AU2001270604A1 - Method for producing cathodes and anodes for electrochemical systems, metallised material used therein, method and device for production of said metallised material - Google Patents
Method for producing cathodes and anodes for electrochemical systems, metallised material used therein, method and device for production of said metallised materialInfo
- Publication number
- AU2001270604A1 AU2001270604A1 AU2001270604A AU7060401A AU2001270604A1 AU 2001270604 A1 AU2001270604 A1 AU 2001270604A1 AU 2001270604 A AU2001270604 A AU 2001270604A AU 7060401 A AU7060401 A AU 7060401A AU 2001270604 A1 AU2001270604 A1 AU 2001270604A1
- Authority
- AU
- Australia
- Prior art keywords
- fibres
- production
- anodes
- cathodes
- metallised material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0402—Methods of deposition of the material
- H01M4/0421—Methods of deposition of the material involving vapour deposition
- H01M4/0428—Chemical vapour deposition
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0402—Methods of deposition of the material
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0402—Methods of deposition of the material
- H01M4/0404—Methods of deposition of the material by coating on electrode collectors
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0402—Methods of deposition of the material
- H01M4/0421—Methods of deposition of the material involving vapour deposition
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0402—Methods of deposition of the material
- H01M4/0421—Methods of deposition of the material involving vapour deposition
- H01M4/0423—Physical vapour deposition
- H01M4/0426—Sputtering
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/043—Processes of manufacture in general involving compressing or compaction
- H01M4/0435—Rolling or calendering
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0438—Processes of manufacture in general by electrochemical processing
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0438—Processes of manufacture in general by electrochemical processing
- H01M4/045—Electrochemical coating; Electrochemical impregnation
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0438—Processes of manufacture in general by electrochemical processing
- H01M4/045—Electrochemical coating; Electrochemical impregnation
- H01M4/0452—Electrochemical coating; Electrochemical impregnation from solutions
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/049—Manufacturing of an active layer by chemical means
- H01M4/0492—Chemical attack of the support material
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/64—Carriers or collectors
- H01M4/66—Selection of materials
- H01M4/661—Metal or alloys, e.g. alloy coatings
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/64—Carriers or collectors
- H01M4/70—Carriers or collectors characterised by shape or form
- H01M4/72—Grids
- H01M4/74—Meshes or woven material; Expanded metal
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/64—Carriers or collectors
- H01M4/70—Carriers or collectors characterised by shape or form
- H01M4/80—Porous plates, e.g. sintered carriers
- H01M4/806—Nonwoven fibrous fabric containing only fibres
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/64—Carriers or collectors
- H01M4/70—Carriers or collectors characterised by shape or form
- H01M4/80—Porous plates, e.g. sintered carriers
- H01M4/808—Foamed, spongy materials
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2913—Rod, strand, filament or fiber
- Y10T428/2933—Coated or with bond, impregnation or core
- Y10T428/294—Coated or with bond, impregnation or core including metal or compound thereof [excluding glass, ceramic and asbestos]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2913—Rod, strand, filament or fiber
- Y10T428/2933—Coated or with bond, impregnation or core
- Y10T428/294—Coated or with bond, impregnation or core including metal or compound thereof [excluding glass, ceramic and asbestos]
- Y10T428/2942—Plural coatings
- Y10T428/2947—Synthetic resin or polymer in plural coatings, each of different type
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2913—Rod, strand, filament or fiber
- Y10T428/2933—Coated or with bond, impregnation or core
- Y10T428/294—Coated or with bond, impregnation or core including metal or compound thereof [excluding glass, ceramic and asbestos]
- Y10T428/2958—Metal or metal compound in coating
Abstract
The invention relates to the production of composite cathodes and anodes for lithium batteries, and the cathodes and anodes thereby produced. The active mass in the form of a thin film is incorporated into a material, or the active mass together with a matrix metal or a matrix alloy is deposited on a substrate. The invention also relates to a metallized, textile material made of insulating fibres which have been made conductive and which have been completely galvanically or electrolessly plated. The fibres lying on crossovers are not baked with other fibres, but can move freely. The surface of the material is thereby optimally used. Said material is preferably used as an anode or a cathode for batteries, especially a lithium battery, and fuel cells. During the galvanizing or electroless application stage in the production of the material, the fibres in the material move relatively to each other in order to avoid baking. A device for said production process comprises first rollers ( 13 ) with an elliptical cross-section and second rollers ( 14 ) with a diagonal circumferential profile ( 15 ), which extend or move the material ( 10 ) passing thereover, and conveyed thereby, in the longitudinal and lateral direction.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10031633.6 | 2000-06-29 | ||
DE10031633 | 2000-06-29 | ||
PCT/EP2001/007467 WO2002001656A2 (en) | 2000-06-29 | 2001-06-29 | Method for producing cathodes and anodes for electrochemical systems, metallised material used therein, method and device for production of said metallised material |
Publications (1)
Publication Number | Publication Date |
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AU2001270604A1 true AU2001270604A1 (en) | 2002-01-08 |
Family
ID=7647179
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AU2001270604A Abandoned AU2001270604A1 (en) | 2000-06-29 | 2001-06-29 | Method for producing cathodes and anodes for electrochemical systems, metallised material used therein, method and device for production of said metallised material |
Country Status (7)
Country | Link |
---|---|
US (2) | US7344776B2 (en) |
EP (1) | EP1299916B1 (en) |
AT (1) | ATE270791T1 (en) |
AU (1) | AU2001270604A1 (en) |
DE (1) | DE50102800D1 (en) |
ES (1) | ES2225574T3 (en) |
WO (1) | WO2002001656A2 (en) |
Families Citing this family (40)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ATE270791T1 (en) * | 2000-06-29 | 2004-07-15 | Wolfgang Kollmann | METHOD FOR PRODUCING A METALIZED MATERIAL, AND BATTERY AND FUEL CELL CONTAINING SAME |
AT409973B (en) * | 2001-09-28 | 2002-12-27 | Funktionswerkstoffe Forschungs | Flexible electrically conductive layer used for flat positive electrode of alkali or alkali ion battery comprises support having surface partially covered by alloy coating |
DE10342974A1 (en) * | 2003-09-17 | 2005-04-14 | Wühr, Manfred, Dr. | Primer for bonding electrochemically active layers to electrodes in electrochemical cells, e.g. lithium cells and lithium ion cells, contains a lithium borosilicate compound as binder |
DE102006019669A1 (en) * | 2006-04-27 | 2007-11-15 | Lisa Dräxlmaier GmbH | Decorative trim for automobile, truck, bus, boat or aircraft interior has non-woven textile whose fibers incorporate metallic component |
DE102006019675B3 (en) * | 2006-04-27 | 2007-11-15 | Lisa Dräxlmaier GmbH | Interior trim part for use in e.g. passenger car, has lower layer made of leather such as cracked leather or leather-like material, and opaque upper layer covering lower layer, where upper layer has metalized textile fleece |
DE102006019668A1 (en) * | 2006-04-27 | 2007-11-15 | Lisa Dräxlmaier GmbH | Textile fibrous web for shielding e.g. car telephone, has metallic coating as visible component of interior fitting part that has coating laid on fibrous web, where fibrous web is made of fabric such as polyester fiber |
ATE446393T1 (en) * | 2006-06-08 | 2009-11-15 | Bct Coating Technologies Ag | DEVICE FOR THE GALVANIC DEPOSITION OF SURFACES AND GALVANIZING SYSTEM |
US7718319B2 (en) | 2006-09-25 | 2010-05-18 | Board Of Regents, The University Of Texas System | Cation-substituted spinel oxide and oxyfluoride cathodes for lithium ion batteries |
DE102008033217A1 (en) * | 2008-07-15 | 2010-01-21 | Dritte Patentportfolio Beteiligungsgesellschaft Mbh & Co.Kg | solar panel |
US8221938B2 (en) * | 2008-08-08 | 2012-07-17 | GM Global Technology Operations LLC | Method of making a stable hydrophilic coating/surface on carbon-based materials for fuel cell applications |
CN102379050B (en) * | 2009-02-04 | 2014-06-11 | 应用材料公司 | Porous three dimensional copper, tin, copper-tin, copper-tin-cobalt, and copper-tin-cobalt-titanium electrodes for batteries and ultra capacitors |
US8206569B2 (en) | 2009-02-04 | 2012-06-26 | Applied Materials, Inc. | Porous three dimensional copper, tin, copper-tin, copper-tin-cobalt, and copper-tin-cobalt-titanium electrodes for batteries and ultra capacitors |
DE102009013058A1 (en) | 2009-03-16 | 2010-09-23 | Wolfgang Kollmann | Metal structure comprises a flat substrate made of non-conductive fibers, which form a cross-linked thread-structure, where the substrate is a non-woven and is metallized with a metal on one side |
CN102714299A (en) * | 2009-10-23 | 2012-10-03 | 应用材料公司 | Nucleation and growth of tin particles into three dimensional composite active anode for lithium high capacity energy storage device |
KR20120102680A (en) * | 2009-11-11 | 2012-09-18 | 암프리우스, 인코포레이티드 | Intermediate layers for electrode fabrication |
DE102010008782A1 (en) | 2010-02-22 | 2011-08-25 | Platingtech Beschichtung Gmbh | Negative electrode, useful for lithium ion battery, comprises metal or metal alloy coated polymer matrix as current collector and composite material embedded in it, which contains metal, semi-metal or alloy and/or intermetallic phase |
FR2958799B1 (en) * | 2010-04-08 | 2012-09-14 | Pragma Ind | ANODE AND CATHODE BONDING STRIPS OF AN ELECTROCHEMICAL CONVERTER AND CONVERTER COMPRISING THE SAME |
KR101271492B1 (en) * | 2010-12-02 | 2013-06-05 | 주식회사 엘지화학 | Novel Device for Cutting Electrode Sheet and Secondary Battery Manufactured Using the Same |
DE102011004233A1 (en) * | 2011-02-16 | 2012-08-16 | Varta Micro Innovation Gmbh | Electrodes for batteries, in particular for lithium-ion batteries, and their manufacture |
US9240585B2 (en) | 2011-02-28 | 2016-01-19 | Applied Materials, Inc. | Manufacturing of high capacity prismatic lithium-ion alloy anodes |
US9012092B2 (en) * | 2011-04-04 | 2015-04-21 | Laor Consulting Llc | Fiber felt capacitors and batteries |
EP2522794A1 (en) | 2011-05-13 | 2012-11-14 | Carpet Concept Objekt-Teppichboden GmbH | System for energy and/or data production and contacting unit for same |
KR101612473B1 (en) * | 2011-06-21 | 2016-04-14 | 하이드로 알루미늄 롤드 프로덕츠 게엠베하 | Chemically treated current collector foil produced of aluminum or an aluminum alloy |
EP2727175A4 (en) | 2011-07-01 | 2015-07-01 | Amprius Inc | Template electrode structures with enhanced adhesion characteristics |
DE102011122658A1 (en) * | 2011-12-30 | 2013-07-04 | Li-Tec Battery Gmbh | Process and system for the production of electrochemical cells for electrochemical energy storage |
KR20130133624A (en) * | 2012-05-29 | 2013-12-09 | (주)오렌지파워 | Electrode for lithium rechargeable battery and lithium rechargeable battery including the same |
CN102903879A (en) * | 2012-08-02 | 2013-01-30 | 龙能科技(苏州)有限公司 | Method for preparing organic-inorganic composite diaphragm used for secondary cell |
EP2793303B1 (en) | 2013-04-16 | 2017-08-09 | VARTA Micro Innovation GmbH | Lithium ion cell having optimized electrode kinetics |
US10311536B1 (en) * | 2014-02-27 | 2019-06-04 | Walgreen Co. | System and method for automating pharmacy processing of electronic prescriptions |
AU2016370962B2 (en) | 2015-12-16 | 2020-09-24 | 6K Inc. | Spheroidal dehydrogenated metals and metal alloy particles |
KR102368088B1 (en) * | 2017-05-19 | 2022-02-24 | 삼성에스디아이 주식회사 | lithium secondary battery |
KR102341464B1 (en) * | 2018-05-04 | 2021-12-22 | 주식회사 엘지에너지솔루션 | Cutting device and method for electrode sheet |
DE102018207391A1 (en) * | 2018-05-14 | 2019-11-14 | Aucos Ag | Process for producing an electrode film and electrode |
EP3962678A4 (en) | 2019-04-30 | 2023-01-11 | 6K Inc. | Mechanically alloyed powder feedstock |
EP4061787A1 (en) | 2019-11-18 | 2022-09-28 | 6K Inc. | Unique feedstocks for spherical powders and methods of manufacturing |
US11590568B2 (en) | 2019-12-19 | 2023-02-28 | 6K Inc. | Process for producing spheroidized powder from feedstock materials |
CN116034496A (en) | 2020-06-25 | 2023-04-28 | 6K有限公司 | Microcosmic composite alloy structure |
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CN117581400A (en) * | 2021-04-29 | 2024-02-20 | 香港理工大学 | Battery current collector and method for manufacturing same |
CN114214711B (en) * | 2021-11-22 | 2023-08-08 | 深圳金美新材料科技有限公司 | Multifunctional composite film production and processing system and production and processing method |
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US5584893A (en) * | 1995-11-17 | 1996-12-17 | Valence Technology, Inc. | Method of preparing electrodes for an electrochemical cell |
JP3703582B2 (en) * | 1996-02-22 | 2005-10-05 | 呉羽化学工業株式会社 | Electrode binder, electrode binder solution, electrode mixture, electrode structure and battery |
US5616152A (en) * | 1996-04-10 | 1997-04-01 | Valence Technology, Inc. | Method of preparing electrodes |
US5789110A (en) * | 1996-09-27 | 1998-08-04 | Valence Technology, Inc. | Cathode-active material blends comprising Lix Mn2 O4 (0<x≦2) |
US6096101A (en) * | 1997-03-05 | 2000-08-01 | Valence Technology, Inc. | Method of preparing electrochemical cells |
ATE270791T1 (en) * | 2000-06-29 | 2004-07-15 | Wolfgang Kollmann | METHOD FOR PRODUCING A METALIZED MATERIAL, AND BATTERY AND FUEL CELL CONTAINING SAME |
-
2001
- 2001-06-29 AT AT01949450T patent/ATE270791T1/en active
- 2001-06-29 EP EP01949450A patent/EP1299916B1/en not_active Expired - Lifetime
- 2001-06-29 US US10/312,618 patent/US7344776B2/en not_active Expired - Fee Related
- 2001-06-29 WO PCT/EP2001/007467 patent/WO2002001656A2/en active IP Right Grant
- 2001-06-29 AU AU2001270604A patent/AU2001270604A1/en not_active Abandoned
- 2001-06-29 ES ES01949450T patent/ES2225574T3/en not_active Expired - Lifetime
- 2001-06-29 DE DE50102800T patent/DE50102800D1/en not_active Expired - Lifetime
-
2008
- 2008-02-14 US US12/031,494 patent/US20080261096A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
US20040013812A1 (en) | 2004-01-22 |
US7344776B2 (en) | 2008-03-18 |
EP1299916B1 (en) | 2004-07-07 |
WO2002001656A2 (en) | 2002-01-03 |
DE50102800D1 (en) | 2004-08-12 |
WO2002001656A9 (en) | 2003-05-15 |
ATE270791T1 (en) | 2004-07-15 |
WO2002001656A3 (en) | 2002-08-08 |
EP1299916A2 (en) | 2003-04-09 |
US20080261096A1 (en) | 2008-10-23 |
ES2225574T3 (en) | 2005-03-16 |
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