WO2017141471A1 - Procédé de production de carburant mixte huile-eau - Google Patents

Procédé de production de carburant mixte huile-eau Download PDF

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Publication number
WO2017141471A1
WO2017141471A1 PCT/JP2016/076724 JP2016076724W WO2017141471A1 WO 2017141471 A1 WO2017141471 A1 WO 2017141471A1 JP 2016076724 W JP2016076724 W JP 2016076724W WO 2017141471 A1 WO2017141471 A1 WO 2017141471A1
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WIPO (PCT)
Prior art keywords
water
fuel
added
producing
mixing
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PCT/JP2016/076724
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English (en)
Japanese (ja)
Inventor
泰弘 山本
高橋　剛
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泰弘 山本
高橋　剛
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Application filed by 泰弘 山本, 高橋　剛 filed Critical 泰弘 山本
Publication of WO2017141471A1 publication Critical patent/WO2017141471A1/fr

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/32—Liquid carbonaceous fuels consisting of coal-oil suspensions or aqueous emulsions or oil emulsions

Definitions

  • the present invention relates to a method and an apparatus for producing an oil-water fusion fuel (hereinafter referred to as water-added fuel) in which water improved by an additive and natural or artificial ore is added to the additive and natural or artificial ore fuel oil.
  • water-added fuel oil-water fusion fuel
  • Patent Document 1 there is a limit to the period during which the oil / water separation phenomenon can be prevented, and the oil / water separation phenomenon may occur after two to three months.
  • the transparency of the water fuel is lower than that of the oil.
  • the present invention has been made in view of the circumstances described above, and its purpose is that once it is synthesized, it is never separated into water and oil, and it is highly transparent and indistinguishable from ordinary oil. It is to provide a method for producing a hydrolyzed fuel.
  • the method for producing a hydrolyzed fuel of the present invention subdivides the molecular assembly of water and ionizes it in the hydrolyzed fuel producing method in which fuel oil and water are mixed to produce hydrolyzed fuel.
  • An ionization process Desirably, as an additive to water, an additive charging step of adding an enzyme having a surfactant activity, sodium hydroxide, potassium hydroxide, sodium, magnesium chloride, magnesium, aqueous hydrogen peroxide, An agitation and mixing step of adding fuel oil to an agitation and mixing tank and mixing and agitating the ionized water added to the additive while circulating the fuel oil by a mixer; and
  • the gist of the present invention is that it comprises a fusing step of repeating a stirring and mixing step in a state where a temperature of 15 to 80 ° C. and an atmospheric pressure of 1.5 to 9 Pa are applied to the fuel oil and water that have been stirred and mixed.
  • the ionization step two irradiation operations of irradiating water with ultrasonic waves of 15 kHz to 60 kHz and irradiating ultrasonic waves of 200 kHz or higher can be performed.
  • the molecular aggregate of water can be subdivided by adding a porous membrane emulsification technique such as an SPG membrane emulsification technique to water.
  • the enzyme may be added in an amount of 0.004% to 2% by weight with respect to each volume of the fuel oil and water, or the sodium hydroxide may be added to the water.
  • the aqueous hydrogen peroxide solution may be added in an amount of less than 0.001% by weight to 0.1% by weight with respect to water.
  • the above-described configuration realizes a water-added fuel that is once separated without being separated into water and oil and that is highly transparent and indistinguishable from ordinary oil.
  • the hydrothermal fuel of the present invention has a calorific value per unit quantity equal to or higher than that of existing fuel oil, and further, compared with existing fuel oil, deterioration and corrosion of the combustion chamber, exhaust pipe, etc. after combustion. There is an effect that there is little.
  • the water-added fuel of the present invention is excellent in complete combustibility, hardly produces carbon monoxide, and has various effects such as low carbon dioxide emission.
  • FIG. 1 is a flowchart for explaining a method for producing a water-added fuel according to the first embodiment of the present invention.
  • the method for producing a water-added fuel according to the present invention comprises an ionization step 1 for subdividing a molecular aggregate of water as a raw material, and an additive addition step 2 for adding an additive to water desirably.
  • the molecular aggregate of water as a raw material is subdivided by various methods.
  • a first method there is a method of subdividing a molecular assembly of water by irradiating water with ultrasonic waves.
  • a porous ionized substance, natural or artificial ore, and an ion generating material are placed in water and brought into contact with water in accordance with the convection of the water.
  • the generation of natural or artificial ore and ions is activated by irradiating ultrasonic waves.
  • the redox potential ORP (mV) of water obtained by irradiating this ultrasonic wave is preferably 100 mV to -900 mV.
  • the redox potential ORP (mV) of ordinary tap water is generally 500 mV to 600 mV.
  • the step of irradiating ultrasonic waves two irradiation operations are performed: a step of irradiating ultrasonic waves of 10 kHz to 60 kHz and a step of irradiating ultrasonic waves of 200 kHz or higher.
  • oxygen is released and the hydrogen content ratio is improved.
  • Examples of natural or artificial ores include pyrite, marcasite, cinnabar, galena, porphyry, halogenated minerals, fluorite, cryolite, tourmaline, obsidian, magnesium, calcite, urexite (TV stone), Colemanite, Examples thereof include borax, howlite, gypsum, barite, celestite, phosphorite uranium, carnotite, brocade, black sandstone, barley stone, and quartz.
  • the particle size of the natural or artificial ore can be determined as appropriate according to the size that can obtain a sufficient function of various materials.
  • the added mineral component and the individual substance to be added.
  • examples include calcium, phosphorus, silicon, magnesium, sodium, selenium, zinc, vanadium, germanium, nickel, manganese, molybdenum, copper, tungsten, cobalt, lithium, barium, iron, potassium, aluminum, rubidium, titanium, etc. is there.
  • a porous membrane emulsification technique such as an SPG (Shirasu Porous Glass) film emulsification technique
  • SPG membrane emulsification is an emulsification method in which the dispersed phase liquid is extruded at a certain pressure through the SPG membrane, and is successively dispersed as uniform particles in the continuous phase liquid slowly flowing on the side to be extruded.
  • the subdividing process using the SPG membrane module is performed before and after the ultrasonic irradiation process of water.
  • FIG. 2 is a cross-sectional view showing the structure of an apparatus for emulsifying water into a film.
  • the membrane emulsifying device 10 includes a device main body 11 forming a housing, an SPG film 12 disposed in the device main body 11, and a cap 13 removably attached to one end (left end in FIG. 2) of the device main body 11. And a sleeve 14 attached to the cap 13, a cap 15 detachably attached to the other end (right end in FIG. 2) of the apparatus body 11, and a sleeve 16 attached to the cap 15.
  • the apparatus main body 11 has a cylindrical structure with both ends opened as a whole, and the SPG film 12 extends in the longitudinal direction inside the cylinder and is installed with a gap 17 between the cylinder inner wall. Further, O-rings 18 and 19 are attached to both end portions of the SPG film 12, respectively, and when the caps 13 and 15 are attached to the apparatus main body 11, the O-rings 18 and 19 are respectively attached to the inner end surfaces of the apparatus main body 11.
  • the inside of the cylinder is kept airtight by crimping.
  • the left cap 13 is shown detached from the apparatus main body 11, and the right cap 15 is shown fastened to the apparatus main body 11 by a method such as screwing.
  • the sleeves 14 and 16 have a female screw structure and are screw-coupled to other members.
  • a lateral hole 20 and a lateral hole 21 are provided in the vicinity of both ends of the apparatus main body 11 to communicate the inside and outside of the cylinder of the apparatus main body 11.
  • This film emulsification apparatus 10 can be used in all scenes such as SPG film emulsification and SPG film bubbling.
  • Model No. MD10L125 (or MD05L125): Device external dimensions (body diameter x length mm) manufactured by spg Techno Co., Ltd. ⁇ 25 ⁇ L160 ⁇ 25 ⁇ L160 Specification of SPG membrane (outer diameter x length mm) ⁇ 10 ⁇ L125 ⁇ 05 ⁇ L125 Material SUS303
  • SPG can be applied as a functional glass because it has an infinite number of micron-sized uniform pores and the pore diameter can be designed in a wide range from nano units to micron units.
  • a method for producing this SPG shirasu lime or boric acid is added and an SPG basic glass is synthesized and formed at a temperature of around 1350 ° C. When this is heated, a phenomenon called “phase separation” occurs in the fine structure of the glass. Since CaO ⁇ B 2 O 3 is a component that is easily dissolved in acid, it is dissolved by treatment with hydrochloric acid or the like, and a porous glass body having an Al 2 O 3 ⁇ SiO 2 glass that does not dissolve in acid as a skeleton can be formed. It is.
  • SPG can be applied to fields such as pharmaceuticals such as separation membranes, adsorbents, and anticancer agents, foods, and cosmetics.
  • SPG features include the following.
  • ⁇ There are countless through pores that are precisely controlled.
  • ⁇ Pore size can be designed over a wide range of pore sizes, ranging from 5 / 100,000 micropores (0.05 ⁇ m) to 1/50 (20 ⁇ m) relatively macropores.
  • ⁇ It is possible to make the surface hydrophilic or hydrophobic by introducing surface chemical modification and to introduce various organic functional groups.
  • ⁇ Despite being porous, it has very high mechanical strength and excellent heat resistance and heat insulation. ⁇ It is not affected by most reagents except strong alkali and hydrofluoric acid. ⁇ Not affected by mold or bacteria.
  • FIG. 3 is a graph showing the relative volume (unit: vol%) of SPG having a pore diameter of 1.45 ⁇ m and a porosity of 56% as an example. From this figure, it can be seen that the relative volume of SPG is almost 100%.
  • the dispersed phase liquid (water in the present embodiment) is passed from the side hole 20 to the side hole 21 of the membrane emulsification apparatus 10 (or vice versa) through the SPG membrane 12, and a certain constant pressure is applied. This is done by extruding.
  • this is an emulsification method in which uniform particles are successively dispersed in a continuous phase liquid that is slowly flowing on the extruded side.
  • this method is called a “direct membrane emulsification method” and can generate a particle size 3-4 times the SPG pore size.
  • Additive charging step Next, the additive charging step will be described.
  • a plurality of additives are charged (added) to the ionized water.
  • An enzyme is added as the first additive. Enzyme addition works well as an additive at an addition amount of 0.004 to 0.1% by weight with respect to water, but a larger ratio may be used, and a maximum of about 1.0% is appropriate. It is. Enzymes may be added to water or oil, or both.
  • NaOH sodium hydroxide
  • Addition of sodium hydroxide sufficiently exhibits the role as an additive at an addition amount of less than 0.001 wt% to 0.1 wt% with respect to water.
  • an aqueous hydrogen peroxide solution is added to water. The addition of the aqueous hydrogen peroxide solution fully functions as an additive at an addition amount of less than 0.001% by weight to 0.1% by weight with respect to water.
  • Each additive is added by adding the additive to a container or tank capable of stirring after the ionization process in which ionization and water fragmentation are performed as described above, and performing a stirring and mixing operation.
  • stirring and mixing step Next, the stirring and mixing step will be described.
  • the water that has been ionized and charged with the additive as described above is mixed with the oil.
  • the operation is performed as follows. First, only the oil is put into the stirring and mixing tank, and this oil is circulated through the stirring and mixing tank OHR mixer. There, the ionized water with the additive added is added and mixed little by little to fuse. At that time, the pressure to the OHR mixer needs to be 3 atm or more.
  • the temperature of the OHR mixer is set to 15 ° C to 80 ° C.
  • the fusion process will be described.
  • the water and oil after stirring and mixing are fused as described above.
  • the operation is performed as follows. That is, the stirring and mixing step is repeatedly performed on the mixed oil and water while heating (40 ° C. to 80 ° C.) and pressurization (1.5 Pa to 20 Pa) are applied.
  • the water fuel thus obtained will never be separated into water and oil, and will function as a liquid fuel.
  • this work process can also be considered as the ionization process of the present invention, and the negative ion water generated in this way may be mixed with water as a separately prepared raw material.
  • normal water is not energized, but negative ion water can be energized.
  • FIG. 4 is a cross-sectional view schematically showing an example of a production apparatus for carrying out the method for producing atomic carbon according to the present embodiment.
  • This manufacturing apparatus is provided with a pipeline having an airtight chamber 29 that does not contain air, a nitrogen injection on / off valve 22, and a pyrolysis gas discharge on / off valve 23.
  • a heater 24 for raising the temperature to a predetermined temperature is incorporated in the manufacturing apparatus.
  • the cartridge 25 is composed of a carbon extraction cartridge 25 having the same atmosphere (nitrogen atmosphere) as the airtight chamber 29, an organic material, and a table 26.
  • the cartridge 25 can be attached to and detached from the airtight chamber 29.
  • reference numeral 27 denotes an organic material in the hermetic chamber 29 and a shutter provided at the entrance / exit of the base 26. When closed, the hermetic chamber 29 is kept airtight or in a nitrogen atmosphere.
  • Reference numeral 28 denotes a lid or an open / close door provided on the cartridge 25, and when closed, the cartridge 25 is kept airtight or in a nitrogen atmosphere.
  • raw materials organic materials such as wood and bamboo
  • nitrogen is injected from the nitrogen injection opening / closing valve 22, and at the same time, the air inside is discharged from the pyrolysis gas discharge opening / closing valve 23 to make the airtight chamber 29 and the inside of the cartridge 25 have a nitrogen atmosphere and heated by the heater 24.
  • the temperature is kept at 100 ° C. to 150 ° C. (preferably a temperature close to 150 ° C.), the moisture is sufficiently vaporized, and the vaporized moisture is discharged out of the hermetic chamber 29.
  • the airtight chamber 29 is always kept in a state where the organic material as a raw material is not oxidized, that is, an airtight nitrogen atmosphere.
  • the completely dried material is heated using the heater 24, and the temperature is sequentially raised to 350 ° C. to 450 ° C. to thermally decompose the components contained in the material. All raw material components generated up to 450 ° C. must be discharged out of the hermetic chamber, and nitrogen must be injected each time to maintain an inert atmosphere.
  • the component bonded to the carbon in the raw material is liberated leaving the carbon, and the atomic carbon according to the present embodiment that does not vaporize at 450 ° C. remains.
  • the allotrope bond that crystallizes with organic carbon and becomes inorganic that is, the excitation energy for graphitization, requires a high temperature of 450 ° C. or higher. Therefore, the atomic carbon of the present embodiment needs to be 450 ° C. or less at which graphite is not formed.
  • the heater 24 is stopped, low temperature nitrogen is injected from the nitrogen injection opening / closing valve 22, and at the same time, high temperature nitrogen gas is discharged from the pyrolysis gas discharge opening / closing valve 23, so that the airtight chamber 29 and the inside of the cartridge 25 are separated by 50.
  • the atomic carbon is moved together with the base 26 from the airtight chamber 29 to the cartridge 25, the lid 28 of the cartridge 25 is closed, and the inside of the cartridge 25 is kept in a nitrogen atmosphere. It is made to leave from the closed room 29.
  • the airtight chamber 29 is also prepared for the next operation by closing the shutter 27.
  • the remaining carbon consists of ultrafine particles with one carbon atom (that is, a simple substance) or a chain of 2 to 5 to 10 carbon atoms, and these ultrafine particles are irregularly formed by interatomic attractive force. Aggregated amorphous atomic carbon can be obtained. Furthermore, since the atomic carbon exhibits the maximum use capability as a material after completing each step, the cartridge 25 needs to be sealed and stored while maintaining a nitrogen atmosphere that does not oxidize the carbon. Since the atomic carbon stored in the cartridge 25 does not come into contact with air, it does not combine with oxygen or other substances. The atomic carbon that does not combine with oxygen or other substances is pulverized as necessary to form particles or ultrafine particles.
  • the pulverization of the atomic carbon may be performed in any manufacturing process after the atomic carbon is obtained.
  • the atomic carbon may be crushed at 450 ° C. or less in the hermetic chamber 29 in a process before being stored in the cartridge 26 in a sealed state. It can be pulverized to a very fine particle size in an inert atmosphere.
  • the particles may be pulverized to an extremely fine particle size in an airtight chamber 1 in an inert atmosphere.
  • the cartridge 26 may be stored in a sealed state and transported, and pulverized by a pulverizer.
  • the above-mentioned atomic carbon itself is composed of one or several carbon atoms and is atomic and is not combined with oxygen or other substances. (PH is 11 or more).
  • the hydrofuel obtained by mixing the oil and the improved water, once synthesized never separates into water and oil, and is highly transparent and has characteristics that are indistinguishable from ordinary oil. It is useful for effective use of fossil fuels.

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Liquid Carbonaceous Fuels (AREA)

Abstract

[Problème] Fournir un procédé de production de carburant avec ajout d'eau par combinaison d'eau et d'huile de sorte que le carburant avec ajout d'eau ne se sépare pas en eau et en huile à nouveau et présente une transparence élevée. [Solution] La présente invention concerne un procédé de production de carburant avec ajout d'eau par mélange de combustible et d'eau pour générer le carburant avec ajout d'eau qui comprend : une étape d'ionisation de rupture et d'ionisation d'agrégats moléculaires d'eau; une étape de mélange agité d'introduction de l'huile combustible dans une cuve de mélange agité, circulation de l'huile combustible avec un mélangeur tout en mélangeant dans l'eau ionisée dans laquelle un additif est introduit et agitation de celle-ci; et une étape de mélange de soumission répétée de l'huile combustible et de l'eau agitées et mélangées à l'étape de mélange agité à une température de 15 à 80 °C avec application d'une pression d'air de 1,5 à 20 Pa. Par conséquent, grâce à l'étape d'ionisation et l'étape d'introduction d'additif, l'eau est significativement améliorée de sorte que l'affinité avec l'huile combustible soit améliorée et l'huile combustible peut être augmentée.
PCT/JP2016/076724 2016-02-16 2016-09-10 Procédé de production de carburant mixte huile-eau WO2017141471A1 (fr)

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JP2016027448A JP6541230B2 (ja) 2016-02-16 2016-02-16 油水融合燃料の製造方法
JP2016-027448 2016-02-16

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JP6867646B2 (ja) 2017-07-27 2021-05-12 三菱重工業株式会社 補償光学システムおよび補償光学方法
WO2019044042A1 (fr) * 2017-08-28 2019-03-07 杉山　修 Batterie ayant une solution électrolytique contenant de l'eau minérale alcaline ionisée, matériau actif d'électrolyte et procédé de production d'une solution électrolytique de batterie

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4355969A (en) * 1980-05-29 1982-10-26 Fnd Company Electrically charged, emulsified carrier-fuel particle combustion
JP2002018439A (ja) * 1995-08-01 2002-01-22 Matsuo Yoshiaki ビタミンｃ入りアルカリ性電解水
JP2006182890A (ja) * 2004-12-27 2006-07-13 Spg Techno Kk エマルション燃料の生成方法及びその装置または燃料改質装置。
JP2008045022A (ja) * 2006-08-15 2008-02-28 Nobuaki Ando エマルジョン燃料
JP4682287B1 (ja) * 2010-06-11 2011-05-11 佳右 長尾 加水燃料の製造方法及び製造装置
JP2014159538A (ja) * 2013-02-19 2014-09-04 Gtr:Kk 小型化した画期的なエマルジョン燃料装置
WO2015037678A1 (fr) * 2013-09-12 2015-03-19 Hattori Mitsuharu Procédé et dispositif de fabrication d'huile aqueuse transparente compatible
JP2016003297A (ja) * 2014-06-18 2016-01-12 合同会社ネクストエナジー 加水燃料の製造方法及び加水燃料

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4355969A (en) * 1980-05-29 1982-10-26 Fnd Company Electrically charged, emulsified carrier-fuel particle combustion
JP2002018439A (ja) * 1995-08-01 2002-01-22 Matsuo Yoshiaki ビタミンｃ入りアルカリ性電解水
JP2006182890A (ja) * 2004-12-27 2006-07-13 Spg Techno Kk エマルション燃料の生成方法及びその装置または燃料改質装置。
JP2008045022A (ja) * 2006-08-15 2008-02-28 Nobuaki Ando エマルジョン燃料
JP4682287B1 (ja) * 2010-06-11 2011-05-11 佳右 長尾 加水燃料の製造方法及び製造装置
JP2014159538A (ja) * 2013-02-19 2014-09-04 Gtr:Kk 小型化した画期的なエマルジョン燃料装置
WO2015037678A1 (fr) * 2013-09-12 2015-03-19 Hattori Mitsuharu Procédé et dispositif de fabrication d'huile aqueuse transparente compatible
JP2016003297A (ja) * 2014-06-18 2016-01-12 合同会社ネクストエナジー 加水燃料の製造方法及び加水燃料

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JP6541230B2 (ja) 2019-07-10

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