CN102584355A - Method for producing organic solid fertilizer by using sludge - Google Patents

Method for producing organic solid fertilizer by using sludge Download PDF

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CN102584355A
CN102584355A CN2012100286809A CN201210028680A CN102584355A CN 102584355 A CN102584355 A CN 102584355A CN 2012100286809 A CN2012100286809 A CN 2012100286809A CN 201210028680 A CN201210028680 A CN 201210028680A CN 102584355 A CN102584355 A CN 102584355A
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mud
organic solid
fertilizer
fermentation
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李少华
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Hubei Dingxin Environmental Protection Technology Co Ltd
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Hubei Dingxin Environmental Protection Technology Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
    • Y02A40/20Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses

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Abstract

The invention relates to a production method for organic fertilizers, in particular to a method for producing organic solid fertilizers by using sludge. The method for producing organic solid fertilizers by using sludge comprises the following steps of: a) sludge collection; b) pretreatment; c) drying; d) crushing; e) fermentation; f) drying; g) packaging, warehousing and the like. The method for producing organic solid fertilizers by using sludge has the advantages that harmful bacteria such as pathogenic microbes and parasitic ova can be effectively removed, only lime powder is used in the entire production method and secondary environmental pollution is not caused. Besides, after the organic solid fertilizers are used for crops such as soybeans, wheat and corns, a better yield increasing effect can be taken.

Description

A kind of method of making organic solid fertilizer with mud
Technical field
The present invention relates to the method for manufacture of fertilizer, be specifically related to a kind of method of making organic solid fertilizer with mud.
Background technology
Mud is the flow-like material that a kind of water ratio is high, become black or chocolate, generally is the aggregate that the zoogloea that formed by multiple mikrobe and adsorbed organic matter thereof and inorganics are combined into; It is mainly derived from municipal sludge, pipe network mud, river and lake silt, industrial sludge.Along with developing rapidly of urbanization; Urban sewage treatment system perfect; The quantity discharged of various mud also increases day by day, and particularly municipal sludge has become one type of maximum mud of quantity discharged, and becoming influences the key factor that can urban construction and urban sewage treatment system normally move.Mud not only water ratio high, perishable, can send the intensive stink after rotting; It has also concentrated nutritive substances such as the most of organic matter in the sewage, nitrogen, phosphorus; Heavy metal and salt and pathogeny mikrobe of discussing and parasitic ovum etc.; If directly get into environment without reasonably handling, can have a strong impact on city appearance, water body and edatope.
Nutritive substances such as the organic matter that contains in the mud, nitrogen, phosphorus; The fertilizer that can be used for plant-growth; But because it contains harmful bacterial classifications such as pathogeny mikrobe and parasitic ovum, directly discharge in the farmland or mountain forest, can produce and make bad, the mashed root of seed development, form problems such as disease.Therefore, must just can be applied through strict processing.
Though the existing method of producing organic fertilizer from sludge material of utilizing has reached the requirement of using to a certain extent; But all need use chemical reagent in these methods; Like other reagent such as acid, alkali, not only cost is higher, and if chemical reagent can not well remove also and can cause secondary pollution.
Summary of the invention
In order to overcome above-mentioned defective, the object of the present invention is to provide a kind of method with mud manufacturing organic solid fertilizer, both made full use of the effective constituent in the mud, can prevent second environmental pollution again.
For realizing above-mentioned purpose, the technical scheme that the present invention adopted is following:
A kind of with the fertile method of mud manufacturing organic solid, it may further comprise the steps
(a) collect mud: introduce in the collecting tank after wet mud is tackled oarse-grained dregs with grid;
(b) pre-treatment: add the heavy metal extraction agent in the mud after collecting, and stir, afterwards individual hour of microwave oscillation 1-5 again;
(c) drying: the mud through after the pre-treatment is sent into drying system through travelling belt, and mud is lower than 10% along with travelling belt is dried to moisture content in drying system;
(d) pulverize: mud can produce caking in drying process, dried mud is transferred in the kibbler pulverizes;
(e) fermentation: add organic matter in the dewatered sludge after pulverizing, after mixing, add living microorganism and ferment; Fermentation time is 5-10 days, during every day stir once;
(f) oven dry: dry by the fire to 7-9 one-tenth the fertilizer after the above-mentioned fermentation completion dried;
(g) packing warehouse-in: after the oven dry, above-mentioned fertilizer is packed, warehouse-in is preserved.
In said (e) step, organic add-on accounts for the 10-20% of dewatered sludge weight, and the consumption of living microorganism is at the gross weight meta 10-20g/ ton of organic and dewatered sludge.
Said heavy metal extraction agent is one or more mixing in Hydrocerol A, sulfuric acid, the nitric acid; The consumption of heavy metal extraction agent is every cubic metre of mud of 15-20g.A kind of extraction agent be difficult to simultaneously to heavy metals all in the mud extraction effect all be best; Can select for use multiple extraction combination to use for various heavy to reach best extraction effect; So this; In the preferred scheme, the heavy metal extraction agent that the present invention added is the two or more mixing of above-mentioned several kinds of extraction agents.
Wherein dry what adopt is heated drying, and the temperature of drying system is arranged on 60-80 ℃, in oven dry, can remove harmful bacterial classifications such as pathogenic bacterium in the mud, parasitic ovum.
Preferably, organic matter of the present invention is a kind of or two or more mixing in feces of livestock and poultry, wheat bran, soyabean bran, Semen Helianthi bran, dead leaf, the stalk.
Preferably, living microorganism according to the invention is one or more mixing in enzymatic microorganism, photosynthetic bacteria, actinomycetes, vinelandii and the phosphate solubilizing bacteria.
In order to guarantee the mud oven dry evenly, in the preferred scheme, drying system of the present invention is the cylinder drying unit, realizes oven dry when travelling belt rotates around cylinder.
In order to guarantee that this fertilizer can satisfy the required various effective constituents of plant-growth, in the preferred scheme, of the present inventionly make in the fertile method of organic solid when the fermentation step with mud, in the mud of doing, adds inorganic microelement before the fermentation beginning.
Described trace element is one or more mixing in sulphur, magnesium, calcium, silicon, boron, zinc, iron and the molybdenum, and the consumption of trace element accounts for the 0.1-0.5 ‰ of fertilizer gross weight.
Compare prior art, beneficial effect of the present invention is: of the present inventionly make the fertile method of organic solid with mud and can effectively remove the harmful bacterial classifications such as pathogeny mikrobe and parasitic ovum in the mud, whole production method can not cause secondary pollution to environment.Organic solid fertile no rotten odor of the present invention in addition is used for can playing production-increasing function preferably like farm crop such as soybean, wheat, corns.
Below in conjunction with embodiment the present invention is done further explain.
Embodiment
A kind of method with mud manufacturing fertilizer, it may further comprise the steps
(a) collect mud: introduce in the collecting tank after wet mud is tackled oarse-grained dregs with grid;
(b) pre-treatment: add the heavy metal extraction agent in the mud after collecting, and stir, afterwards individual hour of microwave oscillation 1-5 again;
(c) drying: the mud through after the pre-treatment is sent into drying system through travelling belt, and mud is lower than 10% along with travelling belt is dried to moisture content in drying system;
(d) pulverize: mud can produce caking in drying process, dried mud is transferred in the kibbler pulverizes;
(e) fermentation: add organic matter in the dewatered sludge after pulverizing, after mixing, add living microorganism and ferment; Fermentation time is 5-10 days, during every day stir once;
(f) oven dry: dry by the fire to 7-9 one-tenth the fertilizer after the above-mentioned fermentation completion dried;
(g) packing warehouse-in: after the oven dry, above-mentioned fertilizer is packed, warehouse-in is preserved.
The mud that is adopted among the present invention is from Wuhan City, Hubei sewage work, and wherein argillaceous analysis situation is seen table 1:
Table 1: the shale analysis (by weight percentage) of mud
Organic (%) ?N(%) ?P(%) ?K(%) Water cut (%)
20-40 2-5 1-3 1-3 50-75
Below be concrete embodiment.
Embodiment 1
According to the step of aforementioned production method, wherein organic content is 20% in the shale, and the N constituent content is 2%, and the P constituent content is 3%, and the K constituent content is 3%, and water cut is 72%; Used heavy metal deactivator is that flyash, ground phosphate rock mix, and its consumption is every cubic metre of mud of 150g; Organic addition accounts for 20% of mud gross weight, and the addition of living microorganism is the 10g/ ton, and the time of fermentation is 5 days, baking to 9 one-tenths dried, packed for standby use afterwards.
Embodiment 2
Step according to aforementioned production method; Wherein organic content is 30% in the shale, and the N constituent content is 5%, and the P constituent content is 3%; The K constituent content is 1%; Water cut is 61%, and used heavy metal deactivator is that flyash, ground phosphate rock and the peat composed of rotten mosses mix, and its consumption is every cubic metre of mud of 180g; Organic addition accounts for 15% of mud gross weight, and the addition of living microorganism is the 15g/ ton, and the time of fermentation is 7 days, baking to 9 one-tenths dried, packed for standby use afterwards.
Embodiment 3
Step according to aforementioned production method; Wherein organic content is 40% in the shale, and the N constituent content is 3%, and the P constituent content is 1%; The K constituent content is 3%; Water cut is 53%, and used heavy metal deactivator is that flyash, ground phosphate rock and the peat composed of rotten mosses mix, and its consumption is every cubic metre of mud of 200g; Organic addition accounts for 10% of mud gross weight, and the addition of living microorganism is the 10g/ ton, and the time of fermentation is 10 days, baking to 9 one-tenths dried, packed for standby use afterwards.
The application implementation example
Organic solid fertilizer of the present invention is used for wheat, corn and cotton and does field experiment, with use commercially available composite fertilizer and do not use any fertilizer and simultaneously the plantation wheat, corn and cotton oppose than test, concrete situation see the table 2-4:
Table 2: the application implementation example is to the processing of wheat
Figure BDA0000134873790000051
Figure BDA0000134873790000061
Table 3: the application implementation example is to the processing of corn
Table 4: the application implementation example is to the processing of cotton
Figure BDA0000134873790000063
Data through table 2-4 can be found out; When the organic solid fertilizer of the mud that the method for utilizing mud to make fertilizer of the present invention is produced is applied to wheat, corn and cotton; Various data all approach the commercially available effect that composite chemical fertilizer brought, and the effect when not using any fertilizer.In addition, through the product of above-mentioned crop being carried out the content analysis of pollution element, wherein Cd≤0.02mg/kg, Hg≤0.005mg/kg, As≤0.12mg/kg, Pb≤0.05mg/kg; " the grain hygienic standard " that meets country's promulgation.

Claims (8)

1. make the fertile method of organic solid with mud for one kind, it is characterized in that: it may further comprise the steps
(a) collect mud: introduce in the collecting tank after wet mud is tackled oarse-grained dregs with grid;
(b) pre-treatment: add the heavy metal extraction agent in the mud after collecting, and stir, afterwards individual hour of microwave oscillation 1-5 again;
(c) drying: the mud through after the pre-treatment is sent into drying system through travelling belt, and mud is lower than 10% along with travelling belt is dried to moisture content in drying system;
(d) pulverize: mud can produce caking in drying process, dried mud is transferred in the kibbler pulverizes;
(e) fermentation: add organic matter in the dewatered sludge after pulverizing, after mixing, add living microorganism and ferment; Fermentation time is 5-10 days, during every day stir once;
(f) oven dry: dry by the fire to 7-9 one-tenth the fertilizer after the above-mentioned fermentation completion dried;
(g) packing warehouse-in: after the oven dry, above-mentioned fertilizer is packed, warehouse-in is preserved.
2. the method for making organic solid fertilizer with mud according to claim 1; It is characterized in that: said heavy metal extraction agent be Hydrocerol A, sulfuric acid, nitric acid, in one or more mix, the consumption of heavy metal extraction agent is every cubic metre of mud of 15-20g.
3. the method for making organic solid fertilizer with mud according to claim 2; It is characterized in that: in said (e) step; Organic add-on accounts for the 10-20% of dewatered sludge weight, and the consumption of living microorganism is at the gross weight meta 10-20g/ ton of organic and dewatered sludge.
4. according to claim 3 with the fertile method of mud manufacturing organic solid, it is characterized in that: described organic matter is a kind of or two or more mixing in Xu Qin Fen Bian ﹑ wheat bran, soyabean bran, Semen Helianthi bran, dead leaf, the stalk.
5. according to claim 4 with the fertile method of mud manufacturing organic solid, it is characterized in that: said living microorganism is one or more mixing in enzymatic microorganism, photosynthetic bacteria, actinomycetes, vinelandii and the phosphate solubilizing bacteria.
6. according to claim 1 it is characterized in that: described drying system is the cylinder drying unit with the fertile method of mud manufacturing organic solid, realizes oven dry when travelling belt rotates around cylinder.
7. the mud that utilizes according to claim 1 is made the fertile method of organic solid, it is characterized in that: in fermentation step, in dewatered sludge, add inorganic microelement before the fermentation beginning.
8. the method for making organic solid fertilizer with mud according to claim 7; It is characterized in that: described trace element is one or more mixing in sulphur, magnesium, calcium, silicon, boron, zinc, iron and the molybdenum, and the consumption of trace element accounts for the 0.1-0.5 ‰ of fertilizer gross weight.
CN2012100286809A 2012-02-09 2012-02-09 Method for producing organic solid fertilizer by using sludge Pending CN102584355A (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103340301A (en) * 2013-06-17 2013-10-09 苏州市阳澄湖现代农业发展有限公司 Special compound microorganism fish fertilizer for carp and preparation method thereof
CN103449848A (en) * 2013-08-28 2013-12-18 杨季冬 Method for producing fertilizer from sludge generated in sewage treatment
CN104291534A (en) * 2014-10-28 2015-01-21 温玉友 Urban sewage treatment device and method
CN104892153A (en) * 2015-05-27 2015-09-09 张家港市山牧新材料技术开发有限公司 Activated sludge fertilizer and preparation method thereof
CN106495941A (en) * 2016-10-14 2017-03-15 安徽格义循环经济产业园有限公司 Environment-friendly type is topdressed and preparation method thereof
CN104692959B (en) * 2015-01-29 2017-12-19 徐海军 A kind of Ecotype composite fertilizer and preparation method
CN108218557A (en) * 2017-12-19 2018-06-29 潍坊友容实业有限公司 The method that saline and alkaline improving fertilizer is prepared using river embankment mud
CN109232134A (en) * 2018-11-22 2019-01-18 孟宪英 A kind of high-efficiency environment friendly organic fertilizer and preparation method thereof
CN110950710A (en) * 2019-11-29 2020-04-03 锦西天然气化工有限责任公司 Organic fertilizer and preparation method thereof
CN113149758A (en) * 2021-04-23 2021-07-23 河海大学 Rural sludge organic fertilizer and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0396390A1 (en) * 1989-05-03 1990-11-07 Kim, Hong-gi Method for processing organic waste and apparatus therefor
CN101665376A (en) * 2009-09-11 2010-03-10 李春泉 Method for treating and comprehensively utilizing sludge after sewage treatment
CN101712579A (en) * 2009-09-15 2010-05-26 珠海园艺研究所 Method for preparing flower organic slow-release fertilizer by utilizing municipal sludge
KR20100117841A (en) * 2009-04-27 2010-11-04 김효제 Manufacturing method of organic fertilizer using sludge of water supply and drainage
CN102093098A (en) * 2011-01-13 2011-06-15 中山市祥源环保工程有限公司 Method for preparing fertilizer by using domestic sludge

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0396390A1 (en) * 1989-05-03 1990-11-07 Kim, Hong-gi Method for processing organic waste and apparatus therefor
KR20100117841A (en) * 2009-04-27 2010-11-04 김효제 Manufacturing method of organic fertilizer using sludge of water supply and drainage
CN101665376A (en) * 2009-09-11 2010-03-10 李春泉 Method for treating and comprehensively utilizing sludge after sewage treatment
CN101712579A (en) * 2009-09-15 2010-05-26 珠海园艺研究所 Method for preparing flower organic slow-release fertilizer by utilizing municipal sludge
CN102093098A (en) * 2011-01-13 2011-06-15 中山市祥源环保工程有限公司 Method for preparing fertilizer by using domestic sludge

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103340301A (en) * 2013-06-17 2013-10-09 苏州市阳澄湖现代农业发展有限公司 Special compound microorganism fish fertilizer for carp and preparation method thereof
CN103449848A (en) * 2013-08-28 2013-12-18 杨季冬 Method for producing fertilizer from sludge generated in sewage treatment
CN103449848B (en) * 2013-08-28 2015-08-12 杨季冬 A kind of mud utilizing sewage disposal to produce produces the method for fertilizer
CN104291534A (en) * 2014-10-28 2015-01-21 温玉友 Urban sewage treatment device and method
CN104692959B (en) * 2015-01-29 2017-12-19 徐海军 A kind of Ecotype composite fertilizer and preparation method
CN104892153A (en) * 2015-05-27 2015-09-09 张家港市山牧新材料技术开发有限公司 Activated sludge fertilizer and preparation method thereof
CN106495941A (en) * 2016-10-14 2017-03-15 安徽格义循环经济产业园有限公司 Environment-friendly type is topdressed and preparation method thereof
CN108218557A (en) * 2017-12-19 2018-06-29 潍坊友容实业有限公司 The method that saline and alkaline improving fertilizer is prepared using river embankment mud
CN109232134A (en) * 2018-11-22 2019-01-18 孟宪英 A kind of high-efficiency environment friendly organic fertilizer and preparation method thereof
CN110950710A (en) * 2019-11-29 2020-04-03 锦西天然气化工有限责任公司 Organic fertilizer and preparation method thereof
CN113149758A (en) * 2021-04-23 2021-07-23 河海大学 Rural sludge organic fertilizer and preparation method thereof

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Application publication date: 20120718