CN101147746A - Method for processing traditional Chinese herbs broken wall powder - Google Patents
Method for processing traditional Chinese herbs broken wall powder Download PDFInfo
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- CN101147746A CN101147746A CNA2006101221717A CN200610122171A CN101147746A CN 101147746 A CN101147746 A CN 101147746A CN A2006101221717 A CNA2006101221717 A CN A2006101221717A CN 200610122171 A CN200610122171 A CN 200610122171A CN 101147746 A CN101147746 A CN 101147746A
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- 239000000843 powder Substances 0.000 title claims abstract description 60
- 238000012545 processing Methods 0.000 title claims description 12
- 238000000034 method Methods 0.000 title description 7
- 235000008216 herbs Nutrition 0.000 title 1
- 239000008187 granular material Substances 0.000 claims abstract description 30
- 238000010298 pulverizing process Methods 0.000 claims abstract description 26
- 238000003672 processing method Methods 0.000 claims abstract description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000005469 granulation Methods 0.000 claims abstract description 8
- 230000003179 granulation Effects 0.000 claims abstract description 8
- 239000000463 material Substances 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 6
- 238000012216 screening Methods 0.000 claims abstract description 6
- 239000007779 soft material Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000003814 drug Substances 0.000 claims description 27
- 230000001413 cellular effect Effects 0.000 claims description 22
- 238000012856 packing Methods 0.000 claims description 21
- 229940079593 drug Drugs 0.000 claims description 20
- 239000012567 medical material Substances 0.000 claims description 17
- 238000002156 mixing Methods 0.000 claims description 10
- 235000013312 flour Nutrition 0.000 claims description 8
- 238000005453 pelletization Methods 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 2
- 235000019441 ethanol Nutrition 0.000 abstract 1
- 238000011049 filling Methods 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
- 241000756943 Codonopsis Species 0.000 description 6
- 238000010521 absorption reaction Methods 0.000 description 4
- 238000010923 batch production Methods 0.000 description 3
- 210000002421 cell wall Anatomy 0.000 description 3
- 238000013461 design Methods 0.000 description 3
- 238000004891 communication Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
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Abstract
The present invention relates to a processing method of Chinese medicinal material wall-broken powder. Said processing method includes the following steps: (1), medicinal material preparation: selecting material, slicing and drying to obtain cleaned medicinal material; (2), pulverization: using universal pulverizing machine to make wall-breaking pulverization of medicinal material so as to obtain crude powder with above 60 meshes; (3), wall-breaking pulverization: using wall-breaking pulverizing machine to make wall-breaking pulverization to obtain superfine powder body with above 300 meshes; (4), granulating: placing the above-mentioned superfine powder body into a mix-stirring machine, adding water or ethyl alcohol to make them into soft material, using granulating machine to make granulation to obtain wet granules and drying said wet granules; (5), finishing and screening; and (6), filling and packaging.
Description
[technical field]
The present invention relates to a kind of processing method of Chinese crude drug breaking cellular wall powder.
[background technology]
Superfine communication technique nearly more than ten years have obtained using widely and developing rapidly in each field, and it can be processed into micron even nano level micropowder to raw material.Superfine communication technique has also obtained extensive studies and practice being applied to the Chinese medicine traditional field in recent years, Chinese crude drug is after superfine powder is broken into micropowder, the medical material utilization rate increases substantially, studies show that the middle survival dose after the ultra micro refinement, only be equivalent to 1/3rd even 1/10th of former prescription dosage, be the method for effectively saving Chinese material medicine resource, particularly have bigger meaning for rare precious medicine resource.
Current micronizing has to use in Chinese crude drug processing and mainly is meant that the cell grade micropowder is broken, mainly is to be that purpose is pulverized with Chinese crude drug cell wall breaking, therefore, claims that also superfine powder is the breaking cellular wall powder.After the Chinese medicine cell wall breaking, show following advantage: increase substantially its bioavailability; Medicinal utilization rate improves; Conservation is convenient to use; The uniformity height of medical material.Meanwhile also show some uncertain factors, the stability that mainly shows as the effective ingredient in the breaking cellular wall medical material reduces, the easy moisture absorption, and easily oxidation, sporoderm-broken rate is low, be difficult for long preservation, and this is the matter of utmost importance that superfine powder exists.
[summary of the invention]
The objective of the invention is to overcome the deficiencies in the prior art part, provide a kind of Chinese crude drug after being processed into the breaking cellular wall powder, to be difficult for the moisture absorption, be difficult for oxidation, stability is strong, and brews the processing method of the breaking cellular wall powder that can take in 5-10 minute with the warm water between the 60-100 degree in share.
The object of the present invention is achieved like this:
A kind of processing method of Chinese crude drug breaking cellular wall powder, its processing steps is:
(1) medicinal material processing: it gets clean medical material after comprising selection, section, drying;
(2) pulverize: with above-mentioned clean medical material, pulverize with the Universalpulverizer of 100 mesh sieves, wall breaking pulverization gets the above coarse powder of 60 orders;
(3) wall breaking pulverization: the coarse powder flour with above gained, be crushed to more than 300 orders through the breaking cellular wall powder, obtain superfine powder;
(4) granulate: get above gained superfine powder, put in the flute profile mixing and blending machine, water or ethanol are made soft material, granulate through the oscillating granulator of 30 mesh sieves, and the wet granular that makes is put in the heated-air circulation oven and dried;
(5) granulate, screening: with upper strata 40 orders, the vibration pelletizing machine of lower floor's 80 mesh sieves is made granule between 40 orders-80 order with above-mentioned granulation granulate screening 1-3 time.
(6) packing and packing: get qualified superfine powder granule, packing and outer package get finished product.
The processing method of aforesaid a kind of Chinese crude drug breaking cellular wall powder is characterized in that, when grinding and processing, temperature is the 18-26 degree between pulverizing, and relative humidity is below 55%, and the air inlet operating pressure is 〉=0.7Mpa that the grader rotating speed is 30-35 revolutions per second.
The processing method of aforesaid a kind of Chinese crude drug breaking cellular wall powder is characterized in that, adds man-hour at wall breaking pulverization, and temperature is the 18-26 degree between pulverizing, and relative humidity is below 55%, and the air inlet operating pressure is 〉=0.7Mpa that the grader rotating speed is 30-35 revolutions per second.
The processing method of aforesaid a kind of Chinese crude drug breaking cellular wall powder is characterized in that, adds man-hour in granulation, and temperature is the 60-70 degree, and being dried to moisture is≤6.5%.
The processing method of aforesaid a kind of Chinese crude drug breaking cellular wall powder is characterized in that, when packing and package processing, the temperature of packing chamber is the 18-26 degree, and relative humidity is the 45-65 degree.
The invention has the beneficial effects as follows:
1. because of after being crushed to more than 300 orders, the cell wall breaking rate reaches more than 90%, makes active ingredient stripping fully, can save the medical material consumption greatly.
2. Chinese crude drug breaking cellular wall powder is made 40-80 purpose granule, has increased stability, the moisture resistance of breaking cellular wall powder, helps storage.
3. take simply, only the warm water between the need 60-100 degree brews and can take in 5-10 minute.
4. Chinese crude drug breaking cellular wall powder is made 40-80 purpose granule, and particulate good fluidity helps packing.
[specific embodiment]
Concrete processing steps of the present invention is:
1. the process of preparing Chinese medicine of medical material: comprise processing procedures such as selection, section, drying,, obtain clean medical material specifically at the characteristic of every flavor Chinese crude drug and decide.
2. coarse pulverization: get the clean medical material after the process of preparing Chinese medicine, pulverize with the Universalpulverizer of 100 mesh sieves, the above coarse powder of 60 orders.
3. wall breaking pulverization: with the coarse powder flour of above gained, temperature was at the 18-26 degree between control was pulverized, relative humidity is below 55%, through wall breaking pulverization, control air inlet operating pressure 〉=0.7Mpa, grader rotating speed (clockwise), 30-35 revolutions per second, through being crushed to behind the wall breaking pulverization more than 300 orders, obtain superfine powder.
4. granulate: get above gained Chinese crude drug breaking cellular wall powder, put in the flute profile mixing and blending machine, water or Different concentrations of alcohol are made an amount of system soft material; oscillating granulator through 30 mesh sieves is granulated; the wet granular that makes is put in the heated-air circulation oven, and design temperature 60-70 degree is dried to moisture≤6.5%.
5. granulate, screening: with pre-installing upper strata 40 orders, the vibration pelletizing machine granulate of lower floor's 80 mesh sieves sieves 1-3 time, and fine powder adds the new granulation again of granulating of next groove, and coarse granule is treated down batch production, adds during pulverizing, makes granule between 40 orders-80 order.
6. packing and packing: get qualified superfine powder granule, the temperature of control packing chamber in the scope of relative humidity 45-65 degree, is carried out packing and outer package by specification at the 18-26 degree, finished product.
Below further illustrate:
Embodiment one: the system Radix Codonopsis
1. impurity, the foreign body that wherein is mingled with removed in selection, and dis-medicinal part gets clean medical material, clean medical material through blocking medicine cutter at a high speed, is cut into the thick thin slice of 1-3mm, and thin slice is put in the thermal cycle baking oven, control temperature≤60 degree, dry about 6h to moisture≤6.0%, cools to room temperature, the poly-bag of packing into immediately, tighten bag mouth, prevent the moisture absorption, get dried clean medical material.Censorship moisture.
2. get dried clean medical material, control temperature 18-22 degree between pulverizing, relative humidity is pulverized once with the Universalpulverizer of prepackage 100 mesh sieves below 45%, and the coarse powder flour is adorned poly-bag immediately, tightens bag mouth, prevents the moisture absorption, gets Radix Codonopsis coarse powder flour.
3. with the Radix Codonopsis coarse powder flour of above gained, control temperature 18-26 degree between pulverizing, relative temperature is below 55%, through micronizing, control air inlet operating pressure 〉=0.7Mpa, 30-35 revolutions per second of grader rotating speed (clockwise), be crushed to more than 300 orders, get the Radix Codonopsis superfine powder.
4. getting above gained Radix Codonopsis superfine powder puts in the flute profile mixing and blending machine; make an amount of system soft material (every kilogram of superfine powder needs 70% ethanol 130g approximately) with 70% ethanol; oscillating granulator through pre-installing 30 mesh sieves is granulated; the wet granular that the makes pallet of packing into; every disc thickness＜1.0cm places heated-air circulation oven, design temperature 60-65 degree; dry about 1h is to moisture≤6.5%.
5. after drying was finished, with pre-installing upper strata 40 orders, the vibration pelletizing machine granulate of lower floor's 80 mesh sieves sieved 1-3 time, and fine powder adds the new granulation again of granulating of next groove, and coarse granule is treated down batch production, adds during pulverizing.Get Radix Codonopsis superfine powder granule.Sampling censorship: moisture, granularity.
6. get qualified superfine powder granule, control packing room temperature 18-26 degree in the scope of relative humidity 45-65%, carries out packing and outer package by specification, gets finished product.
Embodiment two: the system Radix Salviae Miltiorrhizae
1. impurity, the foreign body that wherein is mingled with removed in selection, and dis-medicinal part gets clean medical material.
2. get the clean medical material after the selection, pulverize with the Universalpulverizer of prepackage 100 mesh sieves, Radix Salviae Miltiorrhizae coarse powder flour.
3. micronizing with the Radix Salviae Miltiorrhizae coarse powder flour of above gained, is controlled temperature 18-26 degree between pulverizing, relative temperature through micronizing, is controlled air inlet operating pressure 〉=0.7Mpa below 55%, 30-35 revolutions per second of grader rotating speed (clockwise) is crushed to more than 300 orders, gets the Radix Salviae Miltiorrhizae superfine powder.
4. get above gained Radix Salviae Miltiorrhizae superfine powder, put in the flute profile mixing and blending machine, make an amount of system soft material with the ethanol of 90-95%; oscillating granulator through pre-installing 30 mesh sieves is granulated; the wet granular that makes is put in the heated-air circulation oven, and design temperature 60--70 degree is dried to moisture≤5%
5. with pre-installing upper strata 40 orders, the vibration pelletizing machine granulate of lower floor's 80 mesh sieves sieves 1-3 time, and fine powder adds the new granulation again of granulating of next groove, and coarse granule is treated down batch production, adds during pulverizing.Get Radix Salviae Miltiorrhizae superfine powder granule.Sampling censorship: moisture, granularity.
6. get qualified superfine powder granule, control packing room temperature 18-26 degree in the scope of relative humidity 45-65%, carries out packing and outer package by specification, gets finished product.
Claims (5)
1. the processing method of a Chinese crude drug breaking cellular wall powder, its processing steps is:
(1) medicinal material processing: it gets clean medical material after comprising selection, section, drying;
(2) pulverize: with above-mentioned clean medical material, pulverize with the Universalpulverizer of 100 mesh sieves, wall breaking pulverization gets the above coarse powder of 60 orders;
(3) wall breaking pulverization: the coarse powder flour with above gained, be crushed to more than 300 orders through the breaking cellular wall powder, obtain superfine powder;
(4) granulate: get above gained superfine powder, put in the flute profile mixing and blending machine, water or ethanol are made soft material, granulate through the oscillating granulator of 30 mesh sieves, and the wet granular that makes is put in the heated-air circulation oven and dried;
(5) granulate, screening: with upper strata 40 orders, the vibration pelletizing machine of lower floor's 80 mesh sieves is made granule between 40 orders-80 order with above-mentioned granulation granulate screening 1-3 time.
(6) packing and packing: get qualified superfine powder granule, packing and outer package get finished product.
2. the processing method of a kind of Chinese crude drug breaking cellular wall powder according to claim 1 is characterized in that, when grinding and processing, temperature is the 18-26 degree between pulverizing, and relative humidity is below 55%, and the air inlet operating pressure is 〉=0.7Mpa that the grader rotating speed is 30-35 revolutions per second.
3. the processing method of a kind of Chinese crude drug breaking cellular wall powder according to claim 1 is characterized in that, adds man-hour at wall breaking pulverization, temperature is the 18-26 degree between pulverizing, relative humidity is below 55%, and the air inlet operating pressure is 〉=0.7Mpa that the grader rotating speed is 30-35 revolutions per second.
4. the processing method of a kind of Chinese crude drug breaking cellular wall powder according to claim 1 is characterized in that, adds man-hour in granulation, and temperature is the 60-70 degree, and being dried to moisture is≤6.5%.
5. the processing method of a kind of Chinese crude drug breaking cellular wall powder according to claim 1 is characterized in that, when packing and package processing, the temperature of packing chamber is the 18-26 degree, and relative humidity is the 45-65 degree.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2006101221717A CN101147746B (en) | 2006-09-18 | 2006-09-18 | Method for processing traditional Chinese herbs broken wall powder |
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|---|---|---|---|
| CN2006101221717A CN101147746B (en) | 2006-09-18 | 2006-09-18 | Method for processing traditional Chinese herbs broken wall powder |
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| CN1194667C (en) * | 2001-05-17 | 2005-03-30 | 湖南省中医药研究院 | Process for preparing superfine particles of Chinese medicine |
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