CN101928654B - Natural herbal degerming and parasite-expelling toilet soap and preparation method thereof - Google Patents
Natural herbal degerming and parasite-expelling toilet soap and preparation method thereof Download PDFInfo
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- CN101928654B CN101928654B CN 200910062789 CN200910062789A CN101928654B CN 101928654 B CN101928654 B CN 101928654B CN 200910062789 CN200910062789 CN 200910062789 CN 200910062789 A CN200910062789 A CN 200910062789A CN 101928654 B CN101928654 B CN 101928654B
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- graecum
- lysimachia foenum
- extract
- foenum
- lysimachia
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- 239000000344 soap Substances 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 241001571736 Lysimachia foenum-graecum Species 0.000 claims abstract description 71
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 19
- 229930195729 fatty acid Natural products 0.000 claims abstract description 19
- 239000000194 fatty acid Substances 0.000 claims abstract description 19
- 150000004665 fatty acids Chemical class 0.000 claims abstract description 19
- 239000000376 reactant Substances 0.000 claims abstract description 19
- 238000007127 saponification reaction Methods 0.000 claims abstract description 19
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 24
- 235000013599 spices Nutrition 0.000 claims description 21
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 18
- 239000013543 active substance Substances 0.000 claims description 18
- 239000000975 dye Substances 0.000 claims description 18
- 239000003921 oil Substances 0.000 claims description 17
- 239000000341 volatile oil Substances 0.000 claims description 14
- 238000000605 extraction Methods 0.000 claims description 9
- 238000010438 heat treatment Methods 0.000 claims description 9
- 239000000706 filtrate Substances 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 8
- 239000003960 organic solvent Substances 0.000 claims description 8
- 238000003795 desorption Methods 0.000 claims description 5
- 238000004821 distillation Methods 0.000 claims description 5
- 241000411851 herbal medicine Species 0.000 claims description 5
- 238000000194 supercritical-fluid extraction Methods 0.000 claims description 5
- 239000004210 ether based solvent Substances 0.000 claims description 4
- 239000006260 foam Substances 0.000 abstract description 5
- 244000045947 parasite Species 0.000 abstract description 3
- 239000002304 perfume Substances 0.000 abstract description 3
- 229930182559 Natural dye Natural products 0.000 abstract 1
- 239000000978 natural dye Substances 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000012467 final product Substances 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 229930182490 saponin Natural products 0.000 description 5
- 150000007949 saponins Chemical class 0.000 description 5
- 235000017709 saponins Nutrition 0.000 description 5
- 239000003205 fragrance Substances 0.000 description 4
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 4
- 238000010992 reflux Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 241000238631 Hexapoda Species 0.000 description 2
- 241000612166 Lysimachia Species 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 235000020245 plant milk Nutrition 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- XXUNIGZDNWWYED-UHFFFAOYSA-N 2-methylbenzamide Chemical compound CC1=CC=CC=C1C(N)=O XXUNIGZDNWWYED-UHFFFAOYSA-N 0.000 description 1
- 206010003399 Arthropod bite Diseases 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 244000178870 Lavandula angustifolia Species 0.000 description 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 1
- 244000167230 Lonicera japonica Species 0.000 description 1
- 235000017617 Lonicera japonica Nutrition 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 240000003248 Zanthoxylum nitidum Species 0.000 description 1
- 230000000507 anthelmentic effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000002085 persistent effect Effects 0.000 description 1
- 239000002728 pyrethroid Substances 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention relates to toilet soap, in particular to lysimachia foenum-graecum extract-containing natural herbal degerming and parasite-expelling toilet soap and a preparation method thereof. The toilet soap of the invention comprises the following components in percentage by weight: 91 to 94 percent of fatty acid saponification reactant, 2 to 3 percent of surfactant, 0.1 to 2 percent of lysimachia foenum-graecum extract, 1 to 3 percent of perfume and 1 to 5 percent of natural dye. The toilet soap and the preparation method utilize the efficacies of adding fragtant, enriching foam, degerming, parasite expelling and the like of the lysimachia foenum-graecum, can effectively add the fragtant of the toilet soap, enrich the foam of the toilet soap and make the toilet soap have the efficacies of degerming and parasite expelling.
Description
Technical field
The present invention relates to a kind of perfumed soap, particularly a kind of natural herbal degerming and parasite-expelling toilet soap that contains extract of lysimachiae foenum-graeci herba and preparation method thereof.
Technical background
Perfumed soap is an indispensable articles for washing during people live, and is along with the raising of people's living standard, also more and more higher to the functional requirement of perfumed soap.In order to tackle human consumer's high request, some manufacturers add plant essences such as plant milk extract and plants essential oil in the soap, soap has been possessed preserve moisture, effects such as flavouring and skin care.Plant milk extract commonly used at present has Shinyleaf Pricklyash Root, Japanese Honeysuckle, Flower of Arabian Jasmine, lavandula angustifolia etc.The plant soap has obtained human consumer's extensive approval, but mostly uses chemical insecticides such as pyrethroid and toluamide in degerming and parasite-expelling toilet soap, and it is troubling that it reaches suitability safely.Degerming and parasite-expelling toilet soap can prevent animal particularly the people avoid infection and the mosquito bite of bacterium.Natural phant is a huge treasure-house, has many plants itself just to have functions such as sterilization expelling parasite.
Lysimachia foenum-graecum is a Primulaceae Lysimachia plant, has the special fragrance breath, is famous and precious spices, is widely used in the perfuming of high-grade cigarette, wine; Lysimachia foenum-graecum has heat-clearing anthelmintic effect again, has flavor to kill effect to insects, can use as medicine for oral administration.The Lysimachia plant is in the news and contains abundant saponin component, in the Lysimachia foenum-graecum about the report of specific examples of such components rarely have, we are in the extraction experiment to Lysimachia foenum-graecum, find that it contains more saponin component, saponin component has heat-clearing, biological activity such as antibiotic, has surfactivity, water soluble, can produce a large amount of persistent seemingly saponiform foams during its aqueous solution jolting, be fit to very much add enter perfumed soap.Yet, yet there are no the report that is applied to perfumed soap.
The content of invention
Purpose of the present invention is exactly the shortage at existing plant degerming and parasite-expelling soap, and a kind of natural herbal degerming and parasite-expelling toilet soap that contains extract of lysimachiae foenum-graeci herba is provided, to remedy the deficiency of existing perfumed soap.
Technical scheme of the present invention is achieved in that it is 0.1%～2% extract of lysimachiae foenum-graeci herba that perfumed soap of the present invention contains weight percent.
The present invention's technical scheme preferably is that the weight percent of the component of described perfumed soap is: 91%～94% fatty acid saponification reactant, 2%～3% tensio-active agent, 0.1%～2% extract of lysimachiae foenum-graeci herba, 1%～3% spices and 1%～1.5% natural dyestuff.
The better technical scheme of the present invention is that the weight percent of the component of described perfumed soap is: 93% fatty acid saponification reactant, 2% tensio-active agent, 2% extract of lysimachiae foenum-graeci herba, 2% spices and 1% natural dyestuff.
Extract of lysimachiae foenum-graeci herba described in the present invention comprises Lysimachia foenum-graecum supercritical extract, Lysimachia foenum-graecum extractive of volatile oil, Lysimachia foenum-graecum absolute oil or Lysimachia foenum-graecum extractive with organic solvent.
Wherein said Lysimachia foenum-graecum supercritical extract is that Lysimachia foenum-graecum or Lysimachia foenum-graecum medicinal extract are placed the extraction of supercritical extraction unit mesohigh, desorption pressure is selected 8～20MPa, temperature is selected 40～200 ℃, obtains the herbal medicine volatile oil component behind the liquid releasing high pressure and is the Lysimachia foenum-graecum supercritical extract; Described Lysimachia foenum-graecum extractive of volatile oil is to add in the Lysimachia foenum-graecum in the entry, carries out wet distillation and obtains water-fast volatile component; Described Lysimachia foenum-graecum absolute oil is Lysimachia foenum-graecum to be added hydro-thermal extract 1-3 time, is concentrated into the thick paste of 1.20-1.30 behind the merging filtrate, adds dissolve with ethanol and obtains being dissolved in alcohol component, obtains absolute oil after concentrating; Described extractive with organic solvent is to add in the Lysimachia foenum-graecum in 10～20 times of ethanol, ethyl acetate, sherwood oil or ether solvents, and the extract that obtains is extracted in normal temperature or heating.
Preparation method of the present invention is under heating condition, adds 2%～3% tensio-active agent in 91%～94% fatty acid saponification reactant, 0.1%～2% extract of lysimachiae foenum-graeci herba, and 1%～3% spices and 1%～1.5% natural dyestuff are prepared from.
Wherein said extract of lysimachiae foenum-graeci herba comprises Lysimachia foenum-graecum supercritical extract, Lysimachia foenum-graecum extractive of volatile oil, Lysimachia foenum-graecum absolute oil or Lysimachia foenum-graecum extractive with organic solvent.
Described Lysimachia foenum-graecum supercritical extract is that Lysimachia foenum-graecum or Lysimachia foenum-graecum medicinal extract are placed the extraction of supercritical extraction unit mesohigh, desorption pressure is selected 8～20MPa, temperature is selected 40～200 ℃, obtains the herbal medicine volatile oil component behind the liquid releasing high pressure and is the Lysimachia foenum-graecum supercritical extract; Described Lysimachia foenum-graecum extractive of volatile oil is to add in the Lysimachia foenum-graecum in the entry, carries out wet distillation and obtains water-fast volatile component; Described Lysimachia foenum-graecum absolute oil is Lysimachia foenum-graecum to be added hydro-thermal extract 1-3 time, is concentrated into the thick paste of 1.20-1.30 behind the merging filtrate, adds dissolve with ethanol and obtains being dissolved in alcohol component, obtains absolute oil after concentrating; Described extractive with organic solvent is to add in the Lysimachia foenum-graecum in 10～20 times of ethanol, ethyl acetate, sherwood oil or ether solvents, and the extract that obtains is extracted in normal temperature or heating.
The present invention has utilized effects such as the flavouring of Lysimachia foenum-graecum, saponin(e enrich, degerming and parasite-expelling, can increase the fragrance of perfumed soap effectively, enriches the foam of perfumed soap, makes perfumed soap have the effect of degerming and parasite-expelling.
The invention has the beneficial effects as follows: (one), make perfumed soap have refrigerant perfume (or spice), useful fragrance such as tartaric acid perfume (or spice); (2), enrich the foam of perfumed soap, not volatile, lasting is lasting, and fragrance is had slow releasing function; (3), Lysimachia foenum-graecum itself has the flavor effect of killing to insects, the saponins material has degermation, reaches the effect of degerming and parasite-expelling.
Embodiment
Below in conjunction with embodiment the present invention is further described:
Embodiment 1:
(1) preparation of extract of lysimachiae foenum-graeci herba: place supercritical extraction unit mesohigh extraction desorption pressure to select 8MPa the former grass of the Lysimachia foenum-graecum that crushes, temperature is selected 60 ℃, and liquid obtains the herbal medicine volatile oil component after removing high pressure, and is standby with 10 times of propylene glycol dilutions.
(2) prescription: 93.4% fatty acid saponification reactant, 2% tensio-active agent, 0.1% Lysimachia foenum-graecum supercritical extract, 3% other spices, 1.5% natural dyestuff.
Under 50 ℃, in the fatty acid saponification reactant, add tensio-active agent, spices and natural dyestuff stir, and in the soap frame that impouring is got ready, leave standstill 1 day, it is solidified get final product.
Embodiment 2:
(1) preparation of extract of lysimachiae foenum-graeci herba:
Add 10 times of solution that ethanol, heating and refluxing extraction obtain in the Lysimachia foenum-graecum, use 1% activated carbon decolorizing, filter, filtrate liquid is condensed into the thick paste of density 1.1;
(2) prescription: 91% fatty acid saponification reactant, 3% tensio-active agent, 2% Lysimachia foenum-graecum supercritical extract, 3% other spices, 1% natural dyestuff.
Under 50 ℃, in the fatty acid saponification reactant, add tensio-active agent, spices and natural dyestuff stir, and in the soap frame that impouring is got ready, leave standstill 1 day, it is solidified get final product.
Embodiment 3:
(1) preparation of extract of lysimachiae foenum-graeci herba:
Add 10 times of solution that ethyl acetate, heating and refluxing extraction obtain in the Lysimachia foenum-graecum, use 1% activated carbon decolorizing, filter, filtrate liquid is condensed into density to density 1.07;
(2) prescription: 93% fatty acid saponification reactant, 2% tensio-active agent, 1% Lysimachia foenum-graecum supercritical extract, 3% other spices, 1% natural dyestuff.
Under 50 ℃, in the fatty acid saponification reactant, add tensio-active agent, spices and natural dyestuff stir, and in the soap frame that impouring is got ready, leave standstill 1 day, it is solidified get final product.
Embodiment 4:
(1) preparation of extract of lysimachiae foenum-graeci herba:
Add 15 times of hydro-thermals and extract 2 times, be concentrated into 1.23 thick paste behind the merging filtrate, add dissolve with ethanol and obtain being dissolved in pure composition, obtain absolute oil after concentrating;
(2) prescription: 93% fatty acid saponification reactant, 2.5% tensio-active agent, 1% Lysimachia foenum-graecum supercritical extract, 2% other spices, 1.5% natural dyestuff.
Under 50 ℃, in the fatty acid saponification reactant, add tensio-active agent, spices and natural dyestuff stir, and in the soap frame that impouring is got ready, leave standstill 1 day, it is solidified get final product.
Embodiment 5:
(1) preparation of extract of lysimachiae foenum-graeci herba:
Add the water of 18 times of amounts in the Lysimachia foenum-graecum, carry out wet distillation and obtain water-fast volatile component, with propylene glycol dilute 100 times standby;
(2) prescription: 94% fatty acid saponification reactant, 2% tensio-active agent, 0.1% Lysimachia foenum-graecum supercritical extract, 1.4% other spices, 1.5% natural dyestuff.
Under 50 ℃, in the fatty acid saponification reactant, add tensio-active agent, spices and natural dyestuff stir, and in the soap frame that impouring is got ready, leave standstill 1 day, it is solidified get final product.
Embodiment 6:
(1) preparation of extract of lysimachiae foenum-graeci herba:
Add 10 times of solution that ethyl acetate, heating and refluxing extraction obtain in the Lysimachia foenum-graecum, use 1% activated carbon decolorizing, filter, filtrate liquid is condensed into density to density 1.07;
(2) prescription: 93% fatty acid saponification reactant, 2% tensio-active agent, 2% extract of lysimachiae foenum-graeci herba, 2% spices and 1% natural dyestuff.
Under 50 ℃, in the fatty acid saponification reactant, add tensio-active agent, spices and natural dyestuff stir, and in the soap frame that impouring is got ready, leave standstill 1 day, it is solidified get final product.
Claims (3)
1. natural herbal degerming and parasite-expelling toilet soap, the weight percent of the component of wherein said perfumed soap is: 91%～94% fatty acid saponification reactant, 2%～3% tensio-active agent, 0.1%～2% extract of lysimachiae foenum-graeci herba, 1%～3% spices and 1%～1.5% natural dyestuff; Described extract of lysimachiae foenum-graeci herba comprises Lysimachia foenum-graecum supercritical extract, Lysimachia foenum-graecum extractive of volatile oil, Lysimachia foenum-graecum absolute oil or Lysimachia foenum-graecum extractive with organic solvent; The Lysimachia foenum-graecum supercritical extract is that Lysimachia foenum-graecum or Lysimachia foenum-graecum medicinal extract are placed the extraction of supercritical extraction unit mesohigh, desorption pressure is selected 8～20MPa, temperature is selected 40～200 ℃, obtains the herbal medicine volatile oil component behind the liquid releasing high pressure and is the Lysimachia foenum-graecum supercritical extract; The Lysimachia foenum-graecum extractive of volatile oil is to add in the Lysimachia foenum-graecum in the entry, carries out wet distillation and obtains water-fast volatile component; The Lysimachia foenum-graecum absolute oil is Lysimachia foenum-graecum to be added hydro-thermal extract 1-3 time, is concentrated into the thick paste of 1.20-1.30 behind the merging filtrate, adds dissolve with ethanol and obtains being dissolved in alcohol component, obtains absolute oil after concentrating; Extractive with organic solvent is to add in the Lysimachia foenum-graecum in 10～20 times of ethanol, ethyl acetate, sherwood oil or ether solvents, and the extract that obtains is extracted in normal temperature or heating.
2. a kind of natural herbal degerming and parasite-expelling toilet soap according to claim 1, the weight percent of the component of wherein said perfumed soap is: 93% fatty acid saponification reactant, 2% tensio-active agent, 2% extract of lysimachiae foenum-graeci herba, 2% spices and 1% natural dyestuff.
3. the preparation method of a natural herbal degerming and parasite-expelling toilet soap, it is under heating condition, in 91%～94% fatty acid saponification reactant, add 2%～3% tensio-active agent, 0.1%～2% extract of lysimachiae foenum-graeci herba, 1%～3% spices and 1%～1.5% natural dyestuff are prepared from; Described extract of lysimachiae foenum-graeci herba comprises Lysimachia foenum-graecum supercritical extract, Lysimachia foenum-graecum extractive of volatile oil, Lysimachia foenum-graecum absolute oil or Lysimachia foenum-graecum extractive with organic solvent; The Lysimachia foenum-graecum supercritical extract is that Lysimachia foenum-graecum or Lysimachia foenum-graecum medicinal extract are placed the extraction of supercritical extraction unit mesohigh, desorption pressure is selected 8～20MPa, temperature is selected 40～200 ℃, obtains the herbal medicine volatile oil component behind the liquid releasing high pressure and is the Lysimachia foenum-graecum supercritical extract; The Lysimachia foenum-graecum extractive of volatile oil is to add in the Lysimachia foenum-graecum in the entry, carries out wet distillation and obtains water-fast volatile component; The Lysimachia foenum-graecum absolute oil is Lysimachia foenum-graecum to be added hydro-thermal extract 1-3 time, is concentrated into the thick paste of 1.20-1.30 behind the merging filtrate, adds dissolve with ethanol and obtains being dissolved in alcohol component, obtains absolute oil after concentrating; Extractive with organic solvent is to add in the Lysimachia foenum-graecum in 10～20 times of ethanol, ethyl acetate, sherwood oil or ether solvents, and the extract that obtains is extracted in normal temperature or heating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200910062789 CN101928654B (en) | 2009-06-23 | 2009-06-23 | Natural herbal degerming and parasite-expelling toilet soap and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN 200910062789 CN101928654B (en) | 2009-06-23 | 2009-06-23 | Natural herbal degerming and parasite-expelling toilet soap and preparation method thereof |
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| CN101928654A CN101928654A (en) | 2010-12-29 |
| CN101928654B true CN101928654B (en) | 2011-11-16 |
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Citations (6)
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|---|---|---|---|---|
| CN1126586A (en) * | 1993-11-19 | 1996-07-17 | 姜少华 | Mosquito repelling bath lotion of natural plant material |
| KR20020087568A (en) * | 2001-05-14 | 2002-11-23 | 주식회사 내츄로바이오텍 | Plant containing insecticidal activity and insecticidal chemical compound |
| CN1414077A (en) * | 2002-09-27 | 2003-04-30 | 广西壮族自治区中国科学院广西植物研究所 | Extraction method of high quality lingxiang grass purified oil |
| CN1425303A (en) * | 2001-12-17 | 2003-06-25 | 中国科学院武汉植物研究所 | Plant flea killing agent and its preparing method |
| CN1426686A (en) * | 2001-12-17 | 2003-07-02 | 中国科学院武汉植物研究所 | Plant flea killing spraying agent and its preparation method |
| CN101457178A (en) * | 2008-12-10 | 2009-06-17 | 广西中烟工业有限责任公司 | Method for extracting water-soluble volatilization component from lysimachia foenum-graecum |
-
2009
- 2009-06-23 CN CN 200910062789 patent/CN101928654B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1126586A (en) * | 1993-11-19 | 1996-07-17 | 姜少华 | Mosquito repelling bath lotion of natural plant material |
| KR20020087568A (en) * | 2001-05-14 | 2002-11-23 | 주식회사 내츄로바이오텍 | Plant containing insecticidal activity and insecticidal chemical compound |
| CN1425303A (en) * | 2001-12-17 | 2003-06-25 | 中国科学院武汉植物研究所 | Plant flea killing agent and its preparing method |
| CN1426686A (en) * | 2001-12-17 | 2003-07-02 | 中国科学院武汉植物研究所 | Plant flea killing spraying agent and its preparation method |
| CN1414077A (en) * | 2002-09-27 | 2003-04-30 | 广西壮族自治区中国科学院广西植物研究所 | Extraction method of high quality lingxiang grass purified oil |
| CN101457178A (en) * | 2008-12-10 | 2009-06-17 | 广西中烟工业有限责任公司 | Method for extracting water-soluble volatilization component from lysimachia foenum-graecum |
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| Title |
|---|
| 杨瑞云 等."灵香草提取物的抑菌活性研究".《安徽农业科学》.2009,第37卷(第7期),3035－3036. |
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| CN101928654A (en) | 2010-12-29 |
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