CN102352188A - Precision cerium-zirconium-based solid solution rare earth polishing powder and preparation method thereof - Google Patents
Precision cerium-zirconium-based solid solution rare earth polishing powder and preparation method thereof Download PDFInfo
- Publication number
- CN102352188A CN102352188A CN201110261047XA CN201110261047A CN102352188A CN 102352188 A CN102352188 A CN 102352188A CN 201110261047X A CN201110261047X A CN 201110261047XA CN 201110261047 A CN201110261047 A CN 201110261047A CN 102352188 A CN102352188 A CN 102352188A
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- Prior art keywords
- cerium
- zirconium
- solution
- iron
- salt
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- 238000005498 polishing Methods 0.000 title claims abstract description 40
- 239000000843 powder Substances 0.000 title claims abstract description 34
- 229910052761 rare earth metal Inorganic materials 0.000 title claims abstract description 28
- 150000002910 rare earth metals Chemical class 0.000 title claims abstract description 27
- RCFVMJKOEJFGTM-UHFFFAOYSA-N cerium zirconium Chemical compound [Zr].[Ce] RCFVMJKOEJFGTM-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000006104 solid solution Substances 0.000 title claims abstract description 17
- 229910000420 cerium oxide Inorganic materials 0.000 claims abstract description 10
- BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 9
- 239000000725 suspension Substances 0.000 claims abstract description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 40
- 229910052684 Cerium Inorganic materials 0.000 claims description 23
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 20
- 229910052742 iron Inorganic materials 0.000 claims description 20
- 229910052726 zirconium Inorganic materials 0.000 claims description 20
- 239000012266 salt solution Substances 0.000 claims description 15
- 150000003839 salts Chemical class 0.000 claims description 14
- 239000000243 solution Substances 0.000 claims description 13
- 239000000047 product Substances 0.000 claims description 12
- 235000012538 ammonium bicarbonate Nutrition 0.000 claims description 11
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 10
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 claims description 9
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 claims description 9
- 239000001099 ammonium carbonate Substances 0.000 claims description 9
- 238000001035 drying Methods 0.000 claims description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 5
- 239000004575 stone Substances 0.000 claims description 5
- MVFCKEFYUDZOCX-UHFFFAOYSA-N iron(2+);dinitrate Chemical compound [Fe+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O MVFCKEFYUDZOCX-UHFFFAOYSA-N 0.000 claims description 4
- OERNJTNJEZOPIA-UHFFFAOYSA-N zirconium nitrate Chemical compound [Zr+4].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O OERNJTNJEZOPIA-UHFFFAOYSA-N 0.000 claims description 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 3
- HSJPMRKMPBAUAU-UHFFFAOYSA-N cerium(3+);trinitrate Chemical compound [Ce+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O HSJPMRKMPBAUAU-UHFFFAOYSA-N 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 229910017604 nitric acid Inorganic materials 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 238000000975 co-precipitation Methods 0.000 claims description 2
- 230000008021 deposition Effects 0.000 claims description 2
- 238000009413 insulation Methods 0.000 claims description 2
- 150000002823 nitrates Chemical class 0.000 claims description 2
- 239000002244 precipitate Substances 0.000 claims description 2
- 238000001556 precipitation Methods 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 claims 10
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 abstract description 8
- 230000003287 optical effect Effects 0.000 abstract description 3
- 239000004973 liquid crystal related substance Substances 0.000 abstract description 2
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 abstract 1
- 229910001928 zirconium oxide Inorganic materials 0.000 abstract 1
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 description 13
- 239000008367 deionised water Substances 0.000 description 4
- 229910021641 deionized water Inorganic materials 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 230000018044 dehydration Effects 0.000 description 3
- 238000006297 dehydration reaction Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- GHLITDDQOMIBFS-UHFFFAOYSA-H cerium(3+);tricarbonate Chemical compound [Ce+3].[Ce+3].[O-]C([O-])=O.[O-]C([O-])=O.[O-]C([O-])=O GHLITDDQOMIBFS-UHFFFAOYSA-H 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- XJUNLJFOHNHSAR-UHFFFAOYSA-J zirconium(4+);dicarbonate Chemical compound [Zr+4].[O-]C([O-])=O.[O-]C([O-])=O XJUNLJFOHNHSAR-UHFFFAOYSA-J 0.000 description 2
- 229910004625 Ce—Zr Inorganic materials 0.000 description 1
- VPJQDYNOVJRQLN-UHFFFAOYSA-N [O-2].[La+3].[Ce+3].[F].[O-2].[O-2] Chemical compound [O-2].[La+3].[Ce+3].[F].[O-2].[O-2] VPJQDYNOVJRQLN-UHFFFAOYSA-N 0.000 description 1
- ACDVTYWYUIVEPE-UHFFFAOYSA-N [Pr+3].[O-2].[La+3].[Ce+3].[F] Chemical compound [Pr+3].[O-2].[La+3].[Ce+3].[F] ACDVTYWYUIVEPE-UHFFFAOYSA-N 0.000 description 1
- 239000003082 abrasive agent Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000005357 flat glass Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- CMOAHYOGLLEOGO-UHFFFAOYSA-N oxozirconium;dihydrochloride Chemical compound Cl.Cl.[Zr]=O CMOAHYOGLLEOGO-UHFFFAOYSA-N 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000007517 polishing process Methods 0.000 description 1
- -1 rare earth fluoride Chemical class 0.000 description 1
- 229910001404 rare earth metal oxide Inorganic materials 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
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CN 201110261047 CN102352188B (en) | 2011-09-05 | 2011-09-05 | Precision cerium-zirconium-based solid solution rare earth polishing powder and preparation method thereof |
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CN 201110261047 CN102352188B (en) | 2011-09-05 | 2011-09-05 | Precision cerium-zirconium-based solid solution rare earth polishing powder and preparation method thereof |
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CN102352188A true CN102352188A (en) | 2012-02-15 |
CN102352188B CN102352188B (en) | 2013-08-07 |
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103450811A (en) * | 2013-01-10 | 2013-12-18 | 湖南皓志新材料股份有限公司 | Preparation method of aluminium-doped cerium-zirconium solid-solution polishing powder |
CN103694956A (en) * | 2013-12-27 | 2014-04-02 | 福达合金材料股份有限公司 | Mixed powder capable of rapidly removing punched burrs from sheet-type electrical contact and use method of mixed powder |
CN103773312A (en) * | 2013-12-27 | 2014-05-07 | 福达合金材料股份有限公司 | Mixed powder for rapidly removing forged burrs of rivet electrical contact and application method thereof |
CN104130716A (en) * | 2014-07-01 | 2014-11-05 | 安徽拓普森电池有限责任公司 | Polishing fluid for optical lenses and preparation method thereof |
CN106010298A (en) * | 2016-06-29 | 2016-10-12 | 上海华明高纳稀土新材料有限公司 | Zirconium oxide polishing solution and preparation method thereof |
CN104130716B (en) * | 2014-07-01 | 2016-11-30 | 张连江 | A kind of polishing fluid for optical glass and preparation method thereof |
CN107201178A (en) * | 2017-05-27 | 2017-09-26 | 于长江 | A kind of preparation method of cerium praseodymium stabilizing zirconia polishing powder |
CN111019529A (en) * | 2019-12-30 | 2020-04-17 | 中国科学院长春光学精密机械与物理研究所 | Magnetic jet polishing solution and preparation method thereof |
US11161751B2 (en) | 2017-11-15 | 2021-11-02 | Saint-Gobain Ceramics & Plastics, Inc. | Composition for conducting material removal operations and method for forming same |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1583260A (en) * | 2004-05-28 | 2005-02-23 | 清华大学 | Nano cerium and zirconium based oxide with transition elements added and its preparation |
CN101010402A (en) * | 2004-09-03 | 2007-08-01 | 昭和电工株式会社 | Mixed rare earth oxide, mixed rare earth fluoride, cerium-based abrasive using the materials and production processes thereof |
-
2011
- 2011-09-05 CN CN 201110261047 patent/CN102352188B/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1583260A (en) * | 2004-05-28 | 2005-02-23 | 清华大学 | Nano cerium and zirconium based oxide with transition elements added and its preparation |
CN101010402A (en) * | 2004-09-03 | 2007-08-01 | 昭和电工株式会社 | Mixed rare earth oxide, mixed rare earth fluoride, cerium-based abrasive using the materials and production processes thereof |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103450811A (en) * | 2013-01-10 | 2013-12-18 | 湖南皓志新材料股份有限公司 | Preparation method of aluminium-doped cerium-zirconium solid-solution polishing powder |
CN103694956A (en) * | 2013-12-27 | 2014-04-02 | 福达合金材料股份有限公司 | Mixed powder capable of rapidly removing punched burrs from sheet-type electrical contact and use method of mixed powder |
CN103773312A (en) * | 2013-12-27 | 2014-05-07 | 福达合金材料股份有限公司 | Mixed powder for rapidly removing forged burrs of rivet electrical contact and application method thereof |
CN103694956B (en) * | 2013-12-27 | 2015-06-24 | 福达合金材料股份有限公司 | Mixed powder capable of rapidly removing punched burrs from sheet-type electrical contact and use method of mixed powder |
CN104130716A (en) * | 2014-07-01 | 2014-11-05 | 安徽拓普森电池有限责任公司 | Polishing fluid for optical lenses and preparation method thereof |
CN104130716B (en) * | 2014-07-01 | 2016-11-30 | 张连江 | A kind of polishing fluid for optical glass and preparation method thereof |
CN106010298A (en) * | 2016-06-29 | 2016-10-12 | 上海华明高纳稀土新材料有限公司 | Zirconium oxide polishing solution and preparation method thereof |
CN107201178A (en) * | 2017-05-27 | 2017-09-26 | 于长江 | A kind of preparation method of cerium praseodymium stabilizing zirconia polishing powder |
CN107201178B (en) * | 2017-05-27 | 2018-03-06 | 泰安麦丰新材料科技有限公司 | A kind of preparation method of cerium praseodymium stabilizing zirconia polishing powder |
US11161751B2 (en) | 2017-11-15 | 2021-11-02 | Saint-Gobain Ceramics & Plastics, Inc. | Composition for conducting material removal operations and method for forming same |
CN111019529A (en) * | 2019-12-30 | 2020-04-17 | 中国科学院长春光学精密机械与物理研究所 | Magnetic jet polishing solution and preparation method thereof |
CN111019529B (en) * | 2019-12-30 | 2021-07-06 | 中国科学院长春光学精密机械与物理研究所 | Magnetic jet polishing solution and preparation method thereof |
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CN102352188B (en) | 2013-08-07 |
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GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
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Denomination of invention: Precision cerium zirconium based solid solution rare earth polishing powder and its preparation method Effective date of registration: 20220620 Granted publication date: 20130807 Pledgee: Industrial Bank Co.,Ltd. Shanghai Songjiang sub branch Pledgor: SHANGHAI HUAMING GONA RARE EARTH NEW MATERIALS Co.,Ltd. Registration number: Y2022310000067 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20230625 Granted publication date: 20130807 Pledgee: Industrial Bank Co.,Ltd. Shanghai Songjiang sub branch Pledgor: SHANGHAI HUAMING GONA RARE EARTH NEW MATERIALS Co.,Ltd. Registration number: Y2022310000067 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Precise cerium zirconium based Solid solution rare earth polishing powder and its preparation method Effective date of registration: 20230627 Granted publication date: 20130807 Pledgee: Industrial Bank Co.,Ltd. Shanghai Songjiang sub branch Pledgor: SHANGHAI HUAMING GONA RARE EARTH NEW MATERIALS Co.,Ltd. Registration number: Y2023310000314 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20130807 Pledgee: Industrial Bank Co.,Ltd. Shanghai Songjiang sub branch Pledgor: SHANGHAI HUAMING GONA RARE EARTH NEW MATERIALS Co.,Ltd. Registration number: Y2023310000314 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right |