CN101828550B - Composition of composite potassium peroxymonosulfate disinfection tablet and preparation method thereof - Google Patents

Composition of composite potassium peroxymonosulfate disinfection tablet and preparation method thereof Download PDF

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CN101828550B
CN101828550B CN 201010154464 CN201010154464A CN101828550B CN 101828550 B CN101828550 B CN 101828550B CN 201010154464 CN201010154464 CN 201010154464 CN 201010154464 A CN201010154464 A CN 201010154464A CN 101828550 B CN101828550 B CN 101828550B
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sodium
potassium hydrogen
disinfection
hydrogen persulfate
tablet
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CN101828550A (en
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黄文江
杨庆
张建新
戴荣贵
孔令娣
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Jiangsu Weite Pharmaceutical Co., Ltd
ZHENHAI VICTOR PHARM Co.,Ltd.
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CHENGDU VICTOR PHARMACEUTICALS Ltd
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Abstract

The invention discloses acomposite potassium peroxymonosulfate disinfection tablet which comprises 10.0-70.0 parts by weight of potassium monopersulfate, 1.0-65.0 parts by weight of fillers, 1.0-20.0 parts by weight of adhesives and 0.01-10.0 parts by weight of lubricant, wherein the fillers is formed by one or more then one of sodium sulfate, sodium chloride, potassium chloride, sodium carbonate, sodium bicarbonate, phosphate, inorganic acid, organic acid, starch, dextrin, glucose, solid emulsifier, xylitol and a metal ion complexing agent, the adhesives comprise cellulose, polyvinylpyrrolidone and gelatin; the lubricant is formed by one or more than one of magnesium stearate, talcum powder, micro-powder silica gel, sodium benzoate and polyethylene glycol; in addition, sodium percarbonate, calcium percarbonate, sodium perborate or calcium peroxide 1-2 are added. The invention is convenient to use, has the advantages of quick disintegration and dissolution, can significantly increase the effect of the disinfection tablet and can adjust pH value.

Description

The composition of compound potassium hydrogen peroxymonosulfate disinfection tablet and preparation technology thereof
Technical field
The present invention relates to a kind of disinfectant, particularly a kind of compound potassium hydrogen peroxymonosulfate disinfection tablet.
Background technology
The society high speed development, human living density is large, and various disease carrying germs are wreaked havoc, the harm humans social safety, sterilization is the effective ways that people prevent various disease carrying germs, disinfectant is in field extensive uses such as health and epidemic prevention, drug and food production, livestock and poultry cultivations.
Potassium peroxymonosulfate (molecular formula 2KHSO5KHSO4K2SO4) is comprised of Potassium Monopersulfate, potassium acid sulfate and potassium sulphate, be a kind of can free-pouring white particle sprills, soluble in water, in water, decompose and emit oxygen and potassium sulphate, do not produce harmful substance.Potassium peroxymonosulfate oxidation potential energy is high, chloride, potassium permanganate, hydrogen peroxide etc. have been surpassed, can be oxidized to chlorine to the chlorion in the aqueous solution, can become organic acid to oxidation operations such as alcohols, aldehydes, be a kind of novel active oxygen disinfectant of stablizing, make things convenient for, having extensive use.Monopersulfate clock complex salt is active very strong strong oxidation material, be proved to be with its tackle wreak havoc Europe aftosa and rabid ox disease obtain brilliant effect, European Union is carrying out the product manufacturing research that Potassium Monopersulfate is main active, and be applied to human drinking water disinfection, carried out European Union's standard.
At present potassium peroxymonosulfate sterilization series products mostly is pulvis, as defend can (Virkon S), application number is that 200310110649.0 patent application (application publication number is CN1545883A) also is a kind of pulvis, cooperated by weight percentage by sodium chloride, potassium hydrogen persulfate, sulfamic acid, malic acid, citric acid, calgon, dodecyl sodium sulfate, sodium silicate, but its shortcoming is using dosage inconvenience, and effectively storage life is shorter.
Summary of the invention
The present invention seeks to propose a kind of composition and preparation technology thereof of compound potassium hydrogen peroxymonosulfate disinfection tablet, metering is inaccurate when using to solve powder product, awkward deficiency adopts the peroxide synergist simultaneously, and can proper extension storage life (pressing effective active oxygen calculates).
Realize that technical scheme of the present invention is such, a kind of compound potassium hydrogen peroxymonosulfate disinfection tablet is comprised of potassium peroxymonosulfate, filler, adhesive and lubricant.Wherein filler be sodium sulphate, sodium chloride, potassium chloride, sodium carbonate, sodium bicarbonate, phosphate, etc. one or more compositions in mineral salt, inorganic acid, organic acid, starch, dextrin, glucose, solid emulsifier, xylitol and the complexing of metal ion agent; Adhesive is one or more compositions of cellulose family, polyvinylpyrrolidone class, various natural glues; Lubricant is one or more compositions in dolomol, talcum powder, differential silica gel, Sodium Benzoate and the polyethylene glycol.The composition that forms is by weight:
Potassium peroxymonosulfate 10.0-70.0
Filler 1.0-65.0
Adhesive 1.0-20.0
Lubricant 0.01-10.0
Other adds SODIUM PERCARBONATE, percarbonic acid calcium, sodium perborate or calper calcium peroxide 1-2, adds calcium oxide 0.5-1 again.Especially by following prescription:
Potassium peroxymonosulfate 20.0-30.0
Filler 30-50.0
Adhesive 1.0-10.0
Lubricant 0.01-2.0
SODIUM PERCARBONATE, percarbonic acid calcium, calper calcium peroxide or sodium perborate 1-2
Or add again calcium oxide 0.5-1.
Potassium peroxymonosulfate 50.0-70.0
Filler 20-40
Adhesive 1.0-10.0
Lubricant 0.01-2.0
SODIUM PERCARBONATE, percarbonic acid calcium, calper calcium peroxide or sodium perborate 1-2
Or add again calcium oxide 0.5-1.
A kind of preparation technology of compound potassium hydrogen peroxymonosulfate disinfection tablet: with used material 40~80 ℃ of dryings 2~4 hours, choose 30~100 purpose powders, mix after measuring, be pressed into the tablet of required weight with rotary tablet machine, or make 15~30 purpose particles, be pressed into again the tablet of required weight.Prepared tablet can be ordinary tablet, also can be effervescent tablet, disintegrated tablet or sustained release tablets.The pH value of obtained tablet is 1.0~6.0 (aqueous solution of 2wt% content).Compound potassium hydrogen peroxymonosulfate disinfection tablet dispensing is convenient, special lowered in field environment, lack the disinfectant measuring equipment and during than accurate-metering, can be by the dispensing counting, and simple ratiometric conversion, determine more accurate amount of water, thereby simplify disinfecting process, instructions for use that simultaneously also can be different according to the user, select the tablet of respective type, satisfy the sterilization requirement of specific type.
The invention has the beneficial effects as follows: during use convenient and disintegration and dissolving fast, using dosage is accurate, effectively storage life can prolong more than one month.Because adopt the peroxide synergist can make the medicament notable synergistic, and can regulate the pH value.
Embodiment
Embodiment 1:
Potassium peroxymonosulfate 40~50 ℃ of oven dry 2 hours, is crossed 30 orders for subsequent use; Adhesive is got 60~100 purpose powders for subsequent use 40~80 ℃ of oven dry 3 hours; Filler and lubricant, calcium oxide and peroxide respectively by kind 40~80 ℃ of dryings 3~4 hours, and it is for subsequent use to cross respectively 30 orders and 80 mesh sieves.Compound potassium hydrogen peroxymonosulfate disinfection tablet composed as follows:
Potassium peroxymonosulfate 10-12 (weight portion, lower same)
Filler 55-70.0
Adhesive 15-25.0
Lubricant 8-12.0
Typically take by weighing potassium peroxymonosulfate 10.0, filler 60.0, adhesive 20.0, lubricant 10.0, mix the rear tablet that requires specification that is pressed into tablet press machine.
Filler is sodium sulphate, sodium carbonate, sodium bicarbonate, sodium sesquicarbonate, tetrasodium pyrophosphate, sodium phosphate trimer, sodium silicate, citric acid, malic acid and tartaric acid, an aquation sodium perborate, sodium bicarbonate, one of starch, dextrin, glucose; Other adds 1 part in calcium oxide;
Adhesive is one of cellulose, polyvinylpyrrolidone, gelatin;
Lubricant is a kind of in dolomol, talcum powder, differential silica gel, Sodium Benzoate and the polyethylene glycol;
Add SODIUM PERCARBONATE, calper calcium peroxide, percarbonic acid calcium or sodium perborate 1-2 (weight portion, lower same) on above-mentioned prescription basis.
Embodiment 2
Potassium peroxymonosulfate 20.0-30.0
Filler 30-50.0
Adhesive 1.0-10.0
Lubricant 0.01-2.0
SODIUM PERCARBONATE, calper calcium peroxide or sodium perborate 1-2
Filler is sodium sulphate, sodium carbonate, sodium bicarbonate, sodium sesquicarbonate, tetrasodium pyrophosphate, sodium phosphate trimer, sodium silicate, citric acid, malic acid and tartaric acid, an aquation sodium perborate, sodium bicarbonate, one of starch, dextrin, glucose;
Adhesive is one of cellulose, polyvinylpyrrolidone, gelatin;
Lubricant is a kind of in dolomol, talcum powder, differential silica gel, Sodium Benzoate and the polyethylene glycol;
Add again calcium oxide 0.5-1; And interpolation SODIUM PERCARBONATE, calper calcium peroxide, percarbonic acid calcium or sodium perborate 1.
Embodiment 3
Potassium peroxymonosulfate 50.0-70.0
Filler 20-40
Adhesive 1.0-10.0
Lubricant 0.01-2.0
Filler is sodium sulphate, sodium carbonate, sodium bicarbonate, sodium sesquicarbonate, tetrasodium pyrophosphate, sodium phosphate trimer, sodium silicate, citric acid, malic acid and tartaric acid, an aquation sodium perborate, sodium bicarbonate, one of starch, dextrin, glucose; Adhesive is one of cellulose, polyvinylpyrrolidone, gelatin;
Lubricant is a kind of in dolomol, talcum powder, differential silica gel, Sodium Benzoate and the polyethylene glycol;
Add again calcium oxide 0.5-1, add SODIUM PERCARBONATE, calper calcium peroxide, percarbonic acid calcium or sodium perborate 2.
Potassium peroxymonosulfate 40~50 ℃ of oven dry 2 hours, is crossed 30 orders for subsequent use; Adhesive is got 60~100 purpose powders for subsequent use 40~80 ℃ of oven dry 3 hours; Filler and lubricant, calcium oxide and peroxide respectively by kind 40~80 ℃ of dryings 3~4 hours, and it is for subsequent use to cross respectively 30 orders and 80 mesh sieves.
Embodiment 4
Compound potassium hydrogen peroxymonosulfate disinfection tablet composed as follows:
Potassium peroxymonosulfate 25.0
Filler 65.0
Adhesive 8.0
Lubricant 2.0
Take by weighing potassium peroxymonosulfate 25.0 (weight portion), filler 65.0, adhesive 8.0, lubricant 2.0, SODIUM PERCARBONATE, calper calcium peroxide or sodium perborate 1-2 mix the rear tablet that requires specification that is pressed into tablet press machine.Filler is sodium sulphate, sodium carbonate, sodium bicarbonate, sodium sesquicarbonate, tetrasodium pyrophosphate, sodium phosphate trimer, sodium silicate, citric acid, malic acid and tartaric acid, an aquation sodium perborate, sodium bicarbonate, one of starch, dextrin, glucose; Other adds calcium oxide 1, adds SODIUM PERCARBONATE, percarbonic acid calcium or sodium perborate 1; Adhesive is one of cellulose, polyvinylpyrrolidone, gelatin; Lubricant is a kind of in dolomol, talcum powder, differential silica gel, Sodium Benzoate and the polyethylene glycol.
Embodiment 5:
Potassium peroxymonosulfate 40~50 ℃ of oven dry 2 hours, is crossed 30 orders for subsequent use; Adhesive is got 60~100 purpose powders for subsequent use 40~80 ℃ of oven dry 3 hours; Filler and lubricant respectively by kind 40~80 ℃ of dryings 3~4 hours, and it is for subsequent use to cross respectively 30 orders and 80 mesh sieves.Compound potassium hydrogen peroxymonosulfate disinfection tablet composed as follows:
Potassium peroxymonosulfate 50.0
Filler 37.0
Adhesive 10.0
Lubricant 3.0
Take by weighing potassium peroxymonosulfate 50.0Kg, filler 37.0Kg, adhesive 10.0, lubricant 3.0, mix the rear tablet that requires specification that is pressed into tablet press machine.Filler is sodium sulphate, sodium carbonate, sodium bicarbonate, sodium sesquicarbonate, tetrasodium pyrophosphate, sodium phosphate trimer, sodium silicate, citric acid, malic acid and tartaric acid, an aquation sodium perborate, sodium bicarbonate, one of starch, dextrin, glucose, other adds calcium oxide 1, and adds SODIUM PERCARBONATE, percarbonic acid calcium or sodium perborate 1; Adhesive is one of cellulose, polyvinylpyrrolidone, gelatin;
Lubricant is a kind of in dolomol, talcum powder, differential silica gel, Sodium Benzoate and the polyethylene glycol.
Embodiment 6:
Potassium peroxymonosulfate 40~50 ℃ of oven dry 2 hours, is crossed 30 orders for subsequent use; Adhesive is got 60~100 purpose powders for subsequent use 40~80 ℃ of oven dry 3 hours; Filler and lubricant respectively by kind 40~80 ℃ of dryings 3~4 hours, and it is for subsequent use to cross respectively 30 orders and 80 mesh sieves.Compound potassium hydrogen peroxymonosulfate disinfection tablet composed as follows:
Potassium peroxymonosulfate 70.0
Filler 17.0
Adhesive 12.0
Lubricant 1.0
Calper calcium peroxide 1
Take by weighing potassium peroxymonosulfate 70.0, filler 17.0, adhesive 12.0, lubricant 1.0, mix the rear tablet that requires specification that is pressed into tablet press machine.Filler is sodium sulphate, sodium carbonate, sodium bicarbonate, sodium sesquicarbonate, tetrasodium pyrophosphate, sodium phosphate trimer, sodium silicate, citric acid, malic acid and tartaric acid, an aquation sodium perborate, sodium bicarbonate, one of starch, dextrin, glucose; Other adds calcium oxide 0.5.
Adhesive is one of cellulose, polyvinylpyrrolidone, gelatin;
Lubricant is a kind of in dolomol, talcum powder, differential silica gel, Sodium Benzoate and the polyethylene glycol;
Embodiment 7:
Potassium peroxymonosulfate 40~50 ℃ of oven dry 2 hours, is crossed 30 orders for subsequent use; PVPP is got 60~100 purpose powders for subsequent use 40~80 ℃ of oven dry 3 hours; Anhydrous citric acid, sodium chloride, neopelex, anhydrous sodium sulfate, EDTA-2Na and dolomol respectively by kind 40~80 ℃ of dryings 3~4 hours, and it is for subsequent use to cross respectively 30 mesh sieves; It is for subsequent use that dolomol is crossed 80 mesh sieves.Compound potassium hydrogen peroxymonosulfate disinfection tablet composed as follows:
Potassium peroxymonosulfate 52.0
Sodium chloride 5.0
Anhydrous citric acid 3.0
Neopelex 2.0
Anhydrous sodium sulfate 25.0
PVPP 12.0
EDTA-2Na 0.5
Dolomol 0.5
Calcium oxide 0.5
Calper calcium peroxide 2
Take by weighing potassium peroxymonosulfate 52.0, EDTA-2Na 0.5 anhydrous citric acid 3.0, sodium chloride 5.0, neopelex 2.0, calcium oxide 0.5, calper calcium peroxide 2, anhydrous sodium sulfate 25.0, PVPP 12.0 and dolomol 0.5, mix the rear tablet that requires specification that is pressed into tablet press machine.
Surfactant in the example also can be the A-sodium olefin sulfonate, fatty alcohol-polyoxyethylene ether, polyoxyethylene poly-oxygen propylene aether, dodecyl trimethyl ammonium chloride, sodium carboxymethylcellulose, AESA, the stearic acid monoglyceride, polyoxyethylene nonylphenol ether, the mixture of any one or more of methyl-silicone oil etc., its addition is 0.05%~1% of wet potassium hydrogen persulfate composite salts weight.
Embodiment 8:
Potassium peroxymonosulfate 40~50 ℃ of oven dry 2 hours, is crossed 30 orders for subsequent use; Sodium carboxymethylcellulose is got 60~100 purpose powders for subsequent use 40~80 ℃ of oven dry 3 hours; Anhydrous citric acid, sodium chloride, neopelex, anhydrous sodium sulfate, sodium bicarbonate, EDTA-2Na respectively by kind 40~80 ℃ of dryings 3~4 hours, and it is for subsequent use to cross respectively 30 mesh sieves; It is for subsequent use that dolomol is crossed 80 mesh sieves.Compound potassium hydrogen peroxymonosulfate disinfection tablet composed as follows:
Potassium peroxymonosulfate 52.0
Sodium chloride 2.5
Anhydrous citric acid 5.0
Sodium bicarbonate 2.5
Neopelex 2.0
Anhydrous sodium sulfate 25.0
Sodium carboxymethylcellulose 10.0
EDTA-2Na 0.5
Dolomol 0.5
Calcium oxide 0.5
Calper calcium peroxide 1
Take by weighing potassium peroxymonosulfate 52.0, EDTA-2Na 0.5, anhydrous citric acid 5.0, sodium chloride 2.5, neopelex 2.0, anhydrous sodium sulfate 25.0, calcium oxide 0.5, calper calcium peroxide 1, sodium bicarbonate 2.5, sodium carboxymethylcellulose 10.0 and dolomol 0.5, mix the rear tablet that requires specification that is pressed into tablet press machine.

Claims (8)

1. a compound potassium hydrogen persulfate disinfection tablet is characterized in that being comprised of potassium peroxymonosulfate, filler, adhesive and lubricant; Wherein filler is one or more compositions in sodium sulphate, sodium chloride, potassium chloride, sodium carbonate, sodium bicarbonate, phosphate, SODIUM PERCARBONATE, sodium perborate, inorganic acid, organic acid, starch, dextrin, glucose, solid emulsifier, xylitol and the complexing of metal ion agent; Adhesive is one or more compositions of cellulose family, polyvinylpyrrolidone class, gelatin; Lubricant is one or more compositions in dolomol, talcum powder, differential silica gel, Sodium Benzoate and the polyethylene glycol, and the composition of composition is by weight:
Other adds SODIUM PERCARBONATE, percarbonic acid calcium, sodium perborate or calper calcium peroxide 1.0-2.0.
2. require 1 described compound potassium hydrogen persulfate disinfection tablet according to claim, it is characterized in that adding again calcium oxide 0.5-1.0.
3. require 1 or 2 described compound potassium hydrogen persulfate disinfection tablets according to claim, it is characterized in that
Figure FDA00001690687800012
4. require 1 or 2 described compound potassium hydrogen persulfate disinfection tablets according to claim, it is characterized in that the composed as follows of hydrogen potassium disinfection tablet:
Figure FDA00001690687800013
5. require 1 or 2 described compound potassium hydrogen persulfate disinfection tablets according to claim, it is characterized in that the composed as follows of compound potassium hydrogen persulfate disinfection tablet:
Figure FDA00001690687800014
Other adds calcium oxide 1.0, adds SODIUM PERCARBONATE, calper calcium peroxide, percarbonic acid calcium or sodium perborate 1.0.
6. require 1 or 2 described compound potassium hydrogen persulfate disinfection tablets according to claim, it is characterized in that the composed as follows of compound potassium hydrogen persulfate disinfection tablet:
Figure FDA00001690687800015
Figure FDA00001690687800021
Other adds calcium oxide 1.0, and adds SODIUM PERCARBONATE, calper calcium peroxide, percarbonic acid calcium or sodium perborate 1.0.
7. require 1 or 2 described compound potassium hydrogen persulfate disinfection tablets according to claim, it is characterized in that the composed as follows of compound potassium hydrogen persulfate disinfection tablet:
8. require 1 or 2 described compound potassium hydrogen persulfate disinfection tablets according to claim, it is characterized in that the composed as follows of compound potassium hydrogen persulfate disinfection tablet:
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CN106342884A (en) * 2016-08-29 2017-01-25 连云港永荣生物科技有限公司 Disinfection powder of drinking water

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