WO2022244399A1 - 磁場測定装置および磁場測定方法 - Google Patents
磁場測定装置および磁場測定方法 Download PDFInfo
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- WO2022244399A1 WO2022244399A1 PCT/JP2022/009990 JP2022009990W WO2022244399A1 WO 2022244399 A1 WO2022244399 A1 WO 2022244399A1 JP 2022009990 W JP2022009990 W JP 2022009990W WO 2022244399 A1 WO2022244399 A1 WO 2022244399A1
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- magnetic field
- magnetic resonance
- resonance member
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- magnet
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- 238000005259 measurement Methods 0.000 title claims abstract description 47
- 238000000691 measurement method Methods 0.000 title claims 2
- 230000004907 flux Effects 0.000 claims abstract description 48
- 230000003068 static effect Effects 0.000 claims description 25
- 230000001678 irradiating effect Effects 0.000 claims description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 11
- 230000005284 excitation Effects 0.000 description 11
- 230000003287 optical effect Effects 0.000 description 7
- 230000007547 defect Effects 0.000 description 6
- 238000010586 diagram Methods 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- 239000000758 substrate Substances 0.000 description 6
- 239000013078 crystal Substances 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 229910003460 diamond Inorganic materials 0.000 description 4
- 239000010432 diamond Substances 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 238000000387 optically detected magnetic resonance Methods 0.000 description 4
- 238000004364 calculation method Methods 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 241000238366 Cephalopoda Species 0.000 description 2
- 230000002500 effect on skin Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000001208 nuclear magnetic resonance pulse sequence Methods 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 238000000264 spin echo pulse sequence Methods 0.000 description 2
- 238000004804 winding Methods 0.000 description 2
- 229910000859 α-Fe Inorganic materials 0.000 description 2
- 238000004435 EPR spectroscopy Methods 0.000 description 1
- 229910000828 alnico Inorganic materials 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 230000005283 ground state Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 229910000938 samarium–cobalt magnet Inorganic materials 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R33/00—Arrangements or instruments for measuring magnetic variables
- G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
- G01R33/24—Arrangements or instruments for measuring magnetic variables involving magnetic resonance for measuring direction or magnitude of magnetic fields or magnetic flux
- G01R33/26—Arrangements or instruments for measuring magnetic variables involving magnetic resonance for measuring direction or magnitude of magnetic fields or magnetic flux using optical pumping
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R33/00—Arrangements or instruments for measuring magnetic variables
- G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
- G01R33/60—Arrangements or instruments for measuring magnetic variables involving magnetic resonance using electron paramagnetic resonance
Definitions
- the present invention relates to a magnetic field measuring device and a magnetic field measuring method.
- a certain magnetic field measuring device performs magnetic measurement by Optically Detected Magnetic Resonance (ODMR) using electron spin resonance of a sensing member such as a diamond structure with nitrogen and lattice defects (NV center: Nitrogen Vacancy Center).
- ODMR Optically Detected Magnetic Resonance
- NV center Nitrogen Vacancy Center
- a static magnetic field is applied separately from the magnetic field to be measured to a magnetic resonance member such as a diamond having an NV center, and laser light (excitation light and measurement light) and microwaves are applied in a predetermined sequence.
- the amount of fluorescent light emitted from the magnetic resonance member is detected, and the magnetic flux density of the magnetic field to be measured is derived based on the amount of light.
- the excitation light is applied to the NV center
- the first ⁇ /2 pulse of microwaves is applied to the NV center
- (c) from the first ⁇ /2 pulse Applying a second ⁇ /2 pulse of microwaves to the NV center at a predetermined time interval tt
- the excitation light is applied to the NV center
- the first ⁇ /2 pulse of the microwave is applied to the NV center at a phase of 0 degrees of the magnetic field to be measured
- (c ) apply a ⁇ pulse of microwaves to the NV center at a phase of 180 degrees of the magnetic field to be measured
- (d) apply a second ⁇ /2 pulse of microwaves to the NV center at a phase of 360 degrees of the magnetic field to be measured
- a certain magnetic sensor is equipped with a superconducting quantum interference device (SQUID: Superconducting Quantum Interference Device) and a flux transformer that detects the magnetic field to be measured with a pickup coil and applies it to the SQUID with an input coil (for example, see Patent Document 2).
- SQUID Superconducting Quantum Interference Device
- a flux transformer that detects the magnetic field to be measured with a pickup coil and applies it to the SQUID with an input coil
- the magnetic field measurement apparatus applies laser light, microwaves, and a static magnetic field to the magnetic resonance member in addition to the magnetic field to be measured, laser light, microwaves, and static magnetic fields are applied around the magnetic resonance member. and means for applying a static magnetic field, respectively. Therefore, when applying laser light, microwaves, and a static magnetic field to the magnetic resonance member, the flux transformer should be used without interfering with the application of the laser light, the microwaves, and the static magnetic field. A side coil must be arranged, and it is difficult to efficiently apply a magnetic field corresponding to the magnetic field to be measured by the flux transformer to the magnetic resonance member due to the geometric configuration.
- the present invention has been made in view of the above problems. It is an object of the present invention to provide a magnetic field measuring device and a magnetic field measuring method that facilitate relatively arranging the magnetic flux directions of a flux transformer and easily secure a space for irradiating a laser beam.
- a magnetic field measuring apparatus comprises a magnetic resonance member capable of electron spin quantum manipulation with microwaves, a high frequency magnetic field generator for applying microwaves to the magnetic resonance member, and a magnet for applying a static magnetic field to the magnetic resonance member.
- an irradiation device for irradiating the magnetic resonance member with light of a specific wavelength; a primary coil for sensing a magnetic field to be measured; and a secondary coil for applying an applied magnetic field corresponding to the sensed magnetic field to be measured to the magnetic resonance member.
- a flux transformer The magnetic resonance member is located in the hollow part of the secondary coil of the flux transformer and in the hollow part of the magnet.
- a magnetic field to be measured is sensed by the primary coil of the flux transformer
- an applied magnetic field corresponding to the sensed magnetic field to be measured is sensed by the secondary coil of the flux transformer.
- the magnetic resonance member is located in the hollow part of the secondary coil of the flux transformer and in the hollow part of the magnet.
- a magnetic field corresponding to the magnetic field to be measured is efficiently applied to the magnetic resonance member by the flux transformer, and the directions of the magnetic flux of the magnetic resonance member, the high-frequency generator, the magnet, and the flux transformer are determined relative to each other. It is possible to obtain a magnetic field measuring device and a magnetic field measuring method that are easy to arrange in a space and to easily secure a space for irradiating a laser beam.
- FIG. 1 is a block diagram showing the configuration of a magnetic field measuring device according to an embodiment of the invention.
- FIG. 2 is a cross-sectional view showing a configuration example of an optical system in the magnetic sensor section 10 shown in FIG.
- FIG. 3 is a cross-sectional view showing the primary coil 4a of the transformer 4.
- FIG. 4 is a perspective view showing a configuration example of the magnetic sensor section 10 in the magnetic field measuring device shown in FIG.
- FIG. 5 is a cross-sectional view (in the YZ plane) showing the arrangement of the magnetic resonance member 1, the high-frequency magnetic field generator 2, the secondary coil 4b, etc. in the magnetic sensor section 10 shown in FIG. FIG.
- FIG. 6 is a cross-sectional view (in the XZ plane) showing the arrangement of the magnetic resonance member 1, the high-frequency magnetic field generator 2, the secondary coil 4b, etc. in the magnetic sensor section 10 shown in FIG.
- FIG. 7 is a diagram illustrating an example of magnetic flux density characteristics in the magnetic resonance member 1 by the magnet 3 in FIG. 4 (1/2).
- FIG. 8 is a diagram explaining an example of magnetic flux density characteristics in the magnetic resonance member 1 by the magnet 3 in FIG. 4 (2/2).
- FIG. 9 is a diagram showing the operation of the magnetic field measuring device.
- FIG. 1 is a block diagram showing the configuration of a magnetic field measuring device according to an embodiment of the present invention.
- the magnetic field measuring apparatus shown in FIG. 1 includes a magnetic sensor section 10, a high frequency power source 11, an irradiation device 12, a light receiving device 13, and an arithmetic processing device .
- the magnetic sensor unit 10 detects the magnetic field to be measured (eg, strength, direction, etc. of the magnetic field) at a predetermined position (eg, on or above the surface of the object to be inspected).
- the magnetic field to be measured may be an AC magnetic field with a single frequency, or may be an AC magnetic field with a predetermined period having a plurality of frequency components.
- the magnetic sensor section 10 includes a magnetic resonance member 1, a high frequency magnetic field generator 2, a magnet 3, and a flux transformer 4.
- the magnetic resonance member 1 has a crystal structure, and is a member capable of quantum manipulation of electron spins (based on Rabi oscillation) with microwaves of a frequency corresponding to the arrangement direction of defects and impurities in the crystal lattice.
- the magnetic resonance member 1 is a light-detecting magnetic resonance member having a plurality (that is, ensemble) of specific color centers.
- the specific color center has an energy level capable of Zeeman splitting and can take a plurality of orientations with mutually different energy level shift widths upon Zeeman splitting.
- the magnetic resonance member 1 is a member such as a diamond containing a plurality of NV (Nitrogen Vacancy) centers as single type specific color centers.
- NV Nonrogen Vacancy
- the color center included in the magnetic resonance member 1 may be a color center other than the NV center.
- the high-frequency magnetic field generator 2 applies the microwaves described above to the magnetic resonance member 1 .
- the high-frequency magnetic field generator 2 is a plate-shaped coil, and includes a substantially circular coil portion 2a that emits microwaves, and terminal portions 2b that extend from both ends of the coil portion 2a and are fixed to the substrate 31.
- the high-frequency power supply 11 generates the microwave current and conducts it to the high-frequency magnetic field generator 2 .
- the coil portion 2a of the high-frequency magnetic field generator 2 conducts two currents parallel to each other at a predetermined interval so as to sandwich the magnetic resonance member 1 at both end portions thereof, and emits the above-described microwaves.
- the high-frequency magnetic field generator 2 is a plate-like coil, due to the skin effect, a microwave current flows through the end face portion of the coil portion 2a, so that two currents are formed.
- FIG. 2 is a cross-sectional view showing a configuration example of an optical system in the magnetic sensor section 10 shown in FIG.
- an opening 2c is formed in the side surface of a substantially circular plate-shaped coil portion in the high-frequency magnetic field generator 2, and excitation light and measurement light from the irradiation device 12 pass through this opening. 2c to irradiate the magnetic resonance member 1 (all or part of the magnetic resonance member 1). Also, the size of the opening 2c is determined by the size of the irradiation region in the magnetic resonance member 1 and the size of the region through which current flows under the skin effect.
- the irradiation area of the magnetic resonance member 1 is rectangular or circular, and the plate-like coil of the high-frequency magnetic field generator 2 is substantially circular.
- the opening 2c is designed such that the area of the projection area of the opening 2c onto the member 1 is larger than the area of the irradiation area, and the irradiation area is included in the projection area.
- the magnet 3 applies a static magnetic field (direct current magnetic field) to the magnetic resonance member 1 to Zeeman split the energy levels of a plurality of specific color centers (here, a plurality of NV centers) within the magnetic resonance member 1 .
- the magnet 3 is a ring-shaped permanent magnet, such as a ferrite magnet, an alnico magnet, or a samarium-cobalt magnet.
- the flux transformer 4 also includes a primary coil 4a and a secondary coil 4b electrically connected to the primary coil 4a by a cable (coaxial cable, litz wire, etc.). As shown in FIG. 3, the primary coil 4a is composed of a winding of 0.5 to several tens of turns. Further, the magnetic field to be measured at a predetermined measurement position is sensed by the primary coil 4a, and the applied magnetic field corresponding to the magnetic field to be measured sensed at the measurement position (the magnetic field transmitted from the measurement position by the flux transformer 4) is The voltage is applied to the magnetic resonance member 1 by the secondary coil 4b. That is, the primary coil 4a induces an electric signal corresponding to the sensed magnetic field to be measured, and the secondary coil 4b induces an applied magnetic field corresponding to the electric signal.
- a cable coaxial cable, litz wire, etc.
- FIG. 4 is a perspective view showing a configuration example of the magnetic sensor section 10 in the magnetic field measuring device shown in FIG.
- FIG. 5 is a cross-sectional view (in the YZ plane) showing the arrangement of the magnetic resonance member 1, the high-frequency magnetic field generator 2, the secondary coil 4b, etc. in the magnetic sensor section 10 shown in FIG.
- FIG. 6 is a cross-sectional view (in the XZ plane) showing the arrangement of the magnetic resonance member 1, the high-frequency magnetic field generator 2, the secondary coil 4b, etc. in the magnetic sensor section 10 shown in FIG.
- the magnetic resonance member 1 described above is located in the hollow of the secondary coil 4 b of the flux transformer 4 and in the hollow of the magnet 3 .
- the secondary coil 4b is arranged in the hollow portion of the magnet 3.
- the magnetic resonance member 1 is arranged at the center point.
- a is 30 or less, more preferably 20 or less, still more preferably 10 or less, even more preferably 5 or less.
- the application direction of the above-described applied magnetic field is the same as the above-described application direction of the static magnetic field, and the application of the above-described static magnetic field enhances the fluorescence intensity change at the above-described dip frequency, resulting in sensitivity becomes higher.
- the secondary coil 4b is wound around a cylindrical, non-magnetic bobbin 4b1 at a predetermined turns ratio with respect to the primary coil 4a.
- the bobbin 4b1 is formed with a hollow portion 4b2 (that is, a hollow portion of the secondary coil 4b) and a slit 4b3 for winding out.
- the magnetic resonance member 1 includes a plurality of color centers (here, NV centers) capable of electron spin quantum manipulation with microwaves as described above, and the magnet 3 is a predetermined magnet of the magnetic resonance member 1.
- a substantially uniform static magnetic field is applied to the regions (irradiated regions of excitation light and measurement light).
- the static magnetic field is applied so that the difference or ratio between the maximum value and the minimum value of the strength of the static magnetic field in the predetermined region is equal to or less than a predetermined value.
- the magnetic resonance member 1 is arranged in the central area of the width of the ring-shaped magnet 3 .
- the "central area” means ⁇ (central axis length 1/2 ⁇ b%) along the Z direction (axial direction) shown in FIG. point to space.
- b is 30 or less, more preferably 20 or less, still more preferably 10 or less, even more preferably 5 or less.
- the ring-shaped magnet 3 is arranged at the center of its width (that is, the magnetic resonance member 1 is arranged at positions substantially equidistant from both end faces of the magnet 3).
- the magnetic resonance member 1 is arranged in the central area of the width of the secondary coil 4b.
- the "central area” means ⁇ (central axis length 1/2 ⁇ c%) along the Z direction (axial direction) shown in FIG. 6 from the central point of the central axis of the secondary coil 4b. point to space.
- c is 30 or less, more preferably 20 or less, even more preferably 10 or less, even more preferably 5 or less.
- the magnetic resonance member 1 is arranged at the center of the width of the secondary coil 4b (that is, the magnetic resonance member 1 is arranged at positions substantially equidistant from both end surfaces of the secondary coil 4b). ).
- the cross-sectional area of the hollow portion is 100 times or more the area of the irradiation region of the excitation light and the measurement light in the magnetic resonance member 1, especially the hollow portion
- the diameter length in the radial direction is 10 times or more the diameter of the irradiation region of the measurement light.
- the measurement light irradiation area is 50 ⁇ m ⁇ 100 ⁇ m
- the cross-sectional area of the hollow portion is 500 ⁇ m ⁇ 1000 ⁇ m or more.
- FIGS. 7 and 8 are diagrams for explaining examples of magnetic flux density characteristics in the magnetic resonance member 1 by the magnet 3 (ring-shaped magnet) in FIG. 4.
- FIG. The magnetic flux density characteristics shown in FIGS. 7 and 8 are obtained when the dimensions of the magnetic resonance member 1 are 2 mm ⁇ 2 mm ⁇ 1 mm, and the magnet 3 is a ferrite magnet with a residual magnetic flux density of 385 mT, a relative magnetic permeability of 1.15, and an inner diameter of 30 mm.
- the index #1 ratio between the maximum value and the average value of the magnetic flux density strength in the above region
- the index #2 in the above region (ratio between the minimum value and the average value of the magnetic flux density intensity), and was obtained by simulation.
- FIGS. 7 and 8 by appropriately setting the outer diameter and height (thickness) of the magnet 3, the variation in magnetic flux density in the magnetic resonance member 1 can be reduced to about 0.5% or less. can.
- the crystals of the magnetic resonance member 1 are formed so that the arrangement direction of the defects and impurities substantially coincides with the direction of the static magnetic field (and the direction of the applied magnetic field).
- the orientation of member 1 is set.
- the angle (absolute value) between the arrangement direction of the defects and impurities and the direction of the static magnetic field (and the direction of the applied magnetic field) is preferably 8 degrees or less, and most preferably 0 degrees. .
- the high-frequency magnetic field generator 2 is fixed to one end portion of an L-shaped circuit board 31, and the other end portion of the circuit board 31 is fixed.
- a connector 32 electrically connected to the high-frequency power supply 11 by a cable is fixed to the connector 32, and through a wiring pattern on the circuit board 31, an electric element (resistor, capacitor, etc.) for impedance matching, a via hole, etc., Connectors 32 are electrically connected to both ends (terminal portions 2b) of the high-frequency magnetic field generator 2 .
- a semiconductor substrate such as a SiC substrate having high insulation performance may be used as the circuit substrate 31 .
- the magnetic resonance member 1 is arranged substantially at the center of the hollow portion of the high-frequency magnetic field generator 2 . As a result, microwaves of substantially uniform intensity and direction are applied to the magnetic resonance member 1 .
- an irradiation device 12 and a light receiving device 13 are provided as detection devices for detecting a physical phenomenon (here, fluorescence) from the magnetic resonance member 1 corresponding to the above-described applied magnetic field.
- the irradiation device 12 emits light (excitation light of a predetermined wavelength and measurement light of a predetermined wavelength) to the magnetic resonance member 1 as a light detection magnetic resonance member through the hollow portion of the secondary coil 4b along the Z direction in FIG. to irradiate. Further, the light receiving device 13 detects fluorescence emitted from the magnetic resonance member 1 through the hollow portion of the secondary coil 4b during irradiation of the measurement light. In this embodiment, the irradiation device 12 irradiates the magnetic resonance member 1 with the above-described light along the above-described central axis.
- the hollow portion of the secondary coil 4b becomes an actual sealed space, and a space for the optical path of the laser light (measurement light) from the irradiation device 12 and the optical path of the fluorescence from the magnetic resonance member 1 can be secured. Leakage of measurement light and fluorescence to the external space is eliminated.
- the magnetic resonance member 1 is fixed on a substantially rectangular prism 41, and the magnetic resonance member 1 is positioned substantially at the center of the hollow portion of the high-frequency magnetic field generator 2.
- a prism 41 is fixed to the bobbin 4b1 with a jig 42 so as to be arranged.
- the prism 41 is along the X-axis direction and has a reflective surface that is inclined (for example, at 45 degrees) in the YZ plane, and partially reflects the fluorescence emitted from the magnetic resonance member 1. The light is reflected by this reflecting surface and emitted to the side opposite to the excitation light and the measurement light.
- This fluorescence is condensed toward the light receiving device 13 by a compound parabolic concentrator (CPC) 43 or the like, for example, as shown in FIG.
- the optical system for condensing fluorescence may have another lens configuration.
- an opening is also formed on the side of the coil portion of the high-frequency magnetic field generator 2 facing the compound parabolic concentrator (CPC) 43.
- Part of the emitted fluorescence is also collected toward the light receiving device 13 by a compound parabolic concentrator (CPC) 43 or the like.
- the physical event described above is optically detected here, it may be a change in electrical properties (such as a change in the resistance value of the magnetic resonance member 1) or may be detected electrically.
- the arithmetic processing unit 14 includes, for example, a computer, executes programs on the computer, and operates as various processing units.
- the arithmetic processing unit 14 stores the detected optical or electrical signal data in a storage device (memory or the like) (not shown), and performs control and arithmetic operations as the measurement control unit 21 and the arithmetic unit 22. I do.
- the measurement control unit 21 controls the high-frequency power supply 11 and specifies the detection value of the physical event (here, fluorescence intensity) detected by the above-described detection device (here, the irradiation device 12 and the light receiving device 13). do.
- the detection value of the physical event here, fluorescence intensity
- the measurement control unit 21 controls the high-frequency power supply 11 and the irradiation device 12 according to a predetermined measurement sequence, for example, based on ODMR, and specifies the amount of fluorescence detected by the light receiving device 13.
- the irradiation device 12 is provided with a laser diode or the like as a light source
- the light receiving device 13 is provided with a photodiode or the like as a light receiving element
- the measurement control unit 21 is obtained by performing amplification or the like on the output signal of the light receiving element. Based on the output signal of the light receiving device 13, the detected light amount is specified.
- the calculation unit 22 calculates the magnetic field to be measured (strength, waveform, etc.) at the above-described measurement position based on the detected values obtained by the measurement control unit 21 and stored in the storage device.
- the above measurement sequence is set according to the frequency of the magnetic field to be measured.
- a spin echo pulse sequence such as a Hahn echo sequence
- the measurement sequence is not limited to this.
- the magnetic field to be measured is a relatively low-frequency alternating magnetic field
- the magnetic field is measured a plurality of times in one period of the magnetic field to be measured by the Ramsey pulse sequence (that is, the measurement sequence of the direct magnetic field)
- the The magnetic field to be measured may be specified based on the results of the magnetic field measurement.
- a magnetic shield is provided around the magnetic resonance member 1 in the magnetic sensor section 10 so that a magnetic field from the outside is not directly applied to the magnetic resonance member 1 .
- the primary coil 4a of the flux transformer 4 in the magnetic sensor section 10 is arranged at a desired measurement position and in a desired orientation with respect to the object 101 to be measured.
- the magnetic field to be measured is sensed by the primary coil 4 a , and the applied magnetic field is induced by the secondary coil 4 b and applied to the magnetic resonance member 1 .
- a substantially uniform static magnetic field is applied to the magnetic resonance member 1 by the magnet 3 in the magnetic sensor section 10 .
- the measurement control unit 21 controls the high-frequency power source 11 and the irradiation device 12 to emit microwaves and laser light (excitation light and measurement light) to the magnetic resonance member 1 at predetermined timing and for a predetermined length of time according to a predetermined measurement sequence.
- the detected value of the physical event of the magnetic resonance member 1 here, the fluorescence intensity obtained by the light receiving device 13
- the calculation unit 22 based on the detected value, Calculations corresponding to the measurement sequence are performed to identify the magnetic field (strength, orientation, etc.) at that measurement location.
- the magnetic field at the measurement position is measured by the magnetic sensor section 10 (that is, the magnetic resonance member 1).
- the magnetic sensor section 10 may be scanned along a predetermined scanning path pattern, and the above-described magnetic field measurement may be performed at a plurality of measurement positions on the scanning path.
- the high-frequency magnetic field generator 2 applies microwaves to the magnetic resonance member 1 capable of electron spin quantum manipulation with microwaves.
- Magnet 3 applies a static magnetic field to magnetic resonance member 1 .
- the irradiation device 12 irradiates the magnetic resonance member 1 with light of a specific wavelength.
- the flux transformer 4 senses the magnetic field to be measured with the primary coil 4a, and applies an applied magnetic field corresponding to the sensed magnetic field to be measured to the magnetic resonance member 1 with the secondary coil 4b.
- the magnetic resonance member 1 is located in the hollow of the secondary coil 4 b of the flux transformer 4 and in the hollow of the magnet 3 .
- the magnetic field corresponding to the magnetic field to be measured can be applied to the magnetic resonance member 1 together with the static magnetic field without blocking the optical paths of the excitation light and measurement light (and fluorescence) described above. Therefore, the magnetic field can be measured by efficiently applying a magnetic field corresponding to the magnetic field to be measured to the magnetic resonance member 1 by the flux transformer 4 .
- the magnetic resonance member 1, the high-frequency generator 2, the magnet 3, and the magnetic flux directions of the flux transformer 4 relative to each other, and it becomes easier to secure a space for irradiating laser light.
- the magnetic resonance member 1, the high frequency magnetic field generator 2, the magnet 3 and the flux transformer 4 are prepared.
- the high frequency generator 2 is attached to the circuit board 31 . Further, from the viewpoint of miniaturization, when a semiconductor substrate such as SiC is used, the high frequency generator 2 is integrally mounted on the substrate.
- the circuit board 31 to which the high frequency generator 2 is attached, the magnetic resonance member 1, the prism 41, and the jig 42 are combined with each other.
- the magnetic resonance member 1 is assembled so as to be arranged in the center of the high frequency generator 2, and at the same time, one of the alignment directions of the defects of the magnetic resonance member 1 is aligned with the center of the opening 2c of the high frequency generator 2. assembled to face.
- the magnetic flux generated by the high frequency generator 2 is perpendicular to at least one outer surface of the magnetic resonance member 1 .
- an assembly composed of the high frequency generator 2, the circuit board 31, the magnetic resonance member 1, the prism 41, and the jig 42 is inserted into the hollow portion of the secondary coil 4b of the flux transformer 4. , fixed.
- the magnetic resonance member 1 is arranged in the central area and central area of the secondary coil 4b.
- the center point of the opening 2c of the high-frequency generator 2 is arranged at the central area and the center section of the secondary coil 4b. Further, the orientation and position of each part are adjusted so that the magnetic flux generated from the high frequency generator 2 and the magnetic flux generated from the secondary coil 4b are perpendicular to each other.
- the magnet 3 is attached to the outside of the secondary coil 4b of the transformer 4. Also, the irradiation device 12 is separately installed and fixed.
- the flux transformer 4 and the magnet 3 are first assembled so that their central axes are aligned, and then they are assembled into the high frequency generator 2, the circuit board 31, the magnetic resonance member 1, the prism 41, and the jig 42. You may make it assemble
- the direction of the magnetic flux of the magnetic resonance member 1, the high frequency generator 2, the magnet 3, and the flux transformer 4 can be adjusted step by step. you don't have to do it.
- the secondary coil 4b is arranged in the hollow portion of the magnet 3, but the magnet 3 may be arranged in the hollow portion of the secondary coil 4b.
- the thickness of the magnet 3 as the ring-shaped magnet may be the same as the thickness of the secondary coil 4b (or bobbin 4b1).
- the magnet 3 may be an electromagnet.
- the present invention is applicable, for example, to a magnetic field measuring device and a magnetic field measuring method.
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Abstract
Description
Claims (6)
- マイクロ波で電子スピン量子操作の可能な磁気共鳴部材と、
前記磁気共鳴部材に前記マイクロ波を印加する高周波磁場発生器と、
前記磁気共鳴部材に静磁場を印加する磁石と、
前記磁気共鳴部材に特定波長の光を照射する照射装置と、
1次側コイルで被測定磁場を感受し、感受した前記被測定磁場に対応する印加磁場を2次側コイルで前記磁気共鳴部材に印加するフラックストランスフォーマーとを備え、
前記磁気共鳴部材は、前記フラックストランスフォーマーの前記2次側コイルの中空部にあり、かつ前記磁石の中空部にある位置に配置されていること、
を特徴とする磁場測定装置。 - 前記磁石は、リング型磁石であり、
前記2次側コイルは、リング状に巻回されており、
前記磁石の中心軸および前記2次側コイルの中心軸は互いに一致し、
前記磁気共鳴部材は、前記中心軸上に配置されること、
を特徴とする請求項1記載の磁場測定装置。 - 前記磁気共鳴部材は、前記中心軸の方向において、前記リング型磁石の幅の中心に配置されていることを特徴とする請求項2記載の磁場測定装置。
- 前記照射装置は、前記光を前記中心軸に沿って前記磁気共鳴部材に照射することを特徴とする請求項2または請求項3記載の磁場測定装置。
- 前記磁気共鳴部材は、前記マイクロ波で電子スピン量子操作の可能な複数のカラーセンターを備え、
前記磁石は、前記磁気共鳴部材に対して略均一な静磁場を印加すること、
を特徴とする請求項1記載の磁場測定装置。 - (a)フラックストランスフォーマーの1次側コイルで被測定磁場を感受し、(b)前記フラックストランスフォーマーの2次側コイルで、感受した前記被測定磁場に対応する印加磁場を、マイクロ波で電子スピン量子操作の可能な磁気共鳴部材に印加し、
前記磁気共鳴部材に前記マイクロ波を印加し、
前記磁気共鳴部材に静磁場を印加し、
前記磁気共鳴部材に特定波長の光を照射し、
前記磁気共鳴部材は、前記フラックストランスフォーマーの前記2次側コイルの中空部にあり、かつ前記磁石の中空部にある位置に配置されていること、
を特徴とする磁場測定方法。
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