AR044616A1 - Proceso de extraccion para la remocion de impurezas de solucion madre en la sintesis de acido carboxilico - Google Patents
Proceso de extraccion para la remocion de impurezas de solucion madre en la sintesis de acido carboxilicoInfo
- Publication number
- AR044616A1 AR044616A1 ARP040101945A ARP040101945A AR044616A1 AR 044616 A1 AR044616 A1 AR 044616A1 AR P040101945 A ARP040101945 A AR P040101945A AR P040101945 A ARP040101945 A AR P040101945A AR 044616 A1 AR044616 A1 AR 044616A1
- Authority
- AR
- Argentina
- Prior art keywords
- stream
- solvent
- stock solution
- zone
- aqueous
- Prior art date
Links
- 238000000605 extraction Methods 0.000 title abstract 4
- 239000012535 impurity Substances 0.000 title abstract 4
- -1 CARBOXYL Chemical class 0.000 title 1
- 239000002253 acid Substances 0.000 title 1
- 230000015572 biosynthetic process Effects 0.000 title 1
- 239000010413 mother solution Substances 0.000 title 1
- 238000003786 synthesis reaction Methods 0.000 title 1
- 239000002904 solvent Substances 0.000 abstract 6
- 239000011550 stock solution Substances 0.000 abstract 5
- 238000001704 evaporation Methods 0.000 abstract 4
- 239000003054 catalyst Substances 0.000 abstract 2
- 230000008020 evaporation Effects 0.000 abstract 2
- 239000002184 metal Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 238000000926 separation method Methods 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000012452 mother liquor Substances 0.000 abstract 1
- 238000007670 refining Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J38/00—Regeneration or reactivation of catalysts, in general
- B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
- B01J38/06—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst using steam
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J38/00—Regeneration or reactivation of catalysts, in general
- B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/09—Reaction techniques
- Y10S423/14—Ion exchange; chelation or liquid/liquid ion extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
Reivindicación 1: Un proceso para recuperar un catalizador de metal de una solución madre, dicho proceso comprende los siguientes pasos: a) evaporar dicha solución madre que comprende un ácido carboxílico, dicho catalizador de metal, impurezas, agua y un disolvente en una primera zona de evaporación para producir una corriente de vapor y una corriente de solución madre concentrada; b) evaporar dicha corriente de solución madre concentrada en una segunda zona de evaporación para formar una corriente rica en disolvente y una corriente de solución madre superconcentrada; c) separar impurezas orgánicas con una solución de agua-disolvente de dicha corriente de solución madre superconcentrada en una zona de separación de sólido-líquido para formar una corriente acuosa y una segunda corriente acuosa; d) mezclar en una zona de mezclado agua y opcionalmente un disolvente de extracción con dicha corriente acuosa y dicha segunda corriente acuosa para formar una mezcla acuosa; e) agregar un disolvente de extracción a dicha mezcla acuosa en una zona de extracción para formar una corriente de extracto y una corriente de refinado; y f) opcionalmente separar dicha corriente de extracto en una zona de separación para formar una corriente de impurezas orgánicas de alto punto de ebullición y una corriente de disolvente de extracción recuperado.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/455,016 US7410632B2 (en) | 2003-06-05 | 2003-06-05 | Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid |
Publications (1)
Publication Number | Publication Date |
---|---|
AR044616A1 true AR044616A1 (es) | 2005-09-21 |
Family
ID=33159561
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ARP040101945A AR044616A1 (es) | 2003-06-05 | 2004-06-04 | Proceso de extraccion para la remocion de impurezas de solucion madre en la sintesis de acido carboxilico |
Country Status (15)
Country | Link |
---|---|
US (1) | US7410632B2 (es) |
EP (2) | EP2292581B1 (es) |
JP (1) | JP2004358466A (es) |
KR (1) | KR101169466B1 (es) |
CN (1) | CN1572765B (es) |
AR (1) | AR044616A1 (es) |
BR (1) | BRPI0401884A (es) |
CA (1) | CA2466999C (es) |
ES (1) | ES2437854T3 (es) |
MX (1) | MXPA04005328A (es) |
MY (1) | MY142041A (es) |
PL (1) | PL2292581T3 (es) |
PT (1) | PT2292581E (es) |
RU (1) | RU2345980C2 (es) |
TW (1) | TW200513454A (es) |
Families Citing this family (44)
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US7351396B2 (en) * | 2003-06-05 | 2008-04-01 | Eastman Chemical Company | Extraction process for removal of impurities from an aqueous mixture |
US7381386B2 (en) * | 2003-06-05 | 2008-06-03 | Eastman Chemical Company | Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid |
US7452522B2 (en) * | 2003-06-05 | 2008-11-18 | Eastman Chemical Company | Extraction process for removal of impurities from an oxidizer purge stream in the synthesis of carboxylic acid |
US7494641B2 (en) * | 2003-06-05 | 2009-02-24 | Eastman Chemical Company | Extraction process for removal of impurities from an oxidizer purge stream in the synthesis of carboxylic acid |
US7282151B2 (en) * | 2003-06-05 | 2007-10-16 | Eastman Chemical Company | Process for removal of impurities from mother liquor in the synthesis of carboxylic acid using pressure filtration |
US20070238899A9 (en) * | 2004-09-02 | 2007-10-11 | Robert Lin | Optimized production of aromatic dicarboxylic acids |
US7959879B2 (en) | 2004-09-02 | 2011-06-14 | Grupo Petrotemex, S.A. De C.V. | Optimized production of aromatic dicarboxylic acids |
US7888530B2 (en) * | 2004-09-02 | 2011-02-15 | Eastman Chemical Company | Optimized production of aromatic dicarboxylic acids |
US7273559B2 (en) | 2004-10-28 | 2007-09-25 | Eastman Chemical Company | Process for removal of impurities from an oxidizer purge stream |
US7291270B2 (en) | 2004-10-28 | 2007-11-06 | Eastman Chemical Company | Process for removal of impurities from an oxidizer purge stream |
US7402694B2 (en) * | 2005-08-11 | 2008-07-22 | Eastman Chemical Company | Process for removal of benzoic acid from an oxidizer purge stream |
US7569722B2 (en) * | 2005-08-11 | 2009-08-04 | Eastman Chemical Company | Process for removal of benzoic acid from an oxidizer purge stream |
US20070155987A1 (en) * | 2006-01-04 | 2007-07-05 | O'meadhra Ruairi S | Oxidative digestion with optimized agitation |
US8173836B2 (en) * | 2006-03-01 | 2012-05-08 | Grupo Petrotemex, S.A. De C.V. | Method and apparatus for drying carboxylic acid |
US7897808B2 (en) * | 2006-03-01 | 2011-03-01 | Eastman Chemical Company | Versatile oxidation byproduct purge process |
US7847121B2 (en) * | 2006-03-01 | 2010-12-07 | Eastman Chemical Company | Carboxylic acid production process |
US7326808B2 (en) * | 2006-03-01 | 2008-02-05 | Eastman Chemical Company | Polycarboxylic acid production system employing cooled mother liquor from oxidative digestion as feed to impurity purge system |
US7772424B2 (en) * | 2006-03-01 | 2010-08-10 | Eastman Chemical Company | Polycarboxylic acid production system employing enhanced evaporative concentration downstream of oxidative digestion |
US8697906B2 (en) * | 2006-03-01 | 2014-04-15 | Grupo Petrotemex, S.A. De C.V. | Methods and apparatus for producing a low-moisture carboxylic acid wet cake |
US20070208194A1 (en) | 2006-03-01 | 2007-09-06 | Woodruff Thomas E | Oxidation system with sidedraw secondary reactor |
US20070208199A1 (en) * | 2006-03-01 | 2007-09-06 | Kenny Randolph Parker | Methods and apparatus for isolating carboxylic acid |
US7326807B2 (en) * | 2006-03-01 | 2008-02-05 | Eastman Chemical Company | Polycarboxylic acid production system with enhanced heating for oxidative digestion |
US7420082B2 (en) * | 2006-03-01 | 2008-09-02 | Eastman Chemical Company | Polycarboxylic acid production system employing hot liquor removal downstream of oxidative digestion |
US7501537B2 (en) * | 2006-03-01 | 2009-03-10 | Eastman Chemical Company | Polycarboxylic acid production system employing oxidative digestion with reduced or eliminated upstream liquor exchange |
US7863483B2 (en) * | 2006-03-01 | 2011-01-04 | Eastman Chemical Company | Carboxylic acid production process |
US7816556B2 (en) * | 2006-03-01 | 2010-10-19 | Eastman Chemical Company | Polycarboxylic acid production system employing enhanced multistage oxidative digestion |
US7880032B2 (en) * | 2006-03-01 | 2011-02-01 | Eastman Chemical Company | Versatile oxidation byproduct purge process |
US7863481B2 (en) * | 2006-03-01 | 2011-01-04 | Eastman Chemical Company | Versatile oxidation byproduct purge process |
US7462736B2 (en) * | 2006-03-01 | 2008-12-09 | Eastman Chemical Company | Methods and apparatus for isolating carboxylic acid |
US7393973B2 (en) * | 2006-03-01 | 2008-07-01 | Eastman Chemical Company | Polycarboxylic acid production system with enhanced residence time distribution for oxidative digestion |
US20070203359A1 (en) * | 2006-03-01 | 2007-08-30 | Philip Edward Gibson | Versatile oxidation byproduct purge process |
ATE403636T1 (de) * | 2006-06-12 | 2008-08-15 | Hyosung Corp | Vorrichtung und verfahren zur rückgewinnung von essigsäure und katalysator in einem herstellungsverfahren von naphthalin-2,6- dicarbonsäure |
US7396457B2 (en) * | 2006-06-27 | 2008-07-08 | Hyosung Corporation | Apparatus and method for recovering acetic acid and catalyst in process for preparation of 2,6-naphthalenedicarboxylic acid |
US8466312B2 (en) * | 2010-08-20 | 2013-06-18 | Grupo Petrotemex, S.A. De C.V. | Terephthalic acid purge filtration rate by controlling % water in filter feed slurry |
US8167974B2 (en) * | 2010-08-20 | 2012-05-01 | Grupo Petrotemex, S.A. De C.V. | Terephthalic acid purge filtration rate by controlling % water in filter feed slurry |
KR101189798B1 (ko) * | 2011-08-17 | 2012-10-10 | 한국지질자원연구원 | 폐cmb촉매로부터 cma 액상촉매의 제조방법 |
US9604202B2 (en) * | 2014-05-08 | 2017-03-28 | Eastman Chemical Company | Furan-2,5-dicarboxylic acid purge process |
US10010812B2 (en) | 2014-05-08 | 2018-07-03 | Eastman Chemical Company | Furan-2,5-dicarboxylic acid purge process |
US9943834B2 (en) * | 2014-05-08 | 2018-04-17 | Eastman Chemical Company | Furan-2,5-dicarboxylic acid purge process |
US9944615B2 (en) | 2014-05-08 | 2018-04-17 | Eastman Chemical Company | Purifying crude furan 2,5-dicarboxylic acid by hydrogenation and a purge zone |
US20190023837A1 (en) | 2017-07-20 | 2019-01-24 | Eastman Chemical Company | Production of polyethylene furanoate in a retrofitted polyester plant |
US10344011B1 (en) | 2018-05-04 | 2019-07-09 | Eastman Chemical Company | Furan-2,5-dicarboxylic acid purge process |
US10526301B1 (en) | 2018-10-18 | 2020-01-07 | Eastman Chemical Company | Production of purified dialkyl-furan-2,5-dicarboxylate (DAFD) in a retrofitted DMT plant |
CN114804546B (zh) * | 2022-06-02 | 2023-03-17 | 无锡市兴盛环保设备有限公司 | 一种基于膜技术的pta母液回收处理方法 |
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US7282151B2 (en) * | 2003-06-05 | 2007-10-16 | Eastman Chemical Company | Process for removal of impurities from mother liquor in the synthesis of carboxylic acid using pressure filtration |
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US7863483B2 (en) * | 2006-03-01 | 2011-01-04 | Eastman Chemical Company | Carboxylic acid production process |
US7847121B2 (en) * | 2006-03-01 | 2010-12-07 | Eastman Chemical Company | Carboxylic acid production process |
US20070208199A1 (en) * | 2006-03-01 | 2007-09-06 | Kenny Randolph Parker | Methods and apparatus for isolating carboxylic acid |
-
2003
- 2003-06-05 US US10/455,016 patent/US7410632B2/en active Active
-
2004
- 2004-05-07 CA CA002466999A patent/CA2466999C/en not_active Expired - Lifetime
- 2004-05-14 EP EP10010238.3A patent/EP2292581B1/en not_active Expired - Lifetime
- 2004-05-14 PT PT100102383T patent/PT2292581E/pt unknown
- 2004-05-14 EP EP04011595A patent/EP1484307A1/en not_active Withdrawn
- 2004-05-14 PL PL10010238T patent/PL2292581T3/pl unknown
- 2004-05-14 ES ES10010238.3T patent/ES2437854T3/es not_active Expired - Lifetime
- 2004-05-21 TW TW093114497A patent/TW200513454A/zh unknown
- 2004-05-27 MY MYPI20042045A patent/MY142041A/en unknown
- 2004-05-31 BR BR0401884-2A patent/BRPI0401884A/pt not_active Application Discontinuation
- 2004-06-02 MX MXPA04005328A patent/MXPA04005328A/es active IP Right Grant
- 2004-06-03 KR KR1020040040386A patent/KR101169466B1/ko active IP Right Grant
- 2004-06-04 CN CN2004100452700A patent/CN1572765B/zh not_active Expired - Lifetime
- 2004-06-04 AR ARP040101945A patent/AR044616A1/es unknown
- 2004-06-04 RU RU2004117063/04A patent/RU2345980C2/ru active
- 2004-06-07 JP JP2004168839A patent/JP2004358466A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
PL2292581T3 (pl) | 2014-03-31 |
EP2292581B1 (en) | 2013-09-25 |
US7410632B2 (en) | 2008-08-12 |
RU2004117063A (ru) | 2006-01-10 |
EP2292581A1 (en) | 2011-03-09 |
KR20040108594A (ko) | 2004-12-24 |
EP1484307A1 (en) | 2004-12-08 |
MXPA04005328A (es) | 2007-11-14 |
RU2345980C2 (ru) | 2009-02-10 |
TW200513454A (en) | 2005-04-16 |
US20040244536A1 (en) | 2004-12-09 |
JP2004358466A (ja) | 2004-12-24 |
CA2466999A1 (en) | 2004-12-05 |
CA2466999C (en) | 2009-08-18 |
CN1572765B (zh) | 2013-04-17 |
ES2437854T3 (es) | 2014-01-14 |
CN1572765A (zh) | 2005-02-02 |
PT2292581E (pt) | 2013-12-16 |
KR101169466B1 (ko) | 2012-07-30 |
MY142041A (en) | 2010-08-30 |
BRPI0401884A (pt) | 2005-01-18 |
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