BRPI0401037A - Processo para a preparação de n-metil-dialquilaminas a partir de dialquilaminas secundárias e formaldeìdo - Google Patents
Processo para a preparação de n-metil-dialquilaminas a partir de dialquilaminas secundárias e formaldeìdoInfo
- Publication number
- BRPI0401037A BRPI0401037A BR0401037-0A BRPI0401037A BRPI0401037A BR PI0401037 A BRPI0401037 A BR PI0401037A BR PI0401037 A BRPI0401037 A BR PI0401037A BR PI0401037 A BRPI0401037 A BR PI0401037A
- Authority
- BR
- Brazil
- Prior art keywords
- dialkylamines
- formaldehyde
- methyl
- preparation
- moles
- Prior art date
Links
Classifications
-
- H—ELECTRICITY
- H04—ELECTRIC COMMUNICATION TECHNIQUE
- H04M—TELEPHONIC COMMUNICATION
- H04M1/00—Substation equipment, e.g. for use by subscribers
- H04M1/02—Constructional features of telephone sets
- H04M1/0202—Portable telephone sets, e.g. cordless phones, mobile phones or bar type handsets
- H04M1/0249—Details of the mechanical connection between the housing parts or relating to the method of assembly
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
- C07C209/28—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with other reducing agents
-
- H—ELECTRICITY
- H04—ELECTRIC COMMUNICATION TECHNIQUE
- H04M—TELEPHONIC COMMUNICATION
- H04M1/00—Substation equipment, e.g. for use by subscribers
- H04M1/02—Constructional features of telephone sets
- H04M1/0202—Portable telephone sets, e.g. cordless phones, mobile phones or bar type handsets
- H04M1/026—Details of the structure or mounting of specific components
- H04M1/0277—Details of the structure or mounting of specific components for a printed circuit board assembly
Abstract
"PROCESSO PARA A PREPARAçãO DE N-METILDIALQUILAMINAS A PARTIR DE DIALQUILAMINAS SECUNDáRIAS E FORMALDEìDO". A presente invenção refere-se a um processo para a preparação de N-metil-dialquilaminas mediante reação de dialquilaminas secundárias com formaldeído a uma temperatura de 100 até 200<198>C, sendo que para cada mol de dialquilamina secundária são aplicados 1,5 até 3 moles de formaldeído e o produto de reação obtido é desgaseificado, a fase aquosa é separada e a fase orgânica é destilada.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10316375A DE10316375A1 (de) | 2003-04-10 | 2003-04-10 | Verfahren zur Herstellung von N-Methyl-dialkylaminen aus sekundären Dialkylaminen und Formaldehyd |
Publications (1)
Publication Number | Publication Date |
---|---|
BRPI0401037A true BRPI0401037A (pt) | 2004-12-21 |
Family
ID=32864416
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR0401037-0A BRPI0401037A (pt) | 2003-04-10 | 2004-04-08 | Processo para a preparação de n-metil-dialquilaminas a partir de dialquilaminas secundárias e formaldeìdo |
Country Status (9)
Country | Link |
---|---|
US (1) | US6982352B2 (pt) |
EP (1) | EP1466887A1 (pt) |
JP (1) | JP2004315523A (pt) |
KR (1) | KR20040089533A (pt) |
CN (1) | CN100345818C (pt) |
BR (1) | BRPI0401037A (pt) |
DE (1) | DE10316375A1 (pt) |
MX (1) | MXPA04003288A (pt) |
ZA (1) | ZA200402776B (pt) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20090278794A1 (en) * | 2008-05-09 | 2009-11-12 | Smart Technologies Ulc | Interactive Input System With Controlled Lighting |
EP2279164B1 (de) * | 2008-05-13 | 2012-03-28 | Basf Se | Verfahren zur herstellung von n,n-substituierten-1,3-propandiaminen |
FR2933404B1 (fr) * | 2008-07-04 | 2011-12-30 | Arkema France | N-ethylmethylamine de haute purete et son procede de preparation |
CN102180797A (zh) * | 2011-03-17 | 2011-09-14 | 浙江大学 | N,n–二乙基异丙胺的合成方法 |
US8663457B2 (en) | 2011-11-23 | 2014-03-04 | General Electric Company | Methods and compounds for improving sulfide scavenging activity |
KR20130073822A (ko) * | 2011-12-23 | 2013-07-03 | 가부시키가이샤 한도오따이 에네루기 켄큐쇼 | 이온 액체, 비수 전해질 및 축전 장치 |
US9108899B2 (en) | 2011-12-30 | 2015-08-18 | General Electric Company | Sulfide scavengers, methods for making and methods for using |
DE102012014395B3 (de) * | 2012-07-13 | 2013-08-22 | Oxea Gmbh | Isononylamine ausgehend von 2-Ethylhexanol, Verfahren zu ihrer Herstellung sowie ihre Verwendung |
MX2022007419A (es) * | 2019-12-16 | 2022-07-13 | Basf Se | Proceso para la preparacion de compuestos de piperidina. |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE287802C (pt) | ||||
DE80520C (pt) | ||||
US2298284A (en) * | 1940-05-02 | 1942-10-13 | William S Emerson | Reductive alkylation |
US3025313A (en) * | 1957-06-28 | 1962-03-13 | Dearborn Chemicals Co | Amino-aldehyde condensation product |
US3136819A (en) * | 1958-05-16 | 1964-06-09 | Armour & Co | Preparation of tertiary aliphatic methyl amines |
US3136765A (en) * | 1959-10-22 | 1964-06-09 | Basf Ag | Processes for reacting dialkyl amines and heterocyclic secondary bases with formaldehyde and an alpha-hydroxyacetylene |
US3210349A (en) * | 1961-11-06 | 1965-10-05 | Jefferson Chem Co Inc | Methylation of primary and secondary amines using a small stoichiometric excess of formaldehyde and adding a small stoichiometric excess of formic acid last |
US4190601A (en) * | 1978-05-31 | 1980-02-26 | Union Carbide Corporation | Production of tertiary amines by reductive alkylation |
JPS60130551A (ja) * | 1983-12-16 | 1985-07-12 | Kao Corp | 第3級アミンの製造方法 |
DE3721539A1 (de) * | 1987-06-30 | 1989-01-12 | Ruhrchemie Ag | Verfahren zur herstellung von methylaminen |
US5091584A (en) * | 1989-02-28 | 1992-02-25 | E. I. Du Pont De Nemours And Company | Process of preparing formaldehyde/amine adducts |
DE4035307A1 (de) * | 1990-11-07 | 1992-05-14 | Hoechst Ag | Verfahren zur herstellung von n-methyl-alkylaminen |
US5091585A (en) * | 1990-12-21 | 1992-02-25 | Texaco Chemical Company | Continuous preparatin of tertiary aliphatic methyl amines |
JP3457029B2 (ja) * | 1992-09-11 | 2003-10-14 | チバ スペシャルティ ケミカルズ ホールディング インコーポレーテッド | アミン類の製造方法 |
DE59605564D1 (de) * | 1995-03-28 | 2000-08-17 | Hoffmann La Roche | Aminomethylierung von Tocopherolen |
US6949642B2 (en) * | 2001-04-19 | 2005-09-27 | Bristol-Myers Squibb Co. | Production of tertiary amines by reductive amination |
-
2003
- 2003-04-10 DE DE10316375A patent/DE10316375A1/de not_active Withdrawn
-
2004
- 2004-03-19 US US10/804,747 patent/US6982352B2/en not_active Expired - Fee Related
- 2004-04-01 EP EP04007896A patent/EP1466887A1/de not_active Withdrawn
- 2004-04-07 MX MXPA04003288A patent/MXPA04003288A/es active IP Right Grant
- 2004-04-08 JP JP2004113783A patent/JP2004315523A/ja not_active Ceased
- 2004-04-08 BR BR0401037-0A patent/BRPI0401037A/pt not_active Application Discontinuation
- 2004-04-08 ZA ZA200402776A patent/ZA200402776B/xx unknown
- 2004-04-09 KR KR1020040024457A patent/KR20040089533A/ko not_active Application Discontinuation
- 2004-04-09 CN CNB2004100337312A patent/CN100345818C/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
US6982352B2 (en) | 2006-01-03 |
CN1597659A (zh) | 2005-03-23 |
KR20040089533A (ko) | 2004-10-21 |
ZA200402776B (en) | 2004-10-26 |
EP1466887A1 (de) | 2004-10-13 |
MXPA04003288A (es) | 2004-11-29 |
US20040204611A1 (en) | 2004-10-14 |
CN100345818C (zh) | 2007-10-31 |
JP2004315523A (ja) | 2004-11-11 |
DE10316375A1 (de) | 2004-11-04 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B11A | Dismissal acc. art.33 of ipl - examination not requested within 36 months of filing | ||
B11Y | Definitive dismissal acc. article 33 of ipl - extension of time limit for request of examination expired |