WO2015163589A1 - Cosmetic composition containing mentha haplocalyx as active ingredient - Google Patents

Cosmetic composition containing mentha haplocalyx as active ingredient Download PDF

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WO2015163589A1
WO2015163589A1 PCT/KR2015/002965 KR2015002965W WO2015163589A1 WO 2015163589 A1 WO2015163589 A1 WO 2015163589A1 KR 2015002965 W KR2015002965 W KR 2015002965W WO 2015163589 A1 WO2015163589 A1 WO 2015163589A1
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cosmetic composition
skin
peppermint
formulation example
sebum
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PCT/KR2015/002965
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French (fr)
Korean (ko)
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유지현
김미진
김혜림
채병근
강병영
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주식회사 아모레퍼시픽
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Priority to CN201580021097.7A priority Critical patent/CN106232101B/en
Priority to JP2016563931A priority patent/JP2017513876A/en
Priority to SG11201608845PA priority patent/SG11201608845PA/en
Publication of WO2015163589A1 publication Critical patent/WO2015163589A1/en

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

Definitions

  • the present invention relates to a cosmetic composition containing mint as an active ingredient.
  • the pores are hair growth openings, which are different from the pores, and have a diameter of about 0.02 to 0.05 mm and are known to have about 20,000 dogs on their face only. Through these pores, sebum flows out to the surface of the skin. In puberty, hormones are secreted and the sebaceous glands become larger, so sebum is secreted. In addition, during the period of stress, and warm weather, sebum secretion is active and pores become larger.
  • the present inventors have completed the present invention to discover the pores and sebum clean effect of the skin when used in a cosmetic composition by acetic acid fermented peppermint in order to maximize the efficacy of the mint.
  • the present invention provides a cosmetic composition containing peppermint.
  • the cosmetic composition according to the present invention contains peppermint vinegar fermented using acetic acid bacterium, which is one of the effective organic acids, as an active ingredient, which promotes blood purification, antibacterial, anti-aging and metabolism of the skin, and waste products. Not only does it remove the pores, it also enables the care of the pores. It has excellent astringent effect, which is good for skin with large pores or elasticity, acetic acid fermentation of peppermint which is effective for itching, inflammation and acne, prevents pores from widening. It works.
  • Figure 1 shows the pore size change according to the application of Formulation Example 1 to the skin of the test subject according to Test Example 1, a photograph before the application of Formulation Example 1 to the skin of the test subject.
  • Figure 2 shows the pore size change according to the application of Formulation Example 1 to the test subject's skin according to Test Example 1, it is a photograph after applying Formulation Example 1 to the test subject's skin.
  • Figure 3 shows the pore size change according to the application of Comparative Formulation Example 1 to the skin of the test subject according to Test Example 1, a photograph before applying Comparative Formulation Example 1 to the skin of the test subject.
  • Figure 4 shows a change in pore size according to the comparative formulation example 1 applied to the skin of the test subject according to Test Example 1, a photograph after applying the comparative formulation example 1 to the skin of the test subject.
  • Figure 5 shows the pore size change according to the application of Comparative Formulation Example 2 to the test subject's skin according to Test Example 1, a photograph before applying Comparative Formulation Example 2 to the test subject's skin.
  • Figure 6 shows the pore size change according to the application of Comparative Formulation Example 2 to the test subject's skin according to Test Example 1, a photograph after applying Comparative Formulation Example 2 to the test subject's skin.
  • Figure 7 shows the change in the number of sebum according to the application of Formulation Example 1 to the test subject's skin according to Test Example 1, it is a photograph before the application of Formulation Example 1 to the subject's skin.
  • Figure 8 shows the change in the number of sebum according to the application of Formulation Example 1 to the test subject's skin according to Test Example 1, it is a photograph after the application of Formulation Example 1 to the skin.
  • FIG. 9 shows a change in the number of sebum according to the application of Comparative Formulation Example 1 to the test subject's skin according to Test Example 1, and is a photograph before application of Comparative Formulation Example 1 to the test subject's skin.
  • FIG. 10 shows a change in the number of sebum according to the application of Comparative Formulation Example 1 to the test subject's skin according to Test Example 1, and is a photograph after applying Comparative Formulation Example 1 to the test subject's skin.
  • FIG. 11 is a photograph showing the change in the number of sebum according to the application of Comparative Formulation Example 2 to the test subject's skin according to Test Example 1, before applying Comparative Formulation Example 2 to the test subject's skin.
  • Mint Mentha piperita
  • the essential oil content of peppermint is 2% to 3%, 4% to 6% in petals and 0.3% in stems.
  • the essential ingredient of this peppermint essential oil is 70% to 90% as menthol.
  • Physiological ingredients such as I-menthol, isomentone, pinene, campene and limonene are known to help various skin activation and skin health.
  • vitamin C, carotene, phytol, and betaine help to relieve skin fatigue and maintain healthy and bright skin.
  • the peppermint is acetic acid fermented peppermint.
  • Acetic acid fermentation is the alcohol is oxidized by the action of chosangyun to aerobic fermentation to generate the acid, chosangyun (Acetobacter aceti ) oxidizes ethanol to produce acetic acid.
  • Acetic acid fermentation can be from about 12 hours to 48 hours in logarithmic season, and the amount of acid production increases sharply in 12-24 hours.
  • the culture temperature of acetic acid fermentation is 30 ° C., ethanol 4% added medium, pH 6.5 to 7, the ability to produce acetic acid and sugar is most stable.
  • Vinegar contains more than 60 organic acids, such as acetic acid, citric acid, amino acids, succinic acid, and serves as an accelerator to help the body absorb various nutrients such as vitamins and minerals.
  • organic acids such as acetic acid, citric acid, amino acids, succinic acid
  • Vinegar acts as a blood purifier that cleans our flesh and blood, promotes the metabolism of the human body to increase the natural healing power to the maximum, inhibits blemishes and freckles, inhibits lipid peroxide, which is the main culprit of skin aging, and metabolism of cells. It helps actively metabolize. In addition, it breaks down the lactic acid in the skin and muscles, so that the blood flows smoothly.
  • Acetic acid is superior to other organic acids in blood purification, antibacterial, anti-aging and metabolism.
  • the peppermint vinegar is prepared by a culture method for propagating microorganisms on the surface of the liquid.
  • the peppermint vinegar prepared by the culture method has a characteristic that the membrane of the microorganism is always in contact with the air so that the dissolved oxygen dissolved on the liquid surface can be used well, and can be obtained through the fermentation of acetic acid as well as the efficacy of the components of the existing mint. It also has advantages.
  • the mint is an extract of any one or combination of leaves and stems of mint.
  • Peppermint leaves and stems have excellent antiseptic and antiparasitic effects and prevent bad breath and are used in toothpaste. Grind the leaves and use them as a poultice to help treat inflammation and bruises on the skin, as well as for dermatitis and itching. It calms irritated skin due to large and small wounds, reduces itching and adverse reactions, and helps to maintain light convergence and elasticity while giving vitality and stress relief to the skin. Peppermint leaves contain 2% to 3% essential oil, and peppermint stems contain less than 1% essential oil. Mentholic acid, which accounts for about 70% of essential oils, is the odor and medicinal ingredient peculiar to peppermint.
  • Peppermint's unique fragrance can be obtained from menthol and mentons, and menthol has a converging property, which pulls down sagging skin and constricts pores, giving skin good effects. It also constricts the mucous membranes and blood vessels of the skin, giving a refreshing feeling to the localized areas.
  • Menthol which has a peculiar refreshing odor, is a colorless needle crystal. It is almost insoluble in water, but soluble in ethanol and chloroform. Obtained through the leaves or stems of peppermint, put a large amount in your mouth feels like sticking the tongue, but in a small amount feels refreshing.
  • the cosmetic composition contains alpha hydroxy acid (AHA: ⁇ -Hydroxy Acid).
  • Alpha hydroxy acid is a compound in which alcohol group or alcohol group is added to carbon at ⁇ position of carboxylic acid.
  • Carbocylic acid lowers ion binding energy of keratinocytes to remove keratinocytes or form new cells. It promotes the skin cell activity by shortening the cycle of keratinization process that becomes longer as the skin ages, thereby improving the skin. In addition, it promotes the production of collagen and elastin by Fibroblast to make the skin elastic, soft and promote the production of mucopolysaccharide (Mucopolysaccharide), an important extracellular matrix component of the dermis.
  • AHA alpha hydroxy acid
  • Alpha hydroxy acid is a compound in which alcohol group or alcohol group is added to carbon at ⁇ position of carboxylic acid.
  • Carbocylic acid lowers ion binding energy of keratinocytes to remove keratinocytes
  • the content of the peppermint is 0.001% to 20% by weight based on the total weight of the cosmetic composition. If the peppermint herb is less than 0.001% by weight, it is impossible to expect a sufficient effect of the present invention, and if it exceeds 20% by weight, a temporary irritation may be caused by the menthol component contained in the peppermint herb.
  • the cosmetic composition is for shrinking pores.
  • Peppermint acetic acid fermented peppermint maximizing the efficacy of peppermint with excellent astringent effect prevents the pores widening and has the contraction effect that makes use of the increased pore elasticity.
  • the cosmetic composition is for sebum control.
  • Peppermint is fermented peppermint acetic acid is effective in promoting skin purification, antibacterial, anti-aging, metabolism of the skin, as well as removing waste, and also manage the pores.
  • the cosmetic composition according to the present invention is not particularly limited in its formulation, and may be, for example, formulated with softening cream, nutrient cream, essence, massage cream, nourishing cream, pack, gel or skin adhesive cosmetic.
  • test examples and formulation examples are provided only for the purpose of illustration to help the understanding of the present invention is not limited to the scope and scope of the present invention by the following examples.
  • peppermint extract was prepared. This extract is 100 g of peppermint ingredients (75-80% by weight of mint leaves, 20-25% by weight of stem) and 100 mL of extraction solution (70% -95% of purified water, 5%-butylene glycol based on the total volume of the solution). 30%) was added and extracted at room temperature to prepare 100 mL of peppermint extract.
  • the cosmetic composition containing peppermint vinegar as an active ingredient was prepared by the following method.
  • the cosmetic composition containing peppermint herb as an active ingredient the cosmetic composition of Comparative Formulation Example 1 having the composition of Table 1 was prepared by the following method. (Unit: weight%)
  • Comparative Formulation Example 1 was prepared by putting a soluble image in a transparent aqueous solution dissolved at room temperature and dissolving it uniformly, and then adding a peppermint extract without adding peppermint herb.
  • Comparative Formulation Example 2 was prepared by putting a soluble image in a transparent aqueous solution dissolved at room temperature and dissolving it uniformly, without adding mint and peppermint extract, respectively.
  • Comparative Formulation Example 2 was measured in women in their 20s to 30s.
  • Formulation Example 1, Comparative Formulation Example 1 and Comparative Formulation Example 2 were given to each group, and then evenly applied to the entire face, and the pore reduction effect and sebum control efficacy were evaluated.
  • the pore size, sebum size and number of skin samples of this test sample were measured using the skin touch measuring device developed by AMOREPACIFIC. Skin Touch measures the skin's oil, moisture and elasticity by the integrated sensor, and the measured result is displayed on the external LCD display window. Before using the sample, after 1 week, 2 weeks after the use of the sample by measuring the test site using the skin touch, the pore size, sebum size and number at the time of skin application of the sample was evaluated.

Abstract

The present invention relates to a cosmetic composition containing Mentha haplocalyx as an active ingredient.

Description

박하초를 유효성분으로 함유하는 화장료 조성물Cosmetic composition containing peppermint vinegar as an active ingredient
본 발명은 박하초를 유효성분으로 함유하는 화장료 조성물에 관한 것이다.The present invention relates to a cosmetic composition containing mint as an active ingredient.
본 출원은 2014년 4월 24일에 한국 특허청에 제출된 한국 특허출원 제10-2014-0049216호의 출원일의 이익을 주장하며, 그 내용 전부는 본 명세서에 포함된다.This application claims the benefit of the filing date of Korean Patent Application No. 10-2014-0049216 filed with the Korean Intellectual Property Office on April 24, 2014, the entire contents of which are incorporated herein.
모공은 털이 자라나는 입구로, 땀구멍과는 다르며, 지름은 0.02~0.05㎜ 정도이고, 얼굴에만 약 2만여 개가 있다고 알려져있다. 이 모공을 통해 피지가 피부 표면으로 흘러나온다. 사춘기가 되면 호르몬이 많이 분비되면서 피지선이 커져 피지가 많이 분비되기 때문에 피지 분비 통로인 모공이 커지게 된다. 또 중이거나, 스트레스를 받을 때, 그리고 날씨가 따뜻할 때에도 피지 분비가 활발해져 모공이 커진다.The pores are hair growth openings, which are different from the pores, and have a diameter of about 0.02 to 0.05 mm and are known to have about 20,000 dogs on their face only. Through these pores, sebum flows out to the surface of the skin. In puberty, hormones are secreted and the sebaceous glands become larger, so sebum is secreted. In addition, during the period of stress, and warm weather, sebum secretion is active and pores become larger.
20대 후반이 되면 피부 노화가 시작되면서 모공벽을 지지하고 있던 콜라겐, 엘라스틴 등이 분해되거나 변질되므로 피부의 탄력이 떨어지고 건조하여 피부가 늘어지면서 모공이 쳐지거나 늘어난다. 모공이 커지면 노폐물과 세균이 잘 침투하게 되어 여드름 등 여러 피부병을 일으킬 수 있다.In the late twenties, as skin aging begins, collagen and elastin, which supported the pores wall, are decomposed or deteriorated. Larger pores will allow the waste and bacteria to penetrate well, causing acne and other skin diseases.
화장품 원료들은 대부분 효능이 미진하거나 피부 자극 같은 부작용을 유발하는 등 여러 가지 문제점을 가지고 있었다. 이에, 피부 부작용을 유발하지 않으면서도 피부 재생 증진 효과를 갖는 원료에 대한 연구가 활발히 진행되고 있다. 특히 최근에는 미생물을 이용한 발효 기술이 발전되면서 식물이나 기타 천연 원료로부터 유래되는 물질을 발효 기술을 통해서 얻어낸 2차 대사산물을 생리 활성 물질로 이용하는 경우가 많이 늘어나고 있다. 이 성분들은 다양한 생리활성을 갖는 것으로 알려지고 있어 고기능성 화장품의 신원료로 주목을 받고 있다. 이 기술을 이용하면 천연에 존재하는 물질이지만 그 양이 매우 적거나 피부에 적용하기는 어려웠던 고기능성 활성물질을 경제적으로 생산할 수 있다는 점에서 지금까지 사용하지 못했던 신성분들을 개발하고 응용할 수 있게 될 것으로 기대되고 있다. 특히 기능성 화장품에 대한 고객들의 요구가 증대하는 것만큼 신기능성 소재나 관련 기술의 발전이 충분하지 못했다는 점에서 무수히 많은 신 기능성 성분들을 만들어낼 수 있는 발효 기술을 이용한 화장품은 다양한 피부 효능, 특히 항노화 효능 부분에서 큰 인기를 끌게 될 것이다.Most cosmetic raw materials have various problems such as poor efficacy or causing side effects such as skin irritation. Accordingly, research on raw materials having a skin regeneration-promoting effect without causing side effects of the skin is being actively conducted. In particular, with the development of fermentation technology using microorganisms, the use of secondary metabolites obtained through fermentation technology from materials derived from plants and other natural raw materials is increasing. These ingredients are known to have various physiological activities, attracting attention as a new raw material of high functional cosmetics. Using this technology, it is possible to develop and apply new ingredients that have not been used so far in the economical production of highly functional active substances that are present in nature but are very small or difficult to apply to the skin. It is expected. In particular, since the development of new functional materials and related technologies has not been enough as the demand of functional cosmetics increases, cosmetics using fermentation technology that can produce a myriad of new functional ingredients have various skin effects, especially It will be very popular in terms of aging effects.
부 활성화와 피부 건강에 도움을 주는 박하의 효능을 극대화하여, 노폐물을 제거해줄 뿐만 아니라 모공의 관리도 가능하게 하는 화장료 조성물을 제공하고자 한다.By maximizing the efficacy of peppermint to help inactivation and skin health, to provide a cosmetic composition that not only removes waste, but also manages the pores.
이에, 본 발명자들은 박하의 효능을 극대화시키기 위하여, 박하를 초산 발효하여 화장료 조성물에 사용할 경우 피부의 모공과 피지 청정 효과를 발견하고 본 발명을 완성하게 되었다.Thus, the present inventors have completed the present invention to discover the pores and sebum clean effect of the skin when used in a cosmetic composition by acetic acid fermented peppermint in order to maximize the efficacy of the mint.
상기한 목적을 달성하기 위하여, 본 발명은 박하초를 함유하는 화장료 조성물을 제공한다.In order to achieve the above object, the present invention provides a cosmetic composition containing peppermint.
본 발명에 따른 화장물 조성물은 박하를 유효한 유기산 중 하나인 초산균을 사용하여 발효한 박하초를 유효성분으로 함유하여 피부의 혈액정화, 항균, 노화방지, 신진대사를 촉진하여 주는 효과가 있는 동시에 노폐물을 제거해줄 뿐만 아니라 모공의 관리도 가능하게 한다. 수렴작용이 뛰어나 모공이 크거나 탄력이 떨어진 피부에 좋고 가려움과 염증, 여드름에도 효과적인 성분인 박하를 초산 발효하여 모공이 넓어지는 것을 예방해주며, 늘어난 모공의 탄력을 살려주는 수축 효과가 있으며 소독 및 진정효과가 있다.The cosmetic composition according to the present invention contains peppermint vinegar fermented using acetic acid bacterium, which is one of the effective organic acids, as an active ingredient, which promotes blood purification, antibacterial, anti-aging and metabolism of the skin, and waste products. Not only does it remove the pores, it also enables the care of the pores. It has excellent astringent effect, which is good for skin with large pores or elasticity, acetic acid fermentation of peppermint which is effective for itching, inflammation and acne, prevents pores from widening. It works.
도 1은 시험예 1에 따라 제형예 1을 피시험자의 피부에 도포함에 따른 모공 크기 변화를 나타낸 것으로, 피시험자의 피부에 제형예 1을 도포하기 전의 사진이다.Figure 1 shows the pore size change according to the application of Formulation Example 1 to the skin of the test subject according to Test Example 1, a photograph before the application of Formulation Example 1 to the skin of the test subject.
도 2는 시험예 1에 따라 제형예 1을 피시험자의 피부에 도포함에 따른 모공 크기 변화를 나타낸 것으로, 피시험자의 피부에 제형예 1을 도포한 후의 사진이다.Figure 2 shows the pore size change according to the application of Formulation Example 1 to the test subject's skin according to Test Example 1, it is a photograph after applying Formulation Example 1 to the test subject's skin.
도 3은 시험예 1에 따라 비교 제형예 1을 피시험자의 피부에 도포함에 따른 모공 크기 변화를 나타낸 것으로, 피시험자의 피부에 비교 제형예 1을 도포하기 전의 사진이다.Figure 3 shows the pore size change according to the application of Comparative Formulation Example 1 to the skin of the test subject according to Test Example 1, a photograph before applying Comparative Formulation Example 1 to the skin of the test subject.
도 4는 시험예 1에 따라 비교 제형예 1을 피시험자의 피부에 도포함에 따른 모공 크기 변화를 나타낸 것으로, 피시험자의 피부에 비교 제형예 1을 도포한 후의 사진이다.Figure 4 shows a change in pore size according to the comparative formulation example 1 applied to the skin of the test subject according to Test Example 1, a photograph after applying the comparative formulation example 1 to the skin of the test subject.
도 5는 시험예 1에 따라 비교 제형예 2를 피시험자의 피부에 도포함에 따른 모공 크기 변화를 나타낸 것으로, 피시험자의 피부에 비교 제형예 2를 도포하기 전의 사진이다.Figure 5 shows the pore size change according to the application of Comparative Formulation Example 2 to the test subject's skin according to Test Example 1, a photograph before applying Comparative Formulation Example 2 to the test subject's skin.
도 6은 시험예 1에 따라 비교 제형예 2를 피시험자의 피부에 도포함에 따른 모공 크기 변화를 나타낸 것으로, 피시험자의 피부에 비교 제형예 2를 도포한 후의 사진이다.Figure 6 shows the pore size change according to the application of Comparative Formulation Example 2 to the test subject's skin according to Test Example 1, a photograph after applying Comparative Formulation Example 2 to the test subject's skin.
도 7은 시험예 1에 따라 제형예 1을 피시험자의 피부에 도포함에 따른 피지 개수 변화를 나타낸 것으로, 피시험자의 피부에 제형예 1을 도포하기 전의 사진이다.Figure 7 shows the change in the number of sebum according to the application of Formulation Example 1 to the test subject's skin according to Test Example 1, it is a photograph before the application of Formulation Example 1 to the subject's skin.
도 8은 시험예 1에 따라 제형예 1을 피시험자의 피부에 도포함에 따른 피지 개수 변화를 나타낸 것으로, 피부에 제형예 1을 도포한 후의 사진이다.Figure 8 shows the change in the number of sebum according to the application of Formulation Example 1 to the test subject's skin according to Test Example 1, it is a photograph after the application of Formulation Example 1 to the skin.
도 9는 시험예 1에 따라 비교 제형예 1을 피시험자의 피부에 도포함에 따른 피지 개수 변화를 나타낸 것으로, 피시험자의 피부에 비교 제형예 1을 도포하기 전의 사진이다.FIG. 9 shows a change in the number of sebum according to the application of Comparative Formulation Example 1 to the test subject's skin according to Test Example 1, and is a photograph before application of Comparative Formulation Example 1 to the test subject's skin.
도 10은 시험예 1에 따라 비교 제형예 1을 피시험자의 피부에 도포함에 따른 피지 개수 변화를 나타낸 것으로, 피시험자의 피부에 비교 제형예 1을 도포한 후의 사진이다.FIG. 10 shows a change in the number of sebum according to the application of Comparative Formulation Example 1 to the test subject's skin according to Test Example 1, and is a photograph after applying Comparative Formulation Example 1 to the test subject's skin.
도 11은 시험예 1에 따라 비교 제형예 2를 피시험자의 피부에 도포함에 따른 피지 개수 변화를 나타낸 것으로, 피시험자의 피부에 비교 제형예 2를 도포하기 전의 사진이다.FIG. 11 is a photograph showing the change in the number of sebum according to the application of Comparative Formulation Example 2 to the test subject's skin according to Test Example 1, before applying Comparative Formulation Example 2 to the test subject's skin.
도 12는 시험예 1에 따라 비교 제형예 2를 피시험자의 피부에 도포함에 따른 피지 개수 변화를 나타낸 것으로, 피시험자의 피부에 비교 제형예 1을 도포한 후의 사진이다.12 is a photograph showing the change in the number of sebum according to the application of Comparative Formulation Example 2 to the test subject's skin according to Test Example 1, after applying Comparative Formulation Example 1 to the test subject's skin.
박하 (Mentha piperita)는 꿀 풀과의 다년생 초본으로써 동서양을 막론하고 오랫동안 식용과 약용으로 사용되어온 천연 식물로서, 다양한 약리작용 못지않게 피부 건강에 도움을 주는 다양한 효과들이 있다고 알려져 있다. 박하의 주요 성분들 중 정유의 함량은 2% 내지 3%, 꽃잎에서 4% 내지 6%, 줄기에서 0.3%로 높은 정유 함량을 보여주는데 이러한 박하 정유의 주요 성분으로 70% 내지 90%는 멘톨로서, I-멘톨, 이소멘톤, 피넨, 캄펜, 리모넨 등의 생리 성분들이 다양한 피부 활성화와 피부 건강에 도움을 준다고 알려져 있다. 그 밖에도 비타민C, 카로틴, 피톨, 베타인 등이 피부의 피로감을 해소화고 건강하고 밝은 피부를 유지하게 도와준다.Mint ( Mentha piperita ) is a perennial herb with honey grass. It is a natural plant that has been used for a long time in food and medicinal use both east and west, and is known to have various effects that help skin health as well as various pharmacological actions. The essential oil content of peppermint is 2% to 3%, 4% to 6% in petals and 0.3% in stems. The essential ingredient of this peppermint essential oil is 70% to 90% as menthol. Physiological ingredients such as I-menthol, isomentone, pinene, campene and limonene are known to help various skin activation and skin health. In addition, vitamin C, carotene, phytol, and betaine help to relieve skin fatigue and maintain healthy and bright skin.
본 발명의 일 실시상태에 있어서, 상기 박하초는 박하를 초산 발효한 것이다. 초산 발효는 초산균의 작용으로 알코올이 산화되어 초산을 생성하는 호기적 발효로, 초산균 ( Acetobacter aceti)은 에탄올을 산화하여 초산 (Acetic acid)을 생성한다. 초산 발효는 대수기는 약 12 시간 내지 48 시간 일 수 있으며, 산 생성량은 12~24시간에 급격히 증가한다. 초산 발효의 배양 온도는 30°C, 에탄올 4% 첨가된 배지, pH 6.5 내지 7인 경우, 초산 생성능과 당분해능이 가장 안정적이다.In one embodiment of the present invention, the peppermint is acetic acid fermented peppermint. Acetic acid fermentation is the alcohol is oxidized by the action of chosangyun to aerobic fermentation to generate the acid, chosangyun (Acetobacter aceti ) oxidizes ethanol to produce acetic acid. Acetic acid fermentation can be from about 12 hours to 48 hours in logarithmic season, and the amount of acid production increases sharply in 12-24 hours. The culture temperature of acetic acid fermentation is 30 ° C., ethanol 4% added medium, pH 6.5 to 7, the ability to produce acetic acid and sugar is most stable.
식초는 초산, 구연산, 아미노산, 호박산 등 60여 종 이상의 유기산을 포함하고 있으며, 비타민과 무기질 등 각종 영양소의 체내 흡수를 도와주는 촉진제 역할을 한다. 특히 우리의 살과 피를 깨끗이 하는 혈액 정화제 역할을 하며 인체의 신진대사를 촉진하여 자연 치유력을 최고도로 높여주는 효과가 있고 기미 및 주근깨를 억제하고 피부 노화의 주범인 과산화지질을 억제시키며 세포의 신진대사를 활발하게 도와준다. 이뿐 아니라, 피부와 근육의 젖산을 분해해 혈액의 흐름이 원활하도록 작용한다.Vinegar contains more than 60 organic acids, such as acetic acid, citric acid, amino acids, succinic acid, and serves as an accelerator to help the body absorb various nutrients such as vitamins and minerals. In particular, it acts as a blood purifier that cleans our flesh and blood, promotes the metabolism of the human body to increase the natural healing power to the maximum, inhibits blemishes and freckles, inhibits lipid peroxide, which is the main culprit of skin aging, and metabolism of cells. It helps actively metabolize. In addition, it breaks down the lactic acid in the skin and muscles, so that the blood flows smoothly.
초산은 다른 유기산들에 비해 혈액정화, 항균, 노화방지, 신진대사촉진 능력이 뛰어나다.Acetic acid is superior to other organic acids in blood purification, antibacterial, anti-aging and metabolism.
본 발명의 일 실시상태에 있어서, 상기 박하초는 액체의 표면에서 미생물을 번식시키는 배양법으로 제조된 것이다.In one embodiment of the present invention, the peppermint vinegar is prepared by a culture method for propagating microorganisms on the surface of the liquid.
상기 배양법으로 제조된 박하초는 미생물의 막이 항상 공기와 접촉되어 있어 액체 표면에서 용해된 용존 산소를 잘 이용할 수 있는 특징을 가지며 기존 박하가 가지고 있는 성분으로 인한 효능뿐만 아니라 초산발효를 통해 얻을 수 있는 장점 또한 갖는다.The peppermint vinegar prepared by the culture method has a characteristic that the membrane of the microorganism is always in contact with the air so that the dissolved oxygen dissolved on the liquid surface can be used well, and can be obtained through the fermentation of acetic acid as well as the efficacy of the components of the existing mint. It also has advantages.
본 발명의 일 실시상태에 있어서, 상기 박하는 박하의 잎 및 줄기 중 어느 하나 또는 이들의 조합의 추출물이다. In one embodiment of the present invention, the mint is an extract of any one or combination of leaves and stems of mint.
박하 잎과 줄기는 살균, 구충 효과가 뛰어나고 구취를 방지하여 치약에 쓰인다. 잎을 갈아 습포제로 쓰면 피부의 염증, 타박상 치료에 효과가 있고 피부염, 가려움증에도 좋다. 크고 작은 상처로 인해 자극받은 피부를 진정시키는 한편 가려움 및 이상반응을 줄여주고 피부에 활력과 스트레스 해소를 부여하면서 가벼운 수렴작용 및 탄력 유지에 도움을 준다. 박하의 잎에는 2% 내지 3%의 정유를 함유하고 있으며, 박하의 줄기에는 1% 이내의 정유를 함유하고 있다. 정유의 약 70%를 차지하고 있는 멘톨산은 박하 특유의 냄새와 약효를 내는 성분이다. 박하 고유의 향은 멘톨과 멘톤으로부터 얻을 수 있으며, 멘톨의 경우 수렴하는 성질이 있어 늘어진 피부를 당겨주고 모공을 수축시켜주는 효과가 있어 피부에 좋은 효능을 부여한다. 또한 피부의 점막과 혈관을 수축시켜 국소부위에 청량감을 준다. 독특한 상쾌감이 있는 냄새가 나는 멘톨은 무색의 침상결정으로, 물에는 거의 녹지 않으나, 에탄올, 클로로포름에는 잘 녹는다. 박하의 잎이나 줄기를 통해 얻으며 많은 양을 입에 넣으면 혀를 찌르는 듯한 느낌이 있지만, 소량일 때에는 청량감이 난다.Peppermint leaves and stems have excellent antiseptic and antiparasitic effects and prevent bad breath and are used in toothpaste. Grind the leaves and use them as a poultice to help treat inflammation and bruises on the skin, as well as for dermatitis and itching. It calms irritated skin due to large and small wounds, reduces itching and adverse reactions, and helps to maintain light convergence and elasticity while giving vitality and stress relief to the skin. Peppermint leaves contain 2% to 3% essential oil, and peppermint stems contain less than 1% essential oil. Mentholic acid, which accounts for about 70% of essential oils, is the odor and medicinal ingredient peculiar to peppermint. Peppermint's unique fragrance can be obtained from menthol and mentons, and menthol has a converging property, which pulls down sagging skin and constricts pores, giving skin good effects. It also constricts the mucous membranes and blood vessels of the skin, giving a refreshing feeling to the localized areas. Menthol, which has a peculiar refreshing odor, is a colorless needle crystal. It is almost insoluble in water, but soluble in ethanol and chloroform. Obtained through the leaves or stems of peppermint, put a large amount in your mouth feels like sticking the tongue, but in a small amount feels refreshing.
본 발명의 일 실시상태에 있어서, 상기 화장료 조성물은 알파히드록시산 (AHA: α-Hydroxy Acid)을 함유한다. 알파히드록시산은 카르복시산 (Carboxylic acid)의 α 위치에 있는 탄소에 알코올기 (Alcohol group) 또는 히드록시기 (Hydroxy group)를 첨가한 화합물로 각질 세포의 이온결합 에너지를 낮추어 과각질을 제거하거나 새로운 세포의 형성을 촉진하여 피부가 노화되면서 길어지는 각질화 과정의 주기를 짧게 하여 피부세포의 활성을 촉진시켜 피부를 개선하여 준다. 또한, 섬유아세포 (Fibroblast)에 의한 콜라겐과 엘라스틴의 생성을 촉진하여 피부를 탄력 있고, 부드럽게 하고 진피의 중요한 세포 외 기질 성분인 뮤코폴리사카라이드 (Mucopolysaccharide)의 생성을 촉진하여 피부보습을 증진시킨다.In one embodiment of the present invention, the cosmetic composition contains alpha hydroxy acid (AHA: α-Hydroxy Acid). Alpha hydroxy acid is a compound in which alcohol group or alcohol group is added to carbon at α position of carboxylic acid. Carbocylic acid lowers ion binding energy of keratinocytes to remove keratinocytes or form new cells. It promotes the skin cell activity by shortening the cycle of keratinization process that becomes longer as the skin ages, thereby improving the skin. In addition, it promotes the production of collagen and elastin by Fibroblast to make the skin elastic, soft and promote the production of mucopolysaccharide (Mucopolysaccharide), an important extracellular matrix component of the dermis.
본 발명의 일 실시상태에 있어서, 상기 박하초의 함량은 상기 화장료 조성물 전체 중량에 대하여, 0.001 중량% 내지 20 중량%이다. 상기 박하초가 0.001 중량% 미만인 경우에는 본 발명이 목적하고자 하는 충분한 효과를 기대할 수 없고, 20 중량%를 초과하는 경우에서는 박하초에 함유된 멘톨 성분에 의해 일시적인 자극감이 나타날 수 있다.In one embodiment of the present invention, the content of the peppermint is 0.001% to 20% by weight based on the total weight of the cosmetic composition. If the peppermint herb is less than 0.001% by weight, it is impossible to expect a sufficient effect of the present invention, and if it exceeds 20% by weight, a temporary irritation may be caused by the menthol component contained in the peppermint herb.
본 발명의 일 실시상태에 있어서, 상기 화장용 조성물은 모공 축소용이다. 박하가 초산 발효된 박하초는 수렴작용이 뛰어난 박하의 효능이 극대화되어 모공이 넓어지는 것을 예방해주며 늘어난 모공의 탄력을 살려주는 수축 효과가 있다.In one embodiment of the present invention, the cosmetic composition is for shrinking pores. Peppermint acetic acid fermented peppermint maximizing the efficacy of peppermint with excellent astringent effect prevents the pores widening and has the contraction effect that makes use of the increased pore elasticity.
본 발명의 일 실시상태에 있어서, 상기 화장용 조성물은 피지 조절용이다. 박하가 초산 발효된 박하초는 피부의 혈액정화, 항균, 노화방지, 신진대사를 촉진하여 주는 효과가 있는 동시에 노폐물을 제거해줄 뿐만 아니라, 모공의 관리도 가능하게 한다.In one embodiment of the present invention, the cosmetic composition is for sebum control. Peppermint is fermented peppermint acetic acid is effective in promoting skin purification, antibacterial, anti-aging, metabolism of the skin, as well as removing waste, and also manage the pores.
본 발명에 의한 화장료 조성물은 그 제형에 있어 특별히 한정되는 바가 없으며, 예를 들면 유연화장수, 영양화장수, 에센스, 마사지크림, 영양크림, 팩, 젤 또는 피부 점착타입 화장료의 제형화 될 수 있다.The cosmetic composition according to the present invention is not particularly limited in its formulation, and may be, for example, formulated with softening cream, nutrient cream, essence, massage cream, nourishing cream, pack, gel or skin adhesive cosmetic.
이하, 시험예 및 제형예를 들어 본 발명의 구성 및 효과를 보다 구체적으로 설명한다. 그러나 이들 시험예 및 제형예는 본 발명에 대한 이해를 돕기 위해 예시의 목적으로만 제공된 것일 뿐 본 발명의 범주 및 범위가 하기 예에 의해 제한되는 것은 아니다.Hereinafter, the configuration and effects of the present invention will be described in more detail with reference to test examples and formulation examples. However, these test examples and formulation examples are provided only for the purpose of illustration to help the understanding of the present invention is not limited to the scope and scope of the present invention by the following examples.
<제조예><Production example>
초산균 (Merk사, 균주명: Acetobacter aceti KCTC 1010) 2~3g를 배지 (Mannitol Agar/YPM/Medium)에 미리 준비한 박하 재료 100 g (박하 잎 75~80중량%, 줄기 20~25중량%)을 첨가하고 접종한 후, 48시간 동안, 약 26℃ 온도에서 발효를 시킨 다음, 얻어진 발효물에 추출 용액 (정제수 20mL와 에탄올 50mL의 혼합액)을 첨가하여 상온 (25℃)에서 1시간동안 추출하였다. 1차 여과 (울트라 필터레이션 (pore size=50㎛))로 에탄올 및 재료를 제거한 후, 순수한 발효 상등액만을 취하였다. 상등액을 다시 원심분리 (초고속 원심분리기, 400rpm)와 2차 여과 (울트라 필터레이션 (pore size=10㎛))를 진행한 후 얻어진 여액에, 멸균 용액 100 mL (용액 전체의 부피를 기준으로 정제수 70%~94%, 부틸렌글라이콜 5%~10%, 디소듐이디티에이 0.01%~0.05% 및 방부제 (페녹시에탄올) 0.4%~1.0%)을 혼합하고 120℃에서 10~15분 가량 멸균공정을 거쳐 최종적으로 박하초 100mL를 제조하였다.Acetic acid bacteria (Merk company, strain name: Acetobacter aceti KCTC 1010) 2 g to 3 g of medium (Mannitol Agar / YPM / Medium) 100 g (mint leaf 75-80% by weight, 20-25% by weight of peppermint) prepared in advance and inoculated for 48 hours, After fermentation at a temperature of about 26 ℃, an extract solution (mixture of 20 mL of purified water and 50 mL of ethanol) was added to the obtained fermentation and extracted for 1 hour at room temperature (25 ℃). After ethanol and material were removed by primary filtration (ultra filtration (pore size = 50 μm)), only pure fermentation supernatant was taken. The supernatant was again centrifuged (ultrafast centrifuge, 400 rpm) and secondary filtration (ultra filtration (pore size = 10 μm)) to the filtrate obtained, 100 mL of sterile solution (purified water 70 based on the total volume of the solution). % To 94%, butylene glycol 5% to 10%, disodium idieti 0.01% to 0.05% and preservative (phenoxyethanol) 0.4% to 1.0%), and sterilized for 10-15 minutes at 120 ℃ 100 mL of peppermint vinegar was finally prepared through the process.
한편, 박하초의 효능과 대비하기 위하여, 박하 추출물을 제조하였다. 이 추출물은 박하 재료 100 g (박하 잎 75~80중량%, 줄기 20~25 중량%)에 추출 용액 100 mL (용액 전체의 부피를 기준으로 정제수 70%~95%, 부틸렌글라이콜 5%~30%)을 첨가하여 상온에서 추출하여, 박하 추출물 100mL를 제조하였다.On the other hand, in order to contrast with the efficacy of peppermint, peppermint extract was prepared. This extract is 100 g of peppermint ingredients (75-80% by weight of mint leaves, 20-25% by weight of stem) and 100 mL of extraction solution (70% -95% of purified water, 5%-butylene glycol based on the total volume of the solution). 30%) was added and extracted at room temperature to prepare 100 mL of peppermint extract.
<< 실시예Example 및  And 비교예Comparative example >>
박하초를 유효성분으로 함유하는 화장료 조성물을 하기 표 1의 조성을 갖는 제형예 1의 화장료 조성물을 하기 방법으로 제조하였다. 또한, 본 발명의 범위의 제형예 1과 비교하기 위하여, 박하초를 유효성분으로 함유하는 화장료 조성물을 하기 표 1의 조성을 갖는 비교 제형예 1의 화장료 조성물을 하기 방법으로 제조하였다. (단위: 중량%)The cosmetic composition containing peppermint vinegar as an active ingredient, the cosmetic composition of Formulation Example 1 having the composition of Table 1 was prepared by the following method. In addition, in order to compare it with the formulation example 1 of the scope of the present invention, the cosmetic composition containing peppermint herb as an active ingredient, the cosmetic composition of Comparative Formulation Example 1 having the composition of Table 1 was prepared by the following method. (Unit: weight%)
표 1
성분 제형예 1 비교 제형예 1 비교 제형예 2
수상 정제수 잔량 잔량 잔량
부틸렌글라이콜 3.0 3.0 3.0
베타인 1.5 1.5 1.5
카보머 0.2 0.2 0.2
베타글루칸 5.0 5.0 5.0
가용화상 에탄올 6.0 6.0 6.0
가용화제 0.3 0.3 0.3
방부제 적량 적량 적량
향 적량 적량 적량
추출물상 박하초 1.0 - -
박하 추출물 - 1.0 -
Table 1
ingredient Formulation Example 1 Comparative Formulation Example 1 Comparative Formulation Example 2
Awards Purified water Remaining amount Remaining amount Remaining amount
Butylene Glycol 3.0 3.0 3.0
Betaine 1.5 1.5 1.5
Carbomer 0.2 0.2 0.2
Beta Glucan 5.0 5.0 5.0
Available image ethanol 6.0 6.0 6.0
Solubilizer 0.3 0.3 0.3
antiseptic Quantity Quantity Quantity
incense Quantity Quantity Quantity
Extract phase Peppermint 1.0 - -
Peppermint Extract - 1.0 -
상온에서 투명하게 용해된 수상에 가용화상을 넣어 균일하게 용해시킨 후, 박하초를 투입하여 균일하게 용해하여 제형예 1의 화장료 조성물을 제조하였다. 또한, 비교 제형예1은 상온에서 투명하게 용해된 수상에 가용화상을 넣어 균일하게 용해시킨 후, 박하초를 투입하지 않고 박하 추출물을 투입하여 제조하였다. 비교 제형예 2 는 상온에서 투명하게 용해된 수상에 가용화상을 넣어 균일하게 용해시킨 후, 박하초와 박하 추출물을 각각 투입하지 않고 제조하였다. After dissolving the soluble image in an aqueous phase transparently dissolved at room temperature and dissolving it uniformly, the mint composition was added to dissolve it uniformly to prepare a cosmetic composition of Formulation Example 1. In addition, Comparative Formulation Example 1 was prepared by putting a soluble image in a transparent aqueous solution dissolved at room temperature and dissolving it uniformly, and then adding a peppermint extract without adding peppermint herb. Comparative Formulation Example 2 was prepared by putting a soluble image in a transparent aqueous solution dissolved at room temperature and dissolving it uniformly, without adding mint and peppermint extract, respectively.
<시험예 1> 피부 모공 및 피지 개선 효능 평가<Test Example 1> Evaluation of skin pores and sebum improvement efficacy
상기 제형예 1 및 비교 제형예 1, 비교 제형예 2의 피부 탄력회복 효과, 모공 축소 효과 및 피지 조절 효과를 확인하기 위하여 20대 내지 30대 여성을 대상으로 측정하였다. 각 군에 제형예 1 및 비교 제형예 1, 비교 제형예 2의 제형을 주고 안면 전체에 고르게 도포하게 한 후, 모공 축소 효과 및 피지 조절 효능평가하였다.To determine the skin elasticity recovery effect, pore reduction effect and sebum control effect of Formulation Example 1 and Comparative Formulation Example 1, Comparative Formulation Example 2 was measured in women in their 20s to 30s. Formulation Example 1, Comparative Formulation Example 1 and Comparative Formulation Example 2 were given to each group, and then evenly applied to the entire face, and the pore reduction effect and sebum control efficacy were evaluated.
본 시험은 시험 목적에 적합한 피험자들을 대상으로, 항온 항습 조건에서 해당 시험 제품을 1회 사용하도록 하였다. 모공 고민이 있는 여성 피험자를 대상으로 일반적인 사용 방법에 따라 시료를 사용하고, 시료의 사용 직후 모공관리 효능을 평가하였다. This test was conducted on subjects who were suitable for the purpose of the test and used the test product once under constant temperature and humidity conditions. Female subjects with pore concerns were used according to the general method of use, and the pore management efficacy was evaluated immediately after the use of the sample.
세안 후 시료의 적당량 (2 mg/cm2)을 취하여 얼굴 전체에 손으로 부드럽게 문지르며 골고루 발라주도록 하였다. 시험 기간 중 피험자는 1회 시료 사용 전과 사용 직후에 평가를 진행하였으며 피험자는 측정 시점에 방문하여 세안 직후 항온 항습 조건 (22±2℃, 40±5 RH %)에서 15분 이상 안정을 취한 후, 하기 표 2와 같이 측정 시점 별로 시료 사용 및 평가를 실시하였다.After cleansing, an appropriate amount (2 mg / cm 2 ) of the sample was taken and rubbed gently with hands all over the face. During the test period, the subject evaluated before and immediately after using the sample once, and the subject visited at the time of measurement and immediately stabilized for at least 15 minutes in constant temperature and humidity conditions (22 ± 2 ° C, 40 ± 5 RH%) immediately after washing. Sample use and evaluation were performed for each measurement time point as shown in Table 2 below.
본 시험예의 시료의 피부 적용시의 모공 크기, 피지 크기 및 개수의 측정은 ㈜아모레퍼시픽에서 개발한 측정장비 Skin Touch를 이용하여 평가하였다. Skin Touch는 일체형 센서에 의해 피부의 유분, 수분, 탄력도 측정을 진행하며, 측정된 결과는 외부의 LCD 표시창으로 표현된다. 시료 사용 전, 시료 사용 1주, 2주 경과 후 등을 Skin Touch를 이용하여 시험부위를 측정함으로써 시료의 피부 적용시의 모공 크기, 피지 크기 및 개수를 평가하였다. The pore size, sebum size and number of skin samples of this test sample were measured using the skin touch measuring device developed by AMOREPACIFIC. Skin Touch measures the skin's oil, moisture and elasticity by the integrated sensor, and the measured result is displayed on the external LCD display window. Before using the sample, after 1 week, 2 weeks after the use of the sample by measuring the test site using the skin touch, the pore size, sebum size and number at the time of skin application of the sample was evaluated.
표 2
측정 시점 평가 항목 및 순서
시료 사용 전 세안 후 대기 (15분 이상)피부 모공/피지 측정시료 사용
시료 사용 직후 시료 사용 후 대기 (5분)피부 모공/피지 측정
TABLE 2
Measuring point Evaluation item and order
Before using the sample After washing your face (more than 15 minutes) Use skin pores and sebum measurement samples
Immediately after sample use Standby after sample use (5 minutes) Measure skin pores and sebum
그 결과, 안면 모공부위의 경우 박하초를 유효성분으로 함유한 시료 사용 전에 비하여 사용 직후, 피지의 개수, 피지의 크기 (단위: A.U.), 모공의 크기 (단위: A.U.)가 하기 표 3과 같이 통계적으로 유의하게 감소한 결과가 나타났다.As a result, in the case of facial pores, the number of sebum, sebum size (unit: AU), and pore size (unit: AU) are as shown in Table 3 immediately after use compared to before using the sample containing peppermint herb as an active ingredient. There was a statistically significant decrease.
표 3
제형예 1 비교 제형예 1 비교 제형예 2
피지 개수 평균 도포 전 21 25 23
도포 후 7 12 22
피지 크기 평균(단위: A.U.) 도포 전 156 104 123
도포 후 79 131 135
모공 크기 평균(단위: A.U.) 도포 전 121 121 116
도포 후 101 138 142
TABLE 3
Formulation Example 1 Comparative Formulation Example 1 Comparative Formulation Example 2
Sebum count average Before application 21 25 23
After application 7 12 22
Sebum Size Average in AU Before application 156 104 123
After application 79 131 135
Pore size average in AU Before application 121 121 116
After application 101 138 142
상기 표 3과 도 1 내지 12의 결과에서, 모공 축소 및 피지 조절 효과를 주는 제형예 1의 모공 수축, 피지 개수 감소 및 모공 개수 개선 효과가 비교 제형예 1, 비교 제형예 2에 대비하여 우수한 것을 확인할 수 있었다.In Table 3 and the results of FIGS. 1 to 12, the pore shrinkage, sebum reduction, and pore number improvement effects of Formulation Example 1, which have a pore reduction and sebum control effect, are superior to Comparative Formulation Example 1 and Comparative Formulation Example 2. I could confirm it.

Claims (8)

  1. 박하초를 유효성분으로 함유하는 화장료 조성물.Cosmetic composition containing peppermint vinegar as an active ingredient.
  2. 제1항에 있어서, 상기 박하초는 박하 추출물을 초산 발효한 것임을 특징으로 하는 화장료 조성물.The cosmetic composition according to claim 1, wherein the peppermint vinegar is acetic acid fermented peppermint extract.
  3. 제2항에 있어서, 상기 초산 발효는 초산균 (Acetobacter aceti)을 사용한 것임을 특징으로 하는 화장료 조성물.The method of claim 2, wherein the acetic acid fermentation is Acetobacter aceti ) is used as a cosmetic composition.
  4. 제2항에 있어서, 상기 박하 추출물은 박하의 잎 및 줄기 중 어느 하나 또는 이들의 조합의 추출물인 것을 특징으로 하는 화장용 조성물.According to claim 2, wherein the mint extract is a cosmetic composition, characterized in that the extract of any one or a combination of leaves and stems of peppermint.
  5. 제1항에 있어서, 상기 화장료 조성물은 알파히드록시산을 함유하는 것임을 특징으로 하는 화장료 조성물.The cosmetic composition according to claim 1, wherein the cosmetic composition contains alpha hydroxy acid.
  6. 제1항에 있어서, 상기 박하초의 함량은 상기 화장료 조성물 전체 중량에 대하여, 0.001 중량% 내지 20 중량%인 것을 특징으로 하는 화장용 조성물.According to claim 1, wherein the content of the peppermint is a cosmetic composition, characterized in that 0.001% to 20% by weight relative to the total weight of the cosmetic composition.
  7. 제1항에 있어서, 상기 화장용 조성물은 모공 축소용인 것을 특징으로 하는 화장용 조성물.According to claim 1, wherein the cosmetic composition is a cosmetic composition, characterized in that for reducing pores.
  8. 제1항에 있어서, 상기 화장용 조성물은 피지 조절용인 것을 특징으로 하는 화장용 조성물.According to claim 1, wherein the cosmetic composition is a cosmetic composition, characterized in that for controlling sebum.
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KR101163069B1 (en) * 2010-07-23 2012-07-04 함일한 Cosmetic composition for anti-blemish and anti-wrinkle and method for manufacturing thereof
KR101322850B1 (en) * 2011-08-09 2013-10-28 이상록 The cosmetic composition for pore-minimizing and inhibition of Sebum Secretion containing the extract of leaves of Mentha arvensis var. piperascens, wheat bud, and Platycodon grandiflorum
WO2013102234A1 (en) * 2012-01-06 2013-07-11 Ubs Ultimate Relief Pty Ltd Formulation and method for treatment of pain and/or inflammation associated with a skin condition
KR20140115797A (en) * 2013-03-22 2014-10-01 주식회사 이숨 Cosmetic composition including the oriental medicine mixed extract and fermentation by-product removing hair sebum

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CN106232101B (en) 2020-02-28
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JP6894991B2 (en) 2021-06-30
KR20150122983A (en) 2015-11-03
CN106232101A (en) 2016-12-14
JP2020100663A (en) 2020-07-02
JP2017513876A (en) 2017-06-01

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