CN102888156B - A kind of Uvioresistant fluorocarbon metal anti-rust paint and preparation method thereof - Google Patents
A kind of Uvioresistant fluorocarbon metal anti-rust paint and preparation method thereof Download PDFInfo
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- CN102888156B CN102888156B CN201210340773.5A CN201210340773A CN102888156B CN 102888156 B CN102888156 B CN 102888156B CN 201210340773 A CN201210340773 A CN 201210340773A CN 102888156 B CN102888156 B CN 102888156B
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- 239000003973 paint Substances 0.000 title claims abstract description 46
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 title claims abstract description 19
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 14
- 239000002184 metal Substances 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 22
- 238000004537 pulping Methods 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 26
- 239000006185 dispersion Substances 0.000 claims description 23
- 239000000843 powder Substances 0.000 claims description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 15
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 239000003795 chemical substances by application Substances 0.000 claims description 15
- 239000004576 sand Substances 0.000 claims description 12
- SGUQCKMQPFUEDZ-UHFFFAOYSA-N 6-butoxyhexyl acetate Chemical compound CCCCOCCCCCCOC(C)=O SGUQCKMQPFUEDZ-UHFFFAOYSA-N 0.000 claims description 10
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Diphosphoinositol tetrakisphosphate Chemical compound OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 claims description 10
- 239000002002 slurry Substances 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 9
- 229920001296 polysiloxane Polymers 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- 238000003801 milling Methods 0.000 claims description 6
- QUKFNRQNPQSTPD-UHFFFAOYSA-N 2-methylpropanoic acid;pentane-1,3-diol Chemical compound CC(C)C(O)=O.CCC(O)CCO QUKFNRQNPQSTPD-UHFFFAOYSA-N 0.000 claims description 5
- 229920001661 Chitosan Polymers 0.000 claims description 5
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 5
- 229920002125 Sokalan® Polymers 0.000 claims description 5
- 239000006229 carbon black Substances 0.000 claims description 5
- 125000002433 cyclopentenyl group Chemical group C1(=CCCC1)* 0.000 claims description 5
- MCPKSFINULVDNX-UHFFFAOYSA-N drometrizole Chemical compound CC1=CC=C(O)C(N2N=C3C=CC=CC3=N2)=C1 MCPKSFINULVDNX-UHFFFAOYSA-N 0.000 claims description 5
- 239000000314 lubricant Substances 0.000 claims description 5
- 239000004584 polyacrylic acid Substances 0.000 claims description 5
- 239000011347 resin Substances 0.000 claims description 5
- 229920005989 resin Polymers 0.000 claims description 5
- 238000004062 sedimentation Methods 0.000 claims description 5
- 159000000000 sodium salts Chemical class 0.000 claims description 5
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 5
- 235000011152 sodium sulphate Nutrition 0.000 claims description 5
- 230000009974 thixotropic effect Effects 0.000 claims description 5
- 239000006097 ultraviolet radiation absorber Substances 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- 229910019142 PO4 Inorganic materials 0.000 claims description 3
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 3
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 3
- KOEFSMLBFZGZLD-UHFFFAOYSA-L [bis(2-ethylhexoxy)-oxidophosphaniumyl] dihydrogen phosphate [bis(2-ethylhexoxy)-oxidophosphaniumyl] phosphate ethane-1,2-diolate titanium(4+) Chemical compound [Ti+4].[O-]CC[O-].CCCCC(CC)CO[P+]([O-])(OCC(CC)CCCC)OP(O)(O)=O.CCCCC(CC)CO[P+]([O-])(OCC(CC)CCCC)OP([O-])([O-])=O KOEFSMLBFZGZLD-UHFFFAOYSA-L 0.000 claims description 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 229910021392 nanocarbon Inorganic materials 0.000 claims description 3
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 claims description 3
- 239000010452 phosphate Substances 0.000 claims description 3
- 239000012286 potassium permanganate Substances 0.000 claims description 3
- 238000012216 screening Methods 0.000 claims description 3
- 229910000077 silane Inorganic materials 0.000 claims description 3
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 3
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 3
- 229920002554 vinyl polymer Polymers 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 abstract description 5
- 230000002401 inhibitory effect Effects 0.000 abstract description 3
- 239000007921 spray Substances 0.000 abstract description 3
- 239000002253 acid Substances 0.000 abstract description 2
- 230000032683 aging Effects 0.000 abstract description 2
- 239000011248 coating agent Substances 0.000 abstract description 2
- 238000000576 coating method Methods 0.000 abstract description 2
- 238000001035 drying Methods 0.000 description 2
- 238000005187 foaming Methods 0.000 description 2
- 239000003513 alkali Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 239000011247 coating layer Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000005477 standard model Effects 0.000 description 1
Abstract
The invention discloses a kind of Uvioresistant fluorocarbon metal anti-rust paint and preparation method thereof, be made up of pulping raw material and paint raw material, the paint film that rust-inhibiting paint of the present invention is formed, have that hardness is high, damage resistant, strong adhesion, salt spray resistance, salt water resistance, acid and alkali-resistance, water-fast, oil resistant, ultraviolet light, ageing-resistant, anti-low temperature, wet-heat resisting, reusable at old coating surface, paint film can not be caused to damage, superpower paint film flexibility etc.The general paint film life-span can reach 8-10.
Description
Technical field
The present invention relates to a kind of metallic anti-rust paint, specifically a kind of Uvioresistant fluorocarbon metal anti-rust paint.
Background technology
Various mechanical means appearance all needs coating layer of metal paint, increases attractive in appearance on the one hand, on the other hand dust-proof rust resistance and corrosion resistance; Rust-inhibiting paint of the prior art, because of containing a large amount of volatile organic solvent, produces volatile gases poisonous, harmful in a large number, polluted air and infringement human health.Ubiquity weather resistance is not good, easily comes off, inadaptable complicated, severe environment.
Summary of the invention
The invention provides a kind of Uvioresistant fluorocarbon metal anti-rust paint and preparation method thereof, there is good mechanical stability, snappiness and surface hardness, good weatherability.
Technical scheme of the present invention is:
Uvioresistant fluorocarbon metal anti-rust paint, is characterized in that being made up of the feed composition of following component weight part:
Pulping raw material:
Carbon black 3-8, hexylene glycol monobutyl ether acetate 3-5,2,2,4-trimethylammonium 1,3-pentanediol mono isobutyrate 5-10, anti-sedimentation agent 3300S1-2, flow agent BYK-3001-2, polyoxyethylenated alcohol sodium sulfate 3-5, dispersion agent LBD-11-2, LBCB-1 thixotropic lubricant 1-2, polyacrylic acid sodium salt SN-50001-2, tree ash 10-15, chitosan 3-5, modified Nano diatomite in powder 5-10, modified soluble nano silicone colloidal sol 5-10;
Paint raw material:
Water-based fluorocarbon resin 25-30, myo-Inositol hexaphosphate 20-25, Ultraviolet Absorber UV-P 5-8, double cyclopentenyl polyethoxymethacrylate 3-5, propylene glycol 50-60, ethanol 50-60, hexylene glycol monobutyl ether acetate 1-2;
Modified Nano diatomite in powder is prepared by the following method:
(1), diatomite in powder add (0.8 ~ 1.2) g/L potassium permanganate solution soak 2-3 hour, pulls out, be washed to neutrality, then the sodium radio-phosphate,P-32 solution putting into 2-5% soaks, stirring reaction 3-4 hour at 60-80 DEG C;
(2) in soak solution, add the 3-4% sodium laurylsulfate, 1-2% Di(dioctylpyrophosphato) ethylene titanate, 2-3% vinyl three ('beta '-methoxy oxyethyl group) silane, the 20-25% ferrophosphorus powder that are equivalent to diatomite in powder weight, high speed dispersion 4200-4500 rev/min, 20-30 minute;
(3) dry, pulverize, make ultrafine powder;
Modified soluble nano silicone colloidal sol is prepared by the following method:
Water-soluble nanoscale silica sol adds 4-5% nano-carbon powder, 3-5% ferric oxide, is mixed and heated to 50-60 DEG C, cools after 30-40 minute.
Described Uvioresistant fluorocarbon metal anti-rust paint, is characterized in that being made up of the feed composition of following component weight part:
Pulping raw material:
Carbon black 5, hexylene glycol monobutyl ether acetate 5,2,2,4-trimethylammonium 1,3-pentanediol mono isobutyrate 10, anti-sedimentation agent 3300S2, flow agent BYK-3002, polyoxyethylenated alcohol sodium sulfate 3, dispersion agent LBD-11, LBCB-1 thixotropic lubricant 2, polyacrylic acid sodium salt SN-50002, tree ash 15, chitosan 3, modified Nano diatomite in powder 5, modified soluble nano silicone colloidal sol 5;
Paint raw material:
Water-based fluorocarbon resin 25, myo-Inositol hexaphosphate 25, Ultraviolet Absorber UV-P 5, double cyclopentenyl polyethoxymethacrylate 3, propylene glycol 60, ethanol 60, hexylene glycol monobutyl ether acetate 2.
The preparation method of described Uvioresistant fluorocarbon metal anti-rust paint, is characterized in that comprising the following steps:
(1), slurrying: pulping raw material is poured into batching kettle mixing, then mixed pulping raw material is transported in high-speed dispersing kettle and carries out stirring, disperseing 50-60 minute, rotating speed 3200-3500 rev/min, slurrying component after dispersion is transported in sand mill carries out wet type sand milling, dispersion, obtain slurry, slurry mesh-of-grind is less than or equals 40 microns;
(2) paint: add paint raw material in obtained slurry, be then transported in high-speed dispersing kettle and carry out stirring, disperseing, after dispersion, being transported in sand mill of component carries out wet type sand milling, dispersion, obtains paint vehicle; Again with 3200-3600 rev/min of high speed dispersion 40-50min;
(3) obtained paint vehicle is transported to vibrating filter to carry out filtering and screening, fineness≤40um, then the product after filtration is packed, warehouse-in.
The paint film that rust-inhibiting paint of the present invention is formed, has that hardness is high, damage resistant, strong adhesion, and salt spray resistance, salt water resistance, acid and alkali-resistance, water-fast, oil resistant are reusable at old coating surface, paint film can not be caused to damage, superpower paint film flexibility etc.The general paint film life-span can reach 8-10.
Embodiment
Uvioresistant fluorocarbon metal anti-rust paint, be made up of the feed composition of following component weight part (kilogram):
Pulping raw material:
Carbon black 5, hexylene glycol monobutyl ether acetate 5,2,2,4-trimethylammonium 1,3-pentanediol mono isobutyrate 10, anti-sedimentation agent 3300S2, flow agent BYK-3002, polyoxyethylenated alcohol sodium sulfate 3, dispersion agent LBD-11, LBCB-1 thixotropic lubricant 2, polyacrylic acid sodium salt SN-50002, tree ash 15, chitosan 3, modified Nano diatomite in powder 5, modified soluble nano silicone colloidal sol 5;
Paint raw material:
Water-based fluorocarbon resin 25, myo-Inositol hexaphosphate 25, Ultraviolet Absorber UV-P 5, double cyclopentenyl polyethoxymethacrylate 3, propylene glycol 60, ethanol 60, hexylene glycol monobutyl ether acetate 2.
Modified Nano diatomite in powder is prepared by the following method:
(1), diatomite in powder adds 0.8g/L potassium permanganate solution and soaks 2 hours, pulls out, is washed to neutrality, then the sodium radio-phosphate,P-32 solution putting into 5% soaks, stirring reaction 4 hours at 60-70 DEG C;
(2) in soak solution, add 3% sodium laurylsulfate, 2% Di(dioctylpyrophosphato) ethylene titanate, 2% vinyl three ('beta '-methoxy oxyethyl group) silane, the 20% ferrophosphorus powder that are equivalent to diatomite in powder weight, high speed dispersion 4200-4500 rev/min, 20-30 minute;
(3) dry, pulverize, make ultrafine powder;
Modified soluble nano silicone colloidal sol is prepared by the following method:
Water-soluble nanoscale silica sol adds 5% nano-carbon powder, 3% ferric oxide, and mix and blend, is heated to 50-60 DEG C, cools after 30-40 minute.
The preparation method of Uvioresistant fluorocarbon metal anti-rust paint:
(1), slurrying: pulping raw material is poured into batching kettle mixing, then mixed pulping raw material is transported in high-speed dispersing kettle and carries out stirring, disperseing 50-60 minute, rotating speed 3200-3500 rev/min, slurrying component after dispersion is transported in sand mill carries out wet type sand milling, dispersion, obtain slurry, slurry mesh-of-grind is less than or equals 40 microns;
(2) paint: add paint raw material in obtained slurry, be then transported in high-speed dispersing kettle and carry out stirring, disperseing, after dispersion, being transported in sand mill of component carries out wet type sand milling, dispersion, obtains paint vehicle; Again with 3200-3600 rev/min of high speed dispersion 40-50min;
(3) obtained paint vehicle is transported to vibrating filter to carry out filtering and screening, fineness≤40um, then the product after filtration is packed, warehouse-in.
Metallic anti-rust paint performance index of the present invention:
1, paint film color and outward appearance: flat smooth, color conformance with standard model and aberration scope
2, viscosity (23 ± 1 DEG C of coating-4 viscosity meters, S): 80-120
3, fineness≤50
4, time of drying (25 DEG C): surface drying 25-30min, 48h is done solid work
5, snappiness mm≤2
6, hardness >=2H
7, high temperature resistant (130 DEG C) >=450h
8, shock-resistance 50
9, salt spray resistance (120h level) >=2
10, water tolerance (29 ± 1 DEG C of 240h): non-foaming, does not come off
11, oil resistant (90# gasoline, 56h): non-foaming, does not come off
12, alkali resistance (GB/T9755-2001): by 48 hours
13, artificial weathering ageing resistance (GB/T9755-2001): by 1000 hours.
Claims (3)
1. a Uvioresistant fluorocarbon metal anti-rust paint, is characterized in that being made up of the feed composition of following component weight part:
Pulping raw material:
Carbon black 3-8, hexylene glycol monobutyl ether acetate 3-5,2,2,4-trimethylammonium 1,3-pentanediol mono isobutyrate 5-10, anti-sedimentation agent 3300S1-2, flow agent BYK-3001-2, polyoxyethylenated alcohol sodium sulfate 3-5, dispersion agent LBD-11-2, LBCB-1 thixotropic lubricant 1-2, polyacrylic acid sodium salt SN-50001-2, tree ash 10-15, chitosan 3-5, modified Nano diatomite in powder 5-10, modified soluble nano silicone colloidal sol 5-10;
Paint raw material:
Water-based fluorocarbon resin 25-30, myo-Inositol hexaphosphate 20-25, Ultraviolet Absorber UV-P 5-8, double cyclopentenyl polyethoxymethacrylate 3-5, propylene glycol 50-60, ethanol 50-60, hexylene glycol monobutyl ether acetate 1-2;
Modified Nano diatomite in powder is prepared by the following method:
(1), diatomite in powder add 0.8 ~ 1.2g/L potassium permanganate solution soak 2-3 hour, pulls out, be washed to neutrality, then the sodium radio-phosphate,P-32 solution putting into 2-5% soaks, stirring reaction 3-4 hour at 60-80 DEG C;
(2) in soak solution, add the 3-4% sodium laurylsulfate, 1-2% Di(dioctylpyrophosphato) ethylene titanate, 2-3% vinyl three ('beta '-methoxy oxyethyl group) silane, the 20-25% ferrophosphorus powder that are equivalent to diatomite in powder weight, high speed dispersion 4200-4500 rev/min, 20-30 minute;
(3) dry, pulverize, make ultrafine powder;
Modified soluble nano silicone colloidal sol is prepared by the following method:
Water-soluble nanoscale silica sol adds 4-5% nano-carbon powder, 3-5% ferric oxide, is mixed and heated to 50-60 DEG C, cools after 30-40 minute.
2. Uvioresistant fluorocarbon metal anti-rust paint according to claim 1, is characterized in that being made up of the feed composition of following component weight part:
Pulping raw material:
Carbon black 5, hexylene glycol monobutyl ether acetate 5,2,2,4-trimethylammonium 1,3-pentanediol mono isobutyrate 10, anti-sedimentation agent 3300S2, flow agent BYK-3002, polyoxyethylenated alcohol sodium sulfate 3, dispersion agent LBD-11, LBCB-1 thixotropic lubricant 2, polyacrylic acid sodium salt SN-50002, tree ash 15, chitosan 3, modified Nano diatomite in powder 5, modified soluble nano silicone colloidal sol 5;
Paint raw material:
Water-based fluorocarbon resin 25, myo-Inositol hexaphosphate 25, Ultraviolet Absorber UV-P 5, double cyclopentenyl polyethoxymethacrylate 3, propylene glycol 60, ethanol 60, hexylene glycol monobutyl ether acetate 2.
3. the preparation method of Uvioresistant fluorocarbon metal anti-rust paint according to claim 1, is characterized in that comprising the following steps:
(1), slurrying: pulping raw material is poured into batching kettle mixing, then mixed pulping raw material is transported in high-speed dispersing kettle and carries out stirring, disperseing 50-60 minute, rotating speed 3200-3500 rev/min, pulping raw material after dispersion is transported in sand mill and carries out wet type sand milling, dispersion, obtain slurry, slurry mesh-of-grind is less than or equals 40 microns;
(2) paint: add paint raw material in obtained slurry, be then transported in high-speed dispersing kettle and carry out stirring, disperseing, the component after dispersion is transported in sand mill carries out wet type sand milling, dispersion, obtains paint vehicle; Again with 3200-3600 rev/min of high speed dispersion 40-50min;
(3) obtained paint vehicle is transported to vibrating filter to carry out filtering and screening, fineness≤40 μm, then the product after filtration is packed, warehouse-in.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210340773.5A CN102888156B (en) | 2012-09-15 | 2012-09-15 | A kind of Uvioresistant fluorocarbon metal anti-rust paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210340773.5A CN102888156B (en) | 2012-09-15 | 2012-09-15 | A kind of Uvioresistant fluorocarbon metal anti-rust paint and preparation method thereof |
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| CN102888156B true CN102888156B (en) | 2016-01-20 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103254787A (en) * | 2013-04-17 | 2013-08-21 | 马鞍山拓锐金属表面技术有限公司 | Anti-rust oil employing acetophenone as base oil and preparation method thereof |
| CN103497597B (en) * | 2013-09-23 | 2015-09-16 | 无锡阳工机械制造有限公司 | A kind of anticorrosion coating agent of surface of steel plate |
| CN105482700A (en) * | 2015-12-15 | 2016-04-13 | 吴振宇 | Easy-to-cure wear-resisting raw lacquer coating for concentrating table and preparation method of easy-to-cure wear-resisting raw lacquer coating |
| CN105733376B (en) * | 2016-02-23 | 2018-10-30 | 广东四方威凯新材料有限公司 | Weather resistant halogen-free flame retardant anti-corrosion insulation fluorocarbon coating |
| CN107312408A (en) * | 2017-07-04 | 2017-11-03 | 合肥市大卓电力有限责任公司 | A kind of novel environment friendly paint and preparation method thereof |
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| CN102888156A (en) | 2013-01-23 |
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