WO2021182163A1 - Émulsion pour lingette et lingette - Google Patents

Émulsion pour lingette et lingette Download PDF

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Publication number
WO2021182163A1
WO2021182163A1 PCT/JP2021/007794 JP2021007794W WO2021182163A1 WO 2021182163 A1 WO2021182163 A1 WO 2021182163A1 JP 2021007794 W JP2021007794 W JP 2021007794W WO 2021182163 A1 WO2021182163 A1 WO 2021182163A1
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WO
WIPO (PCT)
Prior art keywords
mass
wet sheet
emulsion
sheet
wet
Prior art date
Application number
PCT/JP2021/007794
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English (en)
Japanese (ja)
Inventor
里奈 鬼澤
Original Assignee
大王製紙株式会社
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Filing date
Publication date
Application filed by 大王製紙株式会社 filed Critical 大王製紙株式会社
Publication of WO2021182163A1 publication Critical patent/WO2021182163A1/fr

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Classifications

    • A—HUMAN NECESSITIES
    • A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47K—SANITARY EQUIPMENT NOT OTHERWISE PROVIDED FOR; TOILET ACCESSORIES
    • A47K7/00—Body washing or cleaning implements
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/06—Emulsions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

Definitions

  • the present invention relates to a wet sheet lotion and a wet sheet.
  • a wet sheet in which a sheet material such as non-woven fabric or paper is impregnated with a chemical solution is known as a wipe for babies, a body for adults, or a wipe (see, for example, Patent Document 1).
  • Patent Document 1 contains water as a main component, the ability to wipe off dirt on the buttocks such as stool and sebum containing a large amount of oil is not very high, and it is necessary to use a large number of wet sheets. was there. Further, the chemical solution containing water as a main component has a problem that the moisturizing property is not so high. On the other hand, the milky lotion containing an oil agent has excellent dirt wiping performance and moisturizing property, but has a problem that it tends to become cloudy and its operability is low.
  • An object of the present invention is to provide a wet sheet emulsion and a wet sheet which can firmly wipe off dirt with a small number of sheets, have excellent moisturizing properties, and have high operability.
  • the invention according to claim 1 is A wet sheet emulsion containing an oil and an emulsifier.
  • the oil agent is blended in an amount of 0.001% by mass to 0.100% by mass.
  • the ratio of the oil agent to the emulsifier is 1: 4 to 1:19. At least two or more kinds of the emulsifiers are used.
  • the invention according to claim 2 is the emulsion for a wet sheet according to claim 1.
  • the wet sheet emulsion contains 1% by mass to 10% by mass of a moisturizer.
  • the invention according to claim 3 is a wet sheet.
  • the base sheet is impregnated with the emulsion for a wet sheet according to claim 1 or 2.
  • the invention according to claim 4 is the wet sheet according to claim 3.
  • the base material sheet is a non-woven fabric containing 1% by mass to 10% by mass of cotton.
  • the invention according to claim 5 is the wet sheet according to claim 3 or 4.
  • the wet sheet emulsion is impregnated with 200% by mass to 500% by mass with respect to the dry mass of the base sheet.
  • a wet sheet emulsion and a wet sheet which can wipe off dirt firmly with a small number of sheets, have excellent moisturizing properties, and have high operability.
  • FIG. 1 is a plan view showing a wet sheet S according to the present embodiment.
  • the wet sheet S is obtained by impregnating a base sheet 10 made of a predetermined fiber with a milky lotion for a wet sheet in which various components are added to purified water.
  • the wet sheet S can be housed in a packaging means such as a closed container having a sheet outlet that can be sealed by an opening / closing lid.
  • the user opens the outlet to open the inner sheet from the one in which the wet sheet S is put directly in the container or bag, or the one in which the bag containing the wet sheet S is put in the container. Pull it out and use it.
  • the base material sheet 10 is a non-woven fabric produced by using a predetermined fiber as a fiber material, for example, by a well-known technique such as spunlace, air-through, airlaid, point bond, spunbond, needle punch and the like.
  • a predetermined fiber include cellulose fibers such as rayon, lyocell, tencel, and cotton, polyolefin fibers such as polyethylene, polypropylene, and polyvinyl alcohol, polyester fibers such as polyethylene terephthalate and polybutylene terephthalate, and polyamide fibers such as nylon.
  • cellulose fibers such as rayon, lyocell, tencel, and cotton
  • polyolefin fibers such as polyethylene, polypropylene, and polyvinyl alcohol
  • polyester fibers such as polyethylene terephthalate and polybutylene terephthalate
  • polyamide fibers such as nylon.
  • the wet sheet S may be formed by ply (laminating) a plurality of base sheets 10 or may be formed from one base sheet 10.
  • the wet sheet S has a multi-layer structure, if the inner layer contains 6% by mass to 10% by mass and the outer layer contains 0% by mass to 4% by mass, the chemical retention property can be enhanced and the inner layer contains 0% by mass.
  • % to 4% by mass and 6% to 10% by mass are contained in the outer layer, the user can feel more moisture.
  • the content ratio of cotton in the inner layer and the outer layer is not limited to the above, and may be contained in each layer in a uniform ratio.
  • the base sheet 10 may be made of paper.
  • the base material sheet 10 has a convex portion composed of a high fiber density region 11 and a concave portion composed of a low fiber density region 12, and the high fiber density region 11 and the low fiber density region 11 are formed.
  • a predetermined pattern is formed by arranging the fiber density regions 12 alternately.
  • a predetermined pattern for example, as shown in FIG. 1, a cedar twill pattern in which a continuous V-shaped portion is formed by lines that bend in the opposite direction at predetermined intervals can be mentioned.
  • the angle of the V-shaped portion of the cedar twill pattern is not particularly limited, but for example, by setting it to 5 ° to 60 °, the diffusivity and liquid permeability of the emulsion are maximized. Can be good.
  • a striped pattern, a lattice pattern, a mesh pattern, a curved pattern, or the like can be used in addition to the cedar pattern.
  • 2 to 5 show a base sheet 10 on which a striped pattern (FIG. 2), a lattice pattern (FIG. 3), a mesh pattern (FIG. 4), and a curved pattern (FIG. 5) are formed, respectively.
  • the “high fiber density region 11” as used herein means a region having a higher fiber density than the low fiber density region 12, and the density is not particularly limited as long as it is larger than the low fiber density region 12. .
  • the “low fiber density region 12” means a region having a lower fiber density than the high fiber density region 11, and the density is not particularly limited as long as it is smaller than the high fiber density region 11.
  • the base sheet 10 having the high fiber density region 11 and the low fiber density region 12
  • the contact area with the skin can be reduced and the friction with the skin can be reduced.
  • irritation to the skin can be reduced, so that the wet sheet S of the present invention can be used even by a person with sensitive skin, an infant, or the like.
  • the base sheet 10 has the linear recesses (low fiber density region 12)
  • the liquid diffusivity and the liquid permeability are excellent as compared with the flat base sheet, so that the milky lotion is evenly and uniformly spread on the base sheet 10. It will be applied.
  • the number of lines in each pattern formed by the high fiber density region 11 and the low fiber density region 12 is preferably 3 lines / cm to 7 lines / cm.
  • the number of lines (lines / cm) referred to in the present specification means how many linear high fiber density regions 11 and linear low fiber density regions 12 exist per 1 cm. There is. That is, it means how many lines are present in the direction perpendicular to the direction parallel to the linear high fiber density region 11 and the linear low fiber density region 12 provided in parallel (the direction in which the number is the largest). doing. That is, in the case of 4 fibers / cm, it means that two linear high fiber density regions 11 and two low fiber density regions 12 are provided in 1 cm.
  • the number of lines is less than 3 lines / cm, the surface of the base sheet 10 approaches flatness, so that the dirt once captured is likely to be transferred. Further, when the number of lines exceeds 7 lines / cm, the volume of the space formed by the high fiber density region 11 and the low fiber density region 12 becomes too small, so that a desired amount of dirt is applied to the low fiber density region 12. It will not be possible to secure it.
  • FIG. 6 is a cross-sectional view of the VI-VI portion in FIGS. 1 to 5.
  • the height (thickness) Hm from the back surface of the high fiber density region 11 is preferably 200 ⁇ m or more and less than 600 ⁇ m, and the height (thickness) Hd from the back surface of the low fiber density region 12 is, for example, 150 ⁇ m or more. , Less than 200 ⁇ m is preferable.
  • the height difference between the high fiber density region 11 and the low fiber density region 12 is preferably about 50 ⁇ m to 100 ⁇ m. If the height difference is less than 50 ⁇ m, a large capture effect by the low fiber density region 12 cannot be expected, and a desired wiping amount cannot be secured. If the height difference exceeds 100 ⁇ m, the base sheet 10 of the base sheet 10 cannot be expected. This is because the thickness becomes thicker and the flexibility and the feel to the touch are impaired.
  • the fiber basis weight of the high fiber density region 11 is preferably about 40 g / m 2 to 60 g / m 2
  • the fiber basis weight of the low fiber density region 12 is, for example, 10 g / m 2 to 20 g / m. It is preferably about 2.
  • the thickness becomes suitable, and the base sheet 10 can ensure both strength and flexibility.
  • the convex portion is the high fiber density region 11 and the concave portion is the low fiber density region 12, but the present invention is not limited to this, and the convex portion is the low fiber density region 12 and the concave portion is high. It may be the fiber density region 11.
  • the base sheet 10 preferably has a convex portion which is a high fiber density region 11 and a concave portion which is a low fiber density region 12, but the present invention is not limited to this, and a difference in fiber density is not provided. It doesn't matter.
  • the area ratio of the high fiber density region 11 and the low fiber density region 12 in the base sheet 10 does not have to be 5: 5, but is preferably in the range of 2: 8 to 8: 2. If one is provided more than four times as much as the other, it is difficult to feel the unevenness, which is not preferable.
  • the wet sheet emulsion is emulsified with water (purified water) as the main component and an oil agent and an emulsifier mixed in a ratio of 1: 4 to 1:19.
  • water purified water
  • the emulsion for a wet sheet of the present embodiment contains an oil component, so that the stool and sebum stains containing a large amount of oil can be easily removed. Therefore, the wet sheet S impregnated with the milky lotion can firmly wipe off the dirt with a small number of sheets, and the consumer can reduce the purchase amount of the wipe.
  • the oil agent and the emulsifier in such a ratio, the emulsion stability of the emulsion for wet sheets is improved, and water and the oil agent are solubilized to become translucent or transparent, so that impurities in the liquid are contained. Quality control such as confirmation of presence / absence and measurement of pH becomes easier, and operability can be improved.
  • Oil agent for example, since it contains a large amount of oleic acid and stearic acid, it has a low viscosity and a smooth and moist feel, has excellent permeability, and contains long-chain fatty acids and phytosterols, so that it has high moisturizing properties. Shea butter to have is used. The oil agent is not limited to shea butter and may have an emollient effect.
  • Oil persic oil, peach seed oil, castor oil, sunflower oil, grape seed oil, cottonseed oil, coconut oil, wheat germ oil, rice germ oil, evening primrose oil, hybrid sunflower oil, macadamia nut oil, meadowfoam oil, hazelnut oil, palm kernel Oil, palm oil, palm oil, cacao butter, wood wax, mink oil, turtle oil, egg yolk oil, beef fat, milk fat, pork fat, horse oil, jojoba oil, carnauba wax, candela wax, rice bran, orange raffy oil, Mitsuro, Celac, Lanorin, Montan wax, Squalene, Squalane, Liquid paraffin, Paraffin, Microcrystalin wax, Vaseline, Soft liquid isoparaffin, Hydrogenated polyisobutylene, Ozokerite, Celesin, ⁇ -olein fin oligomer, Polybutene, Polyethylene, etc.
  • the oil agent is blended in a ratio of 0.001% by mass to 0.100% by mass with respect to all the components of the emulsion for wet sheets. If it is less than 0.001% by mass, the effect of the oil agent will not be exhibited so much, which is not desirable. On the other hand, if it is more than 0.100% by mass, the viscosity becomes large, stickiness occurs, and the usability deteriorates, which is not desirable.
  • the emulsifier includes nonionics such as polyoxyalkylene alkyl ethers, polyoxyalkylene alkyl phenyl ethers, polyoxyalkylene alkyl esters, polyoxyalkylene sorbitan alkyl esters, sorbitan alkyl esters, polyethylene glycol and polypropylene glycol.
  • a surfactant or the like is used. It is desirable that at least two types of emulsifiers are blended. Since fats and oils such as shea butter are composed of a plurality of types of fatty acids, emulsification can be made easier by blending a plurality of types of emulsifiers.
  • a moisturizer may be added to the emulsion for the wet sheet.
  • a moisturizer glycerin or the like, which is less irritating to the skin, is used, and by blending this with an oil agent, the water retention of the wet sheet S can be improved, and dirt can be wiped off without rubbing many times. It becomes possible to reduce the irritation to the skin.
  • the moisturizing agent is blended in a proportion of 1% by mass to 10% by mass with respect to all the components of the emulsion for wet sheets.
  • the moisturizing effect is not improved so much, and if it is more than 10% by mass, the viscosity of the wet sheet emulsion becomes too high, and the impregnation performance becomes low. In addition, it is not desirable because it causes stickiness and deteriorates usability.
  • hexyl glycerin or ethyl hexyl glycerin may be blended as a preservative in the emulsion for wet sheets, and can be obtained by a commercial product, a chemical synthesis method, a natural product derived from an animal or a plant, a fermentation method or a genetic recombination method. Any of the following may be used.
  • hexylglycerin or ethylhexylglycerin is a substance having a wide antibacterial spectrum and a high antibacterial effect.
  • hexyl glycerin or ethyl hexyl glycerin has a moisturizing function, and by containing this, the water retention property of the wet sheet S can be enhanced.
  • Preservatives also include sodium benzoate.
  • Sodium benzoate is, for example, a substance having an antibacterial effect against molds, yeasts, aerobic bacteria and the like.
  • Sodium benzoate exerts an antiseptic effect at pH 5 or lower. That is, when the pH of the wet sheet emulsion is higher than 5, the antiseptic effect of sodium benzoate is almost eliminated.
  • the pH of the wet sheet emulsion is adjusted to the range of 3 to 5.
  • ethylhexyl glycerin is blended in a proportion of 0.05% by mass to 0.10% by mass and sodium benzoate in a proportion of 0.075% by mass to 0.100% by mass with respect to all the components of the emulsion for a wet sheet. Will be done.
  • hexylglycerin is blended in an proportion of 0.1% by mass to 0.5% by mass and sodium benzoate is blended in a proportion of 0.05% by mass to 0.10% by mass with respect to all the components of the emulsion for a wet sheet.
  • phenoxyethanol for example, phenoxyethanol, benzalkonium chloride, cetylpyridinium chloride, a chelating agent, etc. can be blended as the preservative.
  • the impregnation rate of the wet sheet emulsion can be 200% by mass to 500% by mass with respect to the dry mass of the base sheet 10.
  • the conditions for measuring the dry mass of the base sheet 10 are a temperature of 25 ° C. and a humidity of 40%.
  • the impregnation rate of 200% by mass means that 200 g of the wet sheet emulsion is impregnated with the base sheet 10 having a dry mass of 100 g
  • the impregnation rate of 500% by mass means that the dry mass is 100 g. This means that the base sheet 10 is impregnated with 500 g of a wet sheet emulsion.
  • the impregnation rate is less than 200% by mass, the liquid content does not sufficiently permeate and uneven impregnation occurs, and the components in the wet sheet emulsion tend to be unevenly distributed.
  • the milky lotion for wet sheets tends to drip.
  • the base formulation the oil agent (shear fat), the nonionic surfactant emulsifier I (PEG-20 glyceryl triisostearate), and the emulsifier II (PEG-8) were added in the compounding ratios of the following Examples and Comparative Examples.
  • (Caprylic acid / capric acid) glyceriz) was mixed, and chemical solutions were prepared respectively.
  • Example 1 The base formulation was 99.95% by mass, the oil agent was 0.01% by mass, the emulsifier I was 0.02% by mass, and the emulsifier II was 0.02% by mass.
  • Example 2 The base formulation was 99.80% by mass, the oil agent was 0.01% by mass, the emulsifier I was 0.09% by mass, and the emulsifier II was 0.10% by mass.
  • Example 1-2 The following test 1 was performed using the chemical solutions of Example 1-2 and Comparative Example 1-6.
  • Test 1 Emulsification test
  • the chemical solutions of Example 1-2 and Comparative Example 1-6 are each stirred and dissolved, and it is confirmed whether emulsification is performed. At this time, when the chemical solution is emulsified and the color becomes translucent or transparent, ⁇ , when the chemical solution is emulsified but the color is cloudy, ⁇ , the chemical solution is not emulsified and the aqueous layer and the oil layer are separated. The case was set to x.
  • the results of Test 1 are shown in Table II.
  • a translucent or transparent wet sheet emulsion can be obtained by blending two types of emulsifiers and an oil agent. This is because fats and oils such as shea butter are composed of a plurality of types of fatty acids, and therefore, by blending a plurality of types of emulsifiers, emulsification becomes easier.
  • the emulsion for wet sheets becomes translucent or transparent by blending the emulsifier so as to be 4 times or more the ratio of the oil agent.
  • Example 2 and Comparative Example 6 even if the emulsifier is blended so as to be more than 19 times the ratio of the oil agent, the chemical solution becomes translucent or transparent, but the oil agent and the emulsifier are 1: 1. Since the emulsifying effect is not so high and the cost of the emulsifier increases as compared with the case of blending at a ratio of 19, it is desirable to blend the emulsifier so that it is 19 times or less the ratio of the oil agent.
  • the chemical solutions of Example 3-4 and Comparative Example 7-8 were prepared in the ratios shown in Table III below, and the chemical solutions of Example 3-4 and Comparative Example 7-8 were respectively 340 on each base sheet 10.
  • the chemical solution of Comparative Example 8 is a chemical solution assuming a conventional water-based chemical solution obtained by removing an oil agent, an emulsifier and a moisturizer from the chemical solution of Example 3 and adding purified water.
  • Example 3 Using the wet sheet of Example 3, the portion 14 cm from the wrist was lightly wiped 5 times.
  • Example 4 Using the wet sheet of Example 4, the portion 17 cm from the wrist was lightly wiped 5 times.
  • Example 3-4 and Comparative Example 7-9 a wet sheet impregnated with a water-based chemical solution was wiped off with a wet sheet S impregnated with a wet sheet emulsion emulsified with an oil agent and an emulsifier. It can be seen that the moisturizing property can be improved as compared with the case of wiping with a sheet. In particular, when Example 3 and Example 4 are compared, the amount of increase in the amount of keratin water in Example 3 is remarkably higher throughout 60 minutes. Therefore, by adding a moisturizer to the wet sheet emulsion, the wet sheet It can be seen that the moisturizing property of S can be further enhanced.
  • Example 3 and Comparative Example 8 in Table V the average value of the number of wipes used in Example 3 is smaller in Example 3 regardless of whether urine stains or stool stains are wiped off.
  • the wet sheet S impregnated with the wet sheet emulsion of the present embodiment containing an oil agent has higher urine and stool stain wiping performance. You can see that.
  • Comparing Example 3 and Comparative Example 8 in Table VI the total number of people who answered that the wipes in Example 3 were "dry” or "smooth" after use. Since the number of respondents who answered that "the buttocks are moist" is small, it can be seen that the user can actually feel the moisturizing property by blending an oil agent, an emulsifier, and a moisturizing agent.
  • the wet sheet S is intended to be used for baby wipes, adult bodies, wipes, and the like, but is not limited thereto.
  • the chemical solution to be blended in the wet sheet emulsion can be changed according to the intended use.
  • the present invention can be used for wet sheet emulsions and wet sheets, which can wipe off dirt firmly with a small number of sheets, have excellent moisturizing properties, and have high operability.

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • Birds (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Dermatology (AREA)
  • Dispersion Chemistry (AREA)
  • Cosmetics (AREA)

Abstract

Dans la présente invention, une composition hautement fonctionnelle, semi-transparente à transparente pour une lingette peut être obtenue suite à l'émulsionnement d'un agent de graissage et d'eau par mélange de l'agent de graissage et d'au moins deux émulsifiants dans une formulation de base selon un rapport de 1:4 à 1:19. A l'aide de cet agent de graissage dans l'émulsion pour une lingette, il est possible d'éliminer de manière appropriée les salissures contenant une grande quantité d'un composant huileux, telles que les selles et le sébum. De plus, la propriété de rétention d'humidité de cette émulsion pour une lingette est davantage améliorée par le mélange d'un hydratant dans l'émulsion.
PCT/JP2021/007794 2020-03-13 2021-03-02 Émulsion pour lingette et lingette WO2021182163A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2020043732A JP7448379B2 (ja) 2020-03-13 2020-03-13 ウェットシート
JP2020-043732 2020-03-13

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WO2021182163A1 true WO2021182163A1 (fr) 2021-09-16

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007524638A (ja) * 2003-07-09 2007-08-30 ザ プロクター アンド ギャンブル カンパニー 皮膚に優しい湿性の拭う物のための水中油型エマルション組成物
JP2010194255A (ja) * 2009-02-27 2010-09-09 Kao Corp 肛門又は陰部周辺清浄用シート
JP2016540804A (ja) * 2013-12-20 2016-12-28 ファイザー・インク 肛門直腸の炎症および障害の治療において使用するための事前湿潤ワイプ
JP2017136189A (ja) * 2016-02-03 2017-08-10 オオサキメディカル株式会社 水分含有量の少ない便の拭取シート

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007524638A (ja) * 2003-07-09 2007-08-30 ザ プロクター アンド ギャンブル カンパニー 皮膚に優しい湿性の拭う物のための水中油型エマルション組成物
JP2010194255A (ja) * 2009-02-27 2010-09-09 Kao Corp 肛門又は陰部周辺清浄用シート
JP2016540804A (ja) * 2013-12-20 2016-12-28 ファイザー・インク 肛門直腸の炎症および障害の治療において使用するための事前湿潤ワイプ
JP2017136189A (ja) * 2016-02-03 2017-08-10 オオサキメディカル株式会社 水分含有量の少ない便の拭取シート

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