CN101700361A - Dendrobium candidum instant powder and preparation method thereof - Google Patents
Dendrobium candidum instant powder and preparation method thereof Download PDFInfo
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- CN101700361A CN101700361A CN200910193293A CN200910193293A CN101700361A CN 101700361 A CN101700361 A CN 101700361A CN 200910193293 A CN200910193293 A CN 200910193293A CN 200910193293 A CN200910193293 A CN 200910193293A CN 101700361 A CN101700361 A CN 101700361A
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Abstract
The invention relates to a dendrobium candidum instant powder and a preparation method of various related formulations thereof. The preparation method of the dendrobium candidum instant powder comprises the steps of: combining low-temperature extract of the dendrobium candidum with raw materials such as maltodextrin and dietary fiber, and the like, wherein the low-temperature extract of the dendrobium candidum is prepared by modern extraction and separation technologies such vacuum exploding, reverse film permeating, freeze drying and spray drying, and the like; and further preparing into formulations such as granules, effervescent tablets, capsules and oral liquid, etc. The invention improves the extraction efficiency of the dendrobium candidum, maximally guarantees the bioavailability of the dendrobium candidum, remains the primary smell of the dendrobium candidum, and leads the dendrobium candidum is conveniently taken.
Description
One, technical field
The invention belongs to the medicines and health protection field of food, be specifically related to the preparation and the application of a kind of dendrobium candidum instant powder and relevant dosage form thereof.
Two, background technology
Enter this century, people's living pressure of working has increased, and the concern of health is also improved day by day.Become the favorite in epoch undoubtedly as the Herba Dendrobii first of " China nine big Herba mesonae chinensis ", Herba Dendrobii is just on the books in Shennong's Herbal, is listed as top grade.Herba Dendrobii slightly sweet flavor, the band viscosity of chewing, tool grass fragrance is clear product of supporting, heat clearing away is too not cold and cool, yin nourishing and relatively do not grow greasy, YIN nourishing benefit essence and born fluid, tonify deficiency labor and clearind deficient heat.The tonifying five ZANG-organs asthenia is won thin, and the reinforcing YIN-essence benefit is smart, obey for a long time, and thick the intestines and stomach, never sufficient in the benefit, flat gastric qi, longue meat, Fructus Alpiniae Oxyphyllae removes frightened, eliminating impediment, the therapeutic method to keep the adverse QI flowing downwards is made light of one's life by commiting suicide and is prolonged life.Be health product, medicine, the raw material that industries such as cosmetics are loved by all.
At present, the product about Herba Dendrobii on the market is a lot, and capsule, oral liquid, drop pill etc. are arranged, and is many with health product.Most of products all are directly to use Herba Dendrobii medicinal powder or its to decoct extract, and the method extraction ratio that is adopted is low, to original itself be exactly a kind of waste with regard to Herba Dendrobii herb resource in short supply.The present invention adopts modern advanced vacuum explosion extracting method, in conjunction with lyophilization and spray drying extract at low temperature and dry Herba Dendrobii extract, primary fragrance of Herba Dendrobii and smooth mouthfeel have been preserved, make the extraction ratio of Herba Dendrobii medical material improve, prepared simultaneously the practical dosage form of various Herba Dendrobii on the basis of dendrobium candidum instant powder, it is convenient that Herba Dendrobii is taken.Therefore, designing a kind of dendrobium candidum instant powder that possesses These characteristics, is the product that meets the existing market needs.
Three, summary of the invention
The objective of the invention is at the Herba Dendrobii extraction ratio low, the present situation that effective ingredient is poorly soluble, utilize various state-of-the-art technologys, solve the drawback that Herba Dendrobii uses, improve the utilization rate of Herba Dendrobii medical material, preserve the fragrance and the smooth mouthfeel of Herba Dendrobii effective ingredient, enrich the practical dosage form of Herba Dendrobii simultaneously, increase the edible way of Herba Dendrobii.
Disclosed by the invention is the Herba Dendrobii extract of 10%-33% and the oral formulations that the 90%-67% pharmaceutic adjuvant is formed by percentage by weight.
Oral formulations of the present invention is meant capsule, tablet, granule, oral liquid, effervescent tablet etc.
Two kinds of bright product of Herba Dendrobii branch that the present invention is used and dry products.Dry product reaches 95% micropowder for the sporoderm-broken rate through micronizing.
It is the preparation method of above-mentioned various Herba Dendrobii preparations that the present invention wants disclosed another problem.
Technical scheme of the present invention is:
A kind of processing method of dendrobium candidum instant powder, this processing method comprises the following steps
1 fresh Herba Dendrobii adopts the method for squeezing the juice to extract, and removes the fibroid composition, and dry product then adopts vacuum explosion extracting method.
The described method of squeezing the juice is to adopt common juice extractor to finish.Described vacuum explosion extracting method is that medicinal powder abrupt release pressure damaged wall dissolving under the 20MPa atmospheric pressure is finished.
2 above-mentioned Herba Dendrobii extracts adopt lyophilization or spray drying
Described lyophilization is at-40 ℃ ,-133 * 10
-3Pa carries out.Spray drying is at 50 ℃, and 5000kPa carries out.
3 above-mentioned desciccates were pulverized 100 mesh sieves, added adjuvants such as dietary fiber and maltodextrin according to recipe quantity, fully mixed according to a conventional method, made granule, promptly got granule; Granule is inserted in the capsulae vacuus, promptly got capsule; Direct compression promptly gets tablet.Add adjuvants such as lactose, citric acid, sodium bicarbonate, PEG6000 according to recipe quantity and make the soda acid granule step by step, even before the tabletting two parts powder mixes, be pressed into tablet, promptly get the Herba Dendrobii effervescent tablet.The extract of above-mentioned Herba Dendrobii filters, and standardize solution adds antiseptic, packing, and sterilization promptly gets oral liquid.
Advantage of the present invention is:
1. the present invention adopts the method for squeezing the juice and vacuum explosion to extract the Herba Dendrobii medical material, and the leaching process temperature is all very low, has preserved thermal sensitivity composition and the fragrance in the Herba Dendrobii.
2. the present invention has adopted the vacuum explosion to extract; medicinal powder has carried out wall breaking pulverization; sporoderm-broken rate requires 95%; adopt the vacuum explosion of moment to discharge intracellular material then; extracting the utilization rate that can significantly improve the Herba Dendrobii medical material again, also is a kind of protection to the Herba Dendrobii herb resource.
3. the present invention adopts lyophilization and spray drying, and baking temperature is lower, forms the dry thing of cellular, water content lower (all being lower than 5%), and the extract dissolving is relatively easy.
4. behind above-mentioned drying means Herba Dendrobii is ground into fine powder, the reuse adjuvant disperses to make the dissolubility that granule has improved Herba Dendrobii.
5. Herba Dendrobii Related product mouthfeel in the market and fragrance all can not have concurrently simultaneously, perhaps cryopreservation fragrance, but medicinal powder directly uses and causes the smooth mouthfeel of Herba Dendrobii all gone, or high temperature decocts the fragrance that has destroyed Herba Dendrobii.But the present invention has guaranteed the mouthfeel and the fragrance of Herba Dendrobii simultaneously.
Four. the specific embodiment
Below in conjunction with specific embodiment technical characterictic of the present invention is further specified.
Embodiment 1: oral liquid preparation (bright product are squeezed the juice)
Get fresh Herba Dendrobii 100g, use the clear water rinsing, remove the fiber sheath on surface, after rinsing finishes it is dried, be cut into the 0.5cm segment, add an amount of water and squeeze the juice, squeeze 3 times, merge 3 times extracting solution, 80 ℃ of heating 10min, put coldly, add sorbic acid 0.5g, fully dissolving, refilter, be settled to 1000ml, heat sterilization, fill becomes ampere, every 10ml.
Embodiment 2: granule preparation (bright product lyophilization)
Choose the clear water rinsing of fresh Herba Dendrobii, remove the fiber sheath on surface, after rinsing finishes it is dried, be cut into the 0.5cm segment, add an amount of water and squeeze the juice, squeeze 3 times, merge 3 times extracting solution, 80 ℃ of heating 10min.Put coldly, place-30 ℃ of refrigerator pre-freeze 24～48h to be placed on the freeze dryer lyophilizing.
Get gained Herba Dendrobii lyophilized powder and pulverize, cross 100 mesh sieves, press recipe quantity and add adjuvants such as dietary fiber, routine is made granule, and granulate is distributed into the 2.5g/ bag.
Embodiment 3: capsule preparation (dry product spray drying)
Get Herba Dendrobii 1000g, spray the sterilization of 70% ethanol, wave most ethanol, micronizing adds water 8000ml, and the vacuum explosion is extracted, extracting solution filters through reverse osmotic membrane, concentrates the concentrate spray drying, get Herba Dendrobii extract extractum, pulverize, cross 100 mesh sieves, add the conventional granulations of adjuvant such as starch according to recipe quantity, granulate, granule are inserted in No. 1 capsulae vacuus, every capsules 0.8g.
Embodiment 4: effervescent tablet preparation (dry product lyophilization)
Get Herba Dendrobii 1000g, spray the sterilization of 70% ethanol, wave most ethanol, micronizing adds water 8000ml, and the vacuum explosion is extracted, and extracting solution filters through reverse osmotic membrane, concentrates, and concentrated solution places-30 ℃ of refrigerator pre-freeze 24～48h to be placed on the freeze dryer lyophilizing.
Get gained Herba Dendrobii lyophilized powder and pulverize, cross 100 mesh sieves, press recipe quantity and add adjuvants such as lactose, sodium bicarbonate, PEG6000, routine is made alkali grain; Take by weighing the citric acid bulky grain and pulverize, sieve, measured the bulky grain and the gained alkali granule mix homogeneously of No. 2 sieves by prescription, tabletting is made the Herba Dendrobii effervescent tablet of every 1.5g.Get 1 of Herba Dendrobii effervescent tablet before taking, add 150ml warm water take after mixing it with water dissolving, i.e. edible.
Claims (5)
1. dendrobium candidum instant powder is characterized in that said preparation is is the oral formulations that the pharmaceutic adjuvant of the Herba Dendrobii extract of 10%-33% and 90%-67% is made by percentage by weight.
2. a kind of dendrobium candidum instant powder processing method as claimed in claim 1, it is characterized in that: described Herba Dendrobii extract is with the bright product of Herba Dendrobii or dry product removes fiber through squeezing the juice or the vacuum explosion is extracted, through the prepared powder needle-like of low temperature drying method Herba Dendrobii extracts such as lyophilization or spray dryinges.
3. a kind of dendrobium candidum instant powder processing method as claimed in claim 1 is characterized in that used Herba Dendrobii dry product is to pass through the cell wall breaking rate of micronizing in the micropowder more than 95%.
4. a dendrobium candidum instant powder preparation as claimed in claim 1 is characterized in that wherein said peroral dosage form comprises dosage forms such as oral liquid, granule, capsule, tablet, effervescent tablet.
5. the preparation method of a dendrobium candidum instant powder preparation as claimed in claim 1 is characterized in that this method comprises:
(1) get fresh Herba Dendrobii medical material through the clear water rinsing, its surperficial fibroid sheath of flush away dries, and is cut into the segment of 0.5cm, adds an amount of water and squeezes the juice, and squeezes 3 times, filters, and merges 3 times filtrate, carries out drying; Get Herba Dendrobii dry product superfine powder and be broken into micropowder, the vacuum explosion is extracted, and extracting solution is collected concentrated solution and carried out drying through the inverse osmosis membrance concentration.
(2) drying mode of above-mentioned Herba Dendrobii extract be lyophilization (40 ℃ ,-133 * 10
-3Pa) or spray drying (50 ℃, 5000kPa).
(3) preparation of oral formulations
Take by weighing the Herba Dendrobii extract by recipe quantity, add required adjuvant, mix, make granule, promptly get dendrobium candidum instant powder according to conventional method.The gained granule is packed in the capsulae vacuus, promptly get capsule; Direct compression promptly gets tablet; If the not direct standardize solution of drying, sterilization, packing of extract promptly gets oral liquid.
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| CN200910193293A CN101700361A (en) | 2009-10-26 | 2009-10-26 | Dendrobium candidum instant powder and preparation method thereof |
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| CN102178847A (en) * | 2011-05-04 | 2011-09-14 | 湖南龙石山铁皮石斛基地有限公司 | Vacuum freeze-drying processing method of dendrobium officinale |
| CN102552699A (en) * | 2012-01-16 | 2012-07-11 | 澄思源生物科技（上海）有限公司 | Preparation method of dendrobium candidum ultrafine powder |
| CN102743598A (en) * | 2012-06-29 | 2012-10-24 | 四川万安石斛产业开发有限公司 | var. Denneanum extract and formula particles thereof |
| CN102772441A (en) * | 2012-07-06 | 2012-11-14 | 周明千 | Method for processing traditional Chinese medicinal ultramicro wall-broken capsule slices |
| CN103386027A (en) * | 2013-06-14 | 2013-11-13 | 李兰星 | Processing technology of fresh dendrobium officinale powder |
| CN103404918A (en) * | 2013-08-30 | 2013-11-27 | 龙陵县红桔苑山庄 | Preparation method of purple dendrobium soup |
| CN103549411A (en) * | 2013-09-25 | 2014-02-05 | *** | Synchronous production technology for preparing dendrobium officinale oral liquid and piece beverage |
| CN103735853A (en) * | 2013-07-16 | 2014-04-23 | 李兰星 | Preparation method of fresh Dendrobium officinale preparation |
| CN103766905A (en) * | 2014-02-10 | 2014-05-07 | 安徽科技学院 | Dendrobium candidum-chuzhou chrysanthemum health-care granule |
| CN103877395A (en) * | 2014-03-27 | 2014-06-25 | 马荣钢 | Method for preparing dendrobium officinale instant powder |
| CN104207131A (en) * | 2014-09-26 | 2014-12-17 | 安徽新津铁皮石斛开发有限公司 | Crab milk flavor dendrobium officinale ultrafine powder beverage and preparation method thereof |
| CN104223063A (en) * | 2014-08-26 | 2014-12-24 | 北京林业大学 | Freeze-dried dendrobium officinale powder and preparation method thereof |
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| CN104544038A (en) * | 2013-10-29 | 2015-04-29 | 广西浙商投资有限公司 | Dendrobium officinale oral liquid preparation and processing method |
| CN104623312A (en) * | 2015-01-27 | 2015-05-20 | 中国农业科学院农产品加工研究所 | Instant dendrobe powder as well as preparation method and application thereof |
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| CN104958567A (en) * | 2015-08-04 | 2015-10-07 | 桂林伯林生物技术有限公司 | Dendrobium candidum wall.ex lindl lozenge and preparation method thereof |
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2009
- 2009-10-26 CN CN200910193293A patent/CN101700361A/en active Pending
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| CN105327148A (en) * | 2015-12-11 | 2016-02-17 | 杭州华都医药有限公司 | Method for preparing dendrobe cream |
| CN105327148B (en) * | 2015-12-11 | 2019-02-01 | 杭州华都医药有限公司 | The preparation method of dendrobium nobile cream |
| CN105725200A (en) * | 2016-02-24 | 2016-07-06 | 云南久丽康源石斛开发有限公司 | Processing method for soluble dendrobium officinale freeze-dried powder |
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| CN105994743A (en) * | 2016-05-22 | 2016-10-12 | 王伟家 | Production method of healthcare dendrobium caffeine |
| CN106039027A (en) * | 2016-06-23 | 2016-10-26 | 云南润紫源生物科技股份有限公司 | Dendrobium candidum leaf lozenge as well as preparation method and application thereof |
| CN106165722A (en) * | 2016-06-29 | 2016-11-30 | 韦智涛 | A kind of preparation method of Herba Dendrobii milk shake powders |
| CN106723013A (en) * | 2016-11-22 | 2017-05-31 | 张家港昊盛实业投资有限公司 | Dendrobium candidum oral liquid and preparation method thereof |
| CN106418516A (en) * | 2016-12-20 | 2017-02-22 | 安徽中医药大学 | Preparation method of fresh dendrobium nobile preparation |
| CN109380725A (en) * | 2018-12-13 | 2019-02-26 | 浙江兰溪锦荣生物科技股份有限公司 | A kind of dendrobium nobile chewable tablets and preparation method thereof containing dendrobium nobile soluble dietary fiber |
| CN109602004A (en) * | 2018-12-21 | 2019-04-12 | 无锡食品科技园发展有限公司 | With the dendrobium candidum effervescent tablet compound and preparation method thereof for improving the immunity of the human body and protecting stomach function |
| CN114963745A (en) * | 2022-05-23 | 2022-08-30 | 舟山市食品药品检验检测研究院 | Optimized processing technology for dendrobium officinale produced in Zhejiang |
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Application publication date: 20100505 |