CN102464933A - Fiber-reinforced high-temperature-resistant thermal insulation and heat preserving ceramic coating and preparation method thereof - Google Patents
Fiber-reinforced high-temperature-resistant thermal insulation and heat preserving ceramic coating and preparation method thereof Download PDFInfo
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- CN102464933A CN102464933A CN2010105477714A CN201010547771A CN102464933A CN 102464933 A CN102464933 A CN 102464933A CN 2010105477714 A CN2010105477714 A CN 2010105477714A CN 201010547771 A CN201010547771 A CN 201010547771A CN 102464933 A CN102464933 A CN 102464933A
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Abstract
The invention relates to a high-temperature-resistant thermal insulation and heat preserving ceramic coating and a preparation method thereof. The coating is prepared from the following raw materials in percentage by weight: 30-50 percent of film forming substance, 30-40 percent of high-temperature-resistant filler, 10-15 percent of hollow micro beads, 2-5 percent of thermal insulation fiber and 2-8 percent of aid and solvent. The coating has the toughness of an organic coating and the rigidity and hardness of an inorganic coating, has high adhesion, can be used at the high temperature of 400-1,200 DEG C for a long time, and is resistant to chemical reagents, acids, alkalis and oil. A coating film has high surface intensity, and can bear strong shear force without being damaged when a high-temperature pipeline is required to be connected mechanically. The coating has excellent heat preserving performance, and the surface temperature of a pipeline of 350 DEG C can be lowered to be below 100 DEG C by coating the coating outside the pipeline in the thickness of 4-6 millimeters. The coating can be widely applied to heat-resistant protection of the inner and outer surfaces of equipment such as high-temperature steam pipelines, metallurgy high-temperature furnaces, high-temperature valves, high-temperature containers and the like.
Description
Technical field
The present invention is a kind of coating, relates in particular to a kind of fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating and preparation method thereof, belongs to field of heat insulating materials.
Background technology
The thermostable heat insulation thermal insulation coatings is a lot of both at home and abroad at present; Being applied to the thermal insulating coating of high temperature service (place) a kind of is to be base-material with the organic resin; Dose the organic and inorganic composite coating that inorganic thermal insulating filling is processed; General temperature resistant range is below 300 ℃, soft, the flexible or toughness of this type coating matter.A kind of is mineral-type coating, can anti-400 ℃~1300 ℃ high temperature, and this type coating nearly all is the rigidity hard, does not almost have toughness, and it is hard and crisp to film, and the coating machine poor performance is prone to be full of cracks, efflorescence, peels off.If be used for the heat insulating of pyritous pipeline; When especially pipeline needs mechanical attachment; Though organic and inorganic compound coating flexible but because of the heat resistance difference is not suitable for though inorganic coating can high temperature resistant fragility because of filming, can't bear mechanical powerful shearing force and destroyed.
Summary of the invention
The problem that the present invention belongs to solution is the deficiency that overcomes prior art; A kind of novel fibre-reinforced can under 400~1200 ℃ of environment, use for a long time is provided, and has the coating surface strength height, can bear heat-insulation and heat-preservation ceramic coating of powerful mechanical shear stress and preparation method thereof.
Technical problem to be solved by this invention realizes through following technological approaches:
Coating adopts following component and proportioning:
Filmogen 30~50%, high temperature resistant filler 30~40%, hollow beads 10~15%, heat insulation fiber 2~10%, auxiliary agent and solvent 2~8%.
Described filmogen specifically is selected from the combination of one of epoxy resin, silicone resin, resol, inorganic high-temperature resistant glue or two kinds of materials.
Described high temperature resistant filler is the combination of several kinds of materials in white titanium pigment, pure aluminium silicate, wilkinite, talcum powder, kaolin, coarse whiting, mica powder, aerosil powder, zirconium white, zinc oxide, aluminum oxide, pearlstone, vermiculite power, the zeyssatite.
Described hollow ceramic microballon is one of hollow glass micropearl, hollow ceramic microspheres, and particle diameter requires in the 0.01-400 micrometer range.
Described heat insulation fiber is the combination of one or more materials in thomel, spun glass, sapphire whisker, aluminum silicate fiber, the aluminosilicate fiber cotton.
Described auxiliary agent and solvent are dispersion agent, skimmer, thickening material, multifunctional regulator, coupling agent, thinner.Wherein dispersion agent is a SN-DISPERSANT5027 polycarboxylate sodium type dispersion agent; Skimmer is a GEORGE G7 silicone skimmer; Thickening material is a S-936 modification alkali swelling type thickening material; Multifunctional regulator is the AMP-5 multifunctional assistant, and coupling agent is N-β-(aminoethyl)-γ-An Bingjisanjiayangjiguiwan, and thinner is an epoxy chloropropane.Above auxiliary agent all can have been bought in market, and its specification meets chemical standard.
The preparation method of fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating of the present invention is following:
(1) various dispersion agents, skimmer are joined in the reaction kettle mix in proportion, stir;
(2) in proportion various high temperature resistant fillers are joined in the reaction kettle, high-speed stirring adds coupling agent simultaneously, stirs, and processes slip; Add multifunctional regulator, regulating slip pH value is 8~10;
(3) in slip, add fiber, high-speed stirring and blue-type mulling make fiber homodisperse in slip;
Add filmogen, add coupling agent, thinner or thickening material, the adjustment slip is to suitable viscosity;
(4) add hollow beads, stirring at low speed mixes, and makes fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating.
The present invention has following advantage:
1, fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating of the present invention adopts heat insulation fiber as enhancing substance, when coating part fiber when mixing is dispersion state coating is played enhancement; Another part forms bulk, because the thermal conductivity of fiber own is low, so when hot-fluid runs into the fiber of bulk; Shunting can appear in coating; Make the bang path of hot-fluid in coating just long and just complicated, cause the heat transfer property of coating to descend, can intercept the conduction of heat effectively.The thermal conductivity of coating is 0.0057W/M.K.
2, the present invention adopts unique filmogen, and the bonding force of coating can be reached more than 2500 newton, and once shaped thickness can reach 4~6mm, and coating surface strength is high, can bear powerful mechanical shear stress.
3, as thermal insulating filling, ducted body is light, thermal capacity is low because cenosphere has with hollow beads in the present invention, and thermal conductivity is little, and reflecting light can form the vacuum cavity crowd in coating consumingly; Rutile type Titanium Dioxide also has the scattering process of visible light all wavelengths intensive; And mica powder and talcum powder can form lamellated material, have selected for use pure aluminium silicate and kaolin as stopping composition simultaneously, can be clipped in the gap of cenosphere.These fillers are when forming coating more than 300 ℃, and coating generation physics, chemical transformation form a lot of small honey-combeds, are in vacuum or partial vacuum state in the honeycomb, stop flowing of thermo-molecular, thereby have constituted ideal thermodynamic barrier layer.
Fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating of the present invention has wide range of applications, and can be used for the insulation, metallurgical with various high-temperature furnace bodies, high temperature valve of heating power transport pipe, the high-temp liquid transmission pipeline of the hot steam of petroleum recovering notes steam pipe, chemical industry etc.Needing to be particularly useful for the place of powerful mechanical shear stress of opposing and anti-impact force.
Embodiment
Embodiment 1
1, take by weighing each raw material by following weight ratio:
Epoxy resin and resol 35%, zirconium white 10%, white titanium pigment 10%, coarse whiting 10%, pure aluminium silicate 5%, wilkinite 4%, skimmer and dispersion agent 1%, coupling agent 2%, hollow glass microbead 10%, ceramic fiber 10%, thinner or thickening material 3%.
2, it is following to adopt above proportioning to prepare the method for fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating:
Skimmer added in the reaction kettle with dispersion agent in proportion mix, stir; Add zirconium white, white titanium pigment, coarse whiting, pure aluminium silicate, wilkinite successively, add coupling agent, stir, process slip, adjustment slip pH value is 8~10.In slip, add ceramic fiber, carry out high-speed stirring and blue-type mulling, make ceramic fiber homodisperse in slip; The mixture that adds epoxy resin and resol adds thinner or thickening material, and the adjustment slip is to suitable viscosity; Add hollow glass microbead, stirring at low speed mixes, and makes fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating.
Embodiment 2
1, take by weighing each raw material by following weight ratio:
Silicone resin and inorganic high-temp glue 40%, pure aluminium silicate 8%, talcum powder 8%, aluminum oxide 4%, pearlstone 2%, zinc oxide 6%, zeyssatite 5.5%, hollow glass microbead 8%, spun glass 15%, dispersion agent and skimmer 1.5%, coupling agent 2%.
2, it is following to adopt above proportioning to prepare the method for fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating:
Skimmer added in the reaction kettle with dispersion agent in proportion mix, stir; Add pure aluminium silicate, talcum powder, aluminum oxide, pearlstone, zinc oxide, zeyssatite successively, add coupling agent, stir, process slip; In slip, add spun glass, carry out high-speed stirring and blue-type mulling, make spun glass homodisperse in slip; The mixture that adds silicone resin and inorganic high-temp glue adds thinner or thickening material, and the adjustment slip is to suitable viscosity; Add hollow glass microbead, stirring at low speed mixes, and makes fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating.
Embodiment 3
1, take by weighing each raw material by following weight ratio:
Inorganic high-temp glue 35%, zirconium white 5%, white titanium pigment 10%, pure aluminium silicate 10%, mica powder 10%, wilkinite 4%, aluminum oxide 6%, hollow ceramic microballon 10%, thomel 5%, skimmer 3%, coupling agent 2%.
2, it is following to adopt above proportioning to prepare the method for fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating:
Skimmer added in the reaction kettle with dispersion agent in proportion mix, stir; Add zirconium white, white titanium pigment, pure aluminium silicate, mica powder, wilkinite, aluminum oxide successively, add coupling agent, stir, process slip; In slip, add thomel, carry out high-speed stirring and blue-type mulling, make thomel homodisperse in slip; Add inorganic high-temp glue and thinner or thickening material, the adjustment slip is to suitable viscosity; Add the hollow ceramic microballon, stirring at low speed mixes, and makes fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating.
3, embodiments of the invention 1, embodiment 2, embodiment 3 are carried out the thermostable heat insulation performance test.Testing method adopts the testing method of international SY/T5324-94.Coating is coated on the outer wall of high-temperature pipe equably, and coating thickness is 6mm, and the pipe interior temperature is 350 ℃.
Resistant high temperature insulating heat insulation test result of the present invention
Embodiment 1: 56 ℃ of the temperature of high-temperature pipe outer wall behind the insulation 6mm, thermal conductivity 0.00572.
Embodiment 2: 58 ℃ of the temperature of high-temperature pipe outer wall behind the insulation 6mm, thermal conductivity 0.00573.
Embodiment 3: 57 ℃ of the temperature of high-temperature pipe outer wall behind the insulation 6mm, thermal conductivity 0.00572.
Claims (6)
1. fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating is characterized in that, raw material is made up of following weight percent:
Filmogen 30~50%, high temperature resistant filler 30~40%, hollow beads 10~15%, heat insulation fiber 2~5%, auxiliary agent and solvent 8~10%.
2. fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating according to claim 1; It is characterized in that described high temperature resistant filler is selected from one or more the combination in mica powder, white titanium pigment, pure aluminium silicate, wilkinite, talcum powder, kaolin, coarse whiting, aerosil powder, zeyssatite, vermiculite power, pearlstone, zirconium white, zinc oxide, the aluminum oxide.
3. fiber reinforced high-temperature-resistant heat insulating coatings according to claim 1 is characterized in that described hollow beads is selected from hollow glass micropearl, hollow ceramic microspheres, is the hollow circular microballoon of particle diameter 0.01-400 micron.
4. fiber reinforced high-temperature-resistant heat insulating coatings according to claim 1 is characterized in that described heat insulation fiber is one or more the combination in thomel, spun glass, sapphire whisker, aluminum silicate fiber, the aluminosilicate fiber cotton.
5. fiber reinforced high-temperature-resistant heat insulating coatings according to claim 1 is characterized in that described auxiliary agent and solvent are one or more the combination in dispersion agent, skimmer, coupling agent, multifunctional regulator, thinner, the thickening material.
6. fiber reinforced high-temperature-resistant heat insulating coatings according to claim 1 is characterized in that described step is following: various dispersion agents, skimmer are joined in the reaction kettle mix in proportion, stir;
(1) in proportion various high temperature resistant fillers are joined in the reaction kettle, high-speed stirring adds coupling agent simultaneously, stirs, and processes slip; Add multifunctional regulator, regulating slip pH value is 8~10;
(2) in slip, add fiber, high-speed stirring and blue-type mulling make fiber homodisperse in slip;
(3) add filmogen, add coupling agent, thinner or thickening material, the adjustment slip is to suitable viscosity;
(4) add hollow beads, stirring at low speed mixes, and makes fiber reinforced high-temperature-resistant heat-insulation and heat-preservation ceramic coating.
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