oil, 2% of cedar essential oil, 2% of frankincense essential oil, span-800.2%, 56.5% of caprylic-capric glyceride and 11.3% of sweet almond oil.
S2, mixing the pummelo peel essential oil, the mint essential oil, the cypress essential oil, the cedar essential oil and the frankincense essential oil at normal temperature, and stirring uniformly to obtain mixed essential oil;
s3, mixing caprylic capric glyceride and sweet almond oil at normal temperature, adding span-80, stirring well, adding the above mixed essential oil, stirring for 0.5h, and vacuum degassing for 10min to obtain the essential oil composition.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
12% of sodium alginate, 2% of Arabic gum, 0.05% of glycerol, 0.5% of carrageenan and 85.45% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing 10% calcium dihydrogen phosphate water solution as curing agent.
S4, placing the prepared essential oil composition into a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the essential oil composition and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the essential oil composition in the capsule wall material, solidifying and forming by using a curing agent, collecting the exploded beads, drying, cleaning by using water, removing the damaged exploded beads, and performing secondary drying to obtain the essential oil exploded beads containing the pummelo peel essential oil.
Example 7
This example provides an essential oil composition and a method for preparing the same, and an essential oil popping bead and a method for preparing the same, which are substantially the same as example 5 except that: the essential oil composition has different grease solvents, different raw material proportions of the capsule wall and different concentrations of the curing agent, and comprises the following specific steps:
(1) preparation of essential oil composition
S1, weighing the following raw materials in percentage by mass:
8% of exocarpium Citri Grandis essential oil, 18% of mint essential oil, 2% of cypress essential oil, 2% of cedar essential oil, 2% of frankincense essential oil, tween-800.2%, 56.5% of caprylic capric glyceride and 11.3% of coconut oil.
S2, mixing the pummelo peel essential oil, the mint essential oil, the cypress essential oil, the cedar essential oil and the frankincense essential oil at normal temperature, and stirring uniformly to obtain mixed essential oil;
s3, mixing caprylic capric glyceride and coconut oil at normal temperature, adding tween-80, stirring, adding the above mixed essential oil, stirring for 2h, and vacuum degassing for 20min to obtain the essential oil composition.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
1% of sodium alginate, 0.1% of Arabic gum, 0.5% of glycerol, 3% of carrageenan and 95.4% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing a calcium dihydrogen phosphate aqueous solution with the mass fraction of 2% as a curing agent.
S4, placing the prepared essential oil composition into a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the essential oil composition and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the essential oil composition in the capsule wall material, solidifying and forming by using a curing agent, collecting the exploded beads, drying, cleaning by using water, removing the damaged exploded beads, and performing secondary drying to obtain the essential oil exploded beads containing the pummelo peel essential oil.
The proportions of the essential oil compositions of examples 1-7 are summarized in Table 1:
TABLE 1
Comparative example 1
The comparative example provides a pummelo peel essential oil bead and a preparation method thereof, which are basically the same as those in example 5, and the differences are mainly as follows: only pummelo peel essential oil is added into the bead blasting core material, and the method comprises the following specific steps:
(1) preparation of blasting bead core material
And S1, stirring the pummelo peel essential oil at normal temperature, stirring for 2 hours, and carrying out vacuum degassing treatment for 20min to obtain the pummelo peel essential oil.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
12% of sodium alginate, 2% of Arabic gum, 0.05% of glycerol, 0.5% of carrageenan and 85.45% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing 10% calcium dihydrogen phosphate water solution as curing agent.
S4, placing the prepared bead blasting core material in a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the core material solution and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the pummelo peel essential oil in the capsule wall material, curing and forming by using a curing agent, collecting the popped beads, drying, cleaning by using water, removing the broken popped beads, and performing secondary drying to obtain the pummelo peel cigarette popped beads.
Comparative example 2
The comparative example provides an essential oil composition and a preparation method thereof, an essential oil popping bead and a preparation method thereof, which are basically the same as the example 5, and are mainly distinguished by: in the formula of the essential oil composition, the mint essential oil is not added, and the specific steps are as follows:
(1) preparation of essential oil composition
S1, weighing the following raw materials in percentage by mass:
8% of exocarpium citri grandis essential oil, 2% of cypress essential oil, 2% of cedar essential oil, 2% of frankincense essential oil, span-800.2% and 85.8% of caprylic capric glyceride.
S2, mixing the pummelo peel essential oil, the cypress essential oil, the cedar essential oil and the frankincense essential oil at normal temperature, and stirring uniformly to obtain mixed essential oil;
s3, stirring the caprylic capric glyceride at normal temperature, adding span-80, stirring uniformly, adding the mixed essential oil, stirring for 2h, and performing vacuum degassing treatment for 20min to obtain the essential oil composition.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
12% of sodium alginate, 2% of Arabic gum, 0.05% of glycerol, 0.5% of carrageenan and 85.45% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing 10% calcium dihydrogen phosphate water solution as curing agent.
S4, placing the prepared essential oil composition into a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the essential oil composition and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the essential oil composition in the capsule wall material, solidifying and forming by using a curing agent, collecting the exploded beads, drying, cleaning by using water, removing the damaged exploded beads, and performing secondary drying to obtain the essential oil exploded beads containing the pummelo peel essential oil.
Comparative example 3
The comparative example provides an essential oil composition and a preparation method thereof, an essential oil popping bead and a preparation method thereof, which are basically the same as the example 5, and are mainly distinguished by: in the formula of the essential oil composition, the cypress essential oil is replaced by tea tree essential oil, and the specific steps are as follows:
(1) preparation of essential oil composition
S1, weighing the following raw materials in percentage by mass:
8% of pummelo peel essential oil, 18% of mint essential oil, 2% of tea tree essential oil, 2% of cedar essential oil, 2% of frankincense essential oil, span-800.2% and 67.8% of caprylic capric glyceride.
S2, mixing the pummelo peel essential oil, the mint essential oil, the tea tree essential oil, the cedar essential oil and the frankincense essential oil at normal temperature, and uniformly stirring to obtain mixed essential oil;
s3, stirring the caprylic capric glyceride at normal temperature, adding span-80, stirring uniformly, adding the mixed essential oil, stirring for 2h, and performing vacuum degassing treatment for 20min to obtain the essential oil composition.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
12% of sodium alginate, 2% of Arabic gum, 0.05% of glycerol, 0.5% of carrageenan and 85.45% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing 10% calcium dihydrogen phosphate water solution as curing agent.
S4, placing the prepared essential oil composition into a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the essential oil composition and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the essential oil composition in the capsule wall material, solidifying and forming by using a curing agent, collecting the exploded beads, drying, cleaning by using water, removing the damaged exploded beads, and performing secondary drying to obtain the essential oil exploded beads containing the pummelo peel essential oil.
Comparative example 4
The comparative example provides an essential oil composition and a preparation method thereof, an essential oil popping bead and a preparation method thereof, which are basically the same as the example 5, and are mainly distinguished by: in the formula of the essential oil composition, no frankincense essential oil is added, and the specific steps are as follows:
(1) preparation of essential oil composition
S1, weighing the following raw materials in percentage by mass:
8% of exocarpium Citri Grandis essential oil, 18% of mint essential oil, 2% of cypress essential oil, 2% of cedar essential oil, span-800.2% and 69.8% of caprylic capric glyceride.
S2, mixing the pummelo peel essential oil, the mint essential oil, the cypress essential oil and the cedar essential oil at normal temperature, and stirring uniformly to obtain mixed essential oil;
s3, stirring the caprylic capric glyceride at normal temperature, adding span-80, stirring uniformly, adding the mixed essential oil, stirring for 2h, and performing vacuum degassing treatment for 20min to obtain the essential oil composition.
(2) Preparation of essential oil popping beads
S1, weighing the raw materials according to the following weight percentage
12% of sodium alginate, 2% of Arabic gum, 0.05% of glycerol, 0.5% of carrageenan and 85.45% of water.
S2, placing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water in a container, heating to melt at 70 ℃, uniformly stirring, standing for 2 hours, and filtering to obtain a capsule wall solution.
S3, preparing 10% calcium dihydrogen phosphate water solution as curing agent.
S4, placing the prepared essential oil composition into a core material groove of a pill dropping machine; adding the capsule wall solution into wall material groove of dripping pill machine, and keeping hot melt state at 70 deg.C; adding curing agent into the collector of the pill dropping machine; and (3) starting a pill dropping machine, respectively dropping the essential oil composition and the capsule wall solution from the core material outlet and the wall material outlet, wrapping the essential oil composition in the capsule wall material, solidifying and forming by using a curing agent, collecting the exploded beads, drying, cleaning by using water, removing the damaged exploded beads, and performing secondary drying to obtain the essential oil exploded beads containing the pummelo peel essential oil.
Example 8
The pummelo peel essential oil poppearls of the examples 1-7 and the comparative examples 1-4 are further prepared into poppearled cigarettes, and sensory evaluation of the cigarettes is carried out.
The preparation method of the bead-blasting cigarette comprises the following steps: in the process of forming a cigarette filter tow, adding the pummelo peel essential oil bead blasting of the embodiments 1 to 7 and the comparative examples 1 to 4 into the tow (cellulose diacetate) to form a bead blasting filter rod, and placing the bead blasting filter rod at the center of the cigarette filter; and then rolling the filter stick and tobacco shreds (double happiness well-developed world) into cigarettes to prepare the essential oil bead-exploded cigarette containing the pummelo peel essential oil.
Cigarettes without the essential oil exploded beads were made as controls under the same conditions.
Before the start of evaluation, an examination was conducted in the form of a questionnaire, and 77 smokers having throat discomfort symptoms were selected to participate in the evaluation. The evaluators are divided into 11 groups respectively, cigarettes of examples 1-6, comparative examples 1-4 and a control group are smoked respectively, after the evaluation is started, the evaluators stop smoking cigarettes of other brands, return visit is carried out after one month, and evaluation opinions are collected.
The highest sensory evaluation score of the cigarettes is 100, and the highest evaluation score of the effect of relieving the throat discomfort is 20. Each item is divided into score units of 0.5. The scoring criteria are referenced in table 2. The score results were counted as the average score of each group, and the statistical results are shown in table 3. Cigarette sensory scoring refers to the fourth part of GB 5606.4-2005 cigarette: sensory technical requirements.
TABLE 2 evaluation item and level reference
TABLE 3 evaluation results of pummelo peel puffed bead cigarettes
The evaluation results show that: after the pummelo peel essential oil bead-blown cigarette is smoked, the throat discomfort symptom score is obviously higher than that of a control group which smokes common cigarettes, and the pummelo peel bead-blown cigarette is beneficial to relieving throat discomfort symptoms caused by smoking.
After the essential oil of examples 1-7 is added, the cigarette fragrance and aftertaste scores are obviously improved, and the difference between harmony, miscellaneous gas, irritation and gloss is not large compared with that of a control group, which shows that after the pummelo peel essential oil is added, the fragrance and aftertaste of the cigarette are obviously increased, and the original harmony, miscellaneous gas, irritation and gloss of the cigarette are not adversely affected.
After the essential oil blasting beads of comparative examples 1-4 are added, the fragrance and aftertaste of cigarettes are improved compared with those of a control group, but the harmony score is lower than that of examples 1-7, which shows that the essential oil blasting beads of comparative examples 1-4 cannot well solve the problem that the fragrance of the pummelo peel essential oil is fused and coordinated with the fragrance of the cigarettes.
The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the present invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (10)
1. The essential oil composition is characterized by being mainly prepared from the following raw materials in percentage by mass:
0.5 to 40 percent of exocarpium citri grandis essential oil, 0.5 to 50 percent of mint essential oil, 0.01 to 20 percent of cypress essential oil, 0.01 to 20 percent of cedar essential oil, 0.01 to 20 percent of frankincense essential oil, 0 to 0.5 percent of emulsifier and 0 to 98 percent of grease solvent.
2. The essential oil composition according to claim 1, which is prepared from the following raw materials in percentage by mass:
2 to 20 percent of pummelo peel essential oil, 2 to 40 percent of mint essential oil, 0.1 to 10 percent of cypress essential oil, 0.1 to 10 percent of cedar essential oil, 0.1 to 10 percent of frankincense essential oil, 0.01 to 0.3 percent of emulsifier and 10 to 95 percent of grease solvent.
3. The essential oil composition as claimed in claim 2, which is prepared from the following raw materials in percentage by mass:
3 to 15 percent of exocarpium citri grandis essential oil, 3 to 20 percent of mint essential oil, 1 to 5 percent of cypress essential oil, 1 to 5 percent of cedar essential oil, 1 to 5 percent of frankincense essential oil, 0.05 to 0.3 percent of emulsifier and 50 to 90 percent of grease solvent.
4. An essential oil composition according to any one of claims 1 to 3, wherein the oil-and-fat solvent is selected from one or more of caprylic-capric glyceride, palm oil, olive oil, corn oil, sunflower oil, peanut oil, wheat germ oil, sweet almond oil, peach kernel oil, jojoba oil, sesame oil and coconut oil.
5. An essential oil composition according to any one of claims 1 to 3, wherein the emulsifier is selected from one or both of span and Tween.
6. A method of preparing an essential oil composition according to any one of claims 1 to 5, comprising the steps of:
mixing the exocarpium Citri Grandis essential oil, herba Menthae essential oil, Cupressus Sempervirens essential oil, Cedar essential oil and Olibanum essential oil, and stirring well to obtain mixed essential oil;
and adding or not adding the grease solvent and the emulsifier into the mixed essential oil, stirring for 0.5-2 h, and then carrying out vacuum degassing treatment for 10-20 min.
7. The essential oil bead is characterized in that the essential oil bead structurally comprises a core material and a capsule wall wrapping the core material;
the core material comprises the essential oil composition according to any one of claims 1 to 5, or the essential oil composition produced by the production method according to claim 6.
8. An essential oil bead filler according to claim 7, wherein the capsule wall is prepared from the following raw materials in percentage by mass: 1 to 12 percent of sodium alginate, 0.1 to 2 percent of Arabic gum, 0.05 to 0.5 percent of glycerol, 0.5 to 3 percent of carrageenan and 83 to 98 percent of water.
9. The method for preparing the essential oil poplock bead as claimed in claim 8, which is characterized by comprising the following steps:
mixing the sodium alginate, the Arabic gum, the glycerol, the carrageenan and the water, heating to melt, uniformly stirring, standing for 1-2 h, and filtering to obtain a capsule wall solution;
and curing and molding the essential oil composition serving as a raw material of a core material and the capsule wall solution serving as a raw material of a capsule wall.
10. The method for preparing essential oil beadlets according to claim 9, wherein the curing agent for curing and forming is selected from one or more of a calcium chloride aqueous solution with a mass fraction of 2-10%, a calcium carbonate aqueous solution with a mass fraction of 2-10% and a dicalcium phosphate aqueous solution with a mass fraction of 2-10%.
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