CN100391663C - 一种纳米镍粉的制备方法 - Google Patents
一种纳米镍粉的制备方法 Download PDFInfo
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- CN100391663C CN100391663C CNB2006100255523A CN200610025552A CN100391663C CN 100391663 C CN100391663 C CN 100391663C CN B2006100255523 A CNB2006100255523 A CN B2006100255523A CN 200610025552 A CN200610025552 A CN 200610025552A CN 100391663 C CN100391663 C CN 100391663C
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- nickel
- nickel powder
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- nanometer
- reduction
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- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims abstract description 212
- 239000000843 powder Substances 0.000 title claims description 40
- 238000004519 manufacturing process Methods 0.000 title abstract description 25
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 62
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 60
- 238000000034 method Methods 0.000 claims abstract description 53
- 230000009467 reduction Effects 0.000 claims abstract description 31
- 229910052751 metal Inorganic materials 0.000 claims abstract description 22
- 239000002184 metal Substances 0.000 claims abstract description 22
- 239000007788 liquid Substances 0.000 claims abstract description 14
- 239000000654 additive Substances 0.000 claims abstract description 12
- 239000004020 conductor Substances 0.000 claims abstract description 12
- 239000003792 electrolyte Substances 0.000 claims abstract description 12
- 238000000926 separation method Methods 0.000 claims abstract description 10
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 238000001291 vacuum drying Methods 0.000 claims abstract description 6
- 230000008569 process Effects 0.000 claims description 25
- 238000006243 chemical reaction Methods 0.000 claims description 24
- 239000002245 particle Substances 0.000 claims description 18
- 238000003487 electrochemical reaction Methods 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 11
- 238000002360 preparation method Methods 0.000 claims description 11
- 238000012856 packing Methods 0.000 claims description 10
- 238000012545 processing Methods 0.000 claims description 9
- WJYIASZWHGOTOU-UHFFFAOYSA-N Heptylamine Chemical class CCCCCCCN WJYIASZWHGOTOU-UHFFFAOYSA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 206010013647 Drowning Diseases 0.000 claims description 5
- 238000002848 electrochemical method Methods 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 238000009736 wetting Methods 0.000 claims description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 239000010949 copper Substances 0.000 claims description 2
- AZHSSKPUVBVXLK-UHFFFAOYSA-N ethane-1,1-diol Chemical compound CC(O)O AZHSSKPUVBVXLK-UHFFFAOYSA-N 0.000 claims description 2
- 239000011521 glass Substances 0.000 claims description 2
- 239000002351 wastewater Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 230000000996 additive effect Effects 0.000 abstract description 10
- 239000002912 waste gas Substances 0.000 abstract description 5
- 230000008901 benefit Effects 0.000 abstract description 3
- 238000010301 surface-oxidation reaction Methods 0.000 abstract description 3
- 239000003638 chemical reducing agent Substances 0.000 abstract description 2
- 239000003344 environmental pollutant Substances 0.000 abstract description 2
- 231100000719 pollutant Toxicity 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 27
- 235000019441 ethanol Nutrition 0.000 description 19
- 229910001453 nickel ion Inorganic materials 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 238000005516 engineering process Methods 0.000 description 6
- 238000001914 filtration Methods 0.000 description 6
- 239000002699 waste material Substances 0.000 description 6
- 238000007599 discharging Methods 0.000 description 5
- 150000005846 sugar alcohols Polymers 0.000 description 5
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 4
- 230000009471 action Effects 0.000 description 4
- 239000003153 chemical reaction reagent Substances 0.000 description 4
- 230000005611 electricity Effects 0.000 description 4
- 238000005868 electrolysis reaction Methods 0.000 description 4
- 239000002086 nanomaterial Substances 0.000 description 4
- 239000003960 organic solvent Substances 0.000 description 4
- 239000004033 plastic Substances 0.000 description 4
- 238000004064 recycling Methods 0.000 description 4
- 238000007789 sealing Methods 0.000 description 4
- 229910000838 Al alloy Inorganic materials 0.000 description 3
- IKHGUXGNUITLKF-XPULMUKRSA-N acetaldehyde Chemical compound [14CH]([14CH3])=O IKHGUXGNUITLKF-XPULMUKRSA-N 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- 238000009834 vaporization Methods 0.000 description 3
- 230000008016 vaporization Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 125000005909 ethyl alcohol group Chemical group 0.000 description 2
- 230000003203 everyday effect Effects 0.000 description 2
- 150000002815 nickel Chemical class 0.000 description 2
- 238000011946 reduction process Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000011858 nanopowder Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CNB2006100255523A CN100391663C (zh) | 2006-04-10 | 2006-04-10 | 一种纳米镍粉的制备方法 |
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CNB2006100255523A CN100391663C (zh) | 2006-04-10 | 2006-04-10 | 一种纳米镍粉的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN1827266A CN1827266A (zh) | 2006-09-06 |
CN100391663C true CN100391663C (zh) | 2008-06-04 |
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CNB2006100255523A Active CN100391663C (zh) | 2006-04-10 | 2006-04-10 | 一种纳米镍粉的制备方法 |
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Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101428348B (zh) * | 2008-07-29 | 2010-09-08 | 张建玲 | 一种水热处理制备球形超细金属粉末的工艺方法 |
KR101576320B1 (ko) * | 2008-10-24 | 2015-12-09 | 가부시키가이샤 닛신 세이훈 구루프혼샤 | 분체의 분급 방법 |
CN101709489B (zh) * | 2009-11-12 | 2011-03-23 | 中南大学 | 一种用纯硫酸镍溶液直接电积生产镍粉的方法 |
CN102586800B (zh) * | 2011-01-17 | 2015-05-13 | 李小毛 | 一种纳米铜粉的制备方法 |
CN102634816B (zh) * | 2011-02-14 | 2014-11-19 | 李小毛 | 一种纳米氧化铟锡粉的制备方法 |
CN103464784B (zh) * | 2013-09-27 | 2016-01-20 | 南开大学 | 一种碳负载纳米镍的制备方法 |
CN103722167A (zh) * | 2013-12-10 | 2014-04-16 | 大连理工大学 | 一种六水氯化镍的乙醇溶液中电沉积制备纳米镍粉的方法 |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH11152507A (ja) * | 1997-09-11 | 1999-06-08 | Mitsui Mining & Smelting Co Ltd | ニッケル微粉末の製造方法 |
CN1457948A (zh) * | 2002-05-15 | 2003-11-26 | 中国科学院过程工程研究所 | 棒状金属镍粉的制备方法 |
JP2004035901A (ja) * | 2002-06-28 | 2004-02-05 | Murata Mfg Co Ltd | ニッケル粉末の製造方法、ニッケル粉末、導電性ペースト、及び積層セラミック電子部品 |
CN1597198A (zh) * | 2003-08-26 | 2005-03-23 | 株式会社村田制作所 | 镍粉末的制造方法 |
CN1631588A (zh) * | 2004-11-18 | 2005-06-29 | 上海大学 | 纳米镍的制造方法 |
CN1644282A (zh) * | 2005-01-13 | 2005-07-27 | 南京大学 | 一种纳米金属镍粉的制备方法 |
JP2005240076A (ja) * | 2004-02-24 | 2005-09-08 | Fujikura Ltd | 酸化物含有ニッケル粉末の製造方法 |
CN1683101A (zh) * | 2004-04-16 | 2005-10-19 | Tdk株式会社 | 镍粉的制造方法、镍粉的制造装置及镍粉制造用坩埚 |
-
2006
- 2006-04-10 CN CNB2006100255523A patent/CN100391663C/zh active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH11152507A (ja) * | 1997-09-11 | 1999-06-08 | Mitsui Mining & Smelting Co Ltd | ニッケル微粉末の製造方法 |
CN1457948A (zh) * | 2002-05-15 | 2003-11-26 | 中国科学院过程工程研究所 | 棒状金属镍粉的制备方法 |
JP2004035901A (ja) * | 2002-06-28 | 2004-02-05 | Murata Mfg Co Ltd | ニッケル粉末の製造方法、ニッケル粉末、導電性ペースト、及び積層セラミック電子部品 |
CN1597198A (zh) * | 2003-08-26 | 2005-03-23 | 株式会社村田制作所 | 镍粉末的制造方法 |
JP2005240076A (ja) * | 2004-02-24 | 2005-09-08 | Fujikura Ltd | 酸化物含有ニッケル粉末の製造方法 |
CN1683101A (zh) * | 2004-04-16 | 2005-10-19 | Tdk株式会社 | 镍粉的制造方法、镍粉的制造装置及镍粉制造用坩埚 |
CN1631588A (zh) * | 2004-11-18 | 2005-06-29 | 上海大学 | 纳米镍的制造方法 |
CN1644282A (zh) * | 2005-01-13 | 2005-07-27 | 南京大学 | 一种纳米金属镍粉的制备方法 |
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Publication number | Publication date |
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CN1827266A (zh) | 2006-09-06 |
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Assignee: Hefei quantum source nano Polytron Technologies Inc Assignor: Li Xiaomao Contract record no.: 2011340000020 Denomination of invention: Nanometer nickel powder preparing process Granted publication date: 20080604 License type: Exclusive License Open date: 20060906 Record date: 20110407 |
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Assignee: Hefei quantum source nano Polytron Technologies Inc Assignor: Li Xiaomao Contract record no.: 2011340000020 Date of cancellation: 20190509 |
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Application publication date: 20060906 Assignee: Hefei quantum source nano Polytron Technologies Inc Assignor: Li Xiaomao Contract record no.: 2019340000006 Denomination of invention: Nanometer nickel powder preparing process Granted publication date: 20080604 License type: Exclusive License Record date: 20190513 |
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Effective date of registration: 20201022 Address after: 244000 office building, No. 618 Hengsheng Road, suburb of Tongling City, Anhui Province Patentee after: Anhui nalomite New Material Technology Co., Ltd Address before: 230000 No. 5, No. 96, Jinzhai Road, Anhui, Hefei, 31 Patentee before: Li Xiaomao |