CN102066544A - 喷雾干燥方法 - Google Patents

喷雾干燥方法 Download PDF

Info

Publication number: CN102066544A
Authority: CN; China
Prior art keywords: weight; detersive surfactant; spray; anionic detersive; alkaline slurry
Prior art date: 2008-06-25
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Pending

Application number

CN2009801246576A

Other languages

English (en)

Chinese (zh)

Inventor

H·H·坦塔维

N·P·索默维尔罗伯茨

S·豪

S·A·考德威尔

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Procter and Gamble Ltd

Procter and Gamble Co

Original Assignee

Procter and Gamble Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2008-06-25

Filing date

2009-06-25

Publication date

2011-05-18

2009-06-25 Application filed by Procter and Gamble Ltd filed Critical Procter and Gamble Ltd

2011-05-18 Publication of CN102066544A publication Critical patent/CN102066544A/zh

Status Pending legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 21
238000001694 spray drying Methods 0.000 title claims abstract description 18
239000002002 slurry Substances 0.000 claims abstract description 70
239000004094 surface-active agent Substances 0.000 claims abstract description 68
125000000129 anionic group Chemical group 0.000 claims abstract description 62
239000000843 powder Substances 0.000 claims abstract description 51
239000000203 mixture Substances 0.000 claims abstract description 44
239000002243 precursor Substances 0.000 claims abstract description 22
238000005507 spraying Methods 0.000 claims abstract description 20
229910021536 Zeolite Inorganic materials 0.000 claims abstract description 15
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 15
239000010457 zeolite Substances 0.000 claims abstract description 15
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
229910019142 PO4 Inorganic materials 0.000 claims abstract description 9
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 9
239000010452 phosphate Substances 0.000 claims abstract description 9
230000002378 acidificating effect Effects 0.000 claims description 20
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 12
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 11
238000001035 drying Methods 0.000 claims description 6
SRSXLGNVWSONIS-UHFFFAOYSA-M benzenesulfonate Chemical compound [O-]S(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-M 0.000 claims description 3
239000002253 acid Substances 0.000 abstract description 5
239000007921 spray Substances 0.000 abstract description 4
238000004519 manufacturing process Methods 0.000 abstract 1
150000004760 silicates Chemical class 0.000 abstract 1
-1 carboxylate salt Chemical class 0.000 description 19
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 14
239000003599 detergent Substances 0.000 description 14
239000000463 material Substances 0.000 description 7
239000002245 particle Substances 0.000 description 7
235000017550 sodium carbonate Nutrition 0.000 description 7
229910000029 sodium carbonate Inorganic materials 0.000 description 7
239000007787 solid Substances 0.000 description 7
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 7
UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 6
238000002360 preparation method Methods 0.000 description 6
229910021653 sulphate ion Inorganic materials 0.000 description 6
239000003945 anionic surfactant Substances 0.000 description 5
150000003839 salts Chemical class 0.000 description 5
239000003795 chemical substances by application Substances 0.000 description 4
238000005660 chlorination reaction Methods 0.000 description 4
239000000975 dye Substances 0.000 description 4
239000004744 fabric Substances 0.000 description 4
239000007788 liquid Substances 0.000 description 4
239000011368 organic material Substances 0.000 description 4
125000001453 quaternary ammonium group Chemical group 0.000 description 4
238000005406 washing Methods 0.000 description 4
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
239000013543 active substance Substances 0.000 description 3
150000001768 cations Chemical class 0.000 description 3
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
238000007046 ethoxylation reaction Methods 0.000 description 3
JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 3
239000011734 sodium Substances 0.000 description 3
229910052708 sodium Inorganic materials 0.000 description 3
235000017557 sodium bicarbonate Nutrition 0.000 description 3
229910000030 sodium bicarbonate Inorganic materials 0.000 description 3
NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 2
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
239000006057 Non-nutritive feed additive Substances 0.000 description 2
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
239000012190 activator Substances 0.000 description 2
125000005599 alkyl carboxylate group Chemical group 0.000 description 2
239000012752 auxiliary agent Substances 0.000 description 2
239000007844 bleaching agent Substances 0.000 description 2
125000002091 cationic group Chemical group 0.000 description 2
150000001875 compounds Chemical class 0.000 description 2
229920001577 copolymer Polymers 0.000 description 2
JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 description 2
238000005187 foaming Methods 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 2
229910052739 hydrogen Inorganic materials 0.000 description 2
239000001257 hydrogen Substances 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
238000005304 joining Methods 0.000 description 2
238000002156 mixing Methods 0.000 description 2
238000012986 modification Methods 0.000 description 2
230000004048 modification Effects 0.000 description 2
238000005502 peroxidation Methods 0.000 description 2
229940044652 phenolsulfonate Drugs 0.000 description 2
235000019353 potassium silicate Nutrition 0.000 description 2
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical group [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 2
229910052938 sodium sulfate Inorganic materials 0.000 description 2
235000011152 sodium sulphate Nutrition 0.000 description 2
235000019832 sodium triphosphate Nutrition 0.000 description 2
239000000126 substance Substances 0.000 description 2
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 2
OSSNTDFYBPYIEC-UHFFFAOYSA-N 1-ethenylimidazole Chemical compound C=CN1C=CN=C1 OSSNTDFYBPYIEC-UHFFFAOYSA-N 0.000 description 1
239000004382 Amylase Substances 0.000 description 1
108010065511 Amylases Proteins 0.000 description 1
102000013142 Amylases Human genes 0.000 description 1
NOWKCMXCCJGMRR-UHFFFAOYSA-N Aziridine Chemical compound C1CN1 NOWKCMXCCJGMRR-UHFFFAOYSA-N 0.000 description 1
102100032487 Beta-mannosidase Human genes 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
239000004215 Carbon black (E152) Substances 0.000 description 1
229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
108010059892 Cellulase Proteins 0.000 description 1
108090000790 Enzymes Proteins 0.000 description 1
102000004190 Enzymes Human genes 0.000 description 1
108010029541 Laccase Proteins 0.000 description 1
239000004367 Lipase Substances 0.000 description 1
102000004882 Lipase Human genes 0.000 description 1
108090001060 Lipase Proteins 0.000 description 1
WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 description 1
102000035195 Peptidases Human genes 0.000 description 1
108091005804 Peptidases Proteins 0.000 description 1
102000003992 Peroxidases Human genes 0.000 description 1
229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
101710194948 Protein phosphatase PhpP Proteins 0.000 description 1
BGRWYDHXPHLNKA-UHFFFAOYSA-N Tetraacetylethylenediamine Chemical compound CC(=O)N(C(C)=O)CCN(C(C)=O)C(C)=O BGRWYDHXPHLNKA-UHFFFAOYSA-N 0.000 description 1
230000002411 adverse Effects 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
239000003513 alkali Substances 0.000 description 1
150000004996 alkyl benzenes Chemical class 0.000 description 1
125000005600 alkyl phosphonate group Chemical group 0.000 description 1
235000019418 amylase Nutrition 0.000 description 1
108010055059 beta-Mannosidase Proteins 0.000 description 1
239000001045 blue dye Substances 0.000 description 1
230000005587 bubbling Effects 0.000 description 1
108010089934 carbohydrase Proteins 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
239000001768 carboxy methyl cellulose Substances 0.000 description 1
235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
239000008112 carboxymethyl-cellulose Substances 0.000 description 1
229940106157 cellulase Drugs 0.000 description 1
239000001913 cellulose Substances 0.000 description 1
229920002678 cellulose Polymers 0.000 description 1
239000004927 clay Substances 0.000 description 1
239000011248 coating agent Substances 0.000 description 1
239000008199 coating composition Substances 0.000 description 1
238000000576 coating method Methods 0.000 description 1
238000004040 coloring Methods 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
238000001816 cooling Methods 0.000 description 1
238000005202 decontamination Methods 0.000 description 1
230000003588 decontaminative effect Effects 0.000 description 1
239000002270 dispersing agent Substances 0.000 description 1
230000000694 effects Effects 0.000 description 1
230000007613 environmental effect Effects 0.000 description 1
229940088598 enzyme Drugs 0.000 description 1
239000002979 fabric softener Substances 0.000 description 1
238000005189 flocculation Methods 0.000 description 1
230000016615 flocculation Effects 0.000 description 1
230000004907 flux Effects 0.000 description 1
239000006260 foam Substances 0.000 description 1
239000007789 gas Substances 0.000 description 1
230000005484 gravity Effects 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
230000007062 hydrolysis Effects 0.000 description 1
238000006460 hydrolysis reaction Methods 0.000 description 1
150000002460 imidazoles Chemical class 0.000 description 1
150000003949 imides Chemical class 0.000 description 1
239000004615 ingredient Substances 0.000 description 1
239000003112 inhibitor Substances 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
235000019421 lipase Nutrition 0.000 description 1
230000014759 maintenance of location Effects 0.000 description 1
150000004702 methyl esters Chemical class 0.000 description 1
235000010755 mineral Nutrition 0.000 description 1
239000011707 mineral Substances 0.000 description 1
238000012544 monitoring process Methods 0.000 description 1
RWQQPWQEDFZMDH-UHFFFAOYSA-N n-acetyl-n-methylnonanamide Chemical compound CCCCCCCCC(=O)N(C)C(C)=O RWQQPWQEDFZMDH-UHFFFAOYSA-N 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
125000001402 nonanoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
238000006384 oligomerization reaction Methods 0.000 description 1
230000003287 optical effect Effects 0.000 description 1
239000001048 orange dye Substances 0.000 description 1
108010087558 pectate lyase Proteins 0.000 description 1
HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 1
108040007629 peroxidase activity proteins Proteins 0.000 description 1
150000004965 peroxy acids Chemical class 0.000 description 1
229920000075 poly(4-vinylpyridine) Polymers 0.000 description 1
229920000768 polyamine Polymers 0.000 description 1
229920000728 polyester Polymers 0.000 description 1
229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
239000001267 polyvinylpyrrolidone Substances 0.000 description 1
235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
239000001047 purple dye Substances 0.000 description 1
150000003856 quaternary ammonium compounds Chemical class 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
238000012216 screening Methods 0.000 description 1
MWNQXXOSWHCCOZ-UHFFFAOYSA-L sodium;oxido carbonate Chemical compound [Na+].[O-]OC([O-])=O MWNQXXOSWHCCOZ-UHFFFAOYSA-L 0.000 description 1
PANBYUAFMMOFOV-UHFFFAOYSA-N sodium;sulfuric acid Chemical compound [Na].OS(O)(=O)=O PANBYUAFMMOFOV-UHFFFAOYSA-N 0.000 description 1
239000008247 solid mixture Substances 0.000 description 1
235000013599 spices Nutrition 0.000 description 1
238000006277 sulfonation reaction Methods 0.000 description 1
238000012546 transfer Methods 0.000 description 1
UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 1
239000002912 waste gas Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Detergent Compositions (AREA)

CN2009801246576A 2008-06-25 2009-06-25 喷雾干燥方法 Pending CN102066544A (zh)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
EP08159025A EP2138565A1 (en)	2008-06-25	2008-06-25	A spray-drying process
EP08159025.9		2008-06-25
PCT/US2009/048559 WO2009158449A1 (en)	2008-06-25	2009-06-25	A spray-drying process

Publications (1)

Publication Number	Publication Date
CN102066544A true CN102066544A (zh)	2011-05-18

Family

ID=40328756

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CN2009801246576A Pending CN102066544A (zh)	2008-06-25	2009-06-25	喷雾干燥方法

Country Status (7)

Country	Link
EP (1)	EP2138565A1 (pt)
JP (1)	JP2011525215A (pt)
CN (1)	CN102066544A (pt)
BR (1)	BRPI0914675A2 (pt)
CA (1)	CA2726023A1 (pt)
MX (1)	MX2010014505A (pt)
WO (1)	WO2009158449A1 (pt)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN114717029A (zh) *	2021-07-06	2022-07-08	湖北清合新能源科技有限公司	一种高效抗静电汽油添加剂及其制备方法

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EP3153425B1 (en)	2015-10-06	2018-07-04	The Procter and Gamble Company	Flexible box bag comprising detergent powder and a scoop
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US11214763B2 (en)	2018-01-26	2022-01-04	Ecolab Usa Inc.	Solidifying liquid amine oxide, betaine, and/or sultaine surfactants with a carrier
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BR112020015098A2 (pt)	2018-01-26	2020-12-08	Ecolab Usa Inc.	Composição de tensoativo líquido solidificado, método para preparar uma composição de tensoativo solidificado e para limpar uma superfície, e, composição sólida de limpeza.
EP3546560A1 (en)	2018-03-28	2019-10-02	The Procter & Gamble Company	Laundry detergent composition
EP3546557B1 (en)	2018-03-28	2020-10-07	The Procter & Gamble Company	Catalase inhibition during a laundering process
MX2020010114A (es)	2018-03-28	2020-11-06	Procter & Gamble	Proceso para preparar una particula detergente secada por aspersion para lavanderia.
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- 2009-06-25 CN CN2009801246576A patent/CN102066544A/zh active Pending
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JP2011525215A (ja)	2011-09-15
CA2726023A1 (en)	2009-12-30
MX2010014505A (es)	2011-02-22
EP2138565A1 (en)	2009-12-30
BRPI0914675A2 (pt)	2015-10-20

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2015-12-23	C12	Rejection of a patent application after its publication
2015-12-23	RJ01	Rejection of invention patent application after publication	Application publication date: 20110518

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