CN102010633A - Dye-type non-dry watercolor ink and manufacturing method thereof - Google Patents
Dye-type non-dry watercolor ink and manufacturing method thereof Download PDFInfo
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- CN102010633A CN102010633A CN2010106117792A CN201010611779A CN102010633A CN 102010633 A CN102010633 A CN 102010633A CN 2010106117792 A CN2010106117792 A CN 2010106117792A CN 201010611779 A CN201010611779 A CN 201010611779A CN 102010633 A CN102010633 A CN 102010633A
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Abstract
The invention provides a dye-type non-dry watercolor ink composition, which comprises the following components in part by weight: (a) 0.5 to 7.0 parts of dye, (b) 10.0 to 15.0 parts of moisturizing agent, (c) 0.05 to 0.3 part of antiseptic and mildew-proof agent, (d) 0.1 to 0.5 part of auxiliary agent and (e) 77.2 to 84.35 parts of water, wherein the components (a) to (e) account for 95 to 100 percent of the total weight of the composition; the (b) moisturizing agent is a compound moisturizing agent consisting of two moisturizing agents, wherein the first moisturizing agent is may be one or more of glycerol, ethylene glycol, propylene glycol, polyethylene glycol, diethylene glycol, triethylene glycol and sorbitol; the second moisturizing agent is selected from one or more of sodium lactate, hyaluronic acid, pyrrolidone carboxylic acid, natural moisturizing factor (NMF) and amino acid; and the weight ratio of the first moisturizing agent to the second moisturizing agent is (2-3): 1.
Description
Technical field
The present invention relates to a kind of ink and manufacture method thereof, relate to a kind of dye-type not color ink of solid carbon dioxide and manufacture method thereof particularly.
Background technology
The watercolor ink is a kind of low viscosity color inks of the children's of being used for paintbrush, and it has the moisture foot, and is bright in luster, slim and graceful lucid and lively characteristics.The use object of watercolor pencil mainly is young children, and they often forget in a process and cover the cap for brush, thereby is easy to cause nib dry, can't use.The major cause that causes this problem is that common watercolor ink moisture retention is poor.
In sum, this area lacks and to open under the cap state the not color ink of solid carbon dioxide of the lasting dye-type of not doing of nib.Therefore, this area presses for exploitation and is opening under the cap state the lasting dye-type color ink of solid carbon dioxide not of not doing and having the good level of normal line of nib.
Summary of the invention
It is good that first purpose of the present invention is to obtain a kind of humidity-holding effect, opening under the cap state the lasting dye-type color composition for ink of solid carbon dioxide not of not doing and having the good level of normal line of nib.
It is good that second purpose of the present invention is to obtain a kind of humidity-holding effect, opening under the cap state the lasting dye-type color ink of solid carbon dioxide not of not doing and having the good level of normal line of nib.
It is good that the 3rd purpose of the present invention is to obtain a kind of humidity-holding effect, opening under the cap state the lasting dye-type preparation method of the color ink of solid carbon dioxide not who does not do and have the good level of normal line of nib.
In a first aspect of the present invention, the not color composition for ink of solid carbon dioxide of a kind of dye-type is provided, it comprises following component:
(a) dyestuff 0.5-7.0 weight part,
(b) wetting Agent for Printing Inks 10.0-15.0 weight part,
(c) Antisepticize and mildew preventive 0.05-0.3 weight part,
(d) auxiliary agent 0.1-0.5 weight part,
(e) water 77.2-84.35 weight part;
The weight summation of above-mentioned (a)～(e) component accounts for 95～100% of composition total weight;
Described (b) wetting Agent for Printing Inks is the composite wetting Agent for Printing Inks that two groups of wetting Agent for Printing Inkss combine, and first group of wetting Agent for Printing Inks is selected from one or more of glycerine, ethylene glycol, propylene glycol, polyoxyethylene glycol, glycol ether, triglycol, sorbyl alcohol; Second group of wetting Agent for Printing Inks is selected from one or more in Sodium.alpha.-hydroxypropionate, hyaluronic acid, pyrrolidone carboxylic acid, natural moisturizing factor (NMF), the amino acid; And the weight ratio of first group of wetting Agent for Printing Inks and second group of wetting Agent for Printing Inks is (2～3): 1.
In a specific embodiment of the present invention, described (a) dyestuff is selected from water-soluble dye.
In a specific embodiment of the present invention, described dyestuff is selected from substantive dyestuff, matching stain, reactive dyestuffs.
In a specific embodiment of the present invention, described dyestuff is selected from Acid Blue 7, acid blue 9, Blue VRS, sun blue 199, sun blue 106, acid red 87, acid red 18, acid yellow 23 or its combination.
A second aspect of the present invention provides the not color ink of solid carbon dioxide of dye-type that a kind of composition of the present invention makes.
A third aspect of the present invention provides the not preparation method of the color ink of solid carbon dioxide of a kind of described dye-type, comprises the steps:
(1) provides dyestuff 0.5-7.0 weight part, wetting Agent for Printing Inks 10.0-15.0 weight part, Antisepticize and mildew preventive 0.05-0.3 weight part, auxiliary agent 0.1-0.5 weight part, (e) deionized water 77.2-84.35 weight part;
The weight summation of above-mentioned (a)～(e) component accounts for 95～100% of composition total weight;
Described (b) wetting Agent for Printing Inks is the composite wetting Agent for Printing Inks that two groups of wetting Agent for Printing Inkss combine, and first group of wetting Agent for Printing Inks is selected from one or more of glycerine, ethylene glycol, propylene glycol, polyoxyethylene glycol, glycol ether, triglycol, sorbyl alcohol; Second group of wetting Agent for Printing Inks is selected from one or more in Sodium.alpha.-hydroxypropionate, hyaluronic acid, pyrrolidone carboxylic acid, natural moisturizing factor (NMF), the amino acid; And the weight ratio of first group of wetting Agent for Printing Inks and second group of wetting Agent for Printing Inks is (2～3): 1;
(2) described wetting Agent for Printing Inks, fungusproof anti-corrosion agent, auxiliary agent are mixed with water;
(3) after stirring fully, add described dyestuff, and restir fully obtains the not color ink of solid carbon dioxide of described dye-type.
In a specific embodiment of the present invention, described (a) dyestuff is selected from water-soluble dye.
In a specific embodiment of the present invention, described dyestuff is selected from substantive dyestuff, matching stain, reactive dyestuffs.
In a specific embodiment of the present invention, described dyestuff is selected from Acid Blue 7, acid blue 9, Blue VRS, sun blue 199, sun blue 106, acid red 87, acid red 18, acid yellow 23 or its combination.
Embodiment
The research that inventor's process is extensive and deep by improvement preparation technology, has obtained to open the ink of the lasting good level of not doing, normally ruling of nib under the cap state.Finished the present invention on this basis.
As used herein, described " watercolor ink " except as otherwise noted, refers to the water-base ink of viscosity between 2-5cps.Particularly, watercolor ink of the present invention is a type of dye ink, and " dye-type " is meant that coloring material is a dye granule.
As used herein, described " humidity-holding effect is good " except as otherwise noted, refers under room temperature state ink and keeps not doing, specifically test determines as described later.
Other aspects of the present invention are because the disclosure of this paper is conspicuous to those skilled in the art.
Raw material of the present invention all can obtain or conventional synthetic method prepares by commercially available.
Below each component of the present invention is elaborated.
Specify as nothing, various raw materials of the present invention all can obtain by commercially available; Or prepare according to the ordinary method of this area.Unless otherwise defined or explanation, same meanings of being familiar with of all specialties used herein and scientific words and those skilled in the art.Any in addition method similar or impartial to described content and material all can be applicable in the inventive method.
Dyestuff
Dyestuff of the present invention is not particularly limited, only otherwise goal of the invention of the present invention is produced restriction to get final product.
Preferably, in order to reach water-soluble good purpose, select acidity or substantive dyestuff for use.For example, can select Acid Blue 7, acid blue 9, Blue VRS, sun blue 199, sun blue 106, acid red 87, acid red 18, acid yellow 23 etc. for use.The consumption of dyestuff is not particularly limited, only otherwise goal of the invention of the present invention is produced restriction to get final product.If consumption is too high, can cause the dyestuff cohesion, stop up nib; If consumption is low excessively, ink color insufficient strength then, writing color and luster dimness.Comparatively suitable, the consumption of dyestuff is at the 0.5-7.0% weight part.(this moment, wetting Agent for Printing Inks content was that 10.0-15.0 weight part, fungus-proof antisepsis agent content are that 0.05-0.3 weight part, auxiliary agent content are that 0.1-0.5 weight part, deionized water content are the 77.2-84.35 weight part)
Wetting Agent for Printing Inks
Wetting Agent for Printing Inks of the present invention is specific composite component.
Preferably, the described lubricant of preserving moisture is selected from one or more in glycerine, ethylene glycol, propylene glycol, Macrogol 200, poly(oxyethylene glycol) 400, poly(oxyethylene glycol) 400, polyoxyethylene glycol 800, glycol ether, triglycol, sorbyl alcohol, Sodium.alpha.-hydroxypropionate, hyaluronic acid, pyrrolidone carboxylic acid, natural moisturizing factor, the amino acid.
The contriver finds, when (b) wetting Agent for Printing Inks be two groups of wetting Agent for Printing Inkss combine composite wetting Agent for Printing Inks the time, the humidity-holding effect that obtains is excellent especially, in order to achieve the above object, first group of wetting Agent for Printing Inks is selected from one or more of glycerine, ethylene glycol, propylene glycol, polyoxyethylene glycol, glycol ether, triglycol, sorbyl alcohol; Second group of wetting Agent for Printing Inks is selected from one or more in Sodium.alpha.-hydroxypropionate, hyaluronic acid, pyrrolidone carboxylic acid, natural moisturizing factor (NMF), the amino acid; And the weight ratio of first group of wetting Agent for Printing Inks and second group of wetting Agent for Printing Inks is (2～3): 1.Wherein first group is the polyalcohols wetting Agent for Printing Inks; Second group is the wetting ability wetting Agent for Printing Inks.The polyalcohols humidity-holding effect is easily affected by environment, and ambient moisture is crossed when hanging down, and keeping the water molecules effect can descend, and long-time humidity-holding effect is undesirable; Hydrophilic class wetting Agent for Printing Inks absorbs combination with it behind the moisture, no matter under low humidity still is high humidity, all has identical water absorbability, thereby has guaranteed the non-drying of ink of the present invention.
The consumption of wetting Agent for Printing Inks of the present invention is the 10.0-15.0 weight part.(this moment, dyestuff content was that 0.5-7.0 weight part, fungus-proof antisepsis agent content are that 0.05-0.3 weight part, auxiliary agent content are that 0.1-0.5 weight part, deionized water content are the 77.2-84.35 weight part)
Antisepticize and mildew preventive
Antisepticize and mildew preventive of the present invention is not particularly limited, only otherwise goal of the invention of the present invention is produced restriction to get final product.
Particularly for example, Antisepticize and mildew preventive of the present invention is selected from Rocima623, Kathon LXE, ProxelXL2, benzotriazole or its combination.Preferably, be selected from Kathon LXE, benzotriazole or its combination.Above-mentioned Antisepticize and mildew preventive is the commercially available product that gets, and for example, described Rocima623, Kathon LXE can be available from Rhom and Hass, and described Proxel XL2 is available from Britain Allied Colloids Ltd.
Antisepticize and mildew preventive consumption of the present invention is the 0.05-0.3 weight part.(this moment, dyestuff content was that 0.5-7.0 weight part, wetting Agent for Printing Inks content are that 10.0-15.0 weight part, auxiliary agent content are that 0.1-0.5 weight part, deionized water content are the 77.2-84.35 weight part)
Auxiliary agent
Auxiliary agent of the present invention is not particularly limited, only otherwise goal of the invention of the present invention is produced restriction to get final product.
Particularly, auxiliary agent of the present invention is selected from (also being tween and peregal) such as TW-20, OPE-9Q, OPE-20.
Auxiliary dosage of the present invention is the 0.1-0.5 weight part.(this moment, dyestuff content was that 0.5-7.0 weight part, wetting Agent for Printing Inks content are that 10.0-15.0 weight part, Antisepticize and mildew preventive content are that 0.05-0.3 weight part, deionized water content are the 77.2-84.35 weight part)
The used peregal of the present invention is a class fatty alcohol-polyoxyethylene ether, and it can use chemical formula RO-(CH
2CH
2O)
n-H represents (R represents alkyl, and n represents positive integer, for example 3,8,9,10,15,20,25,30,35).Particularly preferably be peregal 0-10, peregal 0-15, peregal 0-20, peregal 0-25.
Deionized water
Deionized water consumption of the present invention is the 77.2-84.35 weight part.(this moment, dyestuff content was that 0.5-7.0 weight part, wetting Agent for Printing Inks content are that 10.0-15.0 weight part, fungus-proof antisepsis agent content are that 0.05-0.3 weight part, auxiliary agent content are the 0.1-0.5 weight part)
Composition
In the composition for ink of the present invention, weight (a)-(e) accounts for the 95-100% of gross weight.Described (a)-(e) component is also promptly: (a) dyestuff, (b) wetting Agent for Printing Inks, (c) Antisepticize and mildew preventive, (d) auxiliary agent, (e) deionized water.
In above-mentioned composition, can also contain other auxiliary agent of 0～5%, with watercolor composition for ink total weight.The kind and the composition of described auxiliary agent are not particularly limited, only otherwise goal of the invention of the present invention is produced restriction to get final product.
Other aspects of the present invention are because the disclosure of this paper is conspicuous to those skilled in the art.
Below in conjunction with specific embodiment, further set forth the present invention.Should be understood that these embodiment only to be used to the present invention is described and be not used in and limit the scope of the invention.The experimental technique of unreceipted actual conditions in the following example is measured according to national standard usually.If there is not a corresponding national standards, then carry out according to general international standard, normal condition or according to the condition that manufacturer advises.Unless otherwise indicated, otherwise all umbers are weight part, and all per-cents are weight percentage, and described polymericular weight is a number-average molecular weight.
Unless otherwise defined or explanation, same meanings of being familiar with of all specialties used herein and scientific words and those skilled in the art.Any in addition method similar or impartial to described content and material all can be applicable in the inventive method.
Preparation embodiment 1
80.35 gram water, 10 gram glycerine, 5 gram pyrrolidone carboxylic acids, 0.5 gram TW-20,0.3 gram KathonLXE agent joined have in the reactor that the slurry formula stirs, stir; Under stirring at low speed, slowly add 3.85 gram acid blue 9s then, after adding, improve rotating speed and stir.Filter at last and get product.
Preparation embodiment 2
82.2 gram water, 10 gram glycerine, 5 gram amino acid, 0.5 gram TW-20,0.3 gram Proxel XL2 agent joined have in the reactor that the slurry formula stirs, stir; Under stirring at low speed, slowly add 2.0 gram acid red 18s then, after adding, improve rotating speed and stir.Filter at last and get product.
Preparation embodiment 3
82.7 gram water, 10 gram glycerine, 5 gram Sodium.alpha.-hydroxypropionates, 0.5 gram TW-20,0.3 gram Kathon LXE agent joined have in the reactor that the slurry formula stirs, stir; Under stirring at low speed, slowly add 1.5 gram acid yellow 23s then, after adding, improve rotating speed and stir.Filter at last and get product.
Performance embodiment
Ink with the foregoing description 1～3 is made maca pen, and at 25 ℃, under the condition of humidity 50%-70%, nib was opened cap more than three months, and nib keeps not doing, and normally goes out China ink and writes.Commercially available ink was placed three days under this test condition, and nib becomes dry, and can not write.
The above only is preferred embodiment of the present invention, be not in order to limit essence technology contents scope of the present invention, essence technology contents of the present invention is broadly to be defined in the claim scope of application, any technology entity or method that other people finish, if it is defined identical with the claim scope of application, also or a kind of change of equivalence, all will be regarded as being covered by among this claim scope.
All quote in this application as a reference at all documents that the present invention mentions, just quoted as a reference separately as each piece document.Should be understood that in addition after having read foregoing of the present invention, those skilled in the art can make various changes or modifications the present invention, these equivalent form of values fall within the application's appended claims institute restricted portion equally.
Claims (9)
1. a dye-type color composition for ink of solid carbon dioxide not is characterized in that, comprises following component:
(a) dyestuff 0.5-7.0 weight part,
(b) wetting Agent for Printing Inks 10.0-15.0 weight part,
(c) Antisepticize and mildew preventive 0.05-0.3 weight part,
(d) auxiliary agent 0.1-0.5 weight part,
(e) water 77.2-84.35 weight part;
The weight summation of above-mentioned (a)～(e) component accounts for 95～100% of composition total weight;
Described (b) wetting Agent for Printing Inks is the composite wetting Agent for Printing Inks that two groups of wetting Agent for Printing Inkss combine, and first group of wetting Agent for Printing Inks is selected from one or more of glycerine, ethylene glycol, propylene glycol, polyoxyethylene glycol, glycol ether, triglycol, sorbyl alcohol; Second group of wetting Agent for Printing Inks is selected from one or more in Sodium.alpha.-hydroxypropionate, hyaluronic acid, pyrrolidone carboxylic acid, natural moisturizing factor (NMF), the amino acid; And the weight ratio of first group of wetting Agent for Printing Inks and second group of wetting Agent for Printing Inks is (2～3): 1.
2. composition as claimed in claim 1 is characterized in that, described (a) dyestuff is selected from water-soluble dye.
3. composition as claimed in claim 2 is characterized in that described dyestuff is selected from substantive dyestuff, matching stain, reactive dyestuffs.
4. composition as claimed in claim 3 is characterized in that, described dyestuff is selected from Acid Blue 7, acid blue 9, Blue VRS, sun blue 199, sun blue 106, acid red 87, acid red 18, acid yellow 23 or its combination.
5. a dye-type that makes as the described composition of the claim 1～4 color ink of solid carbon dioxide not.
6. a dye-type as claimed in claim 5 preparation method of the color ink of solid carbon dioxide not comprises the steps:
(1) provides dyestuff 0.5-7.0 weight part, wetting Agent for Printing Inks 10.0-15.0 weight part, Antisepticize and mildew preventive 0.05-0.3 weight part, auxiliary agent 0.1-0.5 weight part, (e) deionized water 77.2-84.35 weight part;
The weight summation of above-mentioned (a)～(e) component accounts for 95～100% of composition total weight;
Described (b) wetting Agent for Printing Inks is the composite wetting Agent for Printing Inks that two groups of wetting Agent for Printing Inkss combine, and first group of wetting Agent for Printing Inks is selected from one or more of glycerine, ethylene glycol, propylene glycol, polyoxyethylene glycol, glycol ether, triglycol, sorbyl alcohol; Second group of wetting Agent for Printing Inks is selected from one or more in Sodium.alpha.-hydroxypropionate, hyaluronic acid, pyrrolidone carboxylic acid, natural moisturizing factor (NMF), the amino acid; And the weight ratio of first group of wetting Agent for Printing Inks and second group of wetting Agent for Printing Inks is (2～3): 1;
(2) described wetting Agent for Printing Inks, fungusproof anti-corrosion agent, auxiliary agent are mixed with water;
(3) after stirring fully, add described dyestuff, and restir fully obtains the not color ink of solid carbon dioxide of described dye-type.
7. method as claimed in claim 6 is characterized in that, described (a) dyestuff is selected from water-soluble dye.
8. method as claimed in claim 6 is characterized in that described dyestuff is selected from substantive dyestuff, matching stain, reactive dyestuffs.
9. method as claimed in claim 6 is characterized in that, described dyestuff is selected from Acid Blue 7, acid blue 9, Blue VRS, sun blue 199, sun blue 106, acid red 87, acid red 18, acid yellow 23 or its combination.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010106117792A CN102010633A (en) | 2010-12-29 | 2010-12-29 | Dye-type non-dry watercolor ink and manufacturing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010106117792A CN102010633A (en) | 2010-12-29 | 2010-12-29 | Dye-type non-dry watercolor ink and manufacturing method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN102010633A true CN102010633A (en) | 2011-04-13 |
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| CN2010106117792A Pending CN102010633A (en) | 2010-12-29 | 2010-12-29 | Dye-type non-dry watercolor ink and manufacturing method thereof |
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| CN104046127A (en) * | 2014-05-26 | 2014-09-17 | 温州大学 | Non-drying gel ink pen blue ink |
| CN104263078A (en) * | 2014-09-28 | 2015-01-07 | 华东理工大学 | Highly stable pigment-type aromatic fluorescent neutral ink and preparation method thereof |
| CN105273499A (en) * | 2015-10-26 | 2016-01-27 | 合肥瑞雪化工科技有限公司 | Water-soluble inkjet ink capable of realizing ink leaking prevention |
| CN105273497A (en) * | 2015-10-26 | 2016-01-27 | 合肥瑞雪化工科技有限公司 | Ink for cross stitch |
| CN105273495A (en) * | 2015-10-26 | 2016-01-27 | 合肥瑞雪化工科技有限公司 | Easy-to-eliminate water soluble ink |
| CN105295521A (en) * | 2015-10-26 | 2016-02-03 | 合肥瑞雪化工科技有限公司 | Cross-stitch ink easy to remove |
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| CN105295538A (en) * | 2015-10-26 | 2016-02-03 | 合肥瑞雪化工科技有限公司 | Water-soluble ink |
| CN105315789A (en) * | 2015-10-26 | 2016-02-10 | 合肥瑞雪化工科技有限公司 | Water-soluble inkjet ink |
| CN105369652A (en) * | 2015-10-08 | 2016-03-02 | 深圳市墨库图文技术有限公司 | Ink and preparing method thereof |
| CN107841172A (en) * | 2017-11-26 | 2018-03-27 | 山西大学 | A kind of seven colors flash of light watercolor and preparation method thereof |
| CN108774428A (en) * | 2018-06-13 | 2018-11-09 | 上海纳诺微新材料科技有限公司 | Marking pen, mark composition for ink and preparation method thereof |
| CN114350210A (en) * | 2022-02-24 | 2022-04-15 | 盐城工业职业技术学院 | Reactive disperse dye ink for cloth painting water color pen |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104046127A (en) * | 2014-05-26 | 2014-09-17 | 温州大学 | Non-drying gel ink pen blue ink |
| CN104263078A (en) * | 2014-09-28 | 2015-01-07 | 华东理工大学 | Highly stable pigment-type aromatic fluorescent neutral ink and preparation method thereof |
| CN105369652B (en) * | 2015-10-08 | 2017-09-12 | 深圳市墨库图文技术有限公司 | A kind of ink and preparation method thereof |
| CN105369652A (en) * | 2015-10-08 | 2016-03-02 | 深圳市墨库图文技术有限公司 | Ink and preparing method thereof |
| CN105295528A (en) * | 2015-10-26 | 2016-02-03 | 合肥瑞雪化工科技有限公司 | Novel cross-stitch ink |
| CN105295521A (en) * | 2015-10-26 | 2016-02-03 | 合肥瑞雪化工科技有限公司 | Cross-stitch ink easy to remove |
| CN105273495A (en) * | 2015-10-26 | 2016-01-27 | 合肥瑞雪化工科技有限公司 | Easy-to-eliminate water soluble ink |
| CN105295516A (en) * | 2015-10-26 | 2016-02-03 | 合肥瑞雪化工科技有限公司 | Novel water-soluble ink |
| CN105295538A (en) * | 2015-10-26 | 2016-02-03 | 合肥瑞雪化工科技有限公司 | Water-soluble ink |
| CN105315789A (en) * | 2015-10-26 | 2016-02-10 | 合肥瑞雪化工科技有限公司 | Water-soluble inkjet ink |
| CN105273497A (en) * | 2015-10-26 | 2016-01-27 | 合肥瑞雪化工科技有限公司 | Ink for cross stitch |
| CN105273499A (en) * | 2015-10-26 | 2016-01-27 | 合肥瑞雪化工科技有限公司 | Water-soluble inkjet ink capable of realizing ink leaking prevention |
| CN107841172A (en) * | 2017-11-26 | 2018-03-27 | 山西大学 | A kind of seven colors flash of light watercolor and preparation method thereof |
| CN108774428A (en) * | 2018-06-13 | 2018-11-09 | 上海纳诺微新材料科技有限公司 | Marking pen, mark composition for ink and preparation method thereof |
| CN114350210A (en) * | 2022-02-24 | 2022-04-15 | 盐城工业职业技术学院 | Reactive disperse dye ink for cloth painting water color pen |
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Application publication date: 20110413 |