CN102924149A - Organic and inorganic matter compound fertilizer prepared from wine waste and preparation method thereof - Google Patents
Organic and inorganic matter compound fertilizer prepared from wine waste and preparation method thereof Download PDFInfo
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- CN102924149A CN102924149A CN2012104116686A CN201210411668A CN102924149A CN 102924149 A CN102924149 A CN 102924149A CN 2012104116686 A CN2012104116686 A CN 2012104116686A CN 201210411668 A CN201210411668 A CN 201210411668A CN 102924149 A CN102924149 A CN 102924149A
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Abstract
The invention provides an organic and inorganic matter compound fertilizer prepared from wine waste. The organic and inorganic matter compound fertilizer is prepared from 10 to 20 parts by weight of wine waste, 10 to 20 parts by weight of humic acid, and 60 to 80 parts by weight of an inorganic fertilizer. The invention also provides a preparation method of the organic and inorganic matter compound fertilizer. The preparation method comprises the following steps of carrying out ammoniation treatment on humic acid, crushing wine waste and the inorganic fertilizer into fine powder, weighing 10 to 20 parts by weight of the fine powder of wine waste, 10 to 20 parts by weight of the treated humic acid and 60 to 80 parts by weight of the fine powder of the inorganic fertilizer, uniformly mixing, adding ammonium bicarbonate into the mixture to adjust a pH value of the mixture until the pH value of the mixture is in a range of 5.5 to 8, and carrying out granulation, screening and packaging. The organic and inorganic matter compound fertilizer prepared from wine waste can effectively increase organic matter content of soil, improve a soil structure and has obvious effects of improving a yield and an income of fruit trees.
Description
Technical field
The present invention relates to a kind of compound organic and inorganic fertilizer and preparation method thereof, particularly a kind of compound organic and inorganic fertilizer that utilizes wine sediment production and preparation method thereof.
Background technology
Modern agriculture mainly relies on a large amount of inputs of chemical fertilizer, agricultural chemicals, this just so that the original balance of the ecosystem be broken, the hardening soil, fertility decline, contaminate environment and soil, the Sustainable Production of impact agricultural so that be described as that mother's of all things on earth water conservation, the fertilizer-preserving ability of soil descends greatly, organism exhaustion, biological activity only reaches 1/10 of traditional agriculture soil.In addition, sharp rising of the prices of the means of agricultural production such as chemical fertilizer rises agriculture production cost in recent years, and the peasant is badly in need of seeking high-quality and efficient, the fertilizer that price is economical of the part or all of replacing fertilizer of a kind of energy, improvement soil.Therefore, under the overall situation of advocating food nutrition, safety, under the megatrend of " pollution-free food " " green food ", wideling popularize fertilizer fiting chemical fertilizer is organic-inorganic composite fertilizer, both can replenish soil with organic matter, improve micro-ecological environment, it is not enough slowly to remedy again the fertilizer fertilizer efficiency.But existing compound organic and inorganic fertilizer often exist heavy metal or intestinal bacteria, roundworm egg to exceed standard, and the fertilizer absorption rate is low, and yield-increasing efficiency is not obvious.
Summary of the invention
The invention provides a kind of compound organic and inorganic fertilizer that utilizes wine sediment production and preparation method thereof, can effectively increase the soil organism, the improvement Soil structure has the effect of obvious increasing both production and income to fruit tree.
Technical scheme of the present invention is achieved in that a kind of compound organic and inorganic fertilizer that utilizes wine sediment to produce, and is made by the raw material that comprises following weight parts: 10 ~ 20 parts of wine sediments, 10 ~ 20 parts of humic acidss, 60 ~ 80 parts in mineral manure.
Compound organic and inorganic fertilizer provided by the invention is preferably made by the raw material that comprises following weight parts: 15 ~ 20 parts of wine sediments, 10 ~ 15 parts of humic acidss, 65 ~ 80 parts in mineral manure.
Described inorganic fertilizer is any one or a few in urea, ammonium sulfate, ammonium nitrate, monoammonium phosphate, calcium superphosphate, the vitriolate of tartar.
The present invention also provides a kind of method for preparing compound organic and inorganic fertilizer, may further comprise the steps:
1) humic acids is processed through ammonification;
2) get wine sediment, mineral manure is ground into fine powder;
3) take by weighing 10 ~ 20 parts of wine sediments of pulverizing, 10 ~ 20 parts of humic acidss, 60 ~ 80 parts of mineral manure of pulverizing, mix, add bicarbonate of ammonia acid adjustment basicity to 5.5 ~ 8; Granulation, screening is packed and be get final product.
Inorganic fertilizer described in the organic and inorganic fertilizer preparation method provided by the invention is any one or a few in urea, ammonium sulfate, ammonium nitrate, monoammonium phosphate, calcium superphosphate, the vitriolate of tartar.
Screening described in the organic and inorganic fertilizer preparation method provided by the invention is to sieve out the particle that particle diameter is 3.35mm ~ 5.6mm.
Material potential of hydrogen measuring method in the preparation process: take by weighing the 10.0g material and put in the 100ml beaker, add the not carbonated water of 50ml, stir 1min, leave standstill 30min, measure with pH meter.
Wine sediment described in the present invention is in the Production of Wine process, the tankage such as the Semen Vitis viniferae of generation, grape vinasse, Grape stems, Semen Vitis viniferae shell, and the present invention adopts is wine sediment through oven dry.Wine sediment comprises Semen Vitis viniferae, Pericarpium Vitis viniferae, stem of Fructus Vitis viniferae etc., and wherein Semen Vitis viniferae accounts for more than 90%.Contain the nutritive ingredients such as rich in protein, fat, Mierocrystalline cellulose, amino acid, minerals and vitamins in the Semen Vitis viniferae, contain in addition powerful antioxidant pycnogenols and cancer-resisting substance trans-resveratrol.This shows that wine sediment is rich in organic matter, macroelement and trace element, especially be suitable as the raw material of producing fruit tree fertilizer.Wherein the massfraction of wine sediment organic matter (in butt) is not less than 45%, the massfraction (in butt) of total nutrient (nitrogen+Vanadium Pentoxide in FLAKES+potassium oxide) is not less than 5%.
Humic acids described in the present invention is the larger molecular organics matter that occurring in nature extensively exists, and is widely used in the every field such as Agriculture, forestry And Animal Husbandry, oil, chemical industry, building materials, medical and health, environmental protection.The organic content that the present invention adopts is not less than 72%, and humic acids content is not less than 50%.
Compound organic and inorganic fertilizer of the present invention forms from raw material, is to utilize wine sediment and humic acid as organic raw material, and using has the inorganic fertilizer of good action as inorganic raw material to fruit tree.The organic and inorganic fertilizer compound generally is conducive to improve fertilizer efficiency.Wine sediment is rich in organic matter, macroelement and trace element, as the soil ulmin of organic main component, preserve the ability of positively charged ion nutrient than the large manyfold of mineral colloid, and the positively charged ions such as main electronegative k adsorption, ammonium, avoid it to outflow with water, and can absorb for crop at any time.Nitrogen chemical fertilizer cooperates organic Fertilizer application, can obtain preferably effect of increasing production.Organic colloid in the organic fertilizer plays encapsulation action to the trioxide in the soil, can reduce the contact of water-soluble phosphorus and fix.Organic mass-energy improves retention capacity of soil, and it is little that soil dry-wet is changed, and can reduce the lattice of potassium and fix.
Description of drawings
Fig. 1 compound organic and inorganic fertilizer preparation technology of the present invention schema.
Embodiment
The below is clearly and completely described the technical scheme in the embodiment of the invention, and obviously, described embodiment only is the present invention's part embodiment, rather than whole embodiment.Based on the embodiment among the present invention, those of ordinary skills belong to the scope of protection of the invention not making the every other embodiment that obtains under the creative work prerequisite.
Embodiment is raw materials used to be described as follows:
Wine sediment, organic (in butt) 81%;
Humic acids, organic content 78%, humic acids 55%;
Urea, Qilu Petrochemical company limited in Shandong produces;
Ammonium sulfate, Jinan century, sensible chemical industry company limited produced;
Ammonium nitrate, Praxair chemical fertilizer company limited in Linyi, Shandong produces;
Monoammonium phosphate, Hebei are sprouted water-soluble fertilizer company limited of side and are produced;
Calcium superphosphate, middle agricultural middle school border chemical fertilizer (Shandong) company limited produces;
Vitriolate of tartar, state throws Lop Nur, Xinjiang sylvite company limited and produces;
Material quantities all among the embodiment are weight part.
Embodiment 1
The raw material of the compound organic and inorganic fertilizer of this example is composed as follows by weight: 16.7 parts of wine sediments, 13 parts of humic acidss, 20 parts in urea, 15 parts in ammonium sulfate, 17 parts of monoammonium phosphates, 18.3 parts of vitriolate of tartar.
Its process flow sheet is processed humic acids first as shown in Figure 1 through ammonification; Take by weighing wine sediment, urea, monoammonium phosphate, kalium slfuricum powder and be broken into fine powder; Take by weighing 16.7 parts of wine sediments of pulverizing, 13 parts of humic acidss, 20 parts of urea of pulverizing, 15 parts of ammonium sulfate of pulverizing, 17 parts of monoammonium phosphates of pulverizing, 18.3 parts of vitriolate of tartar of pulverizing; Mix, add bicarbonate of ammonia acid adjustment basicity to 5.5 ~ 8; Granulation, the screening powder delivery directly is the particle of 3.35mm ~ 5.6mm, packs and get final product.
The process that adds bicarbonate of ammonia acid adjustment basicity: hydrogen-carbonate is joined in the material by solid, stir, the sampling chemical examination; Potential of hydrogen measuring method: take by weighing the 10.0g material and put in the 100ml beaker, add the not carbonated water of 50ml, stir 1min, leave standstill 30min, measure with pH meter.
The compound organic and inorganic fertilizer of making is tested by GB18877-2002 " organic-inorganic complex fertilizer " standard, and every assay all meets the regulation of GB18877-2002 " organic-inorganic complex fertilizer " standard, and assay is as shown in table 1.
Embodiment 2
The raw material of the compound organic and inorganic fertilizer of this example is composed as follows by weight: 11 parts of wine sediments, 19 parts of humic acidss, 20 parts in urea, 25 parts in ammonium nitrate, 15 parts of vitriolate of tartar, calcium superphosphate 10.
Its process flow sheet is processed humic acids first as shown in Figure 1 through ammonification; Take by weighing wine sediment, urea is ground into fine powder; Take by weighing 11 parts of wine sediments of pulverizing, 19 parts of humic acidss, 20 parts of urea of pulverizing, 25 parts of ammonium nitrate of pulverizing, 15 parts of vitriolate of tartar of pulverizing, 10 parts of calcium superphosphate; Mix, add bicarbonate of ammonia acid adjustment basicity to 5.5 ~ 8; Granulation, the screening powder delivery directly is the particle of 3.35mm ~ 5.6mm, packs and get final product.
The process that adds bicarbonate of ammonia acid adjustment basicity: hydrogen-carbonate is joined in the material by solid, stir, the sampling chemical examination; Potential of hydrogen measuring method: take by weighing the 10.0g material and put in the 100ml beaker, add the not carbonated water of 50ml, stir 1min, leave standstill 30min, measure with pH meter.
The compound organic and inorganic fertilizer of making is tested by GB18877-2002 " organic-inorganic complex fertilizer " standard, and every assay all meets the regulation of GB18877-2002 " organic-inorganic complex fertilizer " standard, and assay is as shown in table 1.
Embodiment 3
The raw material of the compound organic and inorganic fertilizer of this example is composed as follows by weight: 20 parts of wine sediments, 11 parts of humic acidss, 15 parts in urea, 20 parts of monoammonium phosphates, 20 parts of vitriolate of tartar, ammonium nitrate 14.
Its process flow sheet is processed humic acids first as shown in Figure 1 through ammonification; Take by weighing wine sediment, urea is ground into fine powder; Take by weighing 20 parts of wine sediments of pulverizing, 11 parts of humic acidss, 15 parts of urea of pulverizing, 20 parts of monoammonium phosphates, 20 parts of vitriolate of tartar of pulverizing, 14 parts of ammonium nitrate of pulverizing; Mix, add bicarbonate of ammonia acid adjustment basicity to 5.5 ~ 8; Granulation, the screening powder delivery directly is the particle of 3.35mm ~ 5.6mm, packs and get final product.
The process that adds bicarbonate of ammonia acid adjustment basicity: hydrogen-carbonate is joined in the material by solid, stir, the sampling chemical examination; Potential of hydrogen measuring method: take by weighing the 10.0g material and put in the 100ml beaker, add the not carbonated water of 50ml, stir 1min, leave standstill 30min, measure with pH meter.
The compound organic and inorganic fertilizer of making is tested by GB18877-2002 " organic-inorganic complex fertilizer " standard, and every assay all meets the regulation of GB18877-2002 " organic-inorganic complex fertilizer " standard, and assay is as shown in table 1.
Table 1 embodiment inspection after construction result
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Outward appearance | White particle | White particle | White particle |
| Total nutrient (N+P 20 5+ K) massfraction, % | 29.6％ | 25.6％ | 28.7％ |
| Organic massfraction, % | 22.3％ | 23.4％ | 24.1％ |
| Granularity (3.35～5.6mm)/% | 4.7 | 4.8 | 4.5 |
| Potential of hydrogen (pH) | 6.5 | 6.8 | 6.7 |
| Induced worm egg death rate/% | 97 | 98 | 99 |
| Colititre 〉= | 10 -1 | 10 -1 | 10 -1 |
Application Example 1
Carried out compound organic and inorganic fertilizer field application test in sorrowful Ge Zhuan orchard, Yantai City, Shandong Mouping District east in 2010 ~ 2011 years.This orchard is brunisolic soil, and fertility is even, and level of management are higher.Supplying the examination fruit tree is 8 years living red fuji apples, and seeding row spacing is 3m * 3m.3 processing are established in test, process 1 and are the blank contrast of not applying fertilizer; Process 2 every mu execute conventional composite fertilizer (N-P
2O
5-K
2O is 13-15-17) 200kg; Process 3 every mu of compound organic and inorganic fertilizer 200kg that execute the embodiment of the invention 1; 6 trees in every residential quarter are repeated 4 times, establish altogether 12 residential quarters, random alignment.Respectively at November every mu of (in conjunction with base manure) and April executing 100kg.
Test-results shows: process 3 compound organic and inorganic fertilizers of executing embodiment 1, every per mu yield apple 4501.8kg; Process the contrast of not applying fertilizer of 1 blank, every per mu yield apple 3576.2kg; Conventional composite fertilizer, every per mu yield apple 4304.6kg are executed in processing 2.Process 3 compound organic and inorganic fertilizers of executing embodiment 1 than processing the 1 blank contrast volume increase 925.6kg that do not apply fertilizer, stimulation ratio is 25.8%, executes conventional composite fertilizer volume increase 197.2kg than processing 2, and stimulation ratio is 4.6%.And the apple quality of executing the compound organic and inorganic fertilizer of embodiment 1 obviously improves, features good taste, and sugariness is large.And increased the soil organism, improved soil fertility.
Application Example 2
Carried out compound organic and inorganic fertilizer field application test in the quiet orchard of Yantai, Shandong monarch in 2011 ~ 2012 years.This orchard is brunisolic soil, and fertility is even, and level of management are higher.Supplying the examination fruit tree is 8 years living red fuji apples, and seeding row spacing is 3m * 3m.3 processing are established in test, process 1 and are the blank contrast of not applying fertilizer; Process 2 every mu execute conventional composite fertilizer (N-P
2O
5-K
2O is 13-15-17) 200kg; Process 3 every mu of compound organic and inorganic fertilizer 200kg that execute the embodiment of the invention 1; 6 trees in every residential quarter are repeated 4 times, establish altogether 12 residential quarters, random alignment.Respectively at November every mu of (in conjunction with base manure) and April executing 100kg.
Test-results shows: process 3 compound organic and inorganic fertilizers of executing embodiment 1, every per mu yield apple 4521.3kg; Process the contrast of not applying fertilizer of 1 blank, every per mu yield apple 3567.0kg; Conventional composite fertilizer, every per mu yield apple 4231.4kg are executed in processing 2.Process 3 compound organic and inorganic fertilizers of executing embodiment 1 than processing the 1 blank contrast volume increase 954.3kg that do not apply fertilizer, stimulation ratio is 26.7%, executes conventional composite fertilizer volume increase 289.9kg than processing 2, and stimulation ratio is 6.8%.And the apple quality of executing the compound organic and inorganic fertilizer of embodiment 1 obviously improves, features good taste, and sugariness is large.And increased the soil organism, improved soil fertility.
By field test and spread as can be known, the compound organic and inorganic fertilizer that utilizes wine sediment to produce has obvious increasing yield and improving quality the effect of increasing income to fruit tree, and can effectively increase soil organic matter content, improving soil physical properties, is the fertilizer that is fit to production of fruit trees.
Claims (6)
1. a compound organic and inorganic fertilizer that utilizes wine sediment to produce is characterized in that, is made by the raw material that comprises following weight parts: 10 ~ 20 parts of wine sediments, 10 ~ 20 parts of humic acidss, 60 ~ 80 parts in mineral manure.
2. compound organic and inorganic fertilizer according to claim 1 is characterized in that, is made by the raw material that comprises following weight parts: 15 ~ 20 parts of wine sediments, 10 ~ 15 parts of humic acidss, 65 ~ 80 parts in mineral manure.
3. compound organic and inorganic fertilizer according to claim 2 is characterized in that, described inorganic fertilizer is any one or a few in urea, ammonium sulfate, ammonium nitrate, monoammonium phosphate, calcium superphosphate, the vitriolate of tartar.
4. a method for preparing compound organic and inorganic fertilizer claimed in claim 1 is characterized in that, may further comprise the steps:
1) humic acids is processed through ammonification;
2) get wine sediment, mineral manure is ground into fine powder;
3) take by weighing 10 ~ 20 parts of wine sediments of pulverizing, 10 ~ 20 parts of humic acidss, 60 ~ 80 parts of mineral manure of pulverizing, mix, add bicarbonate of ammonia acid adjustment basicity to 5.5 ~ 8; Granulation, screening is packed and be get final product.
5. a kind of method for preparing compound organic and inorganic fertilizer according to claim 4 is characterized in that, described inorganic fertilizer is any one or a few in urea, ammonium sulfate, ammonium nitrate, monoammonium phosphate, calcium superphosphate, the vitriolate of tartar.
6. a kind of method for preparing compound organic and inorganic fertilizer according to claim 4, described screening is to sieve out the particle that particle diameter is 3.35mm ~ 5.6mm.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104311204A (en) * | 2014-09-25 | 2015-01-28 | 安徽圣堡利诺葡萄酒庄园有限公司 | Composite fertilizer prepared from waste residue generated during wine production |
| CN104355724A (en) * | 2014-09-25 | 2015-02-18 | 安徽圣堡利诺葡萄酒庄园有限公司 | Extractum-shaped composite fertilizer prepared from waste residues generated in grape wine production |
| CN104402652A (en) * | 2014-11-20 | 2015-03-11 | 柳州市源晨农副产品有限公司 | Special fertilizer for grape culture |
| CN105669272A (en) * | 2016-01-13 | 2016-06-15 | 烟台固特丽生物科技股份有限公司 | Organic high-content flower fertilizer, preparation method thereof and application of organic high-content flower fertilizer as flower seedling substrate |
| WO2017214958A1 (en) * | 2016-06-17 | 2017-12-21 | 张铭强 | Micro-carbon plant anthocyanin for promoting early colouring and plumping of fruits, and preparation method and application thereof |
| CN115368907A (en) * | 2022-07-22 | 2022-11-22 | 山东省葡萄研究院 | Alkaline soil conditioner prepared from grape juice distillation residual liquid and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104311204A (en) * | 2014-09-25 | 2015-01-28 | 安徽圣堡利诺葡萄酒庄园有限公司 | Composite fertilizer prepared from waste residue generated during wine production |
| CN104355724A (en) * | 2014-09-25 | 2015-02-18 | 安徽圣堡利诺葡萄酒庄园有限公司 | Extractum-shaped composite fertilizer prepared from waste residues generated in grape wine production |
| CN104402652A (en) * | 2014-11-20 | 2015-03-11 | 柳州市源晨农副产品有限公司 | Special fertilizer for grape culture |
| CN105669272A (en) * | 2016-01-13 | 2016-06-15 | 烟台固特丽生物科技股份有限公司 | Organic high-content flower fertilizer, preparation method thereof and application of organic high-content flower fertilizer as flower seedling substrate |
| CN105669272B (en) * | 2016-01-13 | 2019-03-19 | 烟台固特丽生物科技股份有限公司 | A kind of organic type high-content fertilizer for flower and preparation method thereof and application as flower seedling raising matrix |
| WO2017214958A1 (en) * | 2016-06-17 | 2017-12-21 | 张铭强 | Micro-carbon plant anthocyanin for promoting early colouring and plumping of fruits, and preparation method and application thereof |
| CN115368907A (en) * | 2022-07-22 | 2022-11-22 | 山东省葡萄研究院 | Alkaline soil conditioner prepared from grape juice distillation residual liquid and preparation method thereof |
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Application publication date: 20130213 |