CN103044157A - Amino acid guniting compound fertilizer and preparation method thereof - Google Patents
Amino acid guniting compound fertilizer and preparation method thereof Download PDFInfo
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- CN103044157A CN103044157A CN201310026585XA CN201310026585A CN103044157A CN 103044157 A CN103044157 A CN 103044157A CN 201310026585X A CN201310026585X A CN 201310026585XA CN 201310026585 A CN201310026585 A CN 201310026585A CN 103044157 A CN103044157 A CN 103044157A
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 58
- 238000002360 preparation method Methods 0.000 title claims abstract description 27
- 150000001875 compounds Chemical class 0.000 title abstract description 9
- 150000001413 amino acids Chemical class 0.000 title abstract 5
- 239000002253 acid Substances 0.000 claims abstract description 30
- 239000002002 slurry Substances 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000005469 granulation Methods 0.000 claims abstract description 11
- 230000003179 granulation Effects 0.000 claims abstract description 11
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 42
- 239000002068 microbial inoculum Substances 0.000 claims description 25
- 229910021529 ammonia Inorganic materials 0.000 claims description 21
- 239000002131 composite material Substances 0.000 claims description 21
- CHKVPAROMQMJNQ-UHFFFAOYSA-M potassium bisulfate Chemical compound [K+].OS([O-])(=O)=O CHKVPAROMQMJNQ-UHFFFAOYSA-M 0.000 claims description 20
- 241000589152 Azotobacter chroococcum Species 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 17
- 241000194107 Bacillus megaterium Species 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 15
- 239000004021 humic acid Substances 0.000 claims description 14
- 239000000843 powder Substances 0.000 claims description 13
- 239000000126 substance Substances 0.000 claims description 13
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 12
- 239000011575 calcium Substances 0.000 claims description 12
- 229910052791 calcium Inorganic materials 0.000 claims description 12
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 11
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 10
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims description 10
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 claims description 10
- 239000004202 carbamide Substances 0.000 claims description 10
- 239000006012 monoammonium phosphate Substances 0.000 claims description 10
- 235000019837 monoammonium phosphate Nutrition 0.000 claims description 10
- 239000007921 spray Substances 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 9
- DWNBOPVKNPVNQG-LURJTMIESA-N (2s)-4-hydroxy-2-(propylamino)butanoic acid Chemical compound CCCN[C@H](C(O)=O)CCO DWNBOPVKNPVNQG-LURJTMIESA-N 0.000 claims description 8
- 239000002994 raw material Substances 0.000 claims description 8
- 238000010790 dilution Methods 0.000 claims description 5
- 239000012895 dilution Substances 0.000 claims description 5
- 239000012467 final product Substances 0.000 claims description 5
- 238000006386 neutralization reaction Methods 0.000 claims description 5
- 244000063299 Bacillus subtilis Species 0.000 claims description 4
- 235000014469 Bacillus subtilis Nutrition 0.000 claims description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 6
- 238000006243 chemical reaction Methods 0.000 abstract description 5
- 238000002156 mixing Methods 0.000 abstract description 4
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 4
- 238000005265 energy consumption Methods 0.000 abstract description 2
- 239000002689 soil Substances 0.000 description 13
- 235000015097 nutrients Nutrition 0.000 description 8
- 239000002609 medium Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- 244000017020 Ipomoea batatas Species 0.000 description 6
- 235000002678 Ipomoea batatas Nutrition 0.000 description 6
- 238000000855 fermentation Methods 0.000 description 6
- 230000004151 fermentation Effects 0.000 description 6
- 238000009630 liquid culture Methods 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 5
- 238000012360 testing method Methods 0.000 description 4
- 238000012549 training Methods 0.000 description 4
- 229920001817 Agar Polymers 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 3
- 240000008067 Cucumis sativus Species 0.000 description 3
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 description 3
- 239000008272 agar Substances 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000001963 growth medium Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 230000000813 microbial effect Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 241000238631 Hexapoda Species 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 210000003608 fece Anatomy 0.000 description 2
- 239000010871 livestock manure Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 229930002875 chlorophyll Natural products 0.000 description 1
- 235000019804 chlorophyll Nutrition 0.000 description 1
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 230000000536 complexating effect Effects 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 230000007850 degeneration Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000003895 organic fertilizer Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002686 phosphate fertilizer Substances 0.000 description 1
- 230000029553 photosynthesis Effects 0.000 description 1
- 238000010672 photosynthesis Methods 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000010496 root system development Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 230000003248 secreting effect Effects 0.000 description 1
- 239000002881 soil fertilizer Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000031068 symbiosis, encompassing mutualism through parasitism Effects 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- Fertilizers (AREA)
Abstract
The invention belongs to the field of agricultural fertilizer, and discloses an amino acid guniting compound fertilizer. A preparation method thereof comprises the following steps of: preparation of slurry, mixing of diluted acid, amino acid guniting and granulation, and the like. The invention also discloses a preparation method for the amino acid guniting compound fertilizer. Amino acid is adopted for reaction so as to release a large amount of heat, so that the energy consumption can be effectively lowered. The output of the crops can be effectively improved by utilizing the compound fertilizer, and the compound fertilizer has good nitrogen fixation and water conservation effects.
Description
Technical field
The invention belongs to technical field of agricultural fertilizers, be specifically related to gynaminic acid whitewashing composite fertilizer and preparation method thereof.
Background technology
China is large agricultural country, and nearly 5,000 ten thousand tons of present annual applying quantity of chemical fertilizer account for more than 1/4th of global chemical fertilizer usage quantity, rank first in the world.But, because people blindly use NPK fertilizers in a large number in conventional fertilizers, make the nutrient accumulation in the soil, cause the fertilizer waste, produce serious environmental problem.It is reported, China's N fertilizer utilization rate is for being less than 50%, phosphate fertilizer utilization efficiency is less than 20%, potassium utilization rate is less than 60%, this mainly is because crop is different to the demand of nutrient in the Different Nutrition stage, and the release of the nutrient of existing fertilizer is often asynchronous to the absorption of nutrient with crop, makes superfluous nutrient enter water body and atmosphere by modes such as volatilizing, drench in soil.
Along with a large amount of uses of chemical fertilizer, the continuous reduction of its utilization ratio has been well known fact.This explanation, it is limited only depending on a large amount of application fertilizers to improve crop yield, also has still more a series of problems such as contaminate environment.The various countries scientist is making great efforts the exploring and enhance chemical fertilizer utilization ratio always and is reaching balance fertilizing, the rational application of fertilizer to overcome the approach of its drawback for this reason.Microbial fertilizer has original effect in solution this respect problem.So, according to China's crop species and edaphic condition, adopt suitable microbial fertilizer and chemical fertilizer compounding application, can guarantee volume increase, reduced again the fertilizer application amount, reduce cost, can also improve soil and crop quality simultaneously, reduce and pollute.
Be rich in organic humic acids and be improved soil physical and chemical property, regulate soil acidity or alkalinity, promote the activity of microorganism in soil, increase the activity of soil enzyme, make loosing soil, constantly regulate the soil water, gas, fertile, the situations such as heat, promote the plant root system development healthy growth, strengthen the not people conversion rate of organic and inorganic fertilizer in the soil, increase plant chlorophyll, improve photosynthesis of plant, can the Effective Raise plant cold-resistant, drought resisting, the degeneration-resistant function such as disease and insect resistance, prevent the soil compaction that soil causes because using excessive inorganic fertilizer, Desertification and contaminate environment, the advantages such as Effective Raise crop yield and raising product quality.
How to obtain that fertilizer efficiency is lasting, the composite fertilizer of fixed nitrogen water conservation is the technical problem that prior art needs to be resolved hurrily.
Summary of the invention
The purpose of this invention is to provide gynaminic acid whitewashing composite fertilizer, this propylhomoserin whitewashing composite fertilizer can improve the output of farm crop effectively, and fixed nitrogen water conservation effect is better.
The objective of the invention is to be achieved through the following technical solutions: gynaminic acid whitewashing composite fertilizer, it is prepared from accordance with the following steps:
(1) slip is produced: sal enixum is put into hopper, adding the water that accounts for sal enixum 1/3rd weight stirs, pump carries out neutralization reaction with liquefied ammonia to tubular reactor subsequently, then squeeze in the geosyncline, adding urea, monoammonium phosphate, humic acids, magnesium powder and calcium powder in geosyncline stirs and obtains slurry, wherein the amount of substance ratio of sal enixum and liquefied ammonia is 1:1.1, and the mass ratio of sal enixum, urea, monoammonium phosphate, humic acids, magnesium powder and calcium powder is 10:3:2:2:1:1;
(2) configuration diluted acid: first 98% the vitriol oil is joined in the dilution trap, slowly add entry in the whipping process and obtain diluted acid, wherein the mass ratio of 98% the vitriol oil and water is 2:1;
(3) propylhomoserin spray granulating: the slurry of (1) preparation is driven in the granulation cylinder by volume pump, and the diluted acid that sprays into simultaneously liquefied ammonia and step (2) preparation carries out granulation and oven dry, then adds microbial inoculum, and stirrer stirs, and get final product; Wherein, the mass ratio of slurry, liquefied ammonia, diluted acid and microbial inoculum is 100:3:2:1.
Microbial inoculum of the present invention comprises the raw material of following weight parts: 3 parts of subtilises (Bacillus subtilis) CGMCC No:0954(CN1554744), 2 parts of bacillus megaterium (Bacillus megatherium) CGMCC No:2267 (CN101215532), 2 parts of azotobacter chroococcums (Azotobacter chroococcum) ATCC4412(Production of exocellular polysaccharide by Azotobacter chroococcum. Appl Biochem Biotechnol., 1991 Sep; 30 (3): 273-84.);
The cultivation of subtilis or bacillus megaterium: be seeded at first respectively subtilis or bacillus megaterium on the beef-protein medium, 30 ℃, making primary inclined plane cultivates, then be inoculated into and do vibration secondary liquid culture in the triangular flask, then change liquid fermentation tank over to and do three grades of liquid culture, be inoculated at last and make level Four on the solid medium and cultivate, viable count reaches 1.0 * 10 to the product
8Individual/gram.
The cultivation of azotobacter chroococcum: azotobacter chroococcum is inoculated on the agar slant culture-medium, 32 ℃ of next stage slant culture, then secondary seed cultivation, mixing fermentation culture to viable count reach 1.0 * 10
8Individual/gram.
The bacterium of above-mentioned cultivation mixed by the 3:2:2 mass ratio obtain microbial inoculum.
The present invention also provides a kind of method for preparing above-mentioned composite fertilizer.
Annotate, strain expanded culture and the method for preparing microbial inoculum are not unique in the above-mentioned steps, and those skilled in the art can select suitable medium and enlarged culturing method according to general knowledge, make viable count reach 10
8Individual/gram, and the method preparation for preparing microbial inoculum according to routine.Bacterial classification of the present invention all can obtain from ATCC or the purchase of CGMCC microbial preservation center.
The present invention has following useful effect:
1. can effectively solve slip by the propylhomoserin chemical reaction and send out the difficult problem that sand can not be produced, make prescription more reasonable, more flexible, more effective raising output; And emit amount of heat by the propylhomoserin reaction, can reduce the energy consumption of material drying.
2. liquefied ammonia and diluted acid carry out chemical reaction on the fertilizer surface, can effectively reduce specific grain surface long-pending, make particle more mellow and fuller, and be glossy, the product prevented from caking.
3. adopt the microbiobacterial agent technology, microbiobacterial agent and conventional fertilizers are organically combined, greatly improved the conservation rate of fertilizer, improved fertilizer efficiency.And added the humic acids of appropriate amount, with physics and chemistry bonding mode complexing nutrient, delayed nutrient and discharge speed, improved soil fertilizer, water retention capacity, pinned nutrient control and run off.
4. add Mg powder and calcium powder in composite fertilizer, replenish and suffered trace element, fertilizer efficiency is comprehensive lastingly, strengthens the crop disease-resistant anti-adversity ability.
5. the multiple-microorganism of the present invention's selection adopts scientific matching, the base-material and the raw material that its useful matter that produces in process of growth and secretory substance thereof are become separately or mutually grow, by the symbiosis Relationship With Proliferation, formed a complexity and stable microecosystem, it acts synergistically with humic acids, effectively the fixed nitrogen water conservation.
Embodiment
Below will adopt the mode of specific embodiment that the present invention is carried out detailed description, but should not be construed limitation of the present invention.
Embodiment 1
One gynaminic acid whitewashing composite fertilizer, it is prepared as follows:
(1) slip is produced: sal enixum is put into hopper, adding the water that accounts for sal enixum 1/3rd weight stirs, pump carries out neutralization reaction with liquefied ammonia to tubular reactor subsequently, then squeeze in the geosyncline, adding urea, monoammonium phosphate, humic acids, magnesium powder and calcium powder in geosyncline stirs and obtains slurry, wherein the amount of substance ratio of sal enixum and liquefied ammonia is 1:1.1, and the mass ratio of sal enixum, urea, monoammonium phosphate, humic acids, magnesium powder and calcium powder is 10:3:2:2:1:1;
(2) configuration diluted acid: first 98% the vitriol oil is joined in the dilution trap, slowly add entry in the whipping process and obtain diluted acid, wherein the mass ratio of 98% the vitriol oil and water is 2:1;
(3) propylhomoserin spray granulating: the slurry of (1) preparation is driven in the granulation cylinder by volume pump, and the diluted acid that sprays into simultaneously liquefied ammonia and step (2) preparation carries out granulation and oven dry, then adds microbial inoculum, and stirrer stirs, and get final product; Wherein, the mass ratio of slurry, liquefied ammonia, diluted acid and microbial inoculum is 100:3:2:1.
Above-mentioned microbial inoculum comprises the raw material of following weight parts: 3 parts of subtilises (Bacillus subtilis) CGMCC No:0954,2 parts of bacillus megateriums (Bacillus megatherium) CGMCC No:2267,2 parts of azotobacter chroococcums (Azotobacter chroococcum) ATCC4412;
Wherein, the training method of subtilis or bacillus megaterium is as follows: be seeded at first respectively subtilis or bacillus megaterium on the beef-protein medium, 30 ℃, making primary inclined plane cultivates, then be inoculated into and do vibration secondary liquid culture in the triangular flask, then change liquid fermentation tank over to and do three grades of liquid culture, be inoculated at last and make level Four on the solid medium and cultivate, viable count reaches 1.0 * 10 to the product
8Individual/gram.
The training method of azotobacter chroococcum is as follows: azotobacter chroococcum is inoculated on the agar slant culture-medium, and 32 ℃ of next stage slant culture, then secondary seed is cultivated, mixing fermentation culture viable count to the product reaches 1.0 * 10
8Individual/gram.
The bacterium of above-mentioned cultivation mixed by the 3:2:2 mass ratio obtain microbial inoculum.
Embodiment 2
One gynaminic acid whitewashing composite fertilizer, it is prepared as follows:
(1) slip is produced: sal enixum is put into hopper, adding the water that accounts for sal enixum 1/3rd weight stirs, pump carries out neutralization reaction with liquefied ammonia to tubular reactor subsequently, then squeeze in the geosyncline, adding urea, monoammonium phosphate, humic acids, magnesium powder and calcium powder in geosyncline stirs and obtains slurry, wherein the amount of substance ratio of sal enixum and liquefied ammonia is 1:1.1, and the mass ratio of sal enixum, urea, monoammonium phosphate, humic acids, magnesium powder and calcium powder is 10:3:2:2:1:1;
(2) configuration diluted acid: first 98% the vitriol oil is joined in the dilution trap, slowly add entry in the whipping process and obtain diluted acid, wherein the mass ratio of 98% the vitriol oil and water is 2:1;
(3) propylhomoserin spray granulating: the slurry of (1) preparation is driven in the granulation cylinder by volume pump, and the diluted acid that sprays into simultaneously liquefied ammonia and step (2) preparation carries out granulation and oven dry, then adds microbial inoculum, and stirrer stirs, and get final product; Wherein, the mass ratio of slurry, liquefied ammonia, diluted acid and microbial inoculum is 100:3:2:1.
Above-mentioned microbial inoculum comprises the raw material of following weight parts: 3 parts of subtilises, 2 parts of bacillus megateriums and 2 parts of azotobacter chroococcums;
Wherein, the training method of subtilis or bacillus megaterium is as follows: be seeded at first respectively subtilis or bacillus megaterium on the beef-protein medium, 30 ℃, making primary inclined plane cultivates, then be inoculated into and do vibration secondary liquid culture in the triangular flask, then change liquid fermentation tank over to and do three grades of liquid culture, be inoculated at last and make level Four on the solid medium and cultivate, viable count reaches 1.0 * 10 to the product
8Individual/gram.
The training method of azotobacter chroococcum is as follows: azotobacter chroococcum is inoculated on the agar slant culture-medium, and 32 ℃ of next stage slant culture, then secondary seed is cultivated, mixing fermentation culture viable count to the product reaches 1.0 * 10
8Individual/gram.
The bacterium of above-mentioned cultivation mixed by the 3:2:2 mass ratio obtain microbial inoculum.
Embodiment 3
The cucumber manure trial
In the warmhouse booth of equal cultivated area, the composite fertilizer's (contrast 2), the composite fertilizer of the present invention (the present invention) that use respectively the common chemical fertilizer of family (contrast 1), do not add microbial inoculum are applied to simultaneously three and process in the residential quarters, through of the same race as shown in the table with receiving comparing result:
Table a kind is planted Tianjin spring No. 4 cucumber simultaneous test of using respectively Common compound fertilizer (10-10-10) (contrast 1), not adding composite fertilizer's (contrast 2) and the composite fertilizer (the present invention) that the embodiment of the invention 1 prepares of microbial inoculum
| ? | Per mu yield (Kg) | Volume increase (%) | Reducing sugar (%) | VC(mg/100g) | Mu has a net increase of income (unit) and calculates by 2 yuan/kg |
| Contrast 1 | 21239 | / | 1.56 | ?10.34 | / |
| Contrast 2 | 24892? | 17.2 | 1.72 | 10.67 | 7306 |
| The present invention | 28476 | 34.1 | 1.97 | 12.01 | 14474 |
In planting process, can find out, use that the growing way of composite fertilizer of the present invention preparation is vigorous and blade is bud green, plant height has increased more than the 10cm, taste the result, generally acknowledge than using the good of contrast 2, more be better than using the Common compound fertilizer of contrast 1, and cucumber disease and insect resistance and anti-adversity are better than using other fertilizer greatly.
Embodiment 4
The experiment of Ipomoea batatas fertilizer efficiency
Mt．Mountain town Ipomoea batatas is planted and cultivates the experiment field is to carry out in sandstone and earth yellow soil half-and-half, and twice repetition, 4 Processing Test residential quarters are established in test.Group 1: Common compound fertilizer (16-22-7); Group 2: according to the embodiment of the invention 1 preparation method, but do not add microbial inoculum, humic acids, calcium powder and magnesium powder; Group 3: according to the embodiment of the invention 1 preparation method, but do not add microbial inoculum; Group 4: the composite fertilizer of the embodiment of the invention 1 preparation.Each is tested and processes all mu fertilising 45Kg of residential quarter, and each residential quarter area is 0.2 mu, and rate of fertilizer application is 9Kg in the residential quarter, and on June 1st, 2011 planted, and November 5 digs to obtain in then and gathers.Its contrast output of Sweet Potato Crops is as follows in above-mentioned four experiment residential quarters:
The yield comparison of each treatment group of table 2 Ipomoea batatas growing area
| ? | Test site output (Kg) | Per mu yield (Kg) | Mu fertilising price (unit) | Mu income (unit) |
| 1 | 390 | 1950 | 135 | 1560 |
| 2 | 451 | 2255 | 144 | 1804 |
| 3 | 468 | 2340 | 144 | 1872 |
| 4 | 503 | 2515 | 144 | 2012 |
Remarks: the composite fertilizer of 3000 yuan/tons of compound manure prices, the present invention's preparation is by 3200 yuan/tons, and Ipomoea batatas is by 0.8 yuan/Kg.Test-results shows, the Ipomoea batatas class crop that vegetative period is long, and the composite fertilizer that uses the present invention's preparation more is conducive to increasing both production and income.
What need statement is, the present invention illustrates preparation method of the present invention by above-described embodiment, but the present invention is not limited to above-mentioned preparation process, does not mean that namely the present invention must rely on above-mentioned preparation process and could implement.The person of ordinary skill in the field should understand, any improvement in the present invention to the interpolation of the equivalence replacement of the selected raw material of the present invention and ancillary component, the selection of concrete mode etc., all drops within protection scope of the present invention and the open scope.
Claims (3)
1. gynaminic acid whitewashing composite fertilizer, it is prepared as follows:
(1) slip is produced: sal enixum is put into hopper, adding the water that accounts for sal enixum 1/3rd weight stirs, pump carries out neutralization reaction with liquefied ammonia to tubular reactor subsequently, then squeeze in the geosyncline, adding urea, monoammonium phosphate, humic acids, magnesium powder and calcium powder in geosyncline stirs and obtains slurry, wherein the amount of substance ratio of sal enixum and liquefied ammonia is 1:1.1, and the mass ratio of sal enixum, urea, monoammonium phosphate, humic acids, magnesium powder and calcium powder can be 10:3:2:2:1:1;
(2) configuration diluted acid: first 98% the vitriol oil is joined in the dilution trap, slowly add entry in the whipping process and obtain diluted acid, wherein the mass ratio of 98% the vitriol oil and water is 2:1;
(3) propylhomoserin spray granulating: the slurry of (1) preparation is driven in the granulation cylinder by volume pump, and the diluted acid that sprays into simultaneously liquefied ammonia and step (2) preparation carries out granulation and oven dry, then adds microbial inoculum, and stirrer stirs, and get final product; Wherein, the mass ratio of slurry, liquefied ammonia, diluted acid and microbial inoculum is about 100:3:2:1; Described microbial inoculum comprises the raw material of following weight parts: 3 parts of subtilises, 2 parts of bacillus megateriums and 2 parts of azotobacter chroococcums.
2. composite fertilizer as claimed in claim 1, it is characterized in that, described microbial inoculum comprises the raw material of following weight parts: 3 parts of subtilises (Bacillus subtilis) CGMCC No:0954,2 parts of bacillus megaterium (Bacillus megatherium) CGMCC No:2267 and 2 parts of azotobacter chroococcums (Azotobacter chroococcum) ATCC4412.
3. the preparation method of gynaminic acid whitewashing composite fertilizer, it comprises the steps:
(1) slip is produced: sal enixum is put into hopper, adding the water that accounts for sal enixum 1/3rd weight stirs, pump carries out neutralization reaction with liquefied ammonia to tubular reactor subsequently, then squeeze in the geosyncline, adding urea, monoammonium phosphate, humic acids, magnesium powder and calcium powder in geosyncline stirs and obtains slurry, wherein the amount of substance ratio of sal enixum and liquefied ammonia is 1:1.1, and the mass ratio of sal enixum, urea, monoammonium phosphate, humic acids, magnesium powder and calcium powder is 10:3:2:2:1:1;
(2) configuration diluted acid: first 98% the vitriol oil is joined in the dilution trap, slowly add entry in the whipping process and obtain diluted acid, wherein the mass ratio of 98% the vitriol oil and water is 2:1;
(3) propylhomoserin spray granulating: the slurry of (1) preparation is driven in the granulation cylinder by volume pump, and the diluted acid that sprays into simultaneously liquefied ammonia and step (2) preparation carries out granulation and oven dry, then adds microbial inoculum, and stirrer stirs, and get final product; Wherein, the mass ratio of slurry, liquefied ammonia, diluted acid and microbial inoculum is 100:3:2:1;
Described microbial inoculum comprises the raw material of following weight parts: 3 parts of subtilises (Bacillus subtilis) CGMCC No:0954,2 parts of bacillus megateriums (Bacillus megatherium) CGMCC No:2267,2 parts of azotobacter chroococcums (Azotobacter chroococcum) ATCC4412.
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| CN201310026585.XA CN103044157B (en) | 2013-01-24 | 2013-01-24 | Amino acid guniting compound fertilizer and preparation method thereof |
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| CN201310026585.XA CN103044157B (en) | 2013-01-24 | 2013-01-24 | Amino acid guniting compound fertilizer and preparation method thereof |
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| CN103044157A true CN103044157A (en) | 2013-04-17 |
| CN103044157B CN103044157B (en) | 2014-05-07 |
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| CN201310026585.XA Expired - Fee Related CN103044157B (en) | 2013-01-24 | 2013-01-24 | Amino acid guniting compound fertilizer and preparation method thereof |
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| CN103524225A (en) * | 2013-10-16 | 2014-01-22 | 崔广记 | Serial compound fertilizer produced by amino acid process and preparation method thereof |
| CN103588578A (en) * | 2013-11-20 | 2014-02-19 | 焦作市地***业有限公司 | Humic acid ecological fertilizer and production method thereof |
| CN104003425A (en) * | 2014-06-09 | 2014-08-27 | 山东红日阿康化工股份有限公司 | Novel process for producing potassium hydrogen sulfate and application of potassium hydrogen sulfate in S-based compound fertilizer |
| CN105152788A (en) * | 2015-10-15 | 2015-12-16 | 天津芦阳化肥股份有限公司 | Ecological compound fertilizer dedicated to cotton and preparation method thereof |
| CN105152791A (en) * | 2015-10-21 | 2015-12-16 | 天津芦阳化肥股份有限公司 | Special humic acid chelated slow-release fertilizer for cotton and preparation method thereof |
| CN105152816A (en) * | 2015-10-21 | 2015-12-16 | 天津芦阳化肥股份有限公司 | Humic acid chelating slow-release fertilizer special for soybeans and preparation method thereof |
| CN105237295A (en) * | 2015-09-21 | 2016-01-13 | 天津芦阳化肥股份有限公司 | Special humic acid chelated slow-release fertilizer for wheat and preparation method thereof |
| CN105272518A (en) * | 2015-09-21 | 2016-01-27 | 天津芦阳化肥股份有限公司 | Humic acid chelating slow release fertilizer special for rice and preparation method thereof |
| CN105272590A (en) * | 2015-10-21 | 2016-01-27 | 天津芦阳化肥股份有限公司 | Special humic acid chelated slow-release fertilizer for corn and preparation method of slow-release fertilizer |
| CN105272383A (en) * | 2015-10-15 | 2016-01-27 | 山西磊鑫化工有限公司 | Spherical magnesium calcium nitrate and manufacture method thereof |
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| CN105272518A (en) * | 2015-09-21 | 2016-01-27 | 天津芦阳化肥股份有限公司 | Humic acid chelating slow release fertilizer special for rice and preparation method thereof |
| CN105152788A (en) * | 2015-10-15 | 2015-12-16 | 天津芦阳化肥股份有限公司 | Ecological compound fertilizer dedicated to cotton and preparation method thereof |
| CN105272383A (en) * | 2015-10-15 | 2016-01-27 | 山西磊鑫化工有限公司 | Spherical magnesium calcium nitrate and manufacture method thereof |
| CN105152791A (en) * | 2015-10-21 | 2015-12-16 | 天津芦阳化肥股份有限公司 | Special humic acid chelated slow-release fertilizer for cotton and preparation method thereof |
| CN105152816A (en) * | 2015-10-21 | 2015-12-16 | 天津芦阳化肥股份有限公司 | Humic acid chelating slow-release fertilizer special for soybeans and preparation method thereof |
| CN105272590A (en) * | 2015-10-21 | 2016-01-27 | 天津芦阳化肥股份有限公司 | Special humic acid chelated slow-release fertilizer for corn and preparation method of slow-release fertilizer |
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