WO2017201767A1 - 一种超临界流体无水染整的打样染杯 - Google Patents

一种超临界流体无水染整的打样染杯 Download PDF

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Publication number
WO2017201767A1
WO2017201767A1 PCT/CN2016/084892 CN2016084892W WO2017201767A1 WO 2017201767 A1 WO2017201767 A1 WO 2017201767A1 CN 2016084892 W CN2016084892 W CN 2016084892W WO 2017201767 A1 WO2017201767 A1 WO 2017201767A1
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pressure
dyeing
way joint
high pressure
cup
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PCT/CN2016/084892
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English (en)
French (fr)
Inventor
龙家杰
郭建中
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南通纺织丝绸产业技术研究院
苏州大学
泗阳众联纺织科技有限公司
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Priority to US15/556,699 priority Critical patent/US10280542B2/en
Publication of WO2017201767A1 publication Critical patent/WO2017201767A1/zh

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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
    • D06B23/10—Devices for dyeing samples
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B19/00—Treatment of textile materials by liquids, gases or vapours, not provided for in groups D06B1/00 - D06B17/00
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
    • D06B23/14—Containers, e.g. vats
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
    • D06B23/14—Containers, e.g. vats
    • D06B23/18—Sealing arrangements
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
    • D06B23/20—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B2700/00—Treating of textile materials, e.g. bleaching, dyeing, mercerising, impregnating, washing; Fulling of fabrics
    • D06B2700/36—Devices or methods for dyeing, washing or bleaching not otherwise provided for
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B9/00—Solvent-treatment of textile materials
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/94—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dyes dissolved in solvents which are in the supercritical state

Definitions

  • the invention relates to the technical field of pressure vessel and textile dyeing and finishing equipment manufacturing, in particular to a proof dyeing cup for supercritical fluid waterless dyeing and finishing.
  • supercritical CO 2 fluid medium can replace the traditional water bath, dyeing and finishing textiles, and can completely eliminate the high energy consumption and serious environmental pollution caused by traditional water bath processing from the source. Therefore, the development of a waterless equipment system represented by supercritical CO 2 fluid has very important practical and strategic significance for the sustainable development of the textile printing and dyeing industry and ecological environment protection.
  • the printing and dyeing processing of textiles has many processes and long process flow, and the product quality is often affected by a variety of complicated factors, especially in the color processing stage of textiles. Therefore, the printing and dyeing processing of textiles usually requires the process of sampling, placing samples, trial production and production. Among them, the sample is the premise of obtaining the basic formula of the production process. Therefore, the development of efficient, reliable and applicable sample proofing equipment system plays an important role in the application, promotion and industrialization of supercritical fluid waterless dyeing and finishing technology.
  • the existing supercritical fluid dye proofing device or its equipment system is generally a system with a fixed dyeing processing unit, and is equipped with a corresponding pressurization system, and A separate separation and recovery system is designed downstream of the dyeing unit to separate and recover the dyeing medium at the end of the process. Therefore, such a processing system can generally only perform dye proofing processing on one sample at a time, and must be cleaned after each proofing to perform the next proofing test. Especially in the case of color change dyeing, thorough cleaning of the system is very important, and most of the existing device systems or their dyeing processing units are cumbersome to clean and difficult to clean. Therefore, the current efficiency of these existing proofing systems is very low, far from meeting the demand for proofing in commercial production. In addition, the pressurization and separation systems of such dyeing and finishing systems have high idle rates and cannot be effectively utilized. Therefore, this also significantly affects and delays the industrial application and promotion of supercritical fluid waterless dyeing and finishing technology.
  • the object of the present invention is to provide a proofing dyeing cup with high proofing efficiency, simple operation, reliability, high cleaning efficiency, economical utility, and wide application range of supercritical fluid waterless dyeing.
  • the invention discloses a proofing dyeing cup for supercritical fluid waterless dyeing and finishing, comprising a high pressure dyeing cup cylinder, a high pressure dyeing cup sealing cover, a high pressure fluid guiding tube, a first high pressure pipeline, a second high pressure pipeline, and a first high pressure
  • the shutoff valve and the second high pressure shutoff valve are characterized by:
  • the high pressure dye cup sealing cover is disposed at an upper end cup mouth of the high pressure dyeing cup cylinder, and one end of the first high pressure pipe is connected to an upper end of the high pressure dye cup sealing cover, the first high pressure pipe The other end is connected to an external air source or a tank charging system, and the first high pressure shutoff valve is mounted on the first high pressure pipeline;
  • the inner bottom of the high-pressure dyeing cup cylinder has a concave arc shape, and the side wall of the high-pressure dyeing cup cylinder is provided with a medium outlet near the cup mouth, and one end of the second high-pressure pipe is connected The other end of the second high-pressure pipe is connected to an external separation and recovery system, and the second high-pressure shut-off valve is installed on the second high-pressure pipe;
  • the high pressure fluid guiding tube is connected at a lower end of the high pressure dye cup sealing cover, and the high pressure fluid guiding tube is vertically suspended in the high pressure dyeing cup cylinder;
  • a wireless pressure-temperature integrated sensor and a safety valve are further included, the wireless pressure-temperature integrated sensor being mounted on the first high-pressure pipe or the second high-pressure pipe, the safety valve being installed in the first high-pressure pipe or the second On the high pressure pipeline.
  • the wireless pressure temperature integrated sensor and the safety valve are both mounted on the second high pressure pipeline, and the second high pressure pipeline is installed with a four-way joint, and the four-way joint is located at the medium outlet and the Between the second high pressure shut-off valves, the wireless pressure temperature integrated sensor and the safety valve are respectively installed at two opposite interfaces of the four-way joint.
  • the wireless pressure temperature integrated sensor and the safety valve are both mounted on the first high pressure pipeline, and the first high pressure pipeline is mounted with a four-way joint, and the four-way joint is located in the high-pressure dye cup seal Between the cover and the first high pressure shut-off valve, the wireless pressure temperature integrated sensor and the safety The full valves are respectively mounted at two opposite interfaces of the four-way joint.
  • the wireless pressure temperature integrated sensor is mounted on the first high pressure pipeline
  • the safety valve is mounted on the second high pressure pipeline
  • the first high pressure pipeline is mounted with a first three-way joint
  • the first three-way joint is located between the high-pressure dye cup sealing cover and the first high-pressure shut-off valve
  • the wireless pressure temperature integrated sensor is installed at an intermediate interface of the first three-way joint
  • a second three-way joint is disposed on the second high pressure pipe
  • the second three-way joint is located between the medium outlet and the second high pressure shutoff valve
  • the safety valve is installed in the middle of the second three-way joint At the interface.
  • the wireless pressure temperature integrated sensor is mounted on the second high pressure pipeline
  • the safety valve is mounted on the first high pressure pipeline
  • the first high pressure pipeline is mounted with a first three-way joint
  • the first three-way joint is located between the high-pressure dye cup sealing cover and the first high-pressure shut-off valve
  • the safety valve is installed at an intermediate interface of the first three-way joint
  • the second high-pressure pipe a second three-way joint is disposed thereon
  • the second three-way joint is located between the medium outlet and the second high-pressure shut-off valve
  • the wireless pressure temperature integrated sensor is installed in the middle of the second three-way joint At the interface.
  • the upper end of the high-pressure fluid guiding tube is connected by thread to the first high-pressure pipe on the high-pressure dye cup sealing cover, and the lower end of the high-pressure fluid guiding tube is 0.5 from the bottom of the high-pressure dyeing cup cylinder. -5cm.
  • the present invention has at least the following advantages: the present invention can not only connect the high-pressure dyeing cup with the supercritical fluid pressurized tank charging and separation recovery system, and realize the separation and recovery of the medium after the filling and processing of the processing medium; It can also be separated and disconnected from the above system, so that the traditional supercritical fluid fixed dye proofing unit becomes a movable dyeing cup, and the plurality of dyeing units (dye cups) can be charged separately or simultaneously. Then concentrate on the purpose of simultaneous temperature proofing processing.
  • the proofing processing efficiency of high-pressure supercritical fluid waterless dyeing and the corresponding utilization rate of the medium pressurized tank filling and separation and recovery system are greatly improved, and the demand for proofing of the commercial production of textile waterless dyeing and finishing is adapted.
  • the wireless pressure and temperature integrated sensor set on the dyeing cup can transmit the medium pressure and temperature in the dyeing cup to the external receiving system in real time, realizing the record and real-time monitoring of the medium pressure and temperature in the dyeing cup.
  • the safety valve set on the dyeing cup can effectively ensure the safe use of the dye cup under high pressure conditions.
  • the high-pressure fluid guiding tube provided in the dyeing cup can realize the stirring and dissolving of the chemicals such as the cup bottom dye by means of the flow rate and pressure of the tank filling medium, and can effectively realize the chemicals such as the bottom dye in the dye cup cleaning stage. Purge, improve cleaning effectiveness. Therefore, the existing fixed supercritical fluid dyeing proofing device or its equipment system has the disadvantages of low utilization efficiency, cumbersome cleaning, and inability to meet the requirements of commercial production for proofing. Therefore, the technology of the invention can significantly improve the proofing efficiency of the supercritical fluid waterless dyeing and finishing production, and has the advantages of high utilization rate of the equipment system, simple operation, reliability, high cleaning efficiency, economy and practicality, wide application range and the like. It is of great application prospect and important practical significance to solve the generation and emission of pollutants in the textile printing and dyeing industry from the source and realize the ecological and green clean production of the textile printing and dyeing industry.
  • FIG. 1 is a schematic structural view of a proof dyeing cup of a supercritical fluid without dyeing and finishing according to a first embodiment of the present invention
  • FIG. 2 is a schematic structural view of a proof dyeing cup of a supercritical fluid without dyeing and finishing according to a second embodiment of the present invention
  • FIG. 3 is a schematic structural view of a proof dyeing cup of a supercritical fluid without dyeing and finishing according to a third embodiment of the present invention
  • FIG. 4 is a schematic structural view of a proof dyeing cup of a supercritical fluid without dyeing and finishing according to a fourth embodiment of the present invention.
  • 1 - first high pressure cut-off valve 1 - first high pressure cut-off valve; 2 - wireless pressure and temperature integrated sensor; 3- safety valve; 4 - high pressure dye cup sealing cover; 5 - second high pressure shut-off valve; 6 - high pressure dye cup cylinder; 7- High pressure fluid guiding tube; 8-first high pressure pipeline; 9-second high pressure pipeline; 10-media outlet; 12-four-way joint; 13-first three-way joint; 14-second three-way joint.
  • Embodiment 1 is a diagrammatic representation of Embodiment 1:
  • a supercritical fluid water-free dyeing and proofing dyeing cup comprises a high-pressure dyeing cup cylinder 6, a high-pressure dye cup sealing cover 4, a high-pressure fluid guiding tube 7, a first high-pressure pipeline 8, and a second a high pressure pipe 9, a first high pressure shutoff valve 1 and a second high pressure shutoff valve 5,
  • the high pressure dye cup sealing cover is disposed at an upper end cup mouth of the high pressure dyeing cup cylinder, and one end of the first high pressure pipe is connected At an upper end of the high-pressure dye cup sealing cover, the other end of the first high-pressure pipe is connected to an external air source or a tank charging system, and the first high-voltage intercepting a check valve is mounted on the first high pressure pipe;
  • the first high pressure shut-off valve allows the filling of the medium tank of the dyeing cup and the separation of the gas source or the tank filling system.
  • the inner bottom of the high-pressure dyeing cup cylinder has a concave arc shape, and the side wall of the high-pressure dyeing cup cylinder is provided with a medium outlet 10 near the cup mouth, and one end of the second high-pressure pipe is connected The other end of the second high-pressure pipe is connected to an external separation and recovery system, and the second high-pressure shut-off valve is installed on the second high-pressure pipe;
  • the second high pressure shut-off valve allows decompression output of the medium in the dyeing cup and separation from the separation and recovery system.
  • the high pressure fluid guiding tube is connected at a lower end of the high pressure dye cup sealing cover, and the high pressure fluid guiding tube is vertically suspended in the high pressure dyeing cup cylinder;
  • the utility model further comprises a wireless pressure and temperature integrated sensor 2 and a safety valve 3, wherein the wireless pressure temperature integrated sensor and the safety valve are both mounted on the second high pressure pipeline, and the fourth high pressure pipeline is provided with a four-way joint 12,
  • the four-way joint is located between the medium outlet and the second high-pressure shut-off valve, and the wireless pressure temperature integrated sensor and the safety valve are respectively installed at two opposite interfaces of the four-way joint.
  • the wireless pressure-temperature integrated sensor enables remote transmission of the medium air pressure in the dyeing cup, and the safety valve enables emergency relief when the pressure inside the cup exceeds the safe pressure.
  • the upper end of the high pressure fluid guiding tube is connected to the first high pressure pipe on the high pressure dye cup sealing cover by a thread, and the lower end of the high pressure fluid guiding tube is 0.5-5 cm away from the bottom of the high pressure dyeing cup cylinder.
  • the stirring and dissolving of chemicals such as the bottom of the cup can be realized, and the cleaning of the bottom dye and the like can be effectively realized in the dyeing cup cleaning stage, thereby improving the cleaning efficiency.
  • the installation position of the wireless pressure-temperature integrated sensor and the safety valve is not limited to that described in the first embodiment, and can be installed at other positions.
  • the following embodiments show other installation positions of the wireless pressure-temperature integrated sensor and the safety valve. .
  • Embodiment 2 is a diagrammatic representation of Embodiment 1:
  • the wireless pressure temperature integrated sensor and the safety valve are both installed in the first a four-way joint 12 is disposed on the high-pressure pipe, and the four-way joint is located between the high-pressure dye cup sealing cover and the first high-pressure shut-off valve, and the wireless pressure temperature integrated sensor And safety valves are respectively installed at two opposite interfaces of the four-way joint.
  • Embodiment 3 is a diagrammatic representation of Embodiment 3
  • the wireless pressure temperature integrated sensor is mounted on the first high pressure pipeline, the safety valve is installed on the second high pressure pipeline, and the first high pressure pipeline is installed with the first three a through joint 13, the first three-way joint is located between the high-pressure dye cup sealing cover and the first high-pressure shut-off valve, and the wireless pressure temperature integrated sensor is installed at an intermediate interface of the first three-way joint a second three-way joint 14 is disposed on the second high-pressure pipe, the second three-way joint is located between the medium outlet and the second high-pressure shut-off valve, and the safety valve is installed in the second The intermediate interface of the tee joint.
  • Embodiment 4 is a diagrammatic representation of Embodiment 4:
  • the wireless pressure temperature integrated sensor is mounted on the second high pressure pipeline, the safety valve is installed on the first high pressure pipeline, and the first high pressure pipeline is installed with the first three a through joint 13 between the high pressure dye cup sealing cover and the first high pressure shutoff valve, the safety valve being installed at an intermediate interface of the first three-way joint, a second three-way joint 14 is disposed on the second high-pressure pipe, the second three-way joint is located between the medium outlet and the second high-pressure shut-off valve, and the wireless pressure temperature integrated sensor is installed in the second The intermediate interface of the tee joint.
  • the dyeing materials such as the quantitative textile products and the quantitative dyes to be dyed and the like are first placed in the high pressure dyeing cup cylinder 6.
  • the high-pressure dye cup sealing cover 4 seals the high-pressure dyeing cup cylinder and assembles and assembles other components.
  • the first high pressure shut-off valve 1 is closed and the dye cup system is separated from the tank filling system. Repeat the above operation to charge the series of dye cups that need to be proofed.
  • the prepared dye cup to be warmed up is placed in a heating system or other heating bath, and concentrated proofing processing is performed according to a predetermined heating program and proofing conditions.
  • the dyeing cups may be separately or simultaneously passed through the second high-pressure pipeline at the outer end of the second high-pressure shut-off valve 5 to a dedicated separation and recovery system to separate and recover the dyeing medium.
  • the dyeing cup is also connected to the processing medium gas source or the medium tank filling system through the upper first high pressure pipeline connected by the first high pressure shut-off valve 1 to use the clean fluid medium to float the sample on the dyeing cup. Color or other residual dyes, as well as the remaining dye in the cup for cleaning.
  • the cleaned medium is passed through the medium outlet 10 at the outer side of the outer side of the high pressure dyeing cylinder 6, and then treated by the above separation and recovery system.
  • the first high-pressure shut-off valve 1 provided on each dye cup is first closed, and then the medium in each dye cup is fully recovered and depressurized by the gas pump configured by the separation and recovery system.
  • the gas pump of the separation recovery system stops the pump.
  • the special processing medium gas source or medium tank charging system connected to the dyeing cup, and the separation and recovery system are separately separated and separated, and the high-pressure dye cup sealing cover 4 is opened, and the proofing sample is taken out to complete the sample proofing without water dyeing. Repeat the above operation to continue the sample proofing of the next round of supercritical fluid waterless finishing.

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Abstract

本发明公开了一种超临界流体无水染整的打样染杯，可有效实现将传统的超临界流体固定染色打样单元变为一种可移动式的染杯，实现了将多个染色单元(染杯)分别或同时进行介质罐充，然后集中同时进行升温打样加工的目的。从而大大提高了高压超临界流体无水染色等打样加工效率，以及相应的介质增压罐充和分离回收***的利用率，适应了纺织品无水染整商业化生产对打样的需求。此外，利用本发明技术还可实现对杯底染化料的进行搅拌助溶，以及对底部染化料的清洗吹扫。从而克服了现有固定式超临界流体染色打样装置或其设备***利用效率低、清洗繁琐、不能满足商业化生产对打样需求等缺点。

Description

一种超临界流体无水染整的打样染杯
本申请要求了申请日为2016年5月30日，申请号为201610362338.0，发明名称为“一种超临界流体无水染整的打样染杯”的中国专利申请的优先权，其全部内容通过引用结合在本申请中。
技术领域
本发明涉及压力容器及纺织染整设备制造技术领域，尤其涉及一种超临界流体无水染整的打样染杯。
背景技术
采用超临界CO2等流体介质可以代替传统水浴，对纺织品进行染整加工，能从源头上彻底消除传统水浴加工所带来能耗高、环境污染严重等困扰。故研发以超临界CO2流体为代表的无水装备***，对纺织印染行业的可持续化发展，以及生态环境保护等都具有非常重要的现实和战略意义。
通常，纺织品的印染加工生产，其工序多、工艺流程长，产品质量往往受到多种复杂因素的综合影响，尤其在纺织品的颜色加工阶段。因而，纺织品的印染加工，通常需要经过打小样、放中样、试生产和生产等环节。其中，打小样是获得生产工艺基础配方的前提。因此，研发高效、可靠、适用的小样打样设备***，对超临界流体无水染整技术的应用、推广和产业化都具有非常重要的作用。
然而，从目前公开的文献报道和实际应用看，现有的超临界流体染色打样装置或其设备***，一般都是一个***设置一个固定染色加工单元，并配备一个对应的加压***，以及在染色单元下游设计一套分离回收***，以便工艺结束时对染色介质实现分离回收。因而，这类加工***一般一次只能对一个样品进行染色打样加工，而且每次打样结束后还须进行清洗，才能进行下一次打样试验。尤其在换色染色时，***的彻底清洗显得非常重要，而现有的多数装置***或其染色加工单元，其清洗过程繁琐，且不易洗净。故目前这些现有打样***的效率非常低，远远不能满足商业化生产对打样的需求。此外，这类染整打样***配置的加压和分离***，其闲置率也很高，不能得到有效充分利用。 因而，这也显著地影响并迟滞了超临界流体无水染整技术的产业化应用和推广。
有鉴于上述的缺陷，本设计人，积极加以研究创新，以期创设一种超临界流体无水染整的打样染杯，使其更具有产业上的利用价值。
发明内容
为解决上述技术问题，本发明的目的是提供一种打样效率高、操作简便、可靠、清洗效率高、经济实用、应用范围广的超临界流体无水染整的打样染杯。
本发明提出的一种超临界流体无水染整的打样染杯，包括高压染杯筒体、高压染杯密封盖、高压流体导流管、第一高压管道、第二高压管道、第一高压截止阀和第二高压截止阀，其特征在于：
所述高压染杯密封盖盖设在所述高压染杯筒体的上端杯口处，所述第一高压管道的一端连接在所述高压染杯密封盖的上端，所述第一高压管道的另一端供外部气源或罐充***连接，所述第一高压截止阀安装在所述第一高压管道上；
所述高压染杯筒体的内侧底部呈下凹的圆弧形，所述高压染杯筒体的侧壁靠近所述杯口的位置设有介质出口，所述第二高压管道的一端连接在所述介质出口处，所述第二高压管道的另一端供外部分离回收***连接，所述第二高压截止阀安装在所述第二高压管道上；
所述高压流体导流管连接在所述高压染杯密封盖的下端，所述高压流体导流管竖直悬挂在所述高压染杯筒体中；
还包括无线压力温度一体化传感器和安全阀，所述无线压力温度一体化传感器安装在所述第一高压管道或第二高压管道上，所述安全阀安装在所述第一高压管道或第二高压管道上。
进一步的，所述无线压力温度一体化传感器和安全阀均安装在所述第二高压管道上，所述第二高压管道上安装有四通接头，所述四通接头位于所述介质出口与所述第二高压截止阀之间，所述无线压力温度一体化传感器和安全阀分别安装在所述四通接头两个相对的接口处。
进一步的，所述无线压力温度一体化传感器和安全阀均安装在所述第一高压管道上，所述第一高压管道上安装有四通接头，所述四通接头位于所述高压染杯密封盖与所述第一高压截止阀之间，所述无线压力温度一体化传感器和安 全阀分别安装在所述四通接头两个相对的接口处。
进一步的，所述无线压力温度一体化传感器安装在所述第一高压管道上，所述安全阀安装在所述第二高压管道上，所述第一高压管道上安装有第一三通接头，所述第一三通接头位于所述高压染杯密封盖与所述第一高压截止阀之间，所述无线压力温度一体化传感器安装在所述第一三通接头的中间接口处，所述第二高压管道上安装有第二三通接头，所述第二三通接头位于所介质出口与所述第二高压截止阀之间，所述安全阀安装在所述第二三通接头的中间接口处。
进一步的，所述无线压力温度一体化传感器安装在所述第二高压管道上，所述安全阀安装在所述第一高压管道上，所述第一高压管道上安装有第一三通接头，所述第一三通接头位于所述高压染杯密封盖与所述第一高压截止阀之间，所述安全阀安装在所述第一三通接头的中间接口处，所述第二高压管道上安装有第二三通接头，所述第二三通接头位于所介质出口与所述第二高压截止阀之间，所述无线压力温度一体化传感器安装在所述第二三通接头的中间接口处。
进一步的，所述高压流体导流管的上端通过螺纹与高压染杯密封盖上的第一高压管道连接，所述高压流体导流管的下端距离所述高压染杯筒体底部的距离为0.5-5cm。
借由上述方案，本发明至少具有以下优点：本发明既可将高压染杯与超临界流体增压罐充和分离回收***进行连接，实现加工介质的罐充和结束后介质的分离回收；同时也可与上述***进行分离断开，从而将传统的超临界流体固定染色打样单元变为了一种可移动式的染杯，实现了将多个染色单元(染杯)分别或同时进行介质罐充，然后集中同时进行升温打样加工的目的。从而大大提高了高压超临界流体无水染色等打样加工效率，以及相应的介质增压罐充和分离回收***的利用率，适应了纺织品无水染整商业化生产对打样的需求。同时，染杯上设置的无线压力温度一体化传感器可将染杯中介质压力、温度实时传输到外置接受***，实现对染杯中介质压力、温度的纪录和实时监控。染杯上设置的安全阀可有效保证高压条件下染杯的使用安全。此外，染杯内设置的高压流体导流管可借助罐充介质的流速和压力，实现对杯底染料等化学品的搅拌助溶，在染杯清洗阶段也可有效实现对底部染料等化学品的吹扫，提高清洗 效率。从而克服了现有固定式超临界流体染色打样装置或其设备***利用效率低、清洗繁琐、不能满足商业化生产对打样需求等缺点。因而，本发明技术可显著提高超临界流体无水染整生产的打样效率，并具有设备***利用率高、操作简便、可靠、清洗效率高、经济实用、应用范围广等优点。对从源头上解决纺织印染行业污染物的产生和排放，实现纺织印染行业的生态、绿色化清洁生产，具有非常广阔的应用前景和重要的实际意义。
上述说明仅是本发明技术方案的概述，为了能够更清楚了解本发明的技术手段，并可依照说明书的内容予以实施，以下以本发明的较佳实施例并配合附图详细说明如后。
附图说明
图1为本发明实施例一中超临界流体无水染整的打样染杯的结构示意图；
图2为本发明实施例二中超临界流体无水染整的打样染杯的结构示意图；
图3为本发明实施例三中超临界流体无水染整的打样染杯的结构示意图；
图4为本发明实施例四中超临界流体无水染整的打样染杯的结构示意图；
其中：1-第一高压截止阀；2-无线压力温度一体化传感器；3-安全阀；4-高压染杯密封盖；5-第二高压截止阀；6-高压染杯筒体；7-高压流体导流管；8-第一高压管道；9-第二高压管道；10-介质出口；12-四通接头；13-第一三通接头；14-第二三通接头。
具体实施方式
下面结合附图和实施例，对本发明的具体实施方式作进一步详细描述。以下实施例用于说明本发明，但不用来限制本发明的范围。
实施例一：
如图1所示，一种超临界流体无水染整的打样染杯，包括高压染杯筒体6、高压染杯密封盖4、高压流体导流管7、第一高压管道8、第二高压管道9、第一高压截止阀1和第二高压截止阀5，所述高压染杯密封盖盖设在所述高压染杯筒体的上端杯口处，所述第一高压管道的一端连接在所述高压染杯密封盖的上端，所述第一高压管道的另一端供外部气源或罐充***连接，所述第一高压截 止阀安装在所述第一高压管道上；
第一高压截止阀可实现对染杯的介质罐充，以及与气源或罐充***的分离断开。
所述高压染杯筒体的内侧底部呈下凹的圆弧形，所述高压染杯筒体的侧壁靠近所述杯口的位置设有介质出口10，所述第二高压管道的一端连接在所述介质出口处，所述第二高压管道的另一端供外部分离回收***连接，所述第二高压截止阀安装在所述第二高压管道上；
第二高压截止阀可实现对染杯内的介质进行解压输出，以及与分离回收***的分离断开。
所述高压流体导流管连接在所述高压染杯密封盖的下端，所述高压流体导流管竖直悬挂在所述高压染杯筒体中；
还包括无线压力温度一体化传感器2和安全阀3，所述无线压力温度一体化传感器和安全阀均安装在所述第二高压管道上，所述第二高压管道上安装有四通接头12，所述四通接头位于所述介质出口与所述第二高压截止阀之间，所述无线压力温度一体化传感器和安全阀分别安装在所述四通接头两个相对的接口处。
无线压力温度一体化传感器可实现对染杯内介质气压的远程传输，安全阀则可实现当杯内压力超过安全压力时进行紧急泄压。
所述高压流体导流管的上端通过螺纹与高压染杯密封盖上的第一高压管道连接，所述高压流体导流管的下端距离所述高压染杯筒体底部的距离为0.5-5cm。
在对染杯进行介质罐充时可实现对杯底染料等化学品的搅拌助溶，在染杯清洗阶段也可有效实现对底部染料等化学品的吹扫，提高清洗效率。
当然无线压力温度一体化传感器和安全阀的安装位置并不局限于实施例一中所述，还可安装在其它位置，以下实施例给出了无线压力温度一体化传感器和安全阀的其它安装位置。
实施例二：
如图2所示，所述无线压力温度一体化传感器和安全阀均安装在所述第一 高压管道上，所述第一高压管道上安装有四通接头12，所述四通接头位于所述高压染杯密封盖与所述第一高压截止阀之间，所述无线压力温度一体化传感器和安全阀分别安装在所述四通接头两个相对的接口处。
实施例三：
如图3所示，所述无线压力温度一体化传感器安装在所述第一高压管道上，所述安全阀安装在所述第二高压管道上，所述第一高压管道上安装有第一三通接头13，所述第一三通接头位于所述高压染杯密封盖与所述第一高压截止阀之间，所述无线压力温度一体化传感器安装在所述第一三通接头的中间接口处，所述第二高压管道上安装有第二三通接头14，所述第二三通接头位于所介质出口与所述第二高压截止阀之间，所述安全阀安装在所述第二三通接头的中间接口处。
实施例四：
如图4所示，所述无线压力温度一体化传感器安装在所述第二高压管道上，所述安全阀安装在所述第一高压管道上，所述第一高压管道上安装有第一三通接头13，所述第一三通接头位于所述高压染杯密封盖与所述第一高压截止阀之间，所述安全阀安装在所述第一三通接头的中间接口处，所述第二高压管道上安装有第二三通接头14，所述第二三通接头位于所介质出口与所述第二高压截止阀之间，所述无线压力温度一体化传感器安装在所述第二三通接头的中间接口处。
本发明的一种超临界流体无水染整的打样染杯工作时，首先将待染色等打样处理的定量纺织制品和定量染料等染化料，置于高压染杯筒体6内。高压染杯密封盖4密封高压染杯筒体，并对其他部件进行相应连接组装。然后关闭第二高压截止阀5，将与第一高压截止阀1连接的上端第一高压管道与加工介质气源或介质罐充***连通，并开启第一高压截止阀1对染杯***进行定量介质罐充。完成后关闭第一高压截止阀1，并将染杯***与罐充***进行分离。重复上述操作，将需打样处理的系列染杯进行介质罐充。然后将准备好的待升温打样的染杯置于加热***或其他升温浴中，并按照预定升温程序和打样条件进行集中打样处理。
打样结束后，可分别或同时将各染杯通过第二高压截止阀5外侧端的第二高压管道接入专用的分离回收***，对染色介质进行分离回收。同时，根据实际打样需求，染杯也通过第一高压截止阀1连接的上端第一高压管道与加工介质气源或介质罐充***连通，以利用干净流体介质对染杯内打样品上的浮色或其他残留染化料，以及杯内残留的染化料进行清洗。清洗的介质通过高压染杯筒体6外侧面上端的介质出口10，再经上述分离回收***进行处理。
分离回收或/和清洗结束后，首先须使各染杯上设置的第一高压截止阀1处于关闭状态，然后利用分离回收***配置的气体泵对各染杯内介质进行充分回收和降压。当无线压力温度一体化传感器2显示的压力等于或小于大气压时，分离回收***的气体泵停泵。然后将与染杯连接的专用加工介质气源或介质罐充***，以及分离回收***分别断开分离，并打开高压染杯密封盖4，取出打样样品，完成无水染整的试样打样。重复上述操作，可继续实现下一轮的超临界流体无水染整的试样打样。
以上所述仅是本发明的优选实施方式，并不用于限制本发明，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明技术原理的前提下，还可以做出若干改进和变型，这些改进和变型也应视为本发明的保护范围。

Claims (6)

  1. 一种超临界流体无水染整的打样染杯，包括高压染杯筒体(6)、高压染杯密封盖(4)、高压流体导流管(7)、第一高压管道(8)、第二高压管道(9)、第一高压截止阀(1)和第二高压截止阀(5)，其特征在于：
    所述高压染杯密封盖盖设在所述高压染杯筒体的上端杯口处，所述第一高压管道的一端连接在所述高压染杯密封盖的上端，所述第一高压管道的另一端供外部气源或罐充***连接，所述第一高压截止阀安装在所述第一高压管道上；
    所述高压染杯筒体的内侧底部呈下凹的圆弧形，所述高压染杯筒体的侧壁靠近所述杯口的位置设有介质出口(10)，所述第二高压管道的一端连接在所述介质出口处，所述第二高压管道的另一端供外部分离回收***连接，所述第二高压截止阀安装在所述第二高压管道上；
    所述高压流体导流管连接在所述高压染杯密封盖的下端，所述高压流体导流管竖直悬挂在所述高压染杯筒体中；
    还包括无线压力温度一体化传感器(2)和安全阀(3)，所述无线压力温度一体化传感器安装在所述第一高压管道或第二高压管道上，所述安全阀安装在所述第一高压管道或第二高压管道上。
  2. 根据权利要求1所述的一种超临界流体无水染整的打样染杯，其特征在于：所述无线压力温度一体化传感器和安全阀均安装在所述第二高压管道上，所述第二高压管道上安装有四通接头(12)，所述四通接头位于所述介质出口与所述第二高压截止阀之间，所述无线压力温度一体化传感器和安全阀分别安装在所述四通接头两个相对的接口处。
  3. 根据权利要求1所述的一种超临界流体无水染整的打样染杯，其特征在于：所述无线压力温度一体化传感器和安全阀均安装在所述第一高压管道上，所述第一高压管道上安装有四通接头(12)，所述四通接头位于所述高压染杯密封盖与所述第一高压截止阀之间，所述无线压力温度一体化传感器和安全阀分别安装在所述四通接头两个相对的接口处。
  4. 根据权利要求1所述的一种超临界流体无水染整的打样染杯，其特征在于：所述无线压力温度一体化传感器安装在所述第一高压管道上，所述安全阀安装在所述第二高压管道上，所述第一高压管道上安装有第一三通接头(13)， 所述第一三通接头位于所述高压染杯密封盖与所述第一高压截止阀之间，所述无线压力温度一体化传感器安装在所述第一三通接头的中间接口处，所述第二高压管道上安装有第二三通接头(14)，所述第二三通接头位于所介质出口与所述第二高压截止阀之间，所述安全阀安装在所述第二三通接头的中间接口处。
  5. 根据权利要求1所述的一种超临界流体无水染整的打样染杯，其特征在于：所述无线压力温度一体化传感器安装在所述第二高压管道上，所述安全阀安装在所述第一高压管道上，所述第一高压管道上安装有第一三通接头(13)，所述第一三通接头位于所述高压染杯密封盖与所述第一高压截止阀之间，所述安全阀安装在所述第一三通接头的中间接口处，所述第二高压管道上安装有第二三通接头(14)，所述第二三通接头位于所介质出口与所述第二高压截止阀之间，所述无线压力温度一体化传感器安装在所述第二三通接头的中间接口处。
  6. 根据权利要求1-5中任意一项所述的一种超临界流体无水染整的打样染杯，其特征在于：所述高压流体导流管的上端通过螺纹与高压染杯密封盖上的第一高压管道连接，所述高压流体导流管的下端距离所述高压染杯筒体底部的距离为0.5-5cm。
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