CN100590173C - 一种荧光粉及其制造方法和所制成的电光源 - Google Patents
一种荧光粉及其制造方法和所制成的电光源 Download PDFInfo
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- CN100590173C CN100590173C CN200610065812A CN200610065812A CN100590173C CN 100590173 C CN100590173 C CN 100590173C CN 200610065812 A CN200610065812 A CN 200610065812A CN 200610065812 A CN200610065812 A CN 200610065812A CN 100590173 C CN100590173 C CN 100590173C
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- fluorescent material
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- light led
- salt
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- 238000004519 manufacturing process Methods 0.000 title claims description 20
- 239000000843 powder Substances 0.000 title abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 39
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 14
- 229910052712 strontium Inorganic materials 0.000 claims abstract description 12
- 239000000126 substance Substances 0.000 claims abstract description 12
- 229910052688 Gadolinium Inorganic materials 0.000 claims abstract description 9
- 229910052746 lanthanum Inorganic materials 0.000 claims abstract description 9
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 9
- 229910052727 yttrium Inorganic materials 0.000 claims abstract description 9
- 229910052684 Cerium Inorganic materials 0.000 claims abstract description 8
- 229910052693 Europium Inorganic materials 0.000 claims abstract description 8
- 229910052689 Holmium Inorganic materials 0.000 claims abstract description 8
- 229910052779 Neodymium Inorganic materials 0.000 claims abstract description 8
- 229910052777 Praseodymium Inorganic materials 0.000 claims abstract description 8
- 229910052706 scandium Inorganic materials 0.000 claims abstract description 8
- 229910052769 Ytterbium Inorganic materials 0.000 claims abstract description 7
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 7
- 229910052744 lithium Inorganic materials 0.000 claims abstract description 6
- 229910052700 potassium Inorganic materials 0.000 claims abstract description 6
- 229910052771 Terbium Inorganic materials 0.000 claims abstract description 5
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 5
- 239000010703 silicon Substances 0.000 claims abstract description 5
- 239000000463 material Substances 0.000 claims description 61
- 150000001875 compounds Chemical class 0.000 claims description 16
- 150000003839 salts Chemical class 0.000 claims description 12
- 239000012535 impurity Substances 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 238000005303 weighing Methods 0.000 claims description 4
- 238000013467 fragmentation Methods 0.000 claims description 3
- 238000006062 fragmentation reaction Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000007873 sieving Methods 0.000 claims description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 2
- 229910002651 NO3 Inorganic materials 0.000 claims description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 claims description 2
- -1 organic acid salt Chemical class 0.000 claims description 2
- 238000005554 pickling Methods 0.000 claims description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 9
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract description 5
- 229910052782 aluminium Inorganic materials 0.000 abstract description 5
- 229910052733 gallium Inorganic materials 0.000 abstract description 5
- 229910052736 halogen Inorganic materials 0.000 abstract description 5
- 150000002367 halogens Chemical class 0.000 abstract description 5
- 229910052761 rare earth metal Inorganic materials 0.000 abstract description 5
- 150000002910 rare earth metals Chemical class 0.000 abstract description 5
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 abstract description 3
- 229910052772 Samarium Inorganic materials 0.000 abstract description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 3
- 229910052760 oxygen Inorganic materials 0.000 abstract description 3
- 239000001301 oxygen Substances 0.000 abstract description 3
- 229910052788 barium Inorganic materials 0.000 abstract 2
- 229910052748 manganese Inorganic materials 0.000 abstract 1
- 230000001960 triggered effect Effects 0.000 abstract 1
- 241001025261 Neoraja caerulea Species 0.000 description 9
- 229910016036 BaF 2 Inorganic materials 0.000 description 4
- 229910004298 SiO 2 Inorganic materials 0.000 description 4
- 150000001342 alkaline earth metals Chemical class 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 230000005284 excitation Effects 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 2
- 230000000295 complement effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000000695 excitation spectrum Methods 0.000 description 2
- 230000004907 flux Effects 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 206010023126 Jaundice Diseases 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 229910052915 alkaline earth metal silicate Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
- C09K11/7783—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing two or more rare earth metals one of which being europium
- C09K11/77924—Aluminosilicates
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
- C09K11/7766—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing two or more rare earth metals
- C09K11/77744—Aluminosilicates
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L33/00—Semiconductor devices having potential barriers specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof
- H01L33/48—Semiconductor devices having potential barriers specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof characterised by the semiconductor body packages
- H01L33/50—Wavelength conversion elements
- H01L33/501—Wavelength conversion elements characterised by the materials, e.g. binder
- H01L33/502—Wavelength conversion materials
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- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Luminescent Compositions (AREA)
- Applications Or Details Of Rotary Compressors (AREA)
- Exhaust Gas Treatment By Means Of Catalyst (AREA)
- Catalysts (AREA)
Abstract
Description
Claims (11)
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200610065812A CN100590173C (zh) | 2006-03-24 | 2006-03-24 | 一种荧光粉及其制造方法和所制成的电光源 |
KR1020087025883A KR101025966B1 (ko) | 2006-03-24 | 2007-03-16 | 형광체 및 그의 제조 방법 및 그를 사용하는 발광 소자 |
PCT/CN2007/000852 WO2007109978A1 (fr) | 2006-03-24 | 2007-03-16 | Phosphore, son procédé de production et dispositif photo-luminescent utilisant ledit phosphore |
DE112007000656.0T DE112007000656B4 (de) | 2006-03-24 | 2007-03-16 | Leuchtstoff, Verfahren zur Herstellung desselben und lichtemittierende Vorrichtungen unter Verwendung desselben |
JP2009500691A JP5005759B2 (ja) | 2006-03-24 | 2007-03-16 | 蛍光粉及びその製造方法並びにそれを用いた発光器具 |
US12/232,604 US7955524B2 (en) | 2006-03-24 | 2008-09-19 | Phosphor, its preparation method and light emitting devices using the same |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200610065812A CN100590173C (zh) | 2006-03-24 | 2006-03-24 | 一种荧光粉及其制造方法和所制成的电光源 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101041775A CN101041775A (zh) | 2007-09-26 |
CN100590173C true CN100590173C (zh) | 2010-02-17 |
Family
ID=38540803
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN200610065812A Active CN100590173C (zh) | 2006-03-24 | 2006-03-24 | 一种荧光粉及其制造方法和所制成的电光源 |
Country Status (6)
Country | Link |
---|---|
US (1) | US7955524B2 (zh) |
JP (1) | JP5005759B2 (zh) |
KR (1) | KR101025966B1 (zh) |
CN (1) | CN100590173C (zh) |
DE (1) | DE112007000656B4 (zh) |
WO (1) | WO2007109978A1 (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104342156A (zh) * | 2013-07-30 | 2015-02-11 | 宁波升谱光电半导体有限公司 | 一种荧光粉及其制备方法和含该荧光粉的发光器件 |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101182416B (zh) * | 2006-11-13 | 2010-09-22 | 北京有色金属研究总院 | 含二价金属元素的铝酸盐荧光粉及制造方法和发光器件 |
CN101307228B (zh) * | 2008-02-29 | 2011-11-30 | 中国计量学院 | 氯铝硅酸盐荧光粉及其制备方法 |
US8703016B2 (en) | 2008-10-22 | 2014-04-22 | General Electric Company | Phosphor materials and related devices |
US8329060B2 (en) * | 2008-10-22 | 2012-12-11 | General Electric Company | Blue-green and green phosphors for lighting applications |
KR20100070731A (ko) | 2008-12-18 | 2010-06-28 | 삼성전자주식회사 | 할로실리케이트 형광체, 이를 포함하는 백색 발광 소자 |
JP5391946B2 (ja) * | 2009-09-07 | 2014-01-15 | 日亜化学工業株式会社 | 蛍光体及びそれを用いた発光装置並びに蛍光体の製造方法 |
CN101705095B (zh) * | 2009-09-21 | 2011-08-10 | 四川新力光源有限公司 | 黄光余辉材料及其制备方法和使用它的led照明装置 |
KR101098006B1 (ko) * | 2009-09-29 | 2011-12-23 | 한국화학연구원 | (할로)실리케이트계 형광체 및 이의 제조방법 |
EP2553049B1 (en) | 2010-03-31 | 2017-03-22 | Osram Sylvania Inc. | Phosphor and leds containing same |
US8932486B2 (en) | 2011-04-07 | 2015-01-13 | Performance Indicator, Llc | Persistent phosphors of alkaline earths modified by halides and 3d ions |
CN103980900B (zh) * | 2014-06-04 | 2015-05-20 | 重庆理工大学 | 一种硅酸盐蓝光荧光粉及其制备方法 |
CN105670626B (zh) * | 2015-12-21 | 2017-11-10 | 厦门百嘉祥微晶材料科技股份有限公司 | 一种超大粒径YAG:Ce3+黄色荧光粉及其制备方法 |
WO2021199677A1 (ja) * | 2020-03-31 | 2021-10-07 | パナソニックIpマネジメント株式会社 | 固体電解質材料、それを用いた電池、および固体電解質材料の製造方法 |
CN116875303A (zh) * | 2023-06-02 | 2023-10-13 | 常熟理工学院 | 一种铝酸盐基红发光材料及其制备方法、应用 |
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DE10355301B3 (de) * | 2003-11-27 | 2005-06-23 | Infineon Technologies Ag | Verfahren zur Abbildung einer Struktur auf einen Halbleiter-Wafer mittels Immersionslithographie |
JP2005175034A (ja) * | 2003-12-09 | 2005-06-30 | Canon Inc | 露光装置 |
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Cited By (2)
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CN104342156A (zh) * | 2013-07-30 | 2015-02-11 | 宁波升谱光电半导体有限公司 | 一种荧光粉及其制备方法和含该荧光粉的发光器件 |
CN104342156B (zh) * | 2013-07-30 | 2016-08-10 | 宁波升谱光电股份有限公司 | 一种荧光粉及其制备方法和含该荧光粉的发光器件 |
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CN101041775A (zh) | 2007-09-26 |
DE112007000656T5 (de) | 2009-02-12 |
JP5005759B2 (ja) | 2012-08-22 |
KR101025966B1 (ko) | 2011-03-30 |
WO2007109978A1 (fr) | 2007-10-04 |
US7955524B2 (en) | 2011-06-07 |
KR20080110857A (ko) | 2008-12-19 |
JP2009530448A (ja) | 2009-08-27 |
US20090050918A1 (en) | 2009-02-26 |
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