CN102511790A - Preparation method of aquatic protein peptide microcapsules - Google Patents
Preparation method of aquatic protein peptide microcapsules Download PDFInfo
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- CN102511790A CN102511790A CN2011103958841A CN201110395884A CN102511790A CN 102511790 A CN102511790 A CN 102511790A CN 2011103958841 A CN2011103958841 A CN 2011103958841A CN 201110395884 A CN201110395884 A CN 201110395884A CN 102511790 A CN102511790 A CN 102511790A
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Abstract
The invention relates to a preparation method of aquatic protein peptide microcapsules. The preparation method comprises the following steps that dry aquatic protein peptide is selected to be used as core materials and is subjected to ultramicro crushing treatment; 0.5 to 1 mass percent of gelatin, 1 to 2 mass percent of arabic gum and 0.5 percent to 0.8 mass percent of xanthan gum are respectively weighed, are completely dissolved through water addition and are used as wall materials through proportional mixing; the wall materials and the core materials are mixed according to a ratio of 6:1 to 7:1, and the emulsification homogenizing treatment is carried out; and the emulsified and homogenized wall materials and the core materials are subjected to spray drying, and the aquatic protein peptide microcapsules are obtained. The microcapsules obtained according to the preparation method provided by the invention have the advantages that the encapsulation efficiency is high, the palatability is good, the acid stability is good, the slow release is realized, and in addition, the digestive absorption of the peptide is not influenced. The preparation method has the advantages that the new addition of equipment is not needed, the process is reasonable, the operation is simple and convenient, and the industrial production is easy to realize.
Description
Technical field
The present invention relates to a kind of processing of edible protein, especially a kind of preparation method of aquatic product protein peptide microcapsules.
Background technology
We know that protein peptides is the material that protein is carried out enzymolysis or ferments and produce afterwards, and it has multiple biologically active.Protein peptides can directly get into human body with complete structure without digest and decompose than the protein utilization that is absorbed by the body more easily, bring into play its physiological function apace.
The native protein hydrophobic structure usually is sequestered in the native protein intramolecule; When becoming relative molecular mass to be lower than the polypeptide of 6000Da through enzyme hydrolysis; Hydrophobic structure will more exposure and go out, and these expose structure and taste bud comes in contact, thereby produce bitter taste.Directly can have a strong impact on the organoleptic quality of product as raw-food material.In addition, this type bitter peptides is because of having hydrophobic group, less stable, and the hygroscopicity of polypeptide dry powder is strong, is difficult for storage.Therefore, bitter taste is the key factor of restriction active peptide product development with stability.
How alleviating the bitter taste of protein peptides and increasing stability is a technical problem that needs to be resolved hurrily.
Summary of the invention
In order to overcome deficiency of the prior art, the present invention provides the preparation technology of a kind of technology aquatic product protein peptide microcapsules reasonable, easy and simple to handle.Adopt the resulting aquatic product protein peptide of this preparation method microcapsules, its embedding rate is high, good palatability, and acid condition is stable, slowly-releasing down, and does not influence digesting and assimilating of peptide.
The technical solution adopted for the present invention to solve the technical problems is: a kind of preparation method of aquatic product protein peptide microcapsules is characterized in that: through following process steps
Choose dry aquatic product protein peptide as core, ultramicro grinding is crossed 100 mesh sieves, and is subsequent use;
Take by weighing gelatin, Arabic gum and xanthans and add water respectively and dissolve fully, equal proportion is mixed the back as the wall material; Wherein, the mass fraction of described gelatin is 0.5-1%, and the mass fraction of Arabic gum is 1-2%, and the mass fraction of xanthans is 0.5%-0.8%;
Is the mixed of 6 ﹕ 1-7 ﹕ 1 with wall material and core according to mass ratio, carries out the emulsification homogenization processing;
With wall material after the emulsification homogenization processing and core spray-drying, get aquatic product protein peptide microcapsules; Wherein spray-dired condition: 180 ℃-200 ℃ of EATs, 80 ℃-90 ℃ of leaving air temps, charging rate 30-50mL/min.
Said core is the resultant protein peptides with physiologically active of various aquatic product protein hydrolysis.
The present invention adopts the ultramicro grinding method that aquatic product protein peptide core is carried out pulverization process; And the compound that adopts gelatin, Arabic gum, xanthans is as compound wall materials; With wall material parcel core, form that embedding rate height, good palatability, absolute acid stability are good, the aquatic product protein peptide microencapsulated product of slowly-releasing through spray drying process.Through measuring: the embedding rate of prepared microcapsule is more than 90%.The present invention carries out microcapsules with the aquatic product protein peptide to handle, and covered that it is bitter and prototype structure that do not destroy protein peptides is distinguished the flavor of with BA, do not influence digesting and assimilating of peptide.The present invention carries out embedding treatment when accomplishing drying process, do not need newly added equipment, reasonable, easy and simple to handle, the easy suitability for industrialized production that realizes of its technology.
The specific embodiment
Below in conjunction with embodiment the present invention is further specified.
Embodiment 1
A kind of preparation method of aquatic product protein peptide microcapsules, the process following process steps:
Choose dry jellyfish protein peptide powder as core, ultramicro grinding is crossed 100 mesh sieves, and is subsequent use;
Take by weighing gelatin, Arabic gum and xanthans and add water by mass fraction 0.5%, 1%, 0.5% respectively and dissolve fully, equal proportion is mixed, as the wall material;
Is the mixed of 6 : 1 with wall material and core according to mass ratio, carries out the emulsification homogenization processing;
With wall material after the emulsification homogenization processing and core spray-drying, get jellyfish protein peptides microcapsules; Wherein spray-dired condition: 180 ℃ of EATs, 80 ℃ of leaving air temps, charging rate 50mL/min.
By the microcapsule embedded rate of the resulting jellyfish protein peptides of this preparation method is 90%, and at the pH3.0 good stability.
Embodiment 2
A kind of preparation method of aquatic product protein peptide microcapsules, the process following process steps:
Choose dry abalone protein peptide powder as core, ultramicro grinding is crossed 100 mesh sieves, and is subsequent use;
Take by weighing gelatin, Arabic gum and xanthans and add water by mass fraction 1%, 2%, 0.8% respectively and dissolve fully, equal proportion is mixed, as the wall material;
Is the mixed of 7 : 1 with wall material and core according to mass ratio, carries out the emulsification homogenization processing;
With wall material after the emulsification homogenization processing and core spray-drying, get abalone protein peptides microcapsules; Wherein spray-dired condition: 185 ℃ of EATs, 85 ℃ of leaving air temps, charging rate 40mL/min.
By the microcapsule embedded rate of the resulting abalone protein peptides of this preparation method is more than 92%, and at the pH3.0 good stability.
Embodiment 3
A kind of preparation method of aquatic product protein peptide microcapsules, the process following process steps:
Choose dry sardine protein peptide powder as core, ultramicro grinding is crossed 100 mesh sieves, and is subsequent use;
Take by weighing gelatin, Arabic gum and xanthans and add water by mass fraction 1%, 1%, 0.8% respectively and dissolve fully, equal proportion is mixed, as the wall material;
Is the mixed of 6 : 1 with wall material and core according to mass ratio, carries out the emulsification homogenization processing;
With wall material after the emulsification homogenization processing and core spray-drying, get sardine protein peptides microcapsules; Wherein spray-dired condition: 190 ℃ of EATs, 90 ℃ of leaving air temps, charging rate 30mL/min.
By the microcapsule embedded rate of the resulting sardine protein peptides of this preparation method is 91%, and at the pH3.0 good stability.
Embodiment 4
A kind of preparation method of aquatic product protein peptide microcapsules, the process following process steps:
Choose dry scallop protein peptide powder as core, ultramicro grinding is crossed 100 mesh sieves, and is subsequent use;
Take by weighing gelatin, Arabic gum and xanthans and add water by mass fraction 0.8%, 1.5%, 0.7% respectively and dissolve fully, equal proportion is mixed, as the wall material;
Is the mixed of 6.5 : 1 with wall material and core according to mass ratio, carries out the emulsification homogenization processing;
With wall material after the emulsification homogenization processing and core spray-drying, get scallop protein peptides microcapsules; Wherein spray-dired condition: 200 ℃ of EATs, 90 ℃ of leaving air temps, charging rate 50mL/min.
By the microcapsule embedded rate of the resulting scallop protein peptides of this preparation method is 91.5%, and at the pH3.0 good stability.
Claims (2)
1. the preparation method of aquatic product protein peptide microcapsules is characterized in that: through following process steps:
Choose dry aquatic product protein peptide as core, ultramicro grinding is crossed 100 mesh sieves, and is subsequent use;
Take by weighing gelatin, Arabic gum and xanthans and add water respectively and dissolve fully, equal proportion is mixed the back as the wall material; Wherein, the mass fraction of described gelatin is 0.5-1%, and the mass fraction of Arabic gum is 1-2%, and the mass fraction of xanthans is 0.5%-0.8%;
Is the mixed of 6 ﹕ 1-7 ﹕ 1 with wall material and core according to mass ratio, carries out the emulsification homogenization processing;
With wall material after the emulsification homogenization processing and core spray-drying, get aquatic product protein peptide microcapsules; Wherein spray-dired condition: 180 ℃-200 ℃ of EATs, 80 ℃-90 ℃ of leaving air temps, charging rate 30-50mL/min.
2. the preparation method of a kind of aquatic product protein peptide microcapsules according to claim 1 is characterized in that: said core is the resultant protein peptides with physiologically active of various aquatic product protein hydrolysis.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103404854A (en) * | 2013-08-02 | 2013-11-27 | 合肥工业大学 | Preparation method of phytosterol ester microcapsules |
| CN103919255A (en) * | 2014-04-03 | 2014-07-16 | 广东润科生物工程有限公司 | Microcapsule embedding method for protein peptide |
| CN107751646A (en) * | 2017-11-08 | 2018-03-06 | 浙江恒兴饲料有限公司 | A kind of special antibacterial additive of aquatic products and its production method |
| CN108576371A (en) * | 2018-03-30 | 2018-09-28 | 大连工业大学 | A kind of microcapsule embedded double protein peptide and preparation method thereof |
| CN109315665A (en) * | 2018-09-14 | 2019-02-12 | 合肥工业大学 | A kind of Functional Polypeptides microcapsules solid beverage and preparation method thereof |
| CN111227257A (en) * | 2020-01-15 | 2020-06-05 | 润科生物工程（福建）有限公司 | Industrial method for refining spirulina protein peptide and spray drying microencapsulation |
| CN114668092A (en) * | 2022-04-14 | 2022-06-28 | 江苏天美健大自然生物工程有限公司 | Fish collagen dipeptide fruit-flavored drink and preparation method thereof |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107998224A (en) * | 2017-12-29 | 2018-05-08 | 武汉市天辰生物科技有限公司 | A kind of aquatic products anti virus herb slow-releasing granules and preparation method |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103404854A (en) * | 2013-08-02 | 2013-11-27 | 合肥工业大学 | Preparation method of phytosterol ester microcapsules |
| CN103919255A (en) * | 2014-04-03 | 2014-07-16 | 广东润科生物工程有限公司 | Microcapsule embedding method for protein peptide |
| CN103919255B (en) * | 2014-04-03 | 2015-09-30 | 广东润科生物工程有限公司 | A kind of microcapsule embedded method of protein peptides |
| CN107751646A (en) * | 2017-11-08 | 2018-03-06 | 浙江恒兴饲料有限公司 | A kind of special antibacterial additive of aquatic products and its production method |
| CN108576371A (en) * | 2018-03-30 | 2018-09-28 | 大连工业大学 | A kind of microcapsule embedded double protein peptide and preparation method thereof |
| CN109315665A (en) * | 2018-09-14 | 2019-02-12 | 合肥工业大学 | A kind of Functional Polypeptides microcapsules solid beverage and preparation method thereof |
| CN111227257A (en) * | 2020-01-15 | 2020-06-05 | 润科生物工程（福建）有限公司 | Industrial method for refining spirulina protein peptide and spray drying microencapsulation |
| CN114668092A (en) * | 2022-04-14 | 2022-06-28 | 江苏天美健大自然生物工程有限公司 | Fish collagen dipeptide fruit-flavored drink and preparation method thereof |
| CN114668092B (en) * | 2022-04-14 | 2023-11-17 | 江苏天美健大自然生物工程有限公司 | Fish collagen dipeptide fruit flavored beverage and preparation method thereof |
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| CN102511790B (en) | 2013-07-24 |
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