WO2020026087A1 - 一种含水口红及其制备方法 - Google Patents
一种含水口红及其制备方法 Download PDFInfo
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- WO2020026087A1 WO2020026087A1 PCT/IB2019/056349 IB2019056349W WO2020026087A1 WO 2020026087 A1 WO2020026087 A1 WO 2020026087A1 IB 2019056349 W IB2019056349 W IB 2019056349W WO 2020026087 A1 WO2020026087 A1 WO 2020026087A1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/0229—Sticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8111—Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Definitions
- the invention belongs to the field of cosmetics and relates to an aqueous lipstick and a preparation method thereof.
- Lipstick is a product that makes lips rosy and shiny, moisturizes, protects lips, increases facial beauty and contours, and is an essential beauty cosmetic for girls.
- the conventional formulas are: oils, waxes, softeners, colorants, antioxidants, and fragrances; the emulsified formula has low water content, lakes, and pigments.
- CN107669518A discloses a lipstick containing fiber, grease, preservative, and auxiliary additives, wherein the weight part containing water is 62-69, the weight part for inorganic filler is 6-9, and the weight part for pigment is 0.3. -1, parts by weight of thickener is 4.06-5.5, parts by weight of fat is 2-3, parts by weight of emulsifier is 1.5-4.5, parts by weight of humectant is 8-13, The parts by weight are 0.68-0.85, and the parts by weight of the auxiliary additive are 0.55-1.
- This lipstick has a large amount of water-based ingredients, a wax-free formula, light texture, no stickiness, refreshing and cold, bright and long-lasting color, it is not easy to detach in case of water and sweat, but this lipstick has poor stability and lower drip point.
- CN107744498A discloses a moisturizing lipstick formula.
- the moisturizing lipstick formula is calculated in percentage and contains the following components: olive oil 15% -28%, jojoba oil 8% -16%, avocado oil 5% -14%, Shea butter 5% -10%, tea tree oil 3% -7%, candelilla wax 10% -20%, beeswax 5% -15%, glyceryl stearate 6% -10%, natural vitamin E0.
- the lipstick prepared by this formula has no irritation to the skin of the lips, has the function of increasing moisturizing, and can prevent inflammation of the skin of the lips. Because all the substances used are natural and have no toxic effect, even if they are accidentally entered into the mouth, they can be used safely. However, the lipstick prepared by this formula has too complicated ingredients, low moisture content, and poor stability.
- CN104606093A discloses an emulsified lipstick, which contains the following components: water; octyldodecanol; pentaerythritol tetraisostearate; cyclopentadimethylsiloxane; ethyl cellulose; ethanol; glycerol; polyglycerol ⁇ 2 triisostearate; ethylene / propylene / styrene copolymer; butene / ethylene / styrene copolymer; isododecane; polyglycerol-6 polyricinoleate; trimethylolpropane tri Isostearate; Colorant; Distearyl montmorillonite; Hydrogenated polyisobutylene; Polyglycerol-2 isostearate; Carrageena rugosa; Sodium chloride; Phenoxyethanol and ethyl Hexyl glycerol.
- This lipstick can also maintain a good makeup condition for a long time, and can effectively cover the lip lines, while not giving a greasy feel like lip gloss, but this Emulsified lipsticks have low water content, and the lipstick residual value is about 50% 4 hours after use, and the stability is not high.
- the purpose of the present invention is to provide a water-containing lipstick and a preparation method thereof, so that the production process of the water-containing lipstick is simple, the water content is high, and the stability is good.
- the present invention provides an aqueous lipstick, which includes the following components in terms of mass percentage: emollients 20% -40%, hardeners 13% -15%, brighteners 10% -15% , Polyglycerin-2-triisostearate 10%-15%, Polyglycerin-2-diisostearate 10%-15%, pigment 0.5%-5%, lake 0.5%-5%, 10% humectant.
- the water-containing lipstick provided by the present invention has a high water content, the water content can reach 10%, can bring in various water-soluble raw materials, high stability, the dropping point can reach 56 ° C-60 ° C, and excellent emulsification effect. No ultrasonic equipment is needed to defoam, ordinary filling equipment can be used, and the obtained lipstick colors are many, the color is developed in one second, and the saturation is high.
- the water-containing lipstick provided by the present invention can have a water content of 10%, which is very advantageous for bringing in various raw materials with effects, so that the lipstick can not only make the lips feel moist, remove dryness, but also moisturize and maintain the lips. Excellent effect.
- the present invention works synergistically through polyglycerol-2 triisostearate and polyglycerol-2-diisostearic acid. If any one of the ingredients is missing from the lipstick, the stability of the lipstick will be reduced, and the taste of the lipstick will be affected at the same time.
- the mass percentage of the emollient is 20% -40%, for example, it may be 20%, 22%, 25%, 28%, 30%, 32%, 35%, 38%, or 40%, etc. .
- the emollient comprises glycerol polyoxyethylene ether cocoate, hexyl palmitate, hexyl palmitate, olive oil, jojoba seed oil, coconut oil, cocamidopropyl Any one or at least two of betaine, octyl methoxycinnamate, white flower seed oil, dihydroxyhydroxystearate, ethylhexyl methoxycinnamate, or butylmethoxydibenzoylmethane In combination, the above emollients can be used alone or in combination.
- it may be hydrogenated polyisobutylene, glycerin polyoxyethylene ether cocoate, hexyl palmitate, hexyl palmitate, olive fruit oil, jojoba seed oil, and coconut oil; hexyl palmitate, A combination of hexanoic acid palmitate, ethylhexyl methoxycinnamate, and butylmethoxydibenzoylmethane.
- the mass percentage of the hardener is 13% -15%, for example, it may be 13%, 13.5%, 14%, 14.5%, or 15%.
- the hardener includes any one or a combination of at least two of beeswax, polyethylene, carnauba wax, or methyl cellulose.
- the mass percentage of the brightener is from 10% to 15%, and may be, for example, 10%, 11%, 12%, 13%, 14%, or 15%.
- the brightener includes any one or a combination of at least two of cetyl alcohol caproate, hydrogenated polyisobutylene, or tridecyl trimellitate.
- the brightener can make the color of the lipstick more beautiful, the application effect is more prominent, and the visual feeling is more obvious.
- the mass percentage of the polyglycerin-2-triisostearate is 10% -15%, and may be, for example, 10%, 11%, 12%, 13%, 14%, or 15%.
- the mass percentage of the polyglycerin-2-diisostearate is 10% -15%, and may be, for example, 10%, 11%, 12%, 13%, 14%, or 15%.
- the addition of polyglycerol-2-triisostearate and polyglycerol-2-diisostearate makes the lipstick more stable.
- the dropping point can generally reach 56 ° C-60 ° C. Has long-lasting moisturization on the lips and maintains a vibrant effect.
- the mass percentage of the pigment is 0.5% -5%, for example, it can be 0.5%, 1%, 2%, 3%, 4%, or 5%.
- the pigment includes iron red, ⁇ -carotene, iron yellow, iron black, black bean red, sorghum red, red yeast rice, black gallon red, sea buckthorn yellow, dense yellow, roselle red, or magenta yellow Any of them.
- the mass percentage of the lake is 0.5% to 5%, and may be, for example, 0.5%, 1%, 2%, 3%, 4%, or 5%.
- the lake includes any one of amaranth red aluminum lake, carmine red aluminum lake, erythro red aluminum lake, new red aluminum lake or lemon yellow aluminum lake.
- any type of pigment and lake can be selected to be matched, so that there are more types of colors available for lipstick.
- the mass percentage of the humectant is 10%.
- the humectant may be a common water-soluble humectant or a water-soluble plant extract.
- the mass percentage of the humectant is 10%, it will make the skin feel the best and the effect will be the best.
- the humectant includes any one or a combination of at least two of hyaluronic acid, chondroitin sulfate, aloe, glyceryl caprylate, glycerol, propylene glycol, 1,2-pentanediol or water.
- Typical but non-limiting combinations include: glyceryl caprylate, 1,2-pentanediol, and water; hyaluronic acid, chondroitin sulfate, aloe, and propylene glycol.
- the aqueous lipstick further includes an antioxidant, a perfume and a preservative.
- the mass percentages of the antioxidants, fragrances and preservatives are 0.5% -2%, for example, they may be 0.5%, 1%, 1.2%, 1.5%, 1.8%, or 2%.
- the antioxidants, fragrances and preservatives can be mixed in any proportion within a defined mass percentage range.
- the antioxidants can be 1%
- the fragrances can be 0.5%
- the preservatives can be 0.2%.
- the antioxidant includes any one of butylated toluene, tocopherol, tea polyphenols, lecithin, ethoxyquin, 2,6-di-tert-butylcresol, ascorbyl stearate or calcium ascorbate, or A combination of at least two of which typical but non-limiting combinations include butylated toluene, tocopherol, and lecithin; tocopherol, tea polyphenols, lecithin, and ethoxyquin.
- the perfume comprises any one or a combination of at least two of vanillin, coumarin, phenethyl alcohol or jasmonaldehyde, wherein a typical but non-limiting combination includes coumarin and phenethyl alcohol; Blue pigment, phenylethanol and jasmonal.
- the preservative includes any one or a combination of at least two of benzoic acid, sodium benzoate, potassium sorbate, calcium diacetate, or ⁇ -polylysine, wherein a typical but non-limiting combination includes benzene Sodium formate and potassium sorbate; benzoic acid, potassium sorbate and calcium diacetate.
- the aqueous lipstick provided by the present invention specifically consists of the following ingredients:
- the lipstick provided by the present invention can still exert a good effect by using such a complicated formula, which provides a new research idea for the research and development direction of lipstick, and has great significance for the development of lipstick formula.
- the present invention provides a method for preparing an aqueous lipstick according to the first aspect, the method comprising the following steps:
- step (3) The aqueous mixed product obtained in step (2) is added to the fatty mixed product obtained in step (1) for fourth mixing, and the water-containing lipstick is obtained by filling molding.
- the preparation method provided by the invention is simple and the process operation is simple. In the preparation process, the order of adding raw materials is specific, otherwise, it will affect the uniformity and stability of the lipstick, and the dropping point will be reduced.
- the heating temperature in step (1) is 87-93 ° C.
- the heating temperature may be 87 ° C, 88 ° C, 89 ° C, 90 ° C, 91 ° C, 92 ° C, or 93 ° C.
- the temperature of the first mixing and the second mixing in step (1) are both 80-85 ° C, for example, 80 ° C, 81 ° C, 82 ° C, 83 ° C, 84 ° C, or 85 ° C.
- the temperature of the third mixing and the fourth mixing in steps (2) and (3) is 80-85 ° C.
- the temperature may be 80 ° C, 81 ° C, 82 ° C, 83 ° C, 84 ° C, or 85 ° C. Wait.
- the polyglycerin-2-triisostearate, pigment, humectant, etc. it is necessary to heat the polyglycerin-2-triisostearate, pigment, humectant, etc. to 80-85 ° C, then mix and dissolve, stir and emulsify, and finally add optional Antioxidants, preservatives and flavors.
- the filling in step (2) is performed in a filling mold.
- the filling temperature is 80-85 ° C, for example, it can be 80 ° C, 81 ° C, 82 ° C, 83 ° C, 84 ° C, or 85 ° C.
- the preparation method provided by the present invention specifically includes the following steps:
- the hardener After the hardener is heated and dissolved at 87-93 ° C, it is mixed with an emollient and a brightener for the first time, and then polyglycerin-2-diisostearate and lake are mixed for the second time to obtain a fat mixed product. Both the first mixing and the second mixing are performed at 80-85 ° C;
- step (3) The aqueous mixed product obtained in step (2) is added to the fatty mixed product obtained in step (1) for fourth mixing, the mixing temperature is 80-85 ° C, and the water-containing lipstick is obtained by filling and molding.
- the mixture is evacuated under vacuum, and then the water-containing lipstick is obtained by filling and molding, so as to reduce the overall appearance of the water-containing lipstick after the bubbles are damaged.
- the aqueous mixed product forms aqueous particles dispersed in the fatty mixed product and the appearance of the aqueous particles is covered by the fatty mixed product, which can effectively prevent the loss of water in the water-containing lipstick after filling molding.
- the water-containing lipstick provided by the present invention has a high water content, the water content can reach 10%, can bring in various water-soluble raw materials, high stability, the dropping point can reach 56 ° C-60 ° C, and excellent emulsification effect. No ultrasonic equipment is needed to defoam, ordinary filling equipment can be used, and the obtained lipstick colors are many, the color is developed in one second, and the saturation is high.
- the water-containing lipstick provided by the present invention has good stability and perfect taste through the reasonable combination of various components, and has a moderate color and is applied to the lips. At the time, it was gorgeous and elegant, in line with the public's aesthetics, and had a good market prospect.
- the preparation method includes the following steps:
- Carnauba wax is heated and dissolved at 90 ° C, and then dissolved with hexyl palmitate, hexanoic acid palmitate, ethylhexyl methoxycinnamate, butylmethoxydibenzoylmethane, and cetyl acetic acid
- Caproate, hydrogenated polyisobutylene and tridecyl trimellitate were mixed for the first time, the mixing temperature was 82 ° C, and polyglycerol-2 diisostearate and carmine aluminum lake were mixed for the second time
- a fatty mixed product was obtained with a mixing temperature of 82 ° C;
- the aqueous mixed product is added to the fat mixed product for fourth mixing, the mixing temperature is 82 ° C., and the water-containing lipstick is obtained by filling molding.
- the preparation method includes the following steps:
- the aqueous mixed product is added to the fat mixed product for fourth mixing, the mixing temperature is 80 ° C., and the water-containing lipstick is obtained by filling and molding.
- White pond flower seed oil 5%, hexyl palmitate 15%, hexanoic acid palmitate 6%, ethylhexyl methoxycinnamate 9%, 5% butylmethoxydibenzoylmethane, carnauba wax 13%, cetyl acetate hexanoate 5%, hydrogenated polyisobutylene 5%, polyglycerin -2-triisostearate 11%, polyglycerin -2-diisostearate 11%, black bean red 0.5 %, Amaranth red aluminum lake 4.5%, 1,2-pentanediol 2%, water 8%;
- the preparation method includes the following steps:
- the aqueous mixed product is added to the fat mixed product for fourth mixing, and the water-containing lipstick is obtained by filling and molding.
- This comparative example differs from Example 1 only in that this comparative example does not include polyglycerol-2-triisostearate, and the mass fraction of polyglycerol-2-diisostearate is 30%, and the rest
- the components and preparation method are the same as those in Example 1, and a water-containing lipstick is prepared.
- This comparative example differs from Example 1 only in that this comparative example does not include polyglycerol-2-diisostearate, and the mass fraction of polyglycerol-2-triisostearate is 30%, and the rest
- the components and preparation method are the same as those in Example 1, and a water-containing lipstick is prepared.
- Example 1 The difference between this comparative example and Example 1 is only that this comparative example does not include polyglycerol-2-triisostearate and polyglycerol-2-diisostearate.
- the remaining components and preparation methods are the same as In the same manner as in Example 1, an aqueous lipstick was prepared.
- Example 1 The difference between this comparative example and Example 1 is only that 15% of carnauba wax is not included in this comparative example, and the remaining components and the preparation method are the same as those in Example 1, and a water-containing lipstick is prepared.
- Example 1 The difference between this comparative example and Example 1 is only that the preparation method is as follows: all raw materials are directly mixed, stirred and emulsified, and finally filled, and a water-containing lipstick is prepared.
- the water-containing lipstick provided by the present invention has complex ingredients, and by setting a reasonable percentage content, such a complex ingredient can exert the best effect, which has high value for practical applications and also provides a new type of lipstick for development A new strategy.
- the present invention illustrates the water-containing lipstick of the present invention and the preparation method thereof through the above examples, but the present invention is not limited to the above detailed methods, which does not mean that the present invention must rely on the above detailed methods to be implemented.
- Those skilled in the art should know that any improvement to the present invention, equivalent replacement of the raw materials of the products of the present invention, addition of auxiliary components, selection of specific methods, etc., all fall within the scope of protection and disclosure of the present invention.
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Abstract
Description
Claims (12)
- 一种含水口红,其特征在于,所述含水口红按质量百分比计包括以下组分:润肤剂20%―40%,硬化剂13%―15%,光亮剂10%―15%,聚甘油―2―三异硬脂酸酯10%―15%,聚甘油―2―二异硬脂酸酯10%―15%,色素0.5%―5%,色淀0.5%―5%,保湿剂10%。
- 根据权利要求1所述的含水口红,其特征在于,所述润肤剂包括甘油聚氧乙烯醚椰油酸酯、棕榈酸乙酸己酯、棕榈酸乙酸己酸酯、油橄榄果油、霍霍巴籽油、椰子油、椰油酰胺基丙基甜菜碱、甲氧基肉桂酸辛酯、白池花籽油、二聚羟基硬脂酸酯、甲氧基肉桂酸乙基己酯或丁基甲氧基二苯甲酰基甲烷中的任意一种或至少两种的组合。
- 根据权利要求1或2所述的含水口红,其特征在于,所述硬化剂包括蜂蜡、巴西棕榈蜡、聚乙烯或甲基纤维素中的任意一种或至少两种的组合。
- 根据权利要求1―3中任一项所述的含水口红,其特征在于,所述光亮剂包括鲸蜡醇乙酸己酸酯、氢化聚异丁烯或十三烷醇偏苯三酸酯中的任意一种或至少两种的组合。
- 根据权利要求1―4中任一项所述的含水口红,其特征在于,所述色素包括铁红、β―胡萝卜素、铁黄、铁黑、黑豆红、高梁红、红曲红、黑加伦红、沙棘黄、密蒙黄、玫瑰茄红或桅子黄中的任意一种;
优选地,所述色淀包括苋菜红铝色淀、胭脂红铝色淀、赤藓红铝色淀、新红铝色淀或柠檬黄铝色淀中的任意一种。 - 根据权利要求1―5中任一项所述的含水口红,其特征在于,所述保湿剂包括透明质酸、硫酸软骨素、芦荟、甘油辛酸酯、甘油、丙二醇、1,2―戊二醇或水中的任意一种或至少两种的组合。
- 根据权利要求1―6中任一项所述的含水口红,其特征在于,所述含水口红还包括抗氧剂、香料和防腐剂;
优选地,所述抗氧剂、香料和防腐剂质量百分比总计为0.5%―2%;
优选地,所述抗氧剂包括丁羟甲苯、生育酚、茶多酚、卵磷脂、乙氧喹、2,6―二叔丁基甲酚、抗坏血酸硬脂酸酯或抗坏血酸钙中的任意一种或至少两种的组合;
优选地,所述香料包括香兰素、香豆素、苯乙醇或洋茉莉醛中的任意一种或至少两种的组合;
优选地,所述防腐剂包括苯甲酸、苯甲酸钠、山梨酸钾、双乙酸钙或ε―聚赖氨酸中的任意一种或至少两种的组合。 - 根据权利要求1―7中任一项所述的含水口红的制备方法,其特征在于,所述方法包括以下步骤:
(1)将硬化剂加热溶解后与润肤剂、光亮剂第一次混合,加入聚甘油―2―二异硬脂酸酯和色淀第二次混合得到脂性混合产物;
(2)将聚甘油―2―三异硬脂酸酯、色素、保湿剂和任选地抗氧剂、防腐剂和香精第三次混合得到水性混合产物;
(3)将步骤(2)得到的水性混合产物加入到步骤(1)得到的脂性混合产物中进行第四次混合,灌装成型得到所述含水口红。 - 根据权利要求8所述的制备方法,其特征在于,步骤(1)所述加热的温度为87―93℃;
优选地,步骤(1)所述第一次混合和第二次混合的温度均为80―85℃ - 根据权利要求8或9所述的制备方法,其特征在于,步骤(2)所述第三次混合的温度为80―85℃;步骤(3)所述第四次混合的温度为80―85℃;
优选地,步骤(3)中所述灌装在灌装模具中进行;
优选地,所述灌装的温度为80―85℃。 - 根据权利要求8所述的制备方法,其特征在于,所述第四次混合后,水性混合产物形成分散在脂性混合产物中的水性颗粒且水性颗粒外表被脂性混合产物所包裹。
- 根据权利要求8所述的制备方法,其特征在于,所述步骤(3)中,水性混合产物加入脂性混合产物中进行第四次混合后,对混合物进行真空排气,再灌装成型得到所述含水口红。
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FR3098720B1 (fr) | 2019-07-16 | 2021-08-06 | S A Color | Utilisation d’une matiere pigmentaire traitee hydrodispersible dans une formulation aqueuse de rouge a levres, procede de la fabrication de ladite matiere pigmentaire et la formulation correspondante |
CN110897907A (zh) * | 2019-12-11 | 2020-03-24 | 花安堂生物科技集团有限公司 | 一种不含peg乳化剂的油包水唇釉及其制备方法 |
FR3134981A1 (fr) * | 2022-04-28 | 2023-11-03 | L'oreal | Procédé de maquillage avec l’application d’une composition comprenant un polyphénol et un composé polyglycérolé, et une matière colorante puis application d’une composition anhydre |
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US3890358A (en) * | 1972-05-08 | 1975-06-17 | Emery Industries Inc | Polyglycerol partial esters and their use in lipstick formulations |
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FR2873033A1 (fr) * | 2004-07-16 | 2006-01-20 | Oreal | Composition cosmetique compenant un polymere de silicone defini et un agent gelifiant. |
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