CN102241714A - 甜菊糖生产工艺 - Google Patents

甜菊糖生产工艺 Download PDF

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CN102241714A
CN102241714A CN2011101410211A CN201110141021A CN102241714A CN 102241714 A CN102241714 A CN 102241714A CN 2011101410211 A CN2011101410211 A CN 2011101410211A CN 201110141021 A CN201110141021 A CN 201110141021A CN 102241714 A CN102241714 A CN 102241714A
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CN102241714B (zh
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徐君
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Jiangsu Steven Biotechnology Co ltd
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Abstract

本发明涉及一种甜菊糖生产工艺。本发明在浸泡时加入阻止剂。本发明的有益效果是：是在浸泡提取时加入阻止剂，阻止了在浸泡时鞣质的浸出，减少了后半部对鞣质及酸中溶解物的处理；本发明的阻止剂优先选用醋酸，因醋酸是弱酸，污染小，阻止性能好。

Description

甜菊糖生产工艺
技术领域
本发明涉及一种甜菊糖生产工艺。
背景技术
目前，公知的是用水40倍浸泡，后加氧化钙，三氯化铁复盐，板框压滤，再进树脂柱脱盐，脱色，吸附，酸洗，碱洗，醇洗，酒精解脱，浓缩，干燥。提取时用水量大，复盐时污染大损耗大，用酸量大，成本上升。
发明内容
本发明针对上述缺陷，目的在于提供一种工序简单、污染小的甜菊糖生产工艺。
本发明所采用的技术方案是：本发明在甜叶菊浸泡时加入阻止剂。
所述阻止剂为醋酸。
所述醋酸浓度为1-3％。
本发明按照以下步骤进行：先用浓度为1.5％的醋酸水浸泡，共四次，每次为甜叶菊重量的6倍，浸泡完毕后，提取浸提液经纳滤膜过滤，纳滤出液反复套用，纳滤后纳滤截留液进入脱色柱脱色、然后进行吸附、碱洗、醇洗、酒精解脱、浓缩、干燥而成。
本发明的有益效果是：是在浸泡提取时加入阻止剂，阻止了在浸泡时鞣质的浸出，减少了后半部对鞣质及酸中溶解物的处理；本发明的阻止剂优先选用醋酸，因醋酸是有机弱酸，的酸性适中，污染小，阻止性能好
具体实施方式
实施例一
本发明先加入浓度为1.5％的醋酸水，每公斤料加六公斤水，浸泡1小时，反复四次。浸泡完毕后，提取浸提液经纳滤膜过滤，纳滤出液反复套用，纳滤截留液进入脱色柱脱色、然后进行吸附、碱洗、醇洗、酒精解脱、浓缩、干燥而成。
实施例二
本发明同样可加入浓度为1.5％的盐酸水，其它步骤同实施例一。

Claims (4)

1.甜菊糖生产工艺，其特征在于，甜叶菊浸泡时加入阻止剂。
2.根据权利要求1所述的甜菊糖生产工艺，其特征在于，所述阻止剂为醋酸。
3.根据权利要求2所述的甜菊糖生产工艺，其特征在于，所述醋酸浓度为1-3％。
4.根据权利要求1至3所述的甜菊糖生产工艺，其特征在于，按照以下步骤进行：先用浓度为1.5％的醋酸水浸泡，浸泡完毕后，提取浸提液经纳滤膜纳滤，纳滤出液反复套用，纳滤截留液进入脱色柱脱色、然后进行吸附、碱洗、醇洗、酒精解脱、浓缩、干燥而成。
CN201110141021.1A 2011-05-30 2011-05-30 甜菊糖生产工艺 Expired - Fee Related CN102241714B (zh)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102977163A (zh) * 2012-12-17 2013-03-20 晨光生物科技集团股份有限公司 甜菊糖的工业化制备方法
CN106722839A (zh) * 2016-12-05 2017-05-31 桂林莱茵生物科技股份有限公司 一种罗汉果苦味剂的制作方法
CN107118243A (zh) * 2017-06-05 2017-09-01 江苏史蒂文生物科技有限公司 一种甜菊糖的工业制备方法
CN109354596A (zh) * 2018-10-09 2019-02-19 山东奥晶生物科技有限公司 一种高效甜菊糖苷的制备方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101805768A (zh) * 2010-03-01 2010-08-18 江苏健佳药业有限公司 高品质甜菊糖生物酶解提纯方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101805768A (zh) * 2010-03-01 2010-08-18 江苏健佳药业有限公司 高品质甜菊糖生物酶解提纯方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
傅长明等: "植物单宁的性质及应用", 《应用技术》, no. 22, 31 December 2010 (2010-12-31), pages 57 - 60 *
汪继成: "《农副产品加工新技术问答》", 31 August 1993, article "101.怎样从甜叶菊中提取甜菊糖甙", pages: 132-133 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102977163A (zh) * 2012-12-17 2013-03-20 晨光生物科技集团股份有限公司 甜菊糖的工业化制备方法
CN102977163B (zh) * 2012-12-17 2015-07-22 晨光生物科技集团股份有限公司 甜菊糖的工业化制备方法
CN106722839A (zh) * 2016-12-05 2017-05-31 桂林莱茵生物科技股份有限公司 一种罗汉果苦味剂的制作方法
CN107118243A (zh) * 2017-06-05 2017-09-01 江苏史蒂文生物科技有限公司 一种甜菊糖的工业制备方法
CN107118243B (zh) * 2017-06-05 2020-06-19 江苏史蒂文生物科技有限公司 一种甜菊糖的工业制备方法
CN109354596A (zh) * 2018-10-09 2019-02-19 山东奥晶生物科技有限公司 一种高效甜菊糖苷的制备方法

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