CN101062769A - 人造金刚石提纯工艺方法 - Google Patents
人造金刚石提纯工艺方法 Download PDFInfo
- Publication number
- CN101062769A CN101062769A CN 200710054425 CN200710054425A CN101062769A CN 101062769 A CN101062769 A CN 101062769A CN 200710054425 CN200710054425 CN 200710054425 CN 200710054425 A CN200710054425 A CN 200710054425A CN 101062769 A CN101062769 A CN 101062769A
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- China
- Prior art keywords
- diamond
- acid
- ball milling
- graphite
- sulfuric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 229910003460 diamond Inorganic materials 0.000 title claims abstract description 41
- 239000010432 diamond Substances 0.000 title claims abstract description 41
- 238000000746 purification Methods 0.000 title claims description 12
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 32
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000002184 metal Substances 0.000 claims abstract description 12
- 229910052751 metal Inorganic materials 0.000 claims abstract description 12
- 239000002245 particle Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000006243 chemical reaction Methods 0.000 claims description 24
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 23
- 230000015572 biosynthetic process Effects 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 16
- 238000003786 synthesis reaction Methods 0.000 claims description 16
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 15
- 238000000498 ball milling Methods 0.000 claims description 15
- 239000010439 graphite Substances 0.000 claims description 15
- 229910002804 graphite Inorganic materials 0.000 claims description 15
- 229910017604 nitric acid Inorganic materials 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 11
- 238000007873 sieving Methods 0.000 claims description 6
- 238000013467 fragmentation Methods 0.000 claims description 2
- 238000006062 fragmentation reaction Methods 0.000 claims description 2
- 239000002699 waste material Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 9
- 239000002253 acid Substances 0.000 abstract description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000003595 mist Substances 0.000 abstract description 3
- FPVGTPBMTFTMRT-NSKUCRDLSA-L fast yellow Chemical compound [Na+].[Na+].C1=C(S([O-])(=O)=O)C(N)=CC=C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 FPVGTPBMTFTMRT-NSKUCRDLSA-L 0.000 abstract description 2
- KCLANYCVBBTKTO-UHFFFAOYSA-N Proparacaine Chemical compound CCCOC1=CC=C(C(=O)OCCN(CC)CC)C=C1N KCLANYCVBBTKTO-UHFFFAOYSA-N 0.000 abstract 1
- 229940087458 alcaine Drugs 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000003672 processing method Methods 0.000 description 6
- 239000012535 impurity Substances 0.000 description 3
- 239000001117 sulphuric acid Substances 0.000 description 3
- 235000011149 sulphuric acid Nutrition 0.000 description 3
- 238000011109 contamination Methods 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 229910052582 BN Inorganic materials 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000002161 passivation Methods 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
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- Carbon And Carbon Compounds (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2007100544250A CN100497169C (zh) | 2007-05-18 | 2007-05-18 | 人造金刚石提纯工艺方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2007100544250A CN100497169C (zh) | 2007-05-18 | 2007-05-18 | 人造金刚石提纯工艺方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101062769A true CN101062769A (zh) | 2007-10-31 |
CN100497169C CN100497169C (zh) | 2009-06-10 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CNB2007100544250A Expired - Fee Related CN100497169C (zh) | 2007-05-18 | 2007-05-18 | 人造金刚石提纯工艺方法 |
Country Status (1)
Country | Link |
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CN (1) | CN100497169C (zh) |
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102757044A (zh) * | 2012-07-23 | 2012-10-31 | 河南省联合磨料磨具有限公司 | 高切削力金刚石微粉及其制备方法 |
CN103043658A (zh) * | 2012-12-14 | 2013-04-17 | 河南富耐克超硬材料股份有限公司 | 一种提纯金刚石或立方氮化硼磨料的方法 |
CN103043632A (zh) * | 2012-12-14 | 2013-04-17 | 河南富耐克超硬材料股份有限公司 | 一种金刚石、立方氮化硼磨料或微粉的提纯方法 |
CN105439138A (zh) * | 2015-11-20 | 2016-03-30 | 西安文理学院 | 一种纳米金刚石及其制备方法 |
CN106365685A (zh) * | 2016-08-29 | 2017-02-01 | 河南飞孟金刚石工业有限公司 | 一种白色人造钻石的提纯工艺 |
WO2017050264A1 (zh) * | 2015-09-25 | 2017-03-30 | 郑州华晶金刚石股份有限公司 | 一种新型可控型的层状结构的纳米钻石烯 |
CN106587046A (zh) * | 2016-12-30 | 2017-04-26 | 郑州大学 | 一种人造金刚石的提纯方法 |
CN106927460A (zh) * | 2015-12-30 | 2017-07-07 | 曾舟华 | 金刚石回收的反应加速器及其使用方法 |
CN107128909A (zh) * | 2017-06-26 | 2017-09-05 | 湖北鄂信钻石科技股份有限公司 | 一种铁基触媒的人造金刚石的提纯方法 |
CN108793154A (zh) * | 2018-07-20 | 2018-11-13 | 河南省亚龙超硬材料有限公司 | 一种高纯度金刚石微粉杂质的处理方法 |
CN109678148A (zh) * | 2018-12-21 | 2019-04-26 | 河南烯碳合成材料有限公司 | 一种人造金刚石生产废渣中石墨的提纯方法、锂离子电池用石墨负极材料及其制备方法 |
CN113772636A (zh) * | 2021-09-27 | 2021-12-10 | 郑州中南杰特超硬材料有限公司 | 一种立方氮化硼单晶的提纯方法 |
CN115340089A (zh) * | 2022-08-24 | 2022-11-15 | 内蒙古唐合科技有限公司 | 一种人造金刚石的提纯方法 |
-
2007
- 2007-05-18 CN CNB2007100544250A patent/CN100497169C/zh not_active Expired - Fee Related
Cited By (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102757044A (zh) * | 2012-07-23 | 2012-10-31 | 河南省联合磨料磨具有限公司 | 高切削力金刚石微粉及其制备方法 |
CN102757044B (zh) * | 2012-07-23 | 2013-06-05 | 河南省联合磨料磨具有限公司 | 高切削力金刚石微粉及其制备方法 |
CN103043658A (zh) * | 2012-12-14 | 2013-04-17 | 河南富耐克超硬材料股份有限公司 | 一种提纯金刚石或立方氮化硼磨料的方法 |
CN103043632A (zh) * | 2012-12-14 | 2013-04-17 | 河南富耐克超硬材料股份有限公司 | 一种金刚石、立方氮化硼磨料或微粉的提纯方法 |
CN103043658B (zh) * | 2012-12-14 | 2014-09-17 | 河南富耐克超硬材料股份有限公司 | 一种提纯金刚石或立方氮化硼磨料的方法 |
CN103043632B (zh) * | 2012-12-14 | 2015-04-08 | 河南富耐克超硬材料股份有限公司 | 一种金刚石、立方氮化硼磨料或微粉的提纯方法 |
WO2017050264A1 (zh) * | 2015-09-25 | 2017-03-30 | 郑州华晶金刚石股份有限公司 | 一种新型可控型的层状结构的纳米钻石烯 |
CN105439138A (zh) * | 2015-11-20 | 2016-03-30 | 西安文理学院 | 一种纳米金刚石及其制备方法 |
CN105439138B (zh) * | 2015-11-20 | 2017-06-27 | 西安文理学院 | 一种纳米金刚石及其制备方法 |
CN106927460A (zh) * | 2015-12-30 | 2017-07-07 | 曾舟华 | 金刚石回收的反应加速器及其使用方法 |
CN106365685A (zh) * | 2016-08-29 | 2017-02-01 | 河南飞孟金刚石工业有限公司 | 一种白色人造钻石的提纯工艺 |
CN106587046A (zh) * | 2016-12-30 | 2017-04-26 | 郑州大学 | 一种人造金刚石的提纯方法 |
CN106587046B (zh) * | 2016-12-30 | 2018-10-23 | 郑州大学 | 一种人造金刚石的提纯方法 |
CN107128909A (zh) * | 2017-06-26 | 2017-09-05 | 湖北鄂信钻石科技股份有限公司 | 一种铁基触媒的人造金刚石的提纯方法 |
CN108793154A (zh) * | 2018-07-20 | 2018-11-13 | 河南省亚龙超硬材料有限公司 | 一种高纯度金刚石微粉杂质的处理方法 |
CN109678148A (zh) * | 2018-12-21 | 2019-04-26 | 河南烯碳合成材料有限公司 | 一种人造金刚石生产废渣中石墨的提纯方法、锂离子电池用石墨负极材料及其制备方法 |
CN113772636A (zh) * | 2021-09-27 | 2021-12-10 | 郑州中南杰特超硬材料有限公司 | 一种立方氮化硼单晶的提纯方法 |
CN115340089A (zh) * | 2022-08-24 | 2022-11-15 | 内蒙古唐合科技有限公司 | 一种人造金刚石的提纯方法 |
CN115340089B (zh) * | 2022-08-24 | 2024-02-06 | 内蒙古唐合科技有限公司 | 一种人造金刚石的提纯方法 |
Also Published As
Publication number | Publication date |
---|---|
CN100497169C (zh) | 2009-06-10 |
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Legal Events
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
ASS | Succession or assignment of patent right |
Owner name: NANYANG SINO-SOUTH AFRICAN DIAMOND COMPANY LIMITE Free format text: FORMER OWNER: HENAN ZHONGNAN INDUSTRIAL CO., LTD. Effective date: 20080111 |
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C41 | Transfer of patent application or patent right or utility model | ||
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Effective date of registration: 20080111 Address after: Nanyang City, Henan Province Town South Gao Gou Cun in Fangcheng County Guangyang company hospital post encoding: 473200 Applicant after: Nanyang Zhongnan Diamond Co., Ltd. Address before: Fangcheng County of Nanyang City, Henan province box 101 Henan Zhongnan Industrial Co Ltd postal encoding: 473000 Applicant before: Nanyang Zhongnan Diamond Co., Ltd. |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: ZHONGNAN DIAMOND CO., LTD. Free format text: FORMER OWNER: NANYANG SINO-SOUTH AFRICAN DIAMOND COMPANY LIMITED Effective date: 20091127 |
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C41 | Transfer of patent application or patent right or utility model | ||
TR01 | Transfer of patent right |
Effective date of registration: 20091127 Address after: Fangcheng County of Nanyang City, Henan province 101. Patentee after: Zhongnan Diamond Co., Ltd. Address before: Nanyang City, Henan Province Town South Gao Gou Cun in Fangcheng County Guangyang company hospital Patentee before: Nanyang Zhongnan Diamond Co., Ltd. |
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C56 | Change in the name or address of the patentee |
Owner name: ZHONGNAN DIOMAND CO., LTD. Free format text: FORMER NAME: ZHONGNAN DIAMOND CO., LTD. |
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CP03 | Change of name, title or address |
Address after: Fangcheng County of Nanyang City, Henan province 473264 box 101 Patentee after: ZHONGNAN DIAMOND CO., LTD. Address before: Fangcheng County of Nanyang City, Henan province 473200 box 101 Patentee before: Zhongnan Diamond Co., Ltd. |
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CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090610 Termination date: 20160518 |