CN100475785C - 经吸附分离用于制备表面活性剂的改进方法及其产物 - Google Patents
经吸附分离用于制备表面活性剂的改进方法及其产物 Download PDFInfo
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- CN100475785C CN100475785C CNB2003101220778A CN200310122077A CN100475785C CN 100475785 C CN100475785 C CN 100475785C CN B2003101220778 A CNB2003101220778 A CN B2003101220778A CN 200310122077 A CN200310122077 A CN 200310122077A CN 100475785 C CN100475785 C CN 100475785C
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
- C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
- C07C303/06—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups by reaction with sulfuric acid or sulfur trioxide
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
- C07C15/02—Monocyclic hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
- C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique
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- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Water Supply & Treatment (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Detergent Compositions (AREA)
- Steroid Compounds (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
Description
A | B | C | D | E | F | |
MAS | 22 | 16.5 | 11 | 1-5.5 | 10-25 | 5-35 |
以下任何组合:C45ASC45E1SLASC16SASC14-17NaPSC14-18MESMBAS16.5MBAE2S15.5 | 0 | 1-5.5 | 11 | 16.5 | 0-5 | 0-10 |
QAS | 0-2 | 0-2 | 0-2 | 0-2 | 0-4 | 0 |
C23E6.5或C457 | 1.5 | 1.5 | 1.5 | 1.5 | 0-4 | 0-4 |
沸石A | 27.8 | 0 | 27.8 | 27.8 | 20-30 | 0 |
沸石MAP | 0 | 27.8 | 0 | 0 | 0 | 0 |
三多磷酸钠 | 0 | 0 | 0 | 0 | 0 | 5-40 |
PAA | 2.3 | 2.3 | 2.3 | 2.3 | 0-5 | 0-5 |
碳酸盐 | 27.3 | 27.3 | 27.3 | 27.3 | 20-30 | 0-30 |
硅酸盐 | 0.6 | 0.6 | 0.6 | 0.6 | 0-2 | 0-6 |
PB1 | 1.0 | 1.0 | 0-10 | 0-10 | 0-10 | 0-20 |
NOBS | 0-1 | 0-1 | 0-1 | 0-1 | 0.5-3 | 0-5 |
LOBS | 0 | 0 | 0-3 | 0 | 0 | 0 |
TAED | 0 | 0 | 0 | 2 | 0 | 0-5 |
MnCAT | 0 | 0 | 0 | 0 | 2ppm | 0-1 |
蛋白酶 | 0-0.5 | 0-0.5 | 0-0.5 | 0-0.5 | 0-0.5 | 0-1 |
纤维素酶 | 0-0.3 | 0-0.3 | 0-0.3 | 0-0.3 | 0-0.5 | 0-1 |
淀粉酶 | 0-0.5 | 0-0.5 | 0-0.5 | 0-0.5 | 0-1 | 0-1 |
SRP1或SRP2 | 0.4 | 0.4 | 0.4 | 0.4 | 0-1 | 0-5 |
增亮剂1或2 | 0.2 | 0.2 | 0.2 | 0.2 | 0-0.3 | 0-5 |
PEG | 1.6 | 1.6 | 1.6 | 1.6 | 0-2 | 0-3 |
聚硅氧烷消泡剂 | 0.42 | 0.42 | 0.42 | 0.42 | 0-0.5 | 0-1 |
硫酸盐,水,次要成分 | 至100% | 至100% | 至100% | 至100% | 至100% | 至100% |
密度(克/升) | 400-700 | 600-700 | 600-700 | 600-700 | 600-700 | 450-750 |
A | B | C | D | E | |
MAS | 1-7 | 7-12 | 12-17 | 17-22 | 1-35 |
以下任何组合:C25AE<sub>x</sub>S<sup>*</sup>Na(x=1.8-2.5)MBAE1.8S15.5MBAS15.5C25AS(线形至高2-烷基)C14-17NaPSC12-16SASC18 1,4硫酸氢盐LASC12-16MES | 15-21 | 10-15 | 5-10 | 0-5 | 0-25 |
LMFAA | 0-3.5 | 0-3.5 | 0-3.5 | 0-3.5 | 0-8 |
C23E9或C23E6.5 | 0-2 | 0-2 | 0-2 | 0-2 | 0-8 |
APA | 0-0.5 | 0-0.5 | 0-0.5 | 0-0.5 | 0-2 |
柠檬酸 | 5 | 5 | 5 | 5 | 0-8 |
脂肪酸(TPK或C12/14)2 | 2 | 2 | 2 | 2 | 0-14 |
EtOH | 4 | 4 | 4 | 4 | 0-8 |
PG | 6 | 6 | 6 | 6 | 0-10 |
MEA | 1 | 1 | 1 | 1 | 0-3 |
NaOH | 3 | 3 | 3 | 3 | 0-7 |
Na TS | 2.3 | 2.3 | 2.3 | 2.3 | 0-4 |
甲酸钠 | 0.1 | 0.1 | 0.1 | 0.1 | 0-1 |
Borax | 2.5 | 2.5 | 2.5 | 2.5 | 0-5 |
蛋白酶 | 0.9 | 0.9 | 0.9 | 0.9 | 0-1.3 |
脂酶 | 0.06 | 0.06 | 0.06 | 0.06 | 0-0.3 |
淀粉酶 | 0.15 | 0.15 | 0.15 | 0.15 | 0-0.4 |
纤维素酶 | 0.05 | 0.05 | 0.05 | 0.05 | 0-0.2 |
PAE | 0-0.6 | 0-0.6 | 0-0.6 | 0-0.6 | 0-2.5 |
PIE | 1.2 | 1.2 | 1.2 | 1.2 | 0-2.5 |
PAEC | 0-0.4 | 0-04 | 0-0.4 | 0-0.4 | 0-2 |
SRP2 | 0.2 | 0.2 | 0.2 | 0.2 | 0-0.5 |
增亮剂1或2 | 0.15 | 0.15 | 0.15 | 0.15 | 0-0.5 |
聚硅氧烷消泡剂 | 0.12 | 0.12 | 0.12 | 0.12 | 0-0.3 |
发烟硫酸 | 0.0015 | 0.0015 | 0.0015 | 0.0015 | 0-0.003 |
香料 | 0.3 | 0.3 | 0.3 | 0.3 | 0-0.6 |
染料 | 0.0013 | 0.0013 | 0.0013 | 0.0013 | 0-0.003 |
水分/次要成分 | 剩余部分 | 剩余部分 | 剩余部分 | 剩余部分 | 剩余部分 |
产品pH(在DI水中10%) | 7.7 | 7.7 | 7.7 | 7.7 | 6-9.5 |
Claims (31)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US5543797P | 1997-08-08 | 1997-08-08 | |
US60/055437 | 1997-08-08 |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB988097990A Division CN100339343C (zh) | 1997-08-08 | 1998-08-04 | 经吸附分离用于制备表面活性剂的改进方法及其产物 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1510029A CN1510029A (zh) | 2004-07-07 |
CN100475785C true CN100475785C (zh) | 2009-04-08 |
Family
ID=21997789
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB988097990A Expired - Fee Related CN100339343C (zh) | 1997-08-08 | 1998-08-04 | 经吸附分离用于制备表面活性剂的改进方法及其产物 |
CNA2003101220763A Pending CN1508126A (zh) | 1997-08-08 | 1998-08-04 | 经吸附分离用于制备表面活性剂的改进方法及其产物 |
CNB2003101220778A Expired - Fee Related CN100475785C (zh) | 1997-08-08 | 1998-08-04 | 经吸附分离用于制备表面活性剂的改进方法及其产物 |
Family Applications Before (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB988097990A Expired - Fee Related CN100339343C (zh) | 1997-08-08 | 1998-08-04 | 经吸附分离用于制备表面活性剂的改进方法及其产物 |
CNA2003101220763A Pending CN1508126A (zh) | 1997-08-08 | 1998-08-04 | 经吸附分离用于制备表面活性剂的改进方法及其产物 |
Country Status (16)
Country | Link |
---|---|
US (2) | US6525233B1 (zh) |
EP (1) | EP1027312B1 (zh) |
JP (1) | JP4434480B2 (zh) |
KR (1) | KR100447695B1 (zh) |
CN (3) | CN100339343C (zh) |
AT (1) | ATE286867T1 (zh) |
AU (4) | AU737587B2 (zh) |
BR (1) | BR9811870B1 (zh) |
CA (1) | CA2298618C (zh) |
CZ (1) | CZ299717B6 (zh) |
DE (1) | DE69828633T2 (zh) |
EG (1) | EG22740A (zh) |
ES (1) | ES2236930T3 (zh) |
HU (1) | HUP0003855A3 (zh) |
TR (1) | TR200000362T2 (zh) |
WO (1) | WO1999007656A2 (zh) |
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- 1998-08-04 KR KR10-2000-7001332A patent/KR100447695B1/ko not_active IP Right Cessation
- 1998-08-04 CN CNB988097990A patent/CN100339343C/zh not_active Expired - Fee Related
- 1998-08-04 CN CNA2003101220763A patent/CN1508126A/zh active Pending
- 1998-08-04 JP JP2000507194A patent/JP4434480B2/ja not_active Expired - Fee Related
- 1998-08-04 AU AU87719/98A patent/AU737587B2/en not_active Ceased
- 1998-08-04 TR TR2000/00362T patent/TR200000362T2/xx unknown
- 1998-08-04 AT AT98939249T patent/ATE286867T1/de not_active IP Right Cessation
- 1998-08-04 DE DE69828633T patent/DE69828633T2/de not_active Expired - Lifetime
- 1998-08-04 BR BRPI9811870-6A patent/BR9811870B1/pt not_active IP Right Cessation
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2000
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