CN110526580A - A kind of bronze glaze and preparation method thereof - Google Patents
A kind of bronze glaze and preparation method thereof Download PDFInfo
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- CN110526580A CN110526580A CN201910935678.1A CN201910935678A CN110526580A CN 110526580 A CN110526580 A CN 110526580A CN 201910935678 A CN201910935678 A CN 201910935678A CN 110526580 A CN110526580 A CN 110526580A
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- glaze
- bronze
- green body
- glazing
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- 229910000906 Bronze Inorganic materials 0.000 title claims abstract description 29
- 239000010974 bronze Substances 0.000 title claims abstract description 29
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 25
- 238000000034 method Methods 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 claims abstract description 12
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 9
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 9
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910021532 Calcite Inorganic materials 0.000 claims abstract description 8
- 229940116318 copper carbonate Drugs 0.000 claims abstract description 8
- GEZOTWYUIKXWOA-UHFFFAOYSA-L copper;carbonate Chemical compound [Cu+2].[O-]C([O-])=O GEZOTWYUIKXWOA-UHFFFAOYSA-L 0.000 claims abstract description 8
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 230000001590 oxidative effect Effects 0.000 claims abstract description 5
- 238000001816 cooling Methods 0.000 claims abstract description 4
- 238000000227 grinding Methods 0.000 claims abstract description 3
- 238000002156 mixing Methods 0.000 claims description 4
- 238000004321 preservation Methods 0.000 claims description 2
- 239000003086 colorant Substances 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- 238000009472 formulation Methods 0.000 abstract 1
- 239000000919 ceramic Substances 0.000 description 10
- 239000000126 substance Substances 0.000 description 8
- 238000010304 firing Methods 0.000 description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- 229910052593 corundum Inorganic materials 0.000 description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000010433 feldspar Substances 0.000 description 3
- 229910001845 yogo sapphire Inorganic materials 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- AYJRCSIUFZENHW-DEQYMQKBSA-L barium(2+);oxomethanediolate Chemical compound [Ba+2].[O-][14C]([O-])=O AYJRCSIUFZENHW-DEQYMQKBSA-L 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- OVFCVRIJCCDFNQ-UHFFFAOYSA-N carbonic acid;copper Chemical compound [Cu].OC(O)=O OVFCVRIJCCDFNQ-UHFFFAOYSA-N 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000002734 clay mineral Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229910000009 copper(II) carbonate Inorganic materials 0.000 description 1
- 239000010431 corundum Substances 0.000 description 1
- 239000011646 cupric carbonate Substances 0.000 description 1
- 235000019854 cupric carbonate Nutrition 0.000 description 1
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000013081 microcrystal Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229910052863 mullite Inorganic materials 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 229910052652 orthoclase Inorganic materials 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a kind of bronze glaze, include following component: potassium feldspar 45-49%, calcite 10-13%, barium carbonate 15-19%, kaolin 15-17%, aluminium oxide 2-3%, copper carbonate 3-4% as mass fraction;The present invention discloses a kind of preparation methods of bronze glaze, include the following steps: step 1, weigh various raw materials in proportion, and after grinding plus water mixes, and cross sieve and obtain the glaze slip of uniform and smooth;Step 2, different glazing method and thickness are selected according to green body size, thickness;Step 3, glazing green body is packed into kiln, is fired under oxidizing atmosphere by following heating curve, keep the temperature natural cooling of ceasing fire after twenty minutes.The beneficial effects of the present invention are the formula and preparation method for the bronze glaze that the present invention is announced can steadily reach glaze colours effect bronzy.Its chromaticness is simple and unsophisticated, thick and heavy, elegant, has dignified sense of history, extremely strong artistic expression and higher artistic value.
Description
Technical field
The present invention relates to ceramic glaze colours technical fields more particularly to a kind of bronze glaze and preparation method thereof.
Background technique
Bronze ware is the principal mode of quotient, all period culture, is the important carrier of Chinese civilization, is successive dynasties ceramic art
The model for practising and imitating.Successive dynasties ceramic art only learns the moulding of bronze ware mostly, but the ware of bronze glaze seldom occurs.
Using copper as colorant in traditional ceramics glaze, various red effects are burnt out in a reducing atmosphere mostly, it is common
Have: the rose-red of an ancient unit of weight kiln, red, under-glaze red of holding a memorial ceremony for for wood-fired kiln etc..And the present invention is used under modern electrical kiln oxidizing atmosphere
Copper carbonate is colorant, burns out dumb light, simple and unsophisticated bronze ware.Ancient times generally use the firings such as bavin, coal, carbon, with
Development in science and technology and modern society focus on environmental protection, electrical kiln extensive utilization at present.In the widely applied overall background of modern electrical kiln, it is desirable that
Ceramic technology is constantly brought forth new ideas on the basis of tradition, is suitble to scientific experiment technique study ceramic glaze and formula various new
Type, the modernization firing mechanism of energy-saving and environmental protection.
Summary of the invention
1. the technical issues that need to address
The present invention needs the technical issues of final result to be, provides a kind of based on the unmanned working path rule in agricultural machinery crop field
The algorithm drawn is debugged with the method for scientific experiment, is expanded utilization of the copper in ceramic glaze, is enriched ceramic glaze chromaticity kind.
2. technical solution
A kind of bronze glaze, includes following component, by mass percentage: potassium feldspar 45-49%, calcite 10-13%, carbon
Sour barium 15-19%, kaolin 15-17%, aluminium oxide 2-3%, copper carbonate 3-4%.
It preferably, include following component, by mass percentage: potassium feldspar 48.4%, calcite 11.6%, barium carbonate
17.2%, kaolin 15.4%, aluminium oxide 3.0%, copper carbonate 4.4%.
The present invention discloses a kind of preparation methods of bronze glaze, include the following steps:
Step 1, various raw materials are weighed in proportion, and after grinding plus water mixes, and crosses 200 mesh standard sieve nets after evenly mixing and obtains
The glaze slip of uniform and smooth;
Step 2, different glazing method and thickness are selected according to green body size, thickness, wherein selection glazing by sufflation method,
Selection leaching glaze method.
Step 3, glazing green body is packed into kiln, is fired under oxidizing atmosphere by following heating curve, ceased fire after keeping the temperature 20min
Natural cooling.
Preferably, the step 2 includes the following steps:
Step 2.1, different glazing methods is selected according to green body size, thickness, adjusts the ratio of bronze glaze and water;
Step 2.2, green body is small and thick selection glaze method, and the mass ratio of glaze and water is 1:1;
Step 2.3, the big and thin selection glazing by sufflation method of green body, and the mass ratio of glaze and water is 1:0.6.
Preferably, from room temperature to 560 DEG C the time 210 minutes, DEG C time 120 minutes from 560 DEG C to 900, then 900 DEG C of left sides
Right heat preservation 10 minutes, DEG C time 240 minutes from 900 DEG C to 1260.
Preferably, the holding temperature of the step 4 is 1260 DEG C.
Preferably, the screen over-size of crossing in the step 1 is no more than 0.5%.
3. beneficial effect
In conclusion the beneficial effects of the present invention are: the electricity modernized is debugged and utilized with the method for scientific experiment
The bronze glaze of kiln plant invention, is a kind of glaze colours with unique artistic effect, can greatly improve the artistic value of works and glad
Reward value.Modernization electrical kiln equipment is largely used in various regions, and the present invention can widely, reproducibility promote the use of.
Specific embodiment
The present invention will be further described combined with specific embodiments below, but the present invention should not be limited by the examples.
Embodiment:
100 jin of bronze glaze, it is made of following raw materials according: 48.4 jin of potassium feldspar, 11.6 jin of calcite, and barium carbonate 17.2
Jin, 15.4 jin of kaolin, 3.0 jin of aluminium oxide, 4.4 jin of copper carbonate.
Above-mentioned bronze glaze and preparation method thereof the following steps are included:
Then plus water step 1, various raw materials are weighed in 100 jin of bronze glaze formula ratio quality, is first screened and is ground,
Mixing crosses 200 mesh standard sieve nets after mixing and obtains fine and smooth glaze slip, and the surplus of sieving is no more than 0.5%.
Step 2, different glazing method and thickness are selected according to green body size, thickness.Big and thin green body selects glazing by sufflation
Glaze method is soaked in method, the small and thick selection of green body.According to the difference of glazing method, the ratio of bronze glaze and water is adjusted.Glaze method:
The mass ratio of glaze and water is 1:1, and glazing by sufflation method: the mass ratio of glaze and water is 1:0.6.
Preferably, glaze layer thickness control is between 0.8-1.5mm.
Step 3, the glazing green body dried is packed into kiln, is fired under oxidizing atmosphere by following heating curve.From room temperature to
560 DEG C the time 210 minutes, 560 DEG C -900 DEG C the time 120 minutes, 900 DEG C or so keep the temperature 10 minutes, 900 DEG C -1260 DEG C when
Between 240 minutes, 1260 DEG C keep the temperature 20 minutes, natural cooling of ceasing fire later.180 DEG C or less, which are dropped to, in kiln temperature opens wicket again,
Obtain the bronze glaze.
The effect of bronze glaze each component:
Potassium feldspar, chemical formula K2O·Al2O3·6SiO2, usually also referred to as orthoclase, color are white, red, milky, density
For 2.54-2.57g/cm3, hardness 6.Ceramic glaze is mainly made by feldspar, quartz and raw clay, and wherein feldspar content is reachable
10-35%.Potassium feldspar is mainly used in ceramic batch and glaze.Feldspar can play the work of non-plastic raw material to potassium feldspar before firing
With, it reduces the dry of green body and shrinks and deform, improvement drying property, shortening drying time.It can be used as flux reduction in firing
Firing temperature promotes quartz and kaolin melting, and diffuses into one another the formation for permeating and accelerating mullite in the liquid phase.In this hair
Bright middle utilization is Pingjiang River potassium feldspar.
Calcite, chemical formula CaCO3, it is a kind of calcium carbonate mineral, chemical composition CaO accounts for 56.03%, CO243.97% is accounted for,
Often contain Mn and Fe, contains Sr sometimes.The color of calcite changes because the impurity wherein contained is different, but general is mostly white or nothing
Color.Its main function is to reduce glaze melting temperature, increases the glossiness of glaze colours and glaze is prevented to be cracked and accumulate.
Barium carbonate, chemical formula BaCO3, inorganic compound, molecular weight 197.35, hexagon micro crystal, white powder.Have
Very strong toxicity is stored in the storehouse of shady and cool ventilation, package encapsulation.It should separately store with acids, edible chemical, never mix
Storage.
Kaolin, chemical formula Al203·2Si02·2H20, it is a kind of nonmetallic clay mineral, in pure white fine and smooth, mollisol
Shape has the physicochemical properties such as good plasticity and fire resistance.Because white and fine and smooth, also known as white clouds are native.Kaolin has
Certain plasticity, adhesiveness.The good caking property of glaze, suspension and binding ability are assigned in glaze.
Aluminium oxide, chemical formula Al2O3, alias corundum, alumina.It is a kind of compound of high rigidity, the white for being insoluble in water is solid
Body, it is odorless, tasteless, matter is extremely hard, 2050 DEG C of fusing point.Hermetically drying is needed to save.
Copper carbonate, chemical formula CuCO3 are the carbonate of copper, are cyan powders shape solid, are the colour formers of bronze glaze.
Although the present invention has been disclosed in the preferred embodiment as above, it is not intended to limit the invention, any to be familiar with this
The people of technology can do various changes and modification, therefore protection of the invention without departing from the spirit and scope of the present invention
Range should subject to the definition of the claims.
Claims (7)
1. a kind of bronze glaze, which is characterized in that include following component, by mass percentage: potassium feldspar 45-49%, calcite
10-13%, barium carbonate 15-19%, kaolin 15-17%, aluminium oxide 2-3%, copper carbonate 3-4%.
2. a kind of bronze glaze according to claim 1, which is characterized in that include following component, by mass percentage: potassium
Feldspar 48.4%, calcite 11.6%, barium carbonate 17.2%, kaolin 15.4%, aluminium oxide 3.0%, copper carbonate 4.4%.
3. a kind of utilize bronze glaze preparation method described in claim 1-2 any one, which is characterized in that including walking as follows
It is rapid:
Step 1, various raw materials are weighed in proportion, and after grinding plus water mixes, and crosses 200 mesh standard sieve nets after evenly mixing and obtains uniformly
Fine and smooth glaze slip;
Step 2, different glazing method and thickness are selected according to green body size, thickness, wherein selection glazing by sufflation method, selection
Soak glaze method.
Step 3, glazing green body is packed into kiln, is fired under oxidizing atmosphere by following heating curve, nature of ceasing fire after heat preservation 20min
It is cooling.
4. a kind of bronze glaze preparation method according to claim 3, which is characterized in that the step 2 includes the following steps:
Step 2.1, different glazing methods is selected according to green body size, thickness, adjusts the ratio of bronze glaze and water;
Step 2.2, green body is small and thick selection glaze method, and the mass ratio of glaze and water is 1:1;
Step 2.3, the big and thin selection glazing by sufflation method of green body, and the mass ratio of glaze and water is 1:0.6.
5. according to a kind of bronze glaze preparation method as claimed in claim 3, which is characterized in that the heating curve in the step 4 are as follows:
From room temperature to 560 DEG C the time 210 minutes, DEG C time 120 minutes from 560 DEG C to 900, then 900 DEG C or so keep the temperature 10 minutes, from
900 DEG C to 1260 DEG C the time 240 minutes.
6. according to a kind of bronze glaze preparation method described in claim 5, which is characterized in that the heating curve in the step 4 are as follows:
The holding temperature of the step 4 is 1260 DEG C.
7. according to a kind of bronze glaze preparation method as claimed in claim 3, which is characterized in that cross screen over-size not in the step 1
More than 0.5%.
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CN201910935678.1A CN110526580B (en) | 2019-09-29 | 2019-09-29 | Bronze glaze and preparation method thereof |
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CN110526580A true CN110526580A (en) | 2019-12-03 |
CN110526580B CN110526580B (en) | 2022-04-19 |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19749858C1 (en) * | 1997-11-11 | 1999-04-22 | Siemens Matsushita Components | Reduction stable low dielectric constant ceramic material for co-firing with copper electrodes |
CN103304274A (en) * | 2013-06-08 | 2013-09-18 | 浙江工业大学之江学院工业研究院 | Bronze green crystalline glaze and firing method thereof |
CN106430977A (en) * | 2016-08-31 | 2017-02-22 | 厦门万仟堂艺术品有限公司 | Light greenish blue matte glaze for pottery product and preparation method of light greenish blue matte glaze |
CN109231825A (en) * | 2018-09-13 | 2019-01-18 | 湖南高峰陶瓷制造有限公司 | Bronze unglazed furnace transmutation glaze and preparation method thereof |
CN109942188A (en) * | 2019-04-16 | 2019-06-28 | 福建省德化问瓷阁陶瓷有限公司 | A kind of green temmoku glaze ceramics of matt and its manufacture craft |
-
2019
- 2019-09-29 CN CN201910935678.1A patent/CN110526580B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19749858C1 (en) * | 1997-11-11 | 1999-04-22 | Siemens Matsushita Components | Reduction stable low dielectric constant ceramic material for co-firing with copper electrodes |
CN103304274A (en) * | 2013-06-08 | 2013-09-18 | 浙江工业大学之江学院工业研究院 | Bronze green crystalline glaze and firing method thereof |
CN106430977A (en) * | 2016-08-31 | 2017-02-22 | 厦门万仟堂艺术品有限公司 | Light greenish blue matte glaze for pottery product and preparation method of light greenish blue matte glaze |
CN109231825A (en) * | 2018-09-13 | 2019-01-18 | 湖南高峰陶瓷制造有限公司 | Bronze unglazed furnace transmutation glaze and preparation method thereof |
CN109942188A (en) * | 2019-04-16 | 2019-06-28 | 福建省德化问瓷阁陶瓷有限公司 | A kind of green temmoku glaze ceramics of matt and its manufacture craft |
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