Summary of the invention
First technical problem to be solved by this invention provides a kind of new nourishing moisturizing emulsion that contains multiple natural component extract.
Second preparation method that technical problem is above-mentioned emulsion to be solved by this invention.
The technical scheme of technical solution problem of the present invention is: a kind of emulsion of nourishing moisturizing, contain following material in every 77g emulsion:
Described Bulbus Lilii extracting solution prepares by the following method:
It is an amount of to take by weighing Bulbus Lilii, is heated to 90-100 ℃, decocts to extract 3 times, adds 8-15 times of water gaging for the first time, extracts 0.5-1.5h; Add for the second time 6-12 times of water gaging, extract 0.5-1.5h; Add for the third time 4-10 times of water gaging, extract 0.5-1.5h; With three layers of filtered through gauze, merging filtrate heats 3-6 times (ml/g) being concentrated into Bulbus Lilii weight, and is with three layers of filtered through gauze, for subsequent use at every turn.
Described HONGQIAOMEI extracting solution prepares by the following method:
It is a certain amount of to take by weighing HONGQIAOMEI, is heated to 90-100 ℃, decocts to extract 3 times, add for the first time 30-50 water doubly, extract 0.5-1.5h, add 25-40 water doubly for the second time, extract 0.5-1.5h, add for the third time 20-30 water doubly, extract 0.5-1.5h, filter with 3 layers of gauze at every turn, merging filtrate, heating is concentrated into 3-6 times (ml/g) of HONGQIAOMEI weight, and is with 3 layers of filtered through gauze, for subsequent use.
Described Semen Benincasae extracting solution prepares by the following method:
It is a certain amount of to take by weighing Semen Benincasae, is heated to 90-100 ℃, decocts to extract 3 times, extract 0.5-1.5h with the 8-15 times of water yield the 1st time, the 2nd time with the 6-12 times of water yield, extract 0.5-1.5h, extract 0.5-1.5h with the 6-10 times of water yield, all be three layers of filtered through gauze at every turn for the 3rd time, filtrate merges, heating is concentrated into 3-6 times (ml/g) of medical material weight, and is with three layers of filtered through gauze, for subsequent use.
Described corncob must prepare by extracting solution by the following method:
Taking by weighing corncob must be a certain amount of, is heated to 90-100 ℃, decocts and extracts 3 times, extract 0.5-1.5h with the 8-15 times of water yield the 1st time, the 2nd time with the 6-10 times of water yield, extract 0.5-1.5h, extract 0.5-1.5h with the 6-10 times of water yield, all be three layers of filtered through gauze at every turn for the 3rd time, filtrate merges, heating is concentrated into 3-6 times (ml/g) of medical material weight, and is with three layers of filtered through gauze, for subsequent use.
Described Sucus Cocois prepares by the following method:
Commercially available Cortex cocois radicis is poured out the new fresh cocoanut juice of the inside, and is for subsequent use.
Described essence is peach flavor, green cucumber essence, rose essence, osmanthus flower fragrance, a kind of in the flavoring pineapple essence.
Described sodium alginate soln prepares by the following method:
Take by weighing sodium alginate 5-15g, adding distil water 100-1000ml places and stirs, and makes it fully be swelled into homogeneous transparent liquid.
Described Carbopol 941 solution prepares by the following method:
Take by weighing Carbopol 941 2-15g, adding distil water 100-1000ml places and stirs, and makes it fully be swelled into homogeneous transparent liquid.
Described nourishing moisturizing emulsion prepares by the following method:
A) take by weighing Jojoba oil 0.5-4.0g, olive oil 0.5-4.0g, glyceryl monostearate 2.0-10g, sorbester p17 0.3-3g, vitamin E 0.1-3.0g is heated to 70-85 ℃, and it is melted fully, mixes, and obtains oil phase;
B) take by weighing poloxamer 1-10g, glycerol 2.0-20g, propylene glycol 0.6-12g, distilled water 14.0-50.0g, Mel 0.3-3g, carbamide 0.1-4.0g, 1% hyaluronate sodium 0.3-3ml, disodiumedetate 0.1-0.5mg, Serine 0.02-1.0g is heated to 70-85 ℃, it is melted fully, mix, obtain water;
C) in the time of 70-85 ℃, pour water into oil phase, add rear stirring 5-15 minute, make it form uniform emulsion, be cooled to room temperature, add Bulbus Lilii extracting solution 1-10ml, HONGQIAOMEI extracting solution 1-10ml, Sucus Cocois 2-15ml, Semen Benincasae extracting solution 1-10ml, corncob palpus extracting solution 1-10ml, essence 0.05-2ml, sodium alginate soln 6-25g, sorbic acid 0.1-2g, Carbopol 941 solution 10-50g, stirring to obtain nourishing moisturizing emulsion.
Various compositions among the present invention are as follows:
Jojoba oil contains collagenic protein, the mineral of vitamin and high nourishing degree, can protect skin, avoids water loss, and deep layer is nourished the care skin, makes it glossy, has elasticity, and relaxes and expose to the weather to the injury of skin.Jojoba oil is the strongest base oil of permeability, very easily is absorbed by the skin, salubrious moist, non-greasy, can recover skin pH balance, the wrinkle removing stricture of vagina effectively improves oily skin, nurse one's health the smegma function, and improve the skin of inflammation, can be used for eczema, chronic eczema, comedo etc.Its energy pore refining also is simultaneously best skin moisture-keeping oil.Its formed oil film is different from mineral oil, but the moisture of Pervaporation also can be controlled the loss of moisture.Its skin-friendly is fine, is the good medium of quintessence oil being brought into skin, and is all very good to hair and beautifying skin.It has natural moistening and Moisture factor, and skin-nourishing is provided, and makes tired skin reply original vigor.
Olive oil rich in vitamin E, A, B, D, K, F also contain carotene, abundant trace element, Squalene, Flavonoid substances and polyphenolic substance, the essential fatty acid etc. splendid with the skin affinity.The phenols antioxidant that contains in the olive oil can be eliminated facial wrinkles, prevents skin aging, and the effects such as skin or hair care and control hand and foot from chapping are arranged.Polyphenol in the olive oil and lipopolysaccharide composition have radiation-resistant function.Smear skin energy ultraviolet rays resistance with olive oil, the prevention skin carcinoma is the health-care skin-protecting products that often makes computer user.Chlorophyll in the olive oil plays metabolism, Promote cell's growth, and accelerating wound healing helps the appearance of beautify people, reduces the generation of wrinkle.These compositions are easy to be absorbed by the skin, and effectively keep skin elasticity and moist, can strengthen the immunity of human body, slow down aging.Olive oil does not contain essence and chemical substance, can prevent moisture of skin evaporation, to the nourishing of skin as mild as a dove, can make rapidly skin tender and glossy.Although be " oil ", with rear clearly oiliness.
Mel is desirable natural enamel.It contains vitamin B
1, B
2, B
6, C, ferrum, calcium, copper, manganese, phosphorus, potassium, aminoacid, hormone, fructose, glucose, inorganic salt, amylase, lipase, invertase etc.If skin lacks nutrition, metabolism reduces, and water content reduces, and it is old and feeble that Skin Cell becomes, and will produce wrinkle, and wrinkle increases, and it is coarse pitch-dark that skin becomes, even can bring the sensation of geromorphism.Mel contains a large amount of nutritional labelings that can be absorbed by the body, that the effect of nourishing cosmetology is arranged, and fragrant odour is good to eat.It is the Skin Cell nourishing agent, and external can be absorbed by the human epidermal cell, thereby has strengthened the vigor of epidermis cell, promotes the metabolism of Skin Cell, improves the nutriture of skin.Can make the pure white exquisiteness of skin, keep nature ruddy, delicate, eliminate and the minimizing wrinkle, prevent skin aging.Oral administration and external has splendid effect to skin care.Mel has very strong bactericidal action, can protect skin, cleaning skin and some skin diseases for the treatment of and wound.
Sucus Cocois contains the mineral such as abundant potassium, magnesium, and its composition is similar to intracellular fluid, but correct dehydration and electrolyte disturbance reach the effect of inducing diuresis to remove edema.Coconut juice contains the trace element of saccharide, fat, protein, growth hormone, vitamin and a large amount of needed by human in addition, often drinks, can beneficial people's strength, replenish intracellular fluid, and expanding blood volume, skin care has the conditioning skin and losing effect.
HONGQIAOMEI contains arginine, aspartic acid, glutamic acid, aminobutyric acid, tyrosine, proline, serine, phenylalanine, crisp propylhomoserin, valine, histidine, alanine, lysine, leucine, glycine and isoleucine.Effect with pathogenic fire reducing antiinflammatory, eliminating toxin and beautifying the skin, slow down aging, the skin care of invigorating blood circulation, skin Caring speckle dispelling.Chang Yinneng QI and blood regulating, skin care speckle removing, skin whitening make skin smooth, are rich in gloss and elasticity, slow down aging, and the chloasma that causes for the treatment of endocrine regulation, freckle, mottle, skin sore etc. are had obvious curative effects, can make skin delicate ruddy.
Semen Benincasae contains saponin, linoleic acid, oleic acid, carbamide, citrulline etc." Japan hanako materia medica ": the black Shao-of peeling skin wind stripping, profit skin.Shennong's Herbal meaning this product can " be made us the good color in happy pool ".Its major function is clean white muscle skin, cures mainly the symptoms such as complexion is withered and yellow, in a sorrowful look, dim complexion, is one of skin Caring skin care item of commonly using ancient times.
Bulbus Lilii contains the plurality of active ingredients such as phospholipid, phenolic acid glyceride, steroid alkaloid, protein, aminoacid.The Bulbus Lilii extracting solution makes an addition in the products such as cream kind in the cosmetics, cleansing milk, bath gel, equal Glycerins enduringly, replenish and regulate nutrition and moisture, lower the skin sensitivity degree, improve blood circulation, strengthen skin metabolism, the mottle recurrence is effectively controlled in the generation of restraint of tyrosinase activity and melanocyte.
The fatty oil of corncob palpus, volatile oil, gummy sample material, resin, vitamin C, pantothenic acid, inositol etc.It has special effect to cosmetic slimming.Stigma Maydis extract is removed free radical and is suppressed lipid peroxidation, helps slow down aging.
The present invention compared with prior art, Mel has the cosmetology effect of nourishing; Carbamide has moisture-keeping functions to skin; Hyaluronate sodium has good moisture-keeping function; VitE has antioxidation, anti-aging effects; Serine makes skin keep elasticity; Jojoba oil makes tired skin reply original vigor; Olive oil effectively keeps skin elasticity and moist.Various components are share, and supply with the sufficient moisture of skin, make epidermis cell mellow and full, and horny layer hydration ability rises, and make skin lubricated, glossy.Because its composition has good permeability, anti-horny layer is aging, promotes regenerative cell regeneration, keeps the skin wet, and increases elasticity.
The specific embodiment
The present invention will be further described below in conjunction with embodiment.
Olive oil of the present invention, Jojoba oil, Mel are commercially available.
Embodiment 1
1.1 the preparation of Bulbus Lilii extracting solution
Take by weighing Bulbus Lilii 10g, be heated to 95 ℃, decoct and extract 3 times, add the water of 150ml for the first time, extract the water that 1h adds 120ml for the second time, extract 1h, add for the third time the water of 80ml, extract 1h, use 3 layers of filtered through gauze at every turn, merging filtrate, heating is concentrated into 60ml, and is with 3 layers of filtered through gauze, for subsequent use.
1.2 the preparation of HONGQIAOMEI extracting solution
Take by weighing HONGQIAOMEI 8g, be heated to 95 ℃, decoct and extract 3 times, add the water of 400ml for the first time, extract 1h, the water that adds for the second time 320ml extracts 1h, adds for the third time the water of 240ml, extracts 1h, filters with 3 layers of gauze at every turn, merging filtrate, heating is concentrated into 48ml, filters with 3 layers of gauze, and is for subsequent use.
1.3 the preparation of Semen Benincasae extracting solution
Take by weighing Semen Benincasae 30g, be heated to 94 ℃, decoct and extract 3 times, the 1st water with 450ml extracts 1h, the 2nd water with 360ml extracts 1h, and the 3rd water with 270ml extracts 1h, all is 3 layers of filtered through gauze at every turn, filtrate merges, and heating is concentrated into 175ml, filters with 3 layers of gauze, and is for subsequent use.
1.4 the preparation of corncob palpus extracting solution
Take by weighing corncob palpus 20g, be heated to 94 ℃, decoct and extract 3 times, the 1st water with 300ml extracts 1h, the 2nd water with 200ml extracts 1h, and the 3rd water with 200ml extracts 1h, all is 3 layers of filtered through gauze at every turn, filtrate merges, and heating is concentrated into 120ml, filters with 3 layers of gauze, and is for subsequent use.
1.5 the preparation of Sucus Cocois
Buy in market complete Cortex cocois radicis, pour out the inside new fresh cocoanut juice 300ml.
1.6 the preparation of sodium alginate soln
Take by weighing sodium alginate 10g, add water 500ml, place and stir, make it fully be swelled into homogeneous transparent liquid.
1.7 the preparation of Carbopol 941 solution
Take by weighing Carbopol 941 2g, add water 200ml, place and stir, make it fully be swelled into homogeneous transparent liquid.
1.8 nourish the preparation of moisturizing emulsion
A) take by weighing Jojoba oil 3g, olive oil 2g, glyceryl monostearate 5g, sorbester p17 1g, VE 0.6g pours in the beaker, puts into 79 ℃ of water-bath heating it is melted fully, mixes, and obtains oil phase;
B) take by weighing poloxamer 3g, glycerol 7g, propylene glycol 2g, distilled water 35g, Mel 2g, carbamide 1g, 1% hyaluronate sodium 2ml, ethylenediaminetetraacetic acid two a propylhomoserins 0.1 g pours in the beaker, puts into 79 ℃ of water-baths, and the heated and stirred mix homogeneously obtains water.
When c) treating that water and oil phase are uniform liquid, on 79 ℃ of water-baths, water is the thread shape slowly pours oil phase into, the limit edged ceaselessly stirs towards same direction, after water is finished down, stirred 10 minutes at water-bath, make it form uniform emulsion, lift down from water-bath and to be cooledly to room temperature, not add Bulbus Lilii extracting solution 4ml, HONGQIAOMEI extracting solution 4ml, Sucus Cocois 8ml, Semen Benincasae extracting solution 3ml, corncob palpus extracting solution 3ml, essence 0.3ml, sodium alginate 15g, sorbic acid 0.5g, 1% Carbopol 941 solution 20g, stirring to obtain this emulsion.
Embodiment 2
2.1 the preparation of Bulbus Lilii extracting solution
Take by weighing Bulbus Lilii 15g, be heated to 94 ℃, decoct and extract 3 times, add the water of 210ml for the first time, extract the water that 1h adds 165ml for the second time, extract 0.9h, add for the third time the water of 135ml, extract 1h, use three layers of filtered through gauze at every turn, merging filtrate, heating is concentrated into 80ml, and is with 3 layers of filtered through gauze, for subsequent use.
2.2 the preparation of HONGQIAOMEI extracting solution
Take by weighing HONGQIAOMEI 10g, be heated to 94 ℃, decoct and extract 3 times, add the water of 450ml for the first time, extract 1.1h, the water that adds for the second time 350ml extracts 1h, adds for the third time 25 times water, extracts 1.1h, filters with 3 layers of gauze at every turn, merging filtrate, heating is concentrated into 50ml, filters with 3 layers of gauze, and is for subsequent use.
2.3 the preparation of Semen Benincasae extracting solution
Take by weighing Semen Benincasae 40g, be heated to 94 ℃, decoct and extract 3 times, the 1st water with 560ml extracts 1.1h, the 2nd water with 450ml extracts 1h, and the 3rd water with 400ml extracts 1h, all is 3 layers of filtered through gauze at every turn, filtrate merges, and heating is concentrated into 240ml, filters with 3 layers of gauze, and is for subsequent use.
2.4 the preparation of corncob palpus extracting solution
Take by weighing corncob palpus 30g, be heated to 94 ℃, decoct and extract 3 times, the 1st water with 500ml extracts 1h, the 2nd water with 350ml extracts 1h, and the 3rd water with 300ml extracts 1h, all is 3 layers of filtered through gauze at every turn, filtrate merges, and heating is concentrated into 160ml, filters with 3 layers of gauze, and is for subsequent use.
2.5 the preparation of Sucus Cocois
Be buy in market complete Cortex cocois radicis, pour out the inside new fresh cocoanut juice 300ml.
2.6 the preparation of sodium alginate soln
Accurately take by weighing sodium alginate 20g, add water 1000ml, place and stir, make it fully be swelled into homogeneous transparent liquid.
2.7 the preparation of Carbopol 941 solution
Accurately take by weighing Carbopol 941 1g, add water 100ml, place and stir, make it fully be swelled into homogeneous transparent liquid.
2.8 nourish the preparation of moisturizing emulsion
A) take by weighing Jojoba oil 1.5g, olive oil 3.5g, glyceryl monostearate 4g, sorbester p17 0.8g, VE 0.5g pours in the beaker, puts into 80 ℃ of water-bath degree pots, and heating is melted it fully, mixes, and obtains oil phase;
B) take by weighing poloxamer 3.5g, glycerol 5g, propylene glycol 1.2g, distilled water 35g, Mel 1.3g, carbamide 0.6g, 1% hyaluronate sodium 1.2ml, disodiumedetate 4.5mg, Serine 0.09g pours in the beaker, puts into 80 ℃ of water-baths, and the heated and stirred mix homogeneously obtains water.
When c) treating that water and oil phase are uniform liquid, on 81 ℃ of water-baths, water is the thread shape slowly pours oil phase into, the limit edged ceaselessly stirs towards same direction, after water is finished down, stirred 8 minutes at water-bath, make it form uniform emulsion, lift down from water-bath and to be cooledly to room temperature, do not add Bulbus Lilii extracting solution 5ml, HONGQIAOMEI extracting solution 5ml, Sucus Cocois 8ml Semen Benincasae extracting solution 5ml, corncob palpus extracting solution 6ml, essence 0.2ml, sodium alginate 15g, sorbic acid 0.7g, Carbopol 941 solution 30g, stirring to obtain this emulsion.
Embodiment 3
Embodiment 1,2 physical and chemical index are as follows:
3.1 character
This product is that viscosity is suitable, good stability, abnormal smells from the patient fragrance, fine and smooth uniformly milky emulsion.
3.2 pH value inspection
Get this product, fixed with the PH instrumentation, recording pH value is between the 6.5-7.0.
3.3 hot and cold test
Emulsion is packaged in the transparent dressing product bottle, observed without lamination in one month in 4 ℃ refrigerator cold-storages.24h in 55 ℃ calorstat, emulsion is without the phenomenon such as layering emulsifying is spoiled.
3.4 centrefuge experiment
Emulsion is packaged in the centrifugal 20min of 3000r/min in the tool plug test tube, without lamination
3.5 room temperature is placed experiment
Embodiment 1,2 made emulsions are placed bottle for cosmetics, and room temperature leaves standstill investigates 6 months, and without lamination, unchanged with aftersensation, abnormal smells from the patient is unchanged.
3.6 irritation test, anaphylaxis experiment
The white mouse back cuts off hair, smears respectively emulsions by embodiment 1,2 preparations in cutting plucked position, and is not coated with the position and compares, and the result does not have zest and anaphylaxis.
Get embodiment 1,2 and be applied in right amount on volunteer (25-65 year, the 170 people) gesture and facial expression, observe after spending 30 minutes, all do not occur rubescent, dermexanthesis, foaming phenomenon.
Embodiment 4
Nourish the experiment of moisturizing emulsion effect
Come Evaluation operation example 1,2 nourishing moistening effect by experiment on probation.The bath foam and the commercially available whitening bath foam that utilize embodiment 1,2 to produce compare experiment.Choose the people of 150 25-65 age brackets as applicable object, they are divided into arbitrarily three groups, use respectively the nourishing moisturizing emulsion of buying on the emulsion of embodiment 1,2 preparation and the market.1 50 of embodiment, 27 male, 23 women; 2 50 of embodiment, 26 male, 24 women; 3 50 of matched groups, 25 male, 25 women.Used two months continuously, sophistication and the pliability of detect by an unaided eye face and hand, this results are shown in Table 1;
Table 1 nourishes the moisturizing experimental result
|
Effectively (people) |
A little effectively (people) |
Invalid (people) |
Total effective rate (%) |
Embodiment 1 |
40 |
5 |
5 |
90 |
Embodiment 2 |
41 |
4 |
5 |
90 |
Matched group |
38 |
3 |
9 |
82 |
Embodiment 5
The resultant effect of emulsion is investigated
Below utilize and try out the effect of feeling to come the emulsion that Evaluation operation example 1,2 produces.Adopt the public-opinion poll point system, the people who chooses 80 25-65 year age bracket is object on probation, is divided into arbitrarily two groups, puts hands and face on the skin with embodiment 1,2 emulsions that prepare respectively.Every day, each used once sooner or later, and be two months service time.Every result of use total points is 5 minutes: five are divided into best result, and expression better, and is very satisfied; 4 be divided into fine; 3 are divided into and can accept; Be bad below 3 minutes, can not accept.Be every average below, the results are shown in Table 2:
Table 2 resultant effect is investigated
Result of use |
Embodiment 1 every average |
Embodiment 2 every averages |
Whitening |
4.5 |
4.6 |
Nourishing property |
4.7 |
4.8 |
Moisture retention |
4.9 |
4.8 |
Armaticity |
4.8 |
4.7 |
In sum, this product has preferably moisture retention, nourishing property, whitening, armaticity, and the sensation skin moistens during use, and is glossy, high resilience, and the skin quality significantly improves behind the life-time service.