CN101961368A - Preparation method of aquatic animal insect repellent - Google Patents
Preparation method of aquatic animal insect repellent Download PDFInfo
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- CN101961368A CN101961368A CN2010102073009A CN201010207300A CN101961368A CN 101961368 A CN101961368 A CN 101961368A CN 2010102073009 A CN2010102073009 A CN 2010102073009A CN 201010207300 A CN201010207300 A CN 201010207300A CN 101961368 A CN101961368 A CN 101961368A
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Abstract
The invention relates to a preparation method of aquatic animal insect repellent, comprising the following implementation steps: (1) weighing the following bulk pharmaceutical chemicals in parts by weight: 200-500 parts of artemisia apiacea, 100-200 parts of antipyretic dichroa and 100-200 parts of granatum; (2) adding water according to the total amount ratio of the bulk pharmaceutical chemicals: 1: 8-12; soaking for 30min by hot water at the temperature of 45 DEG C; decocting according to the conventional method; decocting for 40min by slow fire after boiling for the first time; filtering; decocting for 30min by slow fire after the filter residue boils with 6 times of added water; combing the filter liquor and filtering; concentrating the filter liquor at the temperature of 40-50 DEG C to the condition that the relative density is 1.05; (3) adding alcohol with weight concentration of 95%, leading the alcohol content in final concentration to be 60%, stirring, and standing for 24h; (4) filtering, recovering the alcohol; adding distilled water solution, concentrating the water solution at the temperature of 40-50 DEG C to the condition that the relative density to be 1.05-1.20; and (5) cooling the concentrated solution to room temperature, and subpackaging into 250ml/bottle. The preparation method is simple and effective, insect expelling Chinese herbal medicine is a drug for preventing and curing parasites in the body or out of the body of the cultivating aquatic animals, is harmless and protects the environment, and has obvious preventing and curing effects.
Description
Technical field
The present invention relates to a kind of preparation method of aquatic animal medicine, particularly a kind of preparation method of aquatic animal anthelmintic.
Background technology
Along with the continuous rising of temperature and water temperature, various causal organisms are movable to be strengthened, and makes Fish infect various diseases easily, and especially parasitic disease breaks out easily, and the loss that causes is bigger, and has a strong impact on the aquatic animal individual growth of later stage of surviving.Parasitic disease is common, the multiple and bigger disease of control difficulty of a class in the fishery disease, and therefore, parasite killing plays very important effect aspect the fish diseases preventing and treating, in occupation of the share of Aquatic product medicine about 1/3.Adopted the sick effect of chemical classes parasite killing control eliminating fish parasites pretty good, but As time goes on, Drug resistance constantly manifest in the past; This class medicine has the residual effect of accumulating in the aquatic animal body simultaneously, can cause the aquatic product quality problem.The environmental pollution that the long-term a large amount of utilization of pest control with insecticide medicine causes, pest resistance to insecticide and the uneasy congruent a series of problems of people and animals more and more are subjected to people's attention, current widely popularize healthy nuisanceless aquaculture pattern in, press for the preparation method of seeking a kind of novel non-pollution aquatic animal anthelmintic.
Summary of the invention
The objective of the invention is to overcome above-mentioned weak point, a kind of reasonable recipe is provided, prepares preparation method simple, easy to use, obvious results aquatic animal anthelmintic.
The technical scheme that this utility model adopted is for achieving the above object:
A kind of preparation method of aquatic animal anthelmintic is characterized in that implementation step is as follows:
(1) takes by weighing following various crude drug by weight: Herba Artemisiae Annuae 200-500 part, Radix Dichroae 100-200 part, Pericarpium Granati 100-200 part;
(2) the total amount ratio 1:8-12 in crude drug adds water, and 45 ℃ of hot-water soak 30min decoct according to conventional method; The 40min of boiling back slow fire boiling for the first time filters; Filtering residue adds the water boiling back slow fire boiling 30min of 6 times of amounts again; Merging filtrate filters then, and it is 1.05 that temperature is concentrated into relative density 40 ℃ of-50 ℃ of following filtrates;
(3) add weight concentration 95% ethanol, making final concentration contain the alcohol amount is 60%, stirs, and leaves standstill 24h;
(4) filter, filtrate recycling ethanol adds the aqueous solution after distilling, and temperature is concentrated into relative density with it under 40 ℃-50 ℃ be 1.05-1.20;
(5) above-mentioned concentrated solution is cooled to room temperature, is packed as the 250ml/ bottle.
When using this product, every mu of consumption of culturing pond use product 500ml of the present invention that the depth of water is 1 meter, full pool spilling head; When being used for feeding, can mixing according to the consumption of every kilogram of bait adding 3ml product of the present invention and raise.Use this product can reach the anthelmintic of aquatic animal body surface, reach anthelmintic purpose in the body after can making aquatic animal picked-up bait again.
The characteristic of each component and effect in the product of the present invention:
Herba Artemisiae Annuae bitter in the mouth, suffering, cold in nature, return liver, gallbladder, kidney channel, have clearind deficient heat, move back hectic fever due to YIN-deficiency, the effect of expelling summer-heat preventing the attack (or recurrence) of malaria.Herba Artemisiae Annuae contains amaroid, volatile oil, abrotine, vitamin A, artemisia ketone, aldehydes, glycoside.Be mainly used in anti-multiple protozoon, plasmodium is had killing effect.
The Radix Dichroae toil, cold.Effective ingredient is an orixine, halofuginone hydrobromide.The anthelmintic Main Ingredients and Appearance is a halofuginone hydrobromide, and halofuginone hydrobromide has very strong killing action to coccidiosis, mouthful filaricide, worms on a sucker etc.
Pericarpium Granati is warm in nature, and bitter and puckery flavor is poisonous; Be usually used in treating chronic dysentery, chronic diarrhea, have blood in stool, proctoptosis, metrorrhagia, abdominal pain due to worm stagnation etc.The anthelmintic active ingredient of Pericarpium Granati is tannin, alkaloid etc., and astringing to arrest diarrhea, parasite killing and bacteriostasis are arranged, and is used to prevent and treat ichthyobodiasis, trichodinasis, gyrodactyliasis, nematicide, taeniasis etc.The tannic acid of Pericarpium Granati and alkaloid can make polypide paralysis and polypide protein coagulating and death.
The invention has the beneficial effects as follows: the anthelmintic Chinese herbal medicine has natural sex, the ecotype, low toxicity, no medicine Drug resistance, no hazard residue as the control medicine of the endoparasite and ectoparasite of culturing fish and shrimp, multi-functional, prevention effect is definite, small investment, can gather materials on the spot characteristics such as harmless environmental protection.Reasonable recipe of the present invention, preparation is simple, and prevention effect is obvious.
The specific embodiment
Below in conjunction with specific embodiment technology contents of the present invention is made detailed explanation.
Embodiment 1
A kind of preparation method of aquatic animal anthelmintic is characterized in that implementation step is as follows:
Take by weighing various crude drug by described weight portion: 200 kilograms of Herba Artemisiae Annuaes, 200 kilograms of Radix Dichroaes, 100 kilograms of Pericarpium Granatis.Total amount ratio 1:9 in raw material adds water, 45 ℃ of hot-water soak 30min, and decoct according to conventional method; The 40min of boiling back slow fire boiling for the first time filters; Filtering residue adds the water boiling back slow fire boiling 30min of its 6 times of weight again; Merging filtrate filters then, and it is 1.05 that temperature is concentrated into relative density 40 ℃ of-50 ℃ of following filtrates; Add concentration 95% ethanol, making final concentration contain the alcohol amount is 60%, stirs, and leaves standstill 24h; Filter, filtrate recycling ethanol adds the aqueous solution after distilling, and temperature is concentrated into relative density with it under 40 ℃-50 ℃ be 1.05-1.20; At last, concentrated solution is cooled to room temperature, is packed as the 250ml/ bottle.
Embodiment 2
Take by weighing various crude drug by described weight portion: 150 kilograms of 300 kilograms of Herba Artemisiae Annuaes, Radix Dichroae double centner, Pericarpium Granati.Total amount ratio 1:10 in raw material adds water, 45 ℃ of hot-water soak 30min, and decoct according to conventional method; The 40min of boiling back slow fire boiling for the first time filters; Filtering residue adds the water boiling back slow fire boiling 30min of its 6 times of weight again; Merging filtrate filters then, and it is 1.05 that temperature is concentrated into relative density 40 ℃ of-50 ℃ of following filtrates; Add concentration 95% ethanol, making final concentration contain the alcohol amount is 60%, stirs, and leaves standstill 24h; Filter, filtrate recycling ethanol adds the aqueous solution after distilling, and temperature is concentrated into relative density with it under 40 ℃-50 ℃ be 1.05-1.20; At last, concentrated solution is cooled to room temperature, is packed as the 250ml/ bottle.
Other is with embodiment 1.
Embodiment 3
Take by weighing various crude drug by described weight portion, 500 kilograms of Herba Artemisiae Annuaes, 200 kilograms of Radix Dichroaes, 200 kilograms of Pericarpium Granatis.Total amount ratio 1:12 in raw material adds water, 45 ℃ of hot-water soak 30min, and decoct according to conventional method; The 40min of boiling back slow fire boiling for the first time filters; Filtering residue adds the water boiling back slow fire boiling 30min of its 6 times of weight again; Merging filtrate filters then, and it is 1.05 that temperature is concentrated into relative density 40 ℃ of-50 ℃ of following filtrates; Add concentration 95% ethanol, making final concentration contain the alcohol amount is 60%, stirs, and leaves standstill 24h; Filter, filtrate recycling ethanol adds the aqueous solution after distilling, and temperature is concentrated into relative density with it under 40 ℃-50 ℃ be 1.05-1.20; At last, concentrated solution is cooled to room temperature, is packed as the 250ml/ bottle.
Other is with embodiment 1.
Clinical use-case:
The a certain raiser in Anhui Province cultured Ietalurus Punetaus and broken out ichthyophthiriasis when August, had a small amount of Ietalurus Punetaus slowly to move about along the edge, pond since in April, 2009, and it is inactive to ingest, bradykinesia.Pull unusual juvenile fish discovery fish body out and secrete a large amount of mucus, each tissue of body surface has congested phenomenon; At test under microscope, the point of a small amount of white is arranged on visible fish body, head, the fin ray, be diagnosed as at last and suffered from ichthyophthiriasis.The product that uses the embodiment of the invention 2 to make, every mu of pond depth of water is used 500ml for 1 meter, can find on the 3rd day that the small particles of fish body surface began to reduce, moving about and ingesting and be tending towards normal to the 5th day fish.Sick fish cheek silk and body surface are carried out microscope inspection, do not find little melonworm of larval phase, have only the little melonworm adult of only a few, it is normal that sick fish recovers, the effect highly significant.
Above-mentioned detailed description of the preparation method of aquatic animal anthelmintic being carried out with reference to embodiment; be illustrative rather than determinate; can exemplify out several embodiment according to institute's limited range; therefore in the variation and the modification that do not break away under the general plotting of the present invention, should belong within protection scope of the present invention.
Claims (1)
1. the preparation method of an aquatic animal anthelmintic is characterized in that implementation step is as follows:
(1) takes by weighing following various crude drug by weight: Herba Artemisiae Annuae 200-500 part, Radix Dichroae 100-200 part, Pericarpium Granati 100-200 part;
(2) the total amount ratio 1:8-12 in crude drug adds water, and 45 ℃ of hot-water soak 30min decoct according to conventional method; The 40min of boiling back slow fire boiling for the first time filters; Filtering residue adds the water boiling back slow fire boiling 30min of 6 times of amounts again; Merging filtrate filters then, and it is 1.05 that temperature is concentrated into relative density 40 ℃ of-50 ℃ of following filtrates;
(3) add weight concentration 95% ethanol, making final concentration contain the alcohol amount is 60%, stirs, and leaves standstill 24h;
(4) filter, filtrate recycling ethanol adds the aqueous solution after distilling, and temperature is concentrated into relative density with it under 40 ℃-50 ℃ be 1.05-1.20;
(5) above-mentioned concentrated solution is cooled to room temperature, is packed as the 250ml/ bottle.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2010102073009A CN101961368A (en) | 2010-06-23 | 2010-06-23 | Preparation method of aquatic animal insect repellent |
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| CN2010102073009A CN101961368A (en) | 2010-06-23 | 2010-06-23 | Preparation method of aquatic animal insect repellent |
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| CN101961368A true CN101961368A (en) | 2011-02-02 |
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| CN2010102073009A Pending CN101961368A (en) | 2010-06-23 | 2010-06-23 | Preparation method of aquatic animal insect repellent |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105012610A (en) * | 2015-08-06 | 2015-11-04 | 杨壮志 | Superfine powder traditional Chinese veterinary medicine for treating trichodiniasis of loach and preparing method |
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- 2010-06-23 CN CN2010102073009A patent/CN101961368A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105012610A (en) * | 2015-08-06 | 2015-11-04 | 杨壮志 | Superfine powder traditional Chinese veterinary medicine for treating trichodiniasis of loach and preparing method |
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Application publication date: 20110202 |