BR112014015064A2 - método para preparar composição contendo piperazina e aminoetiletanolamina - Google Patents

método para preparar composição contendo piperazina e aminoetiletanolamina

Info

Publication number
BR112014015064A2
BR112014015064A2 BR112014015064A BR112014015064A BR112014015064A2 BR 112014015064 A2 BR112014015064 A2 BR 112014015064A2 BR 112014015064 A BR112014015064 A BR 112014015064A BR 112014015064 A BR112014015064 A BR 112014015064A BR 112014015064 A2 BR112014015064 A2 BR 112014015064A2
Authority
BR
Brazil
Prior art keywords
aminoethylethanolamine
composition containing
preparing composition
containing piperazine
piperazine
Prior art date
Application number
BR112014015064A
Other languages
English (en)
Inventor
Onam Sadeka
W King Stephen
Z Srnak Thomas
Original Assignee
Dow Global Technologies Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies Llc filed Critical Dow Global Technologies Llc
Publication of BR112014015064A2 publication Critical patent/BR112014015064A2/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/12—Silica and alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/889—Manganese, technetium or rhenium
    • B01J23/8896—Rhenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
    • C07D295/023—Preparation; Separation; Stabilisation; Use of additives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

resumo “método para preparar composição contendo piperazina e aminoetiletanolamina” a invenção provê um método para a aminação redutiva de dietanolamina para formar uma composição de produto que inclui piperazina (pip) e aminoetiletanolamina (aeea). um catalisador com suporte de alumina transitória/segundo óxido metálico e uma mistura de metais catalíticos é utilizada para a reação que resulta em baixos níveis de produtos secundários sem pip e sem aeea. 1/1
BR112014015064A 2011-12-22 2012-11-14 método para preparar composição contendo piperazina e aminoetiletanolamina BR112014015064A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201161579508P 2011-12-22 2011-12-22
PCT/US2012/064966 WO2013095810A1 (en) 2011-12-22 2012-11-14 Reductive amination of diethanolamine and resulting product mixture

Publications (1)

Publication Number Publication Date
BR112014015064A2 true BR112014015064A2 (pt) 2017-06-13

Family

ID=47279064

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112014015064A BR112014015064A2 (pt) 2011-12-22 2012-11-14 método para preparar composição contendo piperazina e aminoetiletanolamina

Country Status (6)

Country Link
US (1) US9353044B2 (pt)
EP (1) EP2794581B1 (pt)
JP (1) JP6158831B2 (pt)
CN (1) CN104144918B (pt)
BR (1) BR112014015064A2 (pt)
WO (1) WO2013095810A1 (pt)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3555043B1 (en) 2016-12-15 2021-10-27 Nouryon Chemicals International B.V. Process for manufacturing hydroxyethyl ethylene amines
CN110072838B (zh) * 2016-12-15 2022-04-15 阿克苏诺贝尔化学品国际有限公司 制备亚乙基胺的方法
US20200171465A1 (en) * 2017-07-28 2020-06-04 Dow Global Technologies Llc Method for preparation of heterogeneous catalysts

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE330699B (pt) 1966-08-02 1970-11-30 Mo Och Domsjoe Ab
IT967651B (it) 1972-09-20 1974-03-11 Sir Soc Italiana Resine Spa Perfezionamenti nei procedimenti per la preparazione di etanolam mine
US4123462A (en) * 1976-01-07 1978-10-31 Union Carbide Corporation Amination process using nickel-rhenium catalysts
US4400539A (en) * 1981-09-30 1983-08-23 Union Carbide Corporation Process for the manufacture of ethylenediamine
SE461095B (sv) 1983-09-09 1990-01-08 Berol Kemi Ab Amineringsfoerfarande med anvaendning av en ruteniumdopad nickel och/eller kovoltkatalysator
US4863890A (en) * 1983-09-09 1989-09-05 Berol Kemi Ab Process for preparing a ruthenium-promoted, halogen-containing nickel and/or cobalt catalyst and a catalyst prepared by the process
DE69512381T2 (de) * 1993-12-22 2000-04-06 Union Carbide Chemicals & Plastics Technology Corp., Danbury Reduktive Aminierung zur selektiven Herstellung von Aminoethylethanolamin
CA2146906C (en) * 1993-12-22 1999-03-16 Stephen Wayne King Reductive amination catalysts
US5851948A (en) 1996-08-20 1998-12-22 Hydrocarbon Technologies, Inc. Supported catalyst and process for catalytic oxidation of volatile organic compounds
US6534441B1 (en) * 1999-03-06 2003-03-18 Union Carbide Chemicals & Plastics Technology Corporation Nickel-rhenium catalyst for use in reductive amination processes
EP1249440A1 (en) 2001-04-10 2002-10-16 Taiwan Styrene Monomer Corporation Process for preparing linear alkylbenzenes
DE10346779A1 (de) 2003-10-08 2005-05-12 Basf Ag Verfahren zur Abtrennung von Triethanolamin aus einem durch die Umsetzung von Ammoniak mit Ethylenoxid erhaltenen Stoffgemisch
WO2006053342A2 (en) 2004-11-12 2006-05-18 Osi Pharmaceuticals, Inc. Integrin antagonists useful as anticancer agents
US20060104895A1 (en) 2004-11-18 2006-05-18 Saint-Gobain Ceramics & Plastics, Inc. Transitional alumina particulate materials having controlled morphology and processing for forming same
CN102239134B (zh) * 2008-10-06 2014-04-16 陶氏环球技术有限责任公司 由环氧乙烷和氨制造乙醇胺类和1，2-亚乙基胺类的方法及相关方法

Also Published As

Publication number Publication date
US20140371452A1 (en) 2014-12-18
US9353044B2 (en) 2016-05-31
EP2794581A1 (en) 2014-10-29
CN104144918B (zh) 2018-06-01
JP6158831B2 (ja) 2017-07-05
WO2013095810A1 (en) 2013-06-27
JP2015508394A (ja) 2015-03-19
EP2794581B1 (en) 2016-05-25
CN104144918A (zh) 2014-11-12

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Legal Events

Date Code Title Description
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]
B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]
B350 Update of information on the portal [chapter 15.35 patent gazette]