CN103284143B - Rubus chingii decoction piece and preparation method thereof - Google Patents
Rubus chingii decoction piece and preparation method thereof Download PDFInfo
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- CN103284143B CN103284143B CN201210093135.8A CN201210093135A CN103284143B CN 103284143 B CN103284143 B CN 103284143B CN 201210093135 A CN201210093135 A CN 201210093135A CN 103284143 B CN103284143 B CN 103284143B
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Abstract
The invention relates to the field of Chinese herbal medicines, and discloses a rubus chingii decoction piece. The rubus chingii decoction piece is prepared into granules or powder from mature rubus chingii fruit as a raw material. The invention also discloses a preparation method of the rubus chingii decoction piece. The preparation method of the rubus chingii decoction piece comprises the processes of selecting materials, dewatering in vacuum, crushing at low temperature, pelletizing, sterilizing and the like. The process is simple. The rubus chingii decoction piece disclosed by the invention can be swallowed, and also can be dissolved into cold or hot liquid to drink. Thus, the rubus chingii decoction piece is convenient to use. No chemical process exists in a preparation method of the rubus chingii decoction piece. Original ecology and nutrition ingredients of the mature rubus chingii are furthest reserved; the purity of the prepared rubus chingii granules can be up to 99% (1% of bonding material); and the purity of the powder can be up to 100%. According to the rubus chingii decoction piece disclosed by the invention, balanced sweetness and acidity, purple fruit, and strong and specific fruit flavor of the original mature rubus chingii fruit are reserved; and the rubus chingii decoction piece has the probiotic effects of resisting aging, preventing cancers, reducing frequent micturition caused by prostate, nourishing the liver and removing freckles, restraining gastritis and elytritis and the like.
Description
Technical field
The present invention relates to herbal decoction piece and preparation field thereof, relate in particular to a kind of Rubus chingii medicine materical crude slice and preparation method thereof.
Background technology
Rubus chingii is a kind of shrub of rose family rubus, and branch is thin, and tool prickle, without hair; Single leaf, subcircular; Fruit is subsphaeroidal, and redness is close by canescence pubescence.Ripe Rubus chingii can eat raw or jam processed, wine brewing, also can do ornamental plant and plant in flakes.Its fruit can be used for treating enuresis with renal asthenia, frequent urination, impotence and premature ejaculation, emission and spermatorrhea.
In Chinese medicine, adopt at present the Chinese olive of immature Rubus chingii, after boiling, naturally dry.This mode has fraud: both made in fruit the functional components such as due anthocyanidin, SOD, raspberry ketone not yet ripe, again in brewed and decoction process, cause thermal sensitivity composition heavy losses, and sour-puckery flavor inedibility, needs to adopt to decoct and to user, has brought certain inconvenience by traditional drink-service mode of juice.
The key point for process of Chinese traditional herbs granular pattern medicine materical crude slice and pulvis medicine materical crude slice: lixiviate liquid (hot water cooking method, alcohol extracting are followed the example of) → separation (dregs of a decoction, alcohol) → cream processed that concentrate → is mixed (its excipient take starch as main and auxiliary with flavor enhancement, other additive, binding agent, anticorrisive agent etc.) → high temperature spray-drying granulation powder process or wet granulation → packing.
The reason that the production technology of Chinese traditional herbs granular pattern medicine materical crude slice is not suitable for Rubus chingii granule pieces of the present invention and the making of pulvis medicine materical crude slice is as follows:
(1) traditional flooding, concentrated juice, extract process processed adopt high-temperature technology again.High-temperature technology must destroy thermal sensitivity, the fragrant volatility effective ingredient (as anthocyanidin, SOD etc.) being rich in Rubus chingii mellow fruit;
(2) traditional handicraft adopts alcohol extracting, secondary separation technique, and not only cost is high, complex process, and in raspberry mellow fruit, efficacy component recovery rate is not high, and quite major part remains in pomace, causes waste;
Conventional particles medicine materical crude slice and pulvis medicine materical crude slice technique for the high raw material of water content processed granulating, must add much starch and multiple additives or be prefabricated into medicinal extract during powder process, thereby cause the purity level of finished product medicine materical crude slice low, during use, dosage is difficult to grasp.
Therefore Rubus chingii medicine materical crude slice of, inventing a kind of full composition, high-purity, delicious edible, both for medicine and food (Ministry of Public Health's regulation kind) and preparation method thereof has important practical value.
Summary of the invention
The present invention's the first object has been to provide a kind of Rubus chingii medicine materical crude slice, and it is really raw material that described Rubus chingii medicine materical crude slice be take ripe Rubus chingii, granulation shape or Powdered.
Above-described Rubus chingii medicine materical crude slice can be instant, can swallow, and also available white wine cold or warm (60 ℃ following) liquid reconstitutes drink-service, uses very conveniently, has the feature of dietotherapeutic.
The present invention's the second object provides the preparation method of Rubus chingii medicine materical crude slice described in more than one, comprises the following steps:
(1) select raw material: choose ripe Fructus Rubi as raw material;
(2) clean: the Fructus Rubi as raw material is cleaned;
(3) freezing: the Fructus Rubi after cleaning is carried out freezing;
(4) dehydration: adopt drier to carry out low temperature dewatering the Fructus Rubi after freezing;
(5) sorting: the Fructus Rubi after dehydration is divided and elects complete Fructus Rubi and incomplete Fructus Rubi as, and complete Fructus Rubi is chosen, and separately uses;
(6) low-temperature grinding: adopt shearing crusher to pulverize the incomplete Fructus Rubi sub-electing, pulverizer need be with the device for inhaling powdery substances of ice water circulation system and two blower fan heat extraction suction powder, and device for inhaling powdery substances need be with screen pack and cocycle air channel;
(7) granulate: the Fructus Rubi powder after pulverizing is adopted to dry cold compacting grain or wet granulation;
(8) sterilizing: the raspberry particle making through (7) is carried out to sterilizing;
(9) packing: the raspberry particle after (8) sterilizing is packed;
(10) freezing sterilizing: the raspberry particle after packing is carried out to freezing sterilizing, obtain Rubus chingii granule pieces.
Or will be crushed to 80 order～120 object Rubus chingii fruit powder through (6), according to (8), carry out sterilizing, according to (9), pack, according to (10), carry out freezing sterilizing, obtain Rubus chingii pulvis medicine materical crude slice.
Preferably, freezing conditions is that Rubus chingii fruit surface temperature reaches-40 ℃, and Rubus chingii fruit DIE Temperature reaches-35 ℃.
Preferably, drier adopts industrial vacuum freeze drier group.
Preferably, the concrete grammar of sterilizing is microwave sterilization 5 minutes or sterilizing 2 hours in ultraviolet seal box at 60 ℃.
Preferably, the concrete grammar of freezing sterilizing is at-30 ℃ freezing 48 hours.
In the present invention, not take leaching liquor, medicinal extract be raw material midbody to the preparation method of Rubus chingii medicine materical crude slice, directly ripe Rubus chingii be take to vacuum freezing drying dehydration mode as basis, then carry out the processes such as low-temperature grinding, granulation, packing, and technique is simple.
Preparation method of the present invention only adopts low form physical property processing technology, there is no chemical technology, therefore farthest retained ecosystem and the nutrition of ripe Rubus chingii, the purity of the Rubus chingii particle of making is up to 99% (1% is sticky object), pulvis purity 100%.
In addition, ripe Rubus chingii fruit originally has that sour-sweet degree is agreeable to the taste, fruit look purple and the speciality that the smell of fruits is very sweet, the ripe Rubus chingii of take is really assisted sugar, sweetener and other adding ingredients without adding in the process of raw material Rubus chingii medicine materical crude slice processed, have anti-ageing, give protection against cancer, alleviate prostate frequent micturition, nourishing the liver nti-freckle, press down the prebiotic effects such as gastritis, vaginitis, therefore, being the good medicine (not bitter to the taste) of curing the disease, is again precious health preserving health-care food raw material.
Accompanying drawing explanation
Fig. 1 is the FB(flow block) of preparation Rubus chingii granule pieces of the present invention;
Fig. 2 is the FB(flow block) of preparation Rubus chingii pulvis medicine materical crude slice of the present invention.
The specific embodiment
Below in conjunction with accompanying drawing and specific embodiment, describe the present invention in detail, in this illustrative examples of the present invention and explanation, be used for explaining the present invention, but not as a limitation of the invention.
Embodiment 1:
The ripe Rubus chingii of take is really raw material, and granulation shape, obtains Rubus chingii granule pieces.Ripe Rubus chingii really has following characteristics: color is scarlet, purplish red, the purple multiple color such as black, apricot yellow, and pericarp, pulp, fruit juice is homochromy; Sugar content is more than or equal to 8% juice content and is greater than 80%, is with sweet in acid; While plucking fruit, fruit and base of fruit energy natural separation, form hollow fruit, and fruit body softness is flexible.
Fig. 1 is the FB(flow block) of preparation Rubus chingii granule pieces of the present invention, and as can be seen from Figure 1, the preparation method of Rubus chingii granule pieces of the present invention is as follows:
The first step: select raw material, choose ripe Rubus chingii fruit as raw material;
Second step: clean, the Rubus chingii as raw material is really carried out to Ozone Water cleaning;
The 3rd step: freezing, the Rubus chingii after cleaning is really carried out freezing, preferably freezing condition is that Rubus chingii fruit surface temperature reaches-40 ℃, Rubus chingii fruit DIE Temperature reaches-35 ℃;
The 4th step: dehydration, really adopts drier to carry out low temperature dewatering the Rubus chingii after freezing.In the preferred storehouse of drier, using dehydration plate area is 200m
2the industrial vacuum freeze drier group of programme-control, concrete dehydrating operations condition is: it is-45～-40 ℃ that (1) Rubus chingii really enters to be dried cabin temperature; (2) vacuum in dry cabin is 80PC～90PC; (3) condenser temperature is-19 ℃ (± 2 ℃); (4) temperature of heating plate is 50～55 ℃; (5) Rubus chingii fruit surface temperature is for being less than or equal to 45 ℃; (6) Rubus chingii fruit central temperature is less than or equal to 45 ℃; (7) in drying machine, dewatering time is 20 to 22 hours; (8) shut down that to stay the storehouse time be 2 hours.Wherein the Key Limit Value of vacuum freeze drier group is moisture≤7%, and operation limit is moisture≤5%.
The 5th step: sorting, the Fructus Rubi after dehydration is divided and elects complete Fructus Rubi and incomplete Fructus Rubi as, complete Fructus Rubi transports another use;
The 6th step: low-temperature grinding, adopt shearing crusher to pulverize the incomplete Fructus Rubi sub-electing, the device for inhaling powdery substances of powder, device for inhaling powdery substances band screen pack and cocycle air channel are inhaled in pulverizer band ice water circulation system and two blower fan heat extraction;
The 7th step: granulate, adopt dry granulation machine carry out dry cold compacting grain or adopt wet granulation machine to carry out wet granulation in the Fructus Rubi powder after pulverizing;
The 8th step: sterilizing, the raspberry particle obtaining after dry cold compacting grain or wet granulation is packed to front sterilizing, the concrete grammar of sterilizing is microwave sterilization 5 minutes or sterilizing 2 hours in ultraviolet seal box at 60 ℃;
The 9th step: packing, the raspberry particle after microwave sterilization or ultraviolet disinfection is packed, can to raspberry particle, pack (vacuum packaging is best) with high-density plastic, aluminium foil, aluminum plastic film or glass etc.;
The tenth step: freezing sterilizing, raspberry granule pieces after packing is carried out to freezing sterilizing, obtain Rubus chingii granule pieces product, the concrete grammar of freezing sterilizing is at-30 ℃ freezing 48 hours, can solve the biological pollution that causes in process (as fly etc. may be residual parasitic ovum).
Embodiment 2
The ripe Rubus chingii of take is really raw material, makes powdery, obtains Rubus chingii pulvis medicine materical crude slice.Ripe Rubus chingii really has following characteristics: color is scarlet, purplish red, the purple multiple color such as black, apricot yellow, and pericarp, pulp, fruit juice is homochromy; Sugar content is more than or equal to 8% juice content and is greater than 80%, is with sweet in acid; While plucking fruit, fruit and base of fruit energy natural separation, form hollow fruit, and fruit body softness is flexible.
Fig. 2 is the FB(flow block) of preparation Rubus chingii pulvis medicine materical crude slice of the present invention, and as can be seen from Figure 2, the preparation method of Rubus chingii pulvis medicine materical crude slice of the present invention is as follows:
The first step: select raw material, choose ripe Rubus chingii fruit as raw material;
Second step: clean, the Rubus chingii as raw material is really carried out to Ozone Water cleaning;
The 3rd step: freezing, the Rubus chingii after cleaning is really carried out freezing, preferably freezing condition is that Rubus chingii fruit surface temperature reaches-40 ℃, Rubus chingii fruit DIE Temperature reaches-35 ℃;
The 4th step: dehydration, really adopts drier to carry out low temperature dewatering the Rubus chingii after freezing.In the preferred storehouse of drier, using dehydration plate area is 200m
2the industrial vacuum freeze drier group of programme-control, concrete dehydrating operations condition is: it is-45～-40 ℃ that (1) Rubus chingii really enters to be dried cabin temperature; (2) vacuum in dry cabin is 80PC～90PC; (3) condenser temperature is-19 ℃ (± 2 ℃); (4) temperature of heating plate is 50～55 ℃; (5) Rubus chingii fruit surface temperature is for being less than or equal to 45 ℃; (6) Rubus chingii fruit central temperature is less than or equal to 45 ℃; (7) in drying machine, dewatering time is 20 to 22 hours; (8) shut down that to stay the storehouse time be 2 hours.Wherein the Key Limit Value of vacuum freeze drier group is moisture≤7%, and operation limit is moisture≤5%.
The 5th step: sorting, the Fructus Rubi after dehydration is divided and elects complete Fructus Rubi and incomplete Fructus Rubi as, complete Fructus Rubi transports another use;
The 6th step: low-temperature grinding, adopt shearing crusher to be crushed to 80 order～120 orders the incomplete Fructus Rubi sub-electing, the device for inhaling powdery substances of powder, device for inhaling powdery substances band screen pack and cocycle air channel are inhaled in pulverizer band ice water circulation system and two blower fan heat extraction;
The 7th step: sterilizing, the Rubus chingii fruit powder after pulverizing is packed to front sterilizing, the concrete grammar of sterilizing is microwave sterilization 5 minutes or sterilizing 2 hours in ultraviolet seal box at 60 ℃;
The 8th step: packing, the Fructus Rubi powder after microwave sterilization or ultraviolet disinfection is packed, can to Fructus Rubi powder, pack (vacuum packaging is best) with high-density plastic, aluminium foil, aluminum plastic film or glass etc.;
The 9th step: freezing sterilizing, raspberry pulvis medicine materical crude slice after packing is carried out to freezing sterilizing, obtain Rubus chingii pulvis medicine materical crude slice product, the concrete grammar of freezing sterilizing is at-30 ℃ freezing 48 hours, can solve the biological pollution that causes in process (as fly etc. may be residual parasitic ovum).
Rubus chingii pulvis medicine materical crude slice in Rubus chingii granule pieces in the embodiment of the present invention 1 and preparation method thereof and embodiment 2 and preparation method thereof has the following advantages:
1, Rubus chingii granule pieces of the present invention and pulvis medicine materical crude slice can be instant, can swallow, also available wine or cold or hot liquid reconstitute drink-service, use very convenient.
2, in the present invention the preparation method of Rubus chingii granule pieces and pulvis medicine materical crude slice not take leaching liquor, medicinal extract and starch based excipient be raw material midbody, directly ripe Rubus chingii be take to vacuum freezing drying dehydration mode as basis, carry out the processes such as low-temperature grinding (granulation), packing, technique is simple again.
3, preparation method's whole process using low form physical property processing technology of the present invention, there is no high-temperature technology and chemistry technique, therefore the ecosystem and the nutrition that have farthest retained ripe Rubus chingii, the purity of the Rubus chingii granule pieces of making up to the purity of 99% (1% is sticky object) pulvis medicine materical crude slice up to 100%.For precision medication provides necessary condition.
4, to take ripe Rubus chingii be really raw material for Rubus chingii particle of the present invention and pulvis, the Rubus chingii that has retained former maturation really has that sour-sweet degree is agreeable to the taste, fruit look purple and the speciality that the smell of fruits is very sweet, in preparation process, without adding, assist sugar, sweetener and anticorrisive agent, have anti-ageing, give protection against cancer, alleviate prostate frequent micturition, nourishing the liver nti-freckle, press down the prebiotic effects such as gastritis, vaginitis, therefore, being the good medicine (not bitter to the taste) of curing the disease, is again precious health care product.
The technical scheme above embodiment of the present invention being provided is described in detail, applied specific case herein the principle of the embodiment of the present invention and embodiment are set forth, the explanation of above embodiment is only applicable to help to understand the principle of the embodiment of the present invention; , for one of ordinary skill in the art, according to the embodiment of the present invention, in the specific embodiment and range of application, all will change, in sum, this description should not be construed as limitation of the present invention meanwhile.
Claims (2)
1. a Rubus chingii medicine materical crude slice, is characterized in that take that ripe Rubus chingii is really raw material, and granulation shape or Powdered, comprises the following steps:
(1) select raw material: choose ripe Rubus chingii fruit as raw material;
(2) clean: the Rubus chingii as raw material is really cleaned;
(3) freezing: the Rubus chingii after cleaning is really carried out freezing;
(4) dehydration: really adopt drier to carry out low temperature dewatering the Rubus chingii after freezing;
(5) sorting: the Rubus chingii after dehydration is really divided and elects complete Rubus chingii fruit and incomplete Rubus chingii fruit as, and complete Rubus chingii really transports;
(6) low-temperature grinding: really adopt shearing crusher to pulverize the incomplete Rubus chingii sub-electing, the device for inhaling powdery substances of powder is inhaled in pulverizer band ice water circulation system and two blower fan heat extraction, and device for inhaling powdery substances need be with screen pack and cocycle air channel;
(7) granulate: the Rubus chingii fruit powder after pulverizing is adopted to dry cold compacting grain or wet granulation;
(8) sterilizing: the Rubus chingii particle making through (7) is carried out to sterilizing;
(9) packing: the Rubus chingii particle after (8) sterilizing is packed;
(10) freezing sterilizing: the Rubus chingii particle after packing is carried out to freezing sterilizing, obtain Rubus chingii granule pieces.
Or will be crushed to 80 order～120 object Rubus chingii fruit powder through (6), according to (8), carry out sterilizing, according to (9), pack, according to (10), carry out freezing sterilizing, obtain Rubus chingii pulvis medicine materical crude slice.
2. according to the method for Rubus chingii medicine materical crude slice described in claim 1, it is characterized in that institute
Stating freezing condition is that Rubus chingii fruit surface temperature reaches-40 ℃, and Rubus chingii fruit DIE Temperature reaches-35 ℃.
3. according to the method for Rubus chingii medicine materical crude slice described in claim 1, it is characterized in that described drier adopts industrial vacuum freeze drier group.
4. according to the method for Rubus chingii medicine materical crude slice described in claim 1, the concrete grammar that it is characterized in that described sterilizing is microwave sterilization 5 minutes at 60 ℃ or sterilizing 2 hours in ultraviolet seal box.
5. according to the method for Rubus chingii medicine materical crude slice described in claim 1, the concrete grammar that it is characterized in that described freezing sterilizing is at-30 ℃ freezing 48 hours.
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Families Citing this family (7)
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| CN104388279A (en) * | 2014-12-10 | 2015-03-04 | 蔡晓鹏 | Chinese herbal medicine rubus chingii hu health wine and preparation method thereof |
| CN104366625A (en) * | 2014-12-10 | 2015-02-25 | 蔡晓鹏 | Sugar-free active fresh pulp beverage made of rubus chingii hu which is Chinese herbal medicine and method for manufacturing sugar-free active fresh pulp beverage |
| CN105011280A (en) * | 2015-07-17 | 2015-11-04 | 合肥一诺生物科技有限公司 | Rubus chingii fruit beverage and preparation method thereof |
| CN110353205A (en) * | 2018-06-15 | 2019-10-22 | 蔡晓鹏 | A kind of citrus freeze-drying chankings derived product and preparation method thereof |
| CN110353141A (en) * | 2018-06-15 | 2019-10-22 | 蔡晓鹏 | A kind of mulberries freeze-drying Chinese herbal medicine formula granule pieces and preparation method thereof |
| CN109010050A (en) * | 2018-06-25 | 2018-12-18 | 广西圣保堂健康产业股份有限公司 | A kind of efficient preparation method for ensureing effective component energy conservation and environmental protection Chinese medicinal granule |
| CN110251569B (en) * | 2019-07-26 | 2021-04-27 | 湖南新汇制药股份有限公司 | Preparation method of raspberry decoction pieces |
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