WO2015145821A1 - 整髪剤組成物 - Google Patents
整髪剤組成物 Download PDFInfo
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- WO2015145821A1 WO2015145821A1 PCT/JP2014/075077 JP2014075077W WO2015145821A1 WO 2015145821 A1 WO2015145821 A1 WO 2015145821A1 JP 2014075077 W JP2014075077 W JP 2014075077W WO 2015145821 A1 WO2015145821 A1 WO 2015145821A1
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- component
- hair styling
- mass
- hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/044—Suspensions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
Definitions
- the present invention relates to a hair styling composition that is suitably used for a hair styling agent for preparing hair.
- various hair conditioner compositions such as liquid, gel, cream and solid are used.
- a film-forming polymer is often used for imparting hair-styling power, which is a main function, to a hair-styling composition.
- the initial hair styling power immediately after hair styling is increased, while the hair styling composition composition on the hair becomes unsuitable and unfit, and stickiness occurs.
- a film is formed on the surface of the hair after hair styling, derived from the film-forming polymer. For this reason, it is difficult to prepare the hair in a natural state, and when the hair is stimulated with hands or a comb after hair styling, the film peels off from the surface of the hair (so-called flaking occurs), Hair styling power is easily reduced.
- Patent Document 1 discusses the use of silicones as a plasticizer in a hairdressing composition containing a film-forming polymer.
- Patent Document 2 discloses a hair cosmetic (hairdressing composition) containing 0.1 to 10% by mass of a fine particle powder having a specific surface area of 50 m 2 / g or more.
- a hair cosmetic hairdressing composition
- Patent Document 2 by using the specific fine particle powder at a specific content, a good feel can be obtained, an excellent hair styling power can be obtained, and a good feel can be maintained for a long time, and an excellent It describes that hair styling properties can be obtained.
- the flexibility of the film formed from the film-forming polymer is increased to some extent.
- the usability of the hairdressing composition is improved to some extent.
- the initial hair styling power which is the main function of the hair styling composition, is reduced as the flexibility of the film is improved.
- the styling state cannot be maintained for a long time. That is, when the hair styling composition described in Patent Document 1 is used for hair shaping, the initial hair styling power and the hair styling holding power may not be sufficiently high.
- the initial hair styling power and hair styling holding power may not be sufficiently high.
- flaking or stickiness may occur.
- the viscosity may increase when stored for a long period of time, and the extension and familiarity of the hairdressing composition on the hair tend to be poor.
- hair styling compositions containing fine particle powders also have the problem that when stored for a long period of time, the powder tends to settle or the composition is water-separated or separated, resulting in poor storage stability.
- the purpose of the present invention is to improve the storage stability by suppressing the sedimentation of powder during storage for a long period of time or the water separation and separation of the composition, and the lengthening and familiarity at the time of application by suppressing an increase in viscosity.
- Providing an agent composition is to improve the storage stability by suppressing the sedimentation of powder during storage for a long period of time or the water separation and separation of the composition, and the lengthening and familiarity at the time of application by suppressing an increase in viscosity.
- a limited object of the present invention is to provide a hair styling composition that can suppress the occurrence of flaking and stickiness, and can enhance the initial hair styling power and the hair styling holding power when hair is stipulated.
- the hairdressing composition according to the present invention includes the following component (A), the following component (B), the following component (C), and the following component (D), and the content of the component (A) is 0. 1 to 10% by mass, and the mass ratio of the component (C) and the component (D) is 2: 1 to 10: 1 It is.
- Component (A) Particles selected from the group consisting of silica, calcium carbonate, magnesium carbonate, hydroxyapatite, titanium oxide, zinc oxide, calcium silicate, magnesium silicate, aluminum silicate, and magnesium hydroxide
- Component (B) Compound selected from the group consisting of monosaccharides, disaccharides, and sugar alcohols
- Component (C) Clay mineral
- the total content of the component (C) and the component (D) is preferably 0.3% by mass or more and 5% by mass or less.
- the hairdressing composition according to the present invention preferably further contains the following component (E).
- the hairdressing composition according to the present invention preferably further contains the following component (F).
- component (F) Compound selected from the group consisting of component (F) polyoxyalkylene alkyl glucoside and polyoxyalkylene glycerin fatty acid ester
- the hairdressing composition according to the present invention includes specific components (A), (B), (C), and (D), and the content of the component (A) is within a specific range. ) Content and the content of component (D) is a specific ratio, so that the storage stability is improved by suppressing sedimentation of the powder during long-term storage or water separation and separation of the composition. In addition, it is possible to suppress the increase in viscosity and increase the elongation and familiarity at the time of application.
- the hairdressing composition according to the present invention was selected from the group consisting of silica, calcium carbonate, magnesium carbonate, hydroxyapatite, titanium oxide, zinc oxide, calcium silicate, magnesium silicate, aluminum silicate, and magnesium hydroxide.
- Particles a compound selected from the group consisting of monosaccharides, disaccharides, and sugar alcohols, clay minerals, and polysaccharide compounds.
- component (A) particles selected from the group consisting of silica, calcium carbonate, magnesium carbonate, hydroxyapatite, titanium oxide, zinc oxide, calcium silicate, magnesium silicate, aluminum silicate, and magnesium hydroxide
- component (B) The “compound selected from the group consisting of monosaccharides, disaccharides, and sugar alcohols” may be referred to as “component (B)”.
- component (C) the “clay mineral”
- component (D) polysaccharide compound”.
- the hairdressing composition according to the present invention preferably further contains polyethylene glycol.
- polyethylene glycol may be referred to as “component (E)”.
- the hair styling composition according to the present invention preferably further contains a compound selected from the group consisting of polyoxyalkylene alkyl glucoside and polyoxyalkylene glycerin fatty acid ester.
- component (F) the “compound selected from the group consisting of polyoxyalkylene alkyl glucoside and polyoxyalkylene glycerin fatty acid ester” may be referred to as “component (F)”.
- component (F1) the “polyoxyalkylene alkyl glucoside”
- component (F2) the “polyoxyalkylene glycerin fatty acid ester”
- the hairdressing composition according to the present invention includes at least the component (A), the component (B), the component (C), and the component (D). It is preferable that the hairdressing composition according to the present invention further includes a component (at least one component) selected from the group consisting of component (E) and component (F). Especially, it is preferable that the hairdressing composition which concerns on this invention contains all of a component (A), a component (B), a component (C), a component (D), a component (E), and a component (F).
- the hairdressing composition according to the present invention may further contain other components. Only one type of each of the above components, for example, the component (A), the component (B), the component (C), the component (D), the component (E), the component (F), and the like is used. Two or more kinds may be used.
- the component (F) is a compound (at least one compound) selected from the group consisting of the component (F1) and the component (F2).
- component (F1) and component (F2) only 1 type may be used respectively and 2 or more types may be used.
- the component (A) is a particle selected from the group consisting of silica, calcium carbonate, magnesium carbonate, hydroxyapatite, titanium oxide, zinc oxide, calcium silicate, magnesium silicate, aluminum silicate, and magnesium hydroxide. .
- the said component (A) has a role which mainly suppresses stickiness and raises initial hair-setting power and hair-styling retention power. Further, by using the component (A), it is possible to facilitate hair styling again after hair styling once and to improve re-hair styling, as compared with the case where a film-forming polymer is used.
- the component (A) was selected from the group consisting of silica, magnesium carbonate, hydroxyapatite, calcium silicate, magnesium silicate, aluminum silicate, and magnesium hydroxide, among others, from the viewpoint of improving hairdressing performance. Particles (at least one particle) are preferred, and particles (at least one particle) selected from the group consisting of silica and magnesium silicate are more preferred. As for the said component (A), only 1 type may be used and 2 or more types may be used.
- silica known and commonly used silica (anhydrous silicic acid) can be used.
- the silica may be silicic anhydride (hydrophilic silica) that has not been hydrophobized or may be hydrophobized silicic anhydride.
- the silica surface-treated with an amino acid, ester or lecithin may be used.
- the silica may be so-called easily disintegrating silica particles.
- 1 type may be used and 2 or more types may be used.
- the hydrophobized silicic anhydride is a substance obtained by hydrophobizing silicic anhydride (for example, untreated silicic anhydride).
- the treating agent used for the hydrophobizing treatment include organic silyl compounds and silicone compounds.
- the organic silyl compound include methyltrichlorosilane, dimethyldichlorosilane, trimethylchlorosilane, hexamethyldisilazane, methyltrialkoxysilane, dimethyldialkoxysilane, trimethylalkoxysilane, ethyltrichlorosilane, propyltrichlorosilane, hexyltrichlorosilane, long Examples include chain alkyltrichlorosilane, ethyltrialkoxysilane, propyltrialkoxysilane, hexyltrialkoxysilane, long chain alkyltrialkoxysilane, methacryl silane, fluoroalky
- silicone compound examples include dimethylpolysiloxane (silicone oil), methylphenylpolysiloxane, methylhydrogenpolysiloxane, and amino-modified silicone.
- a publicly known method can be adopted as a method of the above-mentioned hydrophobic treatment.
- the hydrophobic treatment method include a liquid phase method, a gas phase method, and an autoclave method.
- hydrophobic silicic anhydride examples include dimethylsiloxylated silicic anhydride, trimethylsiloxylated silicic anhydride, octylsiloxylated silicic anhydride, silicone oil treated silicic anhydride and methacrylsiloxylated silicic anhydride. Etc.
- the above easily disintegratable silica particles are particles formed by aggregating a plurality of silica primary particles. Although it does not specifically limit as said silica primary particle, For example, a spherical silica particle, a scaly silica particle, an amorphous silica particle, etc. are mentioned.
- the average particle diameter of the silica primary particles is not particularly limited.
- the easily disintegratable silica particles may contain components other than silica.
- the component other than the silica (hereinafter may be referred to as “encapsulated component”) is not particularly limited, and examples thereof include surfactants, polyhydric alcohols, higher alcohols, sugar alcohols, silicone oils, sequestering agents, Examples include antioxidants, plant extracts, dyes, pigments, fragrances, moisturizers, vitamins, amino acids, and refreshing agents. Of these, amino acids, silicone oils, and vitamins are preferable. Although it does not specifically limit as said amino acids, Dilauroyl glutamate ricin Na (For example, the product name "Perisea" by Asahi Kasei Chemicals Corporation), a trimethylglycine, glutamic acid, etc.
- the easily disintegratable silica particles encapsulate the inclusion component
- the inclusion component is released when the easily disintegratable silica particles are disintegrated during hair styling, and an effect corresponding to the type of the inclusion component is exhibited.
- the easily disintegratable silica particles encapsulate amino acids, thereby exhibiting a hair damage care function.
- the method for producing the easily disintegratable silica particles is not particularly limited, and a known method can be used.
- the silica oil absorption is preferably 100 mL / 100 g or more, more preferably 150 mL / 100 g or more, still more preferably 200 mL / 100 g or more, preferably 1000 mL / 100 g or less, more preferably 800 mL / 100 g or less, more preferably 700 mL / 100 g or less.
- the oil absorption amount of the silica is not less than the above lower limit and not more than the above upper limit, the initial hair styling power, the hair styling holding power, and the re-hair styling property are further improved.
- the oil absorption is measured according to the method described in JIS K5101.
- silica silicic acid manufactured by Fuji Silysia Chemical Co., Ltd., trade name “Silysia 320”, trade name “Silisia 310P”, trade name “Silicia 250”, trade name “Silicia 250N”, product.
- the said calcium carbonate is represented by the INCI name "CALCIUM CARBONATE", for example.
- the said calcium carbonate only 1 type may be used and 2 or more types may be used.
- Sakai Chemical Industry make brand name "Karumaru SCS M5"; Shiraishi calcium company make, brand name "Fuwakaru” etc. are mentioned, for example.
- the magnesium carbonate is represented by, for example, the INCI name “MAGNESIUM CARBONATE”. As for the said magnesium carbonate, only 1 type may be used and 2 or more types may be used. As a commercial item of the said magnesium carbonate, the Toda Pharmaceutical company make, brand name "light magnesium carbonate” etc. are mentioned, for example.
- hydroxyapatite is represented by, for example, the INCI name “HYDROXYAPATITE”. As for the said hydroxyapatite, only 1 type may be used and 2 or more types may be used.
- the hydroxyapatite is not particularly limited, and examples thereof include spherical hydroxyapatite, plate-like hydroxyapatite, and amorphous hydroxyapatite. Among these, spherical hydroxyapatite is preferable from the viewpoint of exhibiting high hair styling performance.
- examples of commercially available hydroxyapatite include, for example, trade name “Plate HAP”, trade name “Spherical HAP”, trade name “HAP-100”, trade name “HAP-200”, and trade name, manufactured by Taihei Chemical Industry Co., Ltd. Examples thereof include “HAP-300”.
- the titanium oxide is represented by, for example, the INCI name “TITANIUM DIOXIDE”.
- the titanium oxide is not particularly limited, and may be fine particle titanium oxide or pigment titanium, for example. As for the said titanium oxide, only 1 type may be used and 2 or more types may be used. Examples of commercially available titanium oxide include trade name “TTO-55 (A)” and trade name “CR-50” manufactured by Ishihara Sangyo Co., Ltd.
- the zinc oxide is represented by, for example, the INCI name “ZINC OXIDE”. As for the said zinc oxide, only 1 type may be used and 2 or more types may be used. Examples of commercially available zinc oxide include trade name “FINEX-30S-LP2” manufactured by Sakai Chemical Industry Co., Ltd.
- the calcium silicate is represented, for example, by the INCI name “CALCIUM SILICATE”. As for the said calcium silicate, only 1 type may be used and 2 or more types may be used. Examples of commercially available products of calcium silicate include Tomita Pharmaceutical Co., Ltd., trade name “FLORITE R”; Nippon Insulation Co., Ltd., trade name “Zonotolite Powder XJ”, and trade name “Tobermorite Powder TK”. .
- the magnesium silicate is represented by, for example, the INCI name “MAGNESIUM SILICATE”. As for the said magnesium silicate, only 1 type may be used and 2 or more types may be used. As a commercial item of the said magnesium silicate, the Tomita Pharmaceutical company make, brand name "magnesium silicate (light)" etc. are mentioned, for example.
- the aluminum silicate is represented by, for example, the INCI name “ALUMINUM SILICATE”. As for the said aluminum silicate, only 1 type may be used and 2 or more types may be used. Although it does not specifically limit as an aluminum silicate, A synthetic aluminum silicate is preferable. Examples of the synthesis method include, for example, a method of adding Na 2 SiO 3 to alum and drying the generated precipitate, a method of producing a silicate sol by electrodialysis, thereby producing a gel, and an aluminum salt in water glass. The method of adding the aqueous solution of this is mentioned. As a commercial item of the said aluminum silicate, the Tomita Pharmaceutical company make, brand name "synthetic aluminum silicate (heavy)" etc. are mentioned, for example.
- the magnesium hydroxide is represented by, for example, the INCI name “MAGNESIUM HYDROXIDE”. As for the said magnesium hydroxide, only 1 type may be used and 2 or more types may be used. As a commercial item of the said magnesium hydroxide, the Tomita Pharmaceutical company make, brand name "magnesium hydroxide (heavy)" etc. are mentioned, for example.
- the content of the component (A) is 0.1% by mass or more, preferably 0.5% by mass or more, more preferably 1% by mass or more and 10% by mass. Hereinafter, it is preferably 7% by mass or less, more preferably 5% by mass or less.
- the content of the component (A) is equal to or more than the above lower limit, the initial hair styling power immediately after hair styling can be increased, the hair styling holding power can be increased, and stickiness can be further suppressed. Generation
- production of flaking can be suppressed because content of the said component (A) is below the said upper limit.
- the content of the component (A) is the total content of all the components (A) in the hairdressing composition according to the present invention.
- the component (B) is a compound (at least one compound) selected from the group consisting of monosaccharides, disaccharides, and sugar alcohols. As for the said component (B), only 1 type may be used and 2 or more types may be used.
- Examples of the monosaccharide and the disaccharide include glyceraldehyde, erythrose, threose, ribose, lyxose, xylose, arabinose, allose, talose, gulose, glucose, altrose, mannose, galactose, and idose; aldoses; Examples include ketoses such as erythrulose, xylulose, ribulose, psicose, fructose, sorbose, and tagatose; disaccharides such as sucrose, lactulose, maltose, trehalose, and cellobiose.
- sugar alcohol examples include maltitol, sorbitol, ribitol, mannitol, arabitol, galactitol, xylitol, erythritol, and inositol.
- the content of the component (B) is preferably 0.05% by mass or more, more preferably 0.1% by mass or more, and further preferably 0.2% by mass. As mentioned above, Preferably it is 20 mass% or less, More preferably, it is 18 mass% or less, More preferably, it is 15 mass% or less.
- the content of the component (B) is not less than the above lower limit, the initial hair styling power is effectively increased.
- the content of the component (B) is not more than the above upper limit, stickiness can be further suppressed.
- the content of the component (B) is the total content of all the components (B) in the hairdressing composition according to the present invention.
- the component (C) is a clay mineral.
- the hairdressing composition is appropriately thickened, so that the dispersibility of the component (A) is further increased. It becomes much better, and water storage and separation of the composition are suppressed, and the storage stability is further improved. Moreover, the elongation at the time of application
- the said component (C) only 1 type may be used and 2 or more types may be used.
- the component (C) may be a natural product or a synthetic product. Although it does not specifically limit as said component (C), For example, kaolin group clay mineral, antigolite group clay mineral, pyrophyllite group clay mineral, mica group clay mineral, smectite group clay mineral, vermiculite group clay mineral, green mud Examples include stone group clay minerals and organically modified clay minerals.
- Examples of the kaolin group clay mineral include kaolin, nacrite, dickite, and halosite.
- examples of the antigolite group clay mineral include antigolite, amesite, and cronstedite.
- examples of the pyrophyllite clay mineral include pyrophyllite and talc (talc).
- examples of the mica group clay minerals include illite, sea chlorite, ceradonite, sericite, mica (mica), muscovite, chromium muscovite and biotite.
- Examples of the smectite clay mineral include bentonite, montmorillonite, beidellite, nontonite, saponite, hectorite, and lucentite. Vermiculite etc.
- vermiculite group clay mineral examples include chlorite.
- examples of the organic modified clay mineral include an organic modified clay mineral obtained by organically modifying a smectite group clay mineral or a vermiculite group clay mineral.
- a quaternary ammonium salt type cationic surfactant is preferably used for the organic modification treatment.
- examples of the quaternary ammonium salt type cationic surfactant include the above alkyltrimethylammonium chloride, dialkyldimethylammonium chloride, and benzalkonium chloride.
- the component (C) is preferably a clay mineral selected from the group consisting of synthetic silicates and derivatives thereof.
- the above-mentioned synthetic silicate and its derivative are not a silicate mineral mainly composed of magnesium silicate or silicic acid (sodium / magnesium) derived from nature, which contains impurities, but silicic acid obtained by synthesis. Refers to salts and silicate derivatives.
- Examples of the synthetic silicate and derivatives thereof include, for example, an INCI name (International Cosmetic Ingredient Dictionary and Handbook, 14th edition, Volume 2, CTFA, 2012, p. 3076): SODIUM MAGNESIUM SILICATE Acid (sodium / magnesium), INCI name (International Cosmetic Ingredient Dictionary and Handbook, 14th edition, Volume 2, CTFA, 2012, p. 1793): MAGNESIUM FLUOROSILICATE Magnesium Fluorosilicate, INCI name Cosmetic gradient Dictionary and Handbook, 14th edition, volume 2, CTFA, 2012, p.
- SODIUM MAGNESIUM FLUOROSILICATE fluorosilicic acid (sodium / magnesium), INCI name (International CosmeticallyIndeticHardbook 14th Edition, Volume 2, CTFA, 2012, p. 1799): MAGNESIUM POTASSIUM FLUOROSILIC Fluorosilicate (magnesium / potassium), INCI name (International Cosmetic Ingredient Dictionary and Han book, 14th edition, volume 2, CTFA, 2012, p. 1800): MAGNESIUM SODIUM FLUOROSILICATE, fluorosilicic acid (magnesium / sodium), INCI name (International Cosmetic Ingredient Dictionary, Handbook 14th edition) Volume 1, CTFA, 2012, p. 156): ALUMINUM, synthetic aluminum silicate represented by SILICATE.
- a clay mineral (at least one clay mineral) selected from the group consisting of synthetic silicic acid (sodium / magnesium) and fluorosilicic acid (sodium / magnesium) is particularly preferable.
- the content of the component (C) is preferably 0.1% by mass or more, more preferably 0.3% by mass or more, and preferably 5% by mass or less. Preferably it is 3 mass% or less.
- the content of the component (C) is not less than the above lower limit, the precipitation of the component (A) is further suppressed, and the separation of the composition is suppressed, so that the storage stability is further improved.
- the content of the component (C) is not more than the above upper limit, the increase in viscosity is suppressed, and the elongation and familiarity at the time of application are further improved.
- Content of the said component (C) is a total amount of content of all the components (C) in the hairdressing composition which concerns on this invention.
- the component (D) is a polysaccharide compound.
- the polysaccharide compound which is the component (D) is a polysaccharide compound having three or more sugars.
- the component (D) is a polysaccharide compound other than the component (B).
- a polysaccharide, modified polysaccharide (for example, alkyl modified polysaccharide etc.), etc. are preferable, for example, alginic acid, carrageenan, agar, ferrule, guar gum, quince seed, konjac mannan, tamarind gum, Plant-derived polysaccharide compounds such as tara gum, dextrin, starch, locust bean gum, gum arabic, gati gum, karaya gum, tragacanth gum, arabinogalactan, pectin and quince; animal-derived polysaccharide compounds such as chitosan and hyaluronic acid; curdlan, xanthan gum , Polysaccharides derived from microorganisms such as gellan gum, cyclodextrin, dextran, pullulan and hyaluronic acid; microcrystalline cellulose, methylcellulose, ethylcellulose, hydroxymethylcellulose
- Non-derived polysaccharide such as
- the component (D) is preferably a compound (at least one compound) selected from the group consisting of xanthan gum, guar gum, tamarind gum and gellan gum.
- the product made from Dainippon Sumitomo Pharmaceutical Co., Ltd. which is a xanthan gum, the brand name "Echo gum T", the brand name "Keldent", and the brand name "Monatogum”; Product name “Inagel Guar Gum CS”; Tamarind Gum made by DSP Gokyo Food & Chemical Co., Ltd. Product name “Glyroid 6C”; Gellan Gum CP Kelco U. S. , Inc. Manufactured and trade name "Kelcogel”.
- the content of the component (D) is preferably 0.01% by mass or more, more preferably 0.1% by mass or more, and preferably 3% by mass or less. Preferably it is 1 mass% or less.
- the content of the component (D) is not less than the above lower limit, water removal and separation of the hairdressing composition are suppressed, and the storage stability is further improved.
- the content of the component (D) is less than or equal to the above upper limit, the increase in viscosity is suppressed and the elongation and familiarity during application are further improved, and the hair styling power is not reduced.
- Content of the said component (D) is a total amount of content of all the components (D) in the hairdressing agent composition which concerns on this invention.
- the total content of the component (C) and the component (D) is preferably 0.3% by mass or more, more preferably 0.4% by mass or more. , Preferably 5% by mass or less, more preferably 4% by mass or less.
- the total content of the component (C) and the component (D) is equal to or more than the lower limit, the settling of the component (A) is suppressed, and the hair removal and separation of the hairdressing composition are suppressed, so that the storage stability is maintained. The property becomes even better.
- the total content of the component (C) and the component (D) is less than or equal to the above upper limit, the increase in viscosity is suppressed, and the elongation and familiarity at the time of application are further improved.
- the mass ratio of the component (C) to the component (D) is 2 in 100% by mass of the hairdressing composition according to the present invention. : 1 to 10: 1, preferably 2.5: 1 to 8: 1.
- the mass ratio is satisfied, the initial hair styling power is further improved, and the storage stability of the hair styling composition is further improved, and an increase in the viscosity of the hair styling composition when stored for a long period of time can be suppressed. Elongation and familiarity during application become even better.
- the component (E) is polyethylene glycol.
- the component (E) mainly has a role of effectively increasing the initial hair styling power and the hair styling holding power. In addition, by using the component (E), it is possible to impart a better touch to the hair after styling while maintaining high initial styling power.
- the said component (E) only 1 type may be used and 2 or more types may be used.
- the number average molecular weight of the component (E) is preferably 150 or higher, more preferably 200 or higher, preferably 6000 or lower, more preferably 4000 or lower.
- the content of the component (E) is preferably 1% by mass or more, more preferably 3% by mass or more, preferably 30% by mass or less, more preferably 25% by mass. % Or less.
- the content of the component (E) is not less than the lower limit, the initial hair styling power and the hair styling holding power can be further enhanced.
- the content of the component (E) is not more than the above upper limit, the occurrence of flaking can be further suppressed, and the hair after styling can be imparted with a better touch by suppressing stiffness and squeaking.
- Content of the said component (E) is a total amount of content of all the components (E) in the hairdressing composition which concerns on this invention.
- the mass ratio between the content of the component (A) and the content of the component (E) (content of the component (A): content of the component (E)). Is preferably 1: 1 to 1:25, more preferably 1: 3 to 1:20.
- the content of the component (A) is relatively increased, the initial hair styling power is further improved.
- the content of the component (E) is relatively increased, the firmness and the creaking are further improved.
- the component (F) is at least one compound selected from the group consisting of the component (F1) and the component (F2).
- flaking can be further suppressed, washing off after hair styling is improved, and good hair feel can be imparted to the hair after styling while maintaining high initial hair styling power.
- the uncomfortable feeling that the hair styling agent is attached to can be suppressed, and hair can be styled in a natural state.
- the said component (F) only 1 type may be used and 2 or more types may be used.
- only 1 type may be used for said component (F1) and said component (F2), respectively, and 2 or more types may be used.
- component (F) only one of the component (F1) and the component (F2) may be used, or the component (F1) and the component (F2) may be used in combination. .
- the component (F1) is a polyoxyalkylene alkyl glucoside.
- the oxyalkylene group in the component (F1) include an oxyethylene group and an oxypropylene group.
- the average addition mole number of the oxyalkylene group in the component (F1) is not particularly limited, but is preferably 5 or more, and preferably 40 or less.
- the number of carbon atoms of the alkyl group in the component (F1) is preferably 1 to 4, more preferably 1 to 3.
- the alkyl group in the component (F1) is preferably a methyl group or an ethyl group.
- the component (F1) is not particularly limited, and examples thereof include polyoxyethylene methyl glucoside, polyoxyethylene ethyl glucoside, polyoxypropylene methyl glucoside, and polyoxypropylene ethyl glucoside.
- the component (F1) is preferably polyoxyethylene methyl glucoside.
- the component (F2) is a polyoxyalkylene glycerin fatty acid ester.
- the number of carbon atoms of the fatty acid in the component (F2) is preferably 8 or more, and preferably 22 or less.
- Examples of the oxyalkylene group in the component (F2) include an oxyethylene group and an oxypropylene group.
- the average added mole number of the oxyalkylene group in the component (F2) is preferably 5 or more, and preferably 40 or less.
- the fatty acid in the component (F2) is preferably a branched fatty acid, and the component (F2) is a polyoxyalkylene. It is preferably a glycerin branched fatty acid ester.
- the number of carbon atoms of the branched fatty acid in the polyoxyalkylene glycerin branched fatty acid ester is preferably 8 or more, and preferably 22 or less.
- Examples of the branched fatty acid in the polyoxyalkylene glycerin branched fatty acid ester include 2-ethylhexanoic acid, isononanoic acid, isopalmitic acid, and isostearic acid.
- the polyoxyalkylene glycerin branched fatty acid ester is particularly preferably polyoxyethylene glyceryl isostearate.
- the content of the component (F) is preferably 0.5% by mass or more, more preferably 1% by mass or more, preferably 20% by mass or less, more preferably. It is 10 mass% or less.
- the content of the component (F) is not less than the above lower limit, the initial hair styling power is further increased, flaking is further suppressed, and washing after hair styling is further improved.
- the content of the component (F) is not more than the above upper limit, a better touch is imparted to the hair after styling.
- Content of the said component (F) is a total amount of content of all the components (F) in the hairdressing agent composition which concerns on this invention.
- the mass ratio of the content of the component (A) to the content of the component (F) is 1 : 0.2 to 1:20 is preferable, and 1: 1 to 1:10 is more preferable.
- content of the component (A) is relatively increased, a better touch can be imparted to the hair after styling while maintaining a high initial styling power.
- content of the component (F) is relatively increased, flaking is further suppressed, and washing off after styling is further improved.
- the hairdressing composition according to the present invention is not particularly limited, but preferably contains water. Although the said water will not be specifically limited if it is the water used for cosmetics, Purified water is preferable. In 100% by mass of the hairdressing composition according to the present invention, the content of water is preferably 20% by mass or more, more preferably 30% by mass or more, preferably 95% by mass or less, more preferably 90% by mass or less. .
- the hairdressing composition according to the present invention is not particularly limited, but preferably contains a lower alcohol having 2 to 5 carbon atoms (particularly ethanol).
- the content of the lower alcohol (particularly ethanol) is preferably 2% by mass or more, more preferably 5% by mass or more, preferably 50% by mass or less, more preferably. 30% by mass or less.
- the hairdressing composition according to the present invention may be used within the range not inhibiting the effects of the present invention, for example, surfactants such as nonionic surfactants, cationic surfactants and amphoteric surfactants; glycerin, 1,3-butylene glycol Polyhydric alcohols such as propylene glycol, 1,2-butanediol, 1,2-pentanediol, 1,2-hexanediol, 1,2-octanediol, 1,2-decanediol; lauryl alcohol, myristyl alcohol, C12-18 higher alcohols such as cetyl alcohol, stearyl alcohol, isostearyl alcohol, cetostearyl alcohol and oleyl alcohol; acrylates copolymer, (acrylates / steareth methacrylate-20) copolymer, (acrylates / steareth methacrylate-20) Including cross polymers and polymers such as (acrylates / vinyl neodecano
- the property of the hairdressing composition according to the present invention is not particularly limited, and examples thereof include liquid, gel, cream, and solid.
- the hair styling composition is preferably liquid or gel.
- the viscosity at 25 ° C. of the hairdressing composition is preferably 1000 mPa ⁇ s or more, more preferably 2000 mPa ⁇ s or more, preferably 100,000 mPa ⁇ s or less, more preferably 50000 mPa ⁇ s or less.
- the viscosity is not less than the above lower limit and not more than the above upper limit, applicability is further enhanced, flaking and stickiness are further suppressed, and initial hair styling power and hair styling holding power are further enhanced.
- the viscosity is not more than the above upper limit and the fluidity is high, the occurrence of flaking and stickiness can be suppressed, and the initial hair styling power and hair styling holding power can be increased.
- the above viscosity is No. using a viscometer. It is measured under the conditions of a rotation speed of 12 rpm and a rotation time of 1 minute using a 4-rotor.
- a viscometer a TV-22 viscometer manufactured by Toki Sangyo Co., Ltd. can be used.
- the method for producing the hairdressing composition according to the present invention is not particularly limited, and a known method for producing a hairdressing composition can be used as the method for producing the hairdressing composition according to the present invention. Although it does not specifically limit as a manufacturing method of the hairdressing agent composition which concerns on this invention, For example, a paddle after stirring a component (A), a component (B), a component (C), a component (D), and water with a disper mixer. The method of mix
- the hairdressing composition according to the present invention includes at least a component (A), a component (B), a component (C), and a component (D) as main components.
- a component (A) a component (B), a component (C), and a component (D) as main components.
- the hairdressing composition is moderately thickened, the dispersibility of (A) is further improved, and water separation and separation of the hairdressing composition are suppressed. Storage stability is further improved.
- the blending ratio of the component (C) and the component (D) into a specific preferable range, the component (A) is less likely to settle or aggregate, and the hairdressing composition is stored for a long time.
- the increase in viscosity of the hairdressing composition is suppressed, and the elongation and familiarity at the time of application are further improved.
- the hairdressing composition which concerns on this invention when hair is set, generation
- the combined use of the component (B) and the other components described above greatly contributes to effectively increasing the initial hair styling power of raising hair.
- the hairdressing composition according to the present invention further includes a component (E).
- a component (E) In contrast to component (E), stickiness occurs, but by using both component (A) and component (E), the initial hair styling power immediately after hair styling can be increased while suppressing stickiness, and the hair styling retention power. Can be increased. Further, by using the component (E), it is possible to suppress the occurrence of flaking (a phenomenon in which white powder or a film appears to adhere to the hair) when the hair is arranged. Thereby, if the hair-styling agent composition according to the present invention is used, not only hair can be properly sculpted, but the state of shampooing can be favorably sustained for a long period of time.
- the hair styling power and flaking suppression effect are further improved, and the effect of shining the hair after hair styling and washing off are improved.
- the hair styling composition according to the present invention is not particularly limited, but can be used, for example, in a form filled in a container.
- Examples of the container include a bottle container, a jar container, and a tube container.
- the container is preferably a bottle container or a tube container.
- Blending ingredients shown in the following Tables 1 and 2 were blended (blending unit is mass%) to prepare a hairdressing composition.
- ⁇ Evaluation criteria for storage stability (appearance and properties)> ⁇ (very good): neither powder sedimentation nor water separation or separation of the composition is observed ⁇ (good): slight change in at least one of powder sedimentation, water separation or separation of the composition is slight X (Poor): At least one of the settling of the powder and the water separation or separation of the composition is clearly observed
- a TV-22 viscometer manufactured by Toki Sangyo Co., Ltd.
- the measurement was performed using a 4-rotor with a rotational speed of 12 rpm and a rotational time of 1 minute.
- the viscosity increase rate was calculated by substituting the viscosity value immediately after preparation (T0) and the viscosity value after storage (T1) into the following equation.
- ⁇ Evaluation criteria for storage stability (viscosity)> ⁇ (pretty good): the rate of increase in viscosity (%) is 100% or more and less than 150% ⁇ (good): the rate of increase in viscosity (%) is 150% or more and less than 180% ⁇ (defect): Viscosity increase rate (%) is 180% or more
- Test Example 3 Elongation familiarity and stickiness evaluation
- Twenty professional panelists responded by sensory evaluation of the stretch familiarity and stickiness during hair styling in Test Example 2. From the above answers, the familiarity and stickiness were evaluated according to the following criteria.
- Test Example 4 Evaluation of hair holding ability
- Twenty professional panels observed the hair of the wig subjected to hair styling after 1 hour of Test Example 2 (Evaluation of initial hair styling ability), and answered whether hair holding ability was present.
- the hair styling holding power was evaluated as having hair styling holding power when the shape of the hair set up in Test Example 2 was kept. Based on the above answers, hair holding ability was evaluated according to the following criteria.
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Abstract
Description
成分(A):シリカ、炭酸カルシウム、炭酸マグネシウム、ヒドロキシアパタイト、酸化チタン、酸化亜鉛、ケイ酸カルシウム、ケイ酸マグネシウム、ケイ酸アルミニウム、及び水酸化マグネシウムからなる群より選ばれた粒子
成分(B):単糖、二糖、及び糖アルコールからなる群より選ばれた化合物
成分(C):粘土鉱物
成分(D):多糖系化合物
成分(E):ポリエチレングリコール
成分(F)ポリオキシアルキレンアルキルグルコシド及びポリオキシアルキレングリセリン脂肪酸エステルからなる群より選ばれた化合物
上記成分(A)は、シリカ、炭酸カルシウム、炭酸マグネシウム、ヒドロキシアパタイト、酸化チタン、酸化亜鉛、ケイ酸カルシウム、ケイ酸マグネシウム、ケイ酸アルミニウム、及び水酸化マグネシウムからなる群より選ばれた粒子である。上記成分(A)は、主として、べたつきを抑え、初期整髪力及び整髪保持力を高める役割を有する。また、上記成分(A)の使用により、皮膜形成ポリマーを用いた場合と比べて、一旦整髪した後に整髪を再度行うことを容易にし、再整髪性を高めることも可能である。
上記シリカとして、公知慣用のシリカ(無水ケイ酸)を用いることができる。上記シリカは、疎水化処理されていない無水ケイ酸(親水性のシリカ)であってもよいし、疎水化無水ケイ酸であってもよい。また、アミノ酸、エステル又はレシチン等で表面処理されたシリカであってもよい。また、上記シリカは、所謂、易崩壊性シリカ粒子であってもよい。上記シリカは、1種のみが用いられてもよく、2種以上が用いられてもよい。
上記炭酸カルシウムは、例えば、INCI名「CALCIUM CARBONATE」で表される。上記炭酸カルシウムは、1種のみが用いられてもよく、2種以上が用いられてもよい。上記炭酸カルシウムの市販品としては、例えば、堺化学工業社製、商品名「かるまる SCS M5」;白石カルシウム社製、商品名「ふわカル」等が挙げられる。
上記炭酸マグネシウムは、例えば、INCI名「MAGNESIUM CARBONATE」で表される。上記炭酸マグネシウムは、1種のみが用いられてもよく、2種以上が用いられてもよい。上記炭酸マグネシウムの市販品としては、例えば、富田製薬社製、商品名「軽質炭酸マグネシウム」等が挙げられる。
上記ヒドロキシアパタイトは、例えば、INCI名「HYDROXYAPATITE」で表される。上記ヒドロキシアパタイトは、1種のみが用いられてもよく、2種以上が用いられてもよい。
上記酸化チタンは、例えば、INCI名「TITANIUM DIOXIDE」で表される。上記酸化チタンは、特に限定されず、例えば、微粒子酸化チタンであってもよく、顔料チタンであってもよい。上記酸化チタンは、1種のみが用いられてもよく、2種以上が用いられてもよい。上記酸化チタンの市販品としては、例えば、石原産業社製、商品名「TTO-55(A)」及び商品名「CR-50」等が挙げられる。
上記酸化亜鉛は、例えば、INCI名「ZINC OXIDE」で表される。上記酸化亜鉛は、1種のみが用いられてもよく、2種以上が用いられてもよい。上記酸化亜鉛の市販品としては、例えば、堺化学工業社製、商品名「FINEX-30S-LP2」等が挙げられる。
上記ケイ酸カルシウムは、例えば、INCI名「CALCIUM SILICATE」で表される。上記ケイ酸カルシウムは、1種のみが用いられてもよく、2種以上が用いられてもよい。上記ケイ酸カルシウムの市販品としては、例えば、富田製薬社製、商品名「フローライトR」;日本インシュレーション社製、商品名「ゾノトライトパウダーXJ」及び商品名「トバモライトパウダーTK」等が挙げられる。
上記ケイ酸マグネシウムは、例えば、INCI名「MAGNESIUM SILICATE」で表される。上記ケイ酸マグネシウムは、1種のみが用いられてもよく、2種以上が用いられてもよい。上記ケイ酸マグネシウムの市販品としては、例えば、富田製薬社製、商品名「ケイ酸マグネシウム(軽質)」等が挙げられる。
上記ケイ酸アルミニウムは、例えば、INCI名「ALUMINUM SILICATE」で表される。上記ケイ酸アルミニウムは、1種のみが用いられてもよく、2種以上が用いられてもよい。ケイ酸アルミニウムとしては、特に限定されないが、合成ケイ酸アルミニウムが好ましい。合成方法としては、例えば、ミョウバンにNa2SiO3を加え、生成した沈殿を乾燥する方法や、電気透析法によりケイ酸ゾルを作り、これによりゲルを生成する方法、並びに、水ガラスにアルミニウム塩の水溶液を加える方法等が挙げられる。上記ケイ酸アルミニウムの市販品としては、例えば、富田製薬社製、商品名「合成ケイ酸アルミニウム(重質)」等が挙げられる。
上記水酸化マグネシウムは、例えば、INCI名「MAGNESIUM HYDROXIDE」で表される。上記水酸化マグネシウムは、1種のみが用いられてもよく、2種以上が用いられてもよい。上記水酸化マグネシウムの市販品としては、例えば、富田製薬社製、商品名「水酸化マグネシウム(重質)」等が挙げられる。
上記成分(B)は、単糖、二糖、及び糖アルコールからなる群より選ばれた化合物(少なくとも1の化合物)である。上記成分(B)は、1種のみが用いられてもよく、2種以上が用いられてもよい。
上記成分(C)は、粘土鉱物である。上記成分(C)の使用により、特に上記成分(C)と上記成分(D)とを併用することにより、整髪剤組成物が適度に増粘するため、上記成分(A)の分散性がより一層良好になり、組成物の離水や分離が抑えられて保存安定性がより一層良好になる。また、整髪剤組成物の粘度上昇を抑えて塗布時の延び及び馴染みを高めることもできる。上記成分(C)は、1種のみが用いられてもよく、2種以上が用いられてもよい。
上記成分(D)は、多糖系化合物である。上記成分(D)である多糖系化合物は、三糖以上の多糖系化合物である。上記成分(D)は、上記成分(B)以外の多糖系化合物である。上記成分(D)の使用により、特に上記成分(D)と上記成分(C)とを併用することにより、整髪剤組成物が適度に増粘するため、上記成分(A)の分散性がより一層良好になり、組成物の離水や分離が抑えられて保存安定性がより一層良好になる。また、整髪剤組成物の粘度上昇を抑えて塗布時の延び及び馴染みを高めることができる。上記成分(D)は、1種のみが用いられてもよく、2種以上が用いられてもよい。
上記成分(E)は、ポリエチレングリコールである。上記成分(E)は、主として、初期整髪力及び整髪保持力を効果的に高める役割を有する。また、上記成分(E)の使用により、高い初期整髪力を維持しつつ整髪後の髪により一層良好な手触りを付与することができる。上記成分(E)は、1種のみが用いられてもよく、2種以上が用いられてもよい。
上記成分(F)は、上記成分(F1)及び上記成分(F2)からなる群より選ばれた少なくとも1の化合物である。上記成分(F)の使用により、フレーキングをより一層抑え、かつ整髪後の洗い落ちを良好にし、かつ高い初期整髪力を維持しつつ整髪後の髪に良好な手触りを付与することができる。また、毛髪に整髪剤が付与され、毛髪が十分に整髪されている状態であっても、整髪剤が付着している違和感が抑えられ、自然な状態で整髪することができる。上記成分(F)は、1種のみが用いられてもよく、2種以上が用いられてもよい。なお、上記成分(F1)、上記成分(F2)も、それぞれ、1種のみが用いられてもよく、2種以上が用いられてもよい。
本発明に係る整髪剤組成物は、特に限定されないが、水を含むことが好ましい。上記水は、化粧料に用いられる水であれば特に限定されないが、精製水が好ましい。本発明に係る整髪剤組成物100質量%中、水の含有量は、好ましくは20質量%以上、より好ましくは30質量%以上、好ましくは95質量%以下、より好ましくは90質量%以下である。
本発明に係る整髪剤組成物の性状は、特に限定されず、例えば、液状、ジェル状、クリーム状及び固形状等が挙げられる。特に、上記整髪剤組成物は、液状又はジェル状であることが好ましい。
商品名「サイリシア320」:シリカ(富士シリシア化学社製)
商品名「水酸化マグネシウム(重質)」:水酸化マグネシウム(富田製薬社製)
商品名「ケイ酸マグネシウム(軽質)」:ケイ酸マグネシウム(富田製薬社製)
商品名「軽質炭酸マグネシウム」:炭酸マグネシウム(富田製薬社製)
商品名「LYCASIN 75/77」:マルチトール液(マルチトール75質量%と精製水25質量%とを含む)
商品名「ラポナイトXL21」:フルオロケイ酸(ナトリウム/マグネシウム)(ロックウッド社製)
商品名「ラポナイトXLG」:合成ケイ酸(ナトリウム/マグネシウム)(ロックウッド社製)
商品名「エコーガムT」:キサンタンガム(大日本住友製薬社製)
商品名「PEG#1000」:ポリエチレングリコール、数平均分子量1000(日油社製)
商品名「ノイゲン GIS-125」:イソステアリン酸ポリオキシエチレングリセリル(第一工業製薬社製)
商品名「マクビオブライド MG-10P」:ポリオキシプロピレンメチルグルコシド(日油社製)
下記の表1,2に示す配合成分を配合(配合単位は質量%)し、整髪剤組成物を調製した。
調製直後の整髪剤組成物の粘度を測定した。次いで、各試料を透明ガラス製容器に充填し、50℃の恒温槽で4週間保管後の各試料の外観及び性状を観察し、評価した。次いで粘度を測定し、保管後の粘度値と調製直後の粘度値から粘度上昇率(%)を算出して下記の基準で評価した。
○(かなり良好):粉体の沈降、及び組成物の離水や分離のいずれも認められない
△(良好):粉体の沈降、及び組成物の離水や分離のうちの少なくとも1つの変化が僅かに認められる
×(不良):粉体の沈降、及び組成物の離水や分離のうちの少なくとも1つの変化が明らかに認められる
○(かなり良好):粘度上昇率(%)が、100%以上、150%未満である
△(良好):粘度上昇率(%)が、150%以上、180%未満である
×(不良):粘度上昇率(%)が、180%以上である
専門パネル20名が、プラスチック製容器内に充填した上記整髪剤組成物をウィッグ(レッスンマネキン:ユーカリジャパン社製)の毛髪上に均一に塗布し、髪を根元から立ち上げてまとめるように整髪を施した後、整髪力の有無を回答した。なお、整髪力の評価は、立ち上げた髪の形状がくっきりと保持されている場合を初期整髪力があると判定した。上記回答から、下記の基準で初期整髪力を評価した。
○(かなり良好):20名中16名以上が、初期整髪力があると回答
△(良好):20名中10~15名が、初期整髪力があると回答
×(不良):20名中9名以下が、初期整髪力があると回答
同専門パネル20名が、試験例2の整髪時における延び馴染み、及びべたつきを官能評価して回答した。上記回答から、下記の基準で延び馴染み及びべたつきを評価した。
○(かなり良好):20名中16名以上が、延び馴染みが良いと回答
△(良好):20名中10~15名が、延び馴染みが良いと回答
×(不良):20名中9名以下が、延び馴染みが良いと回答
○(かなり良好):20名中16名以上が、べたつきが無いと回答
△(良好):20名中10~15名が、べたつきが無いと回答
×(不良):20名中9名以下が、べたつきが無いと回答
同専門パネル20名が、上記試験例2(初期整髪力の評価)の1時間経過後に整髪を施したウィッグの毛髪を観察し、整髪保持力の有無を回答した。なお、整髪保持力の評価は、試験例2の立ち上げた髪の形状が保持され続けている場合を整髪保持力があると判定した。上記回答から、下記の基準で整髪保持力を評価した。
○(かなり良好):20名中16名以上が、整髪保持力があると回答
△(良好):20名中10~15名が、整髪保持力があると回答
×(不良):20名中9名以下が、整髪保持力があると回答
同専門パネル20名が、上記試験例4(整髪保持力の評価)の後、指先で毛髪の根元から毛先へ連続して5回コーミングし、フレーキングの有無を回答した。なお、毛髪上に白い粉が付着しているように見える場合に、フレーキングがあると判定した。上記回答から、下記の基準でフレーキングを評価した。
○(かなり良好):20名中16名以上が、フレーキングが無いと回答
△(良好):20名中10~15名が、フレーキングが無いと回答
×(不良):20名中9名以下が、フレーキングが無いと回答
Claims (4)
- 下記成分Aと、下記成分Bと、下記成分Cと、下記成分Dとを含み、
前記成分Aの含有量が0.1質量%以上、10質量%以下であり、前記成分Cの含有量と前記成分Dの含有量との質量比が、2:1~10:1である、整髪剤組成物。
成分A:シリカ、炭酸カルシウム、炭酸マグネシウム、ヒドロキシアパタイト、酸化チタン、酸化亜鉛、ケイ酸カルシウム、ケイ酸マグネシウム、ケイ酸アルミニウム、及び水酸化マグネシウムからなる群より選ばれた粒子
成分B:単糖、二糖、及び糖アルコールからなる群より選ばれた化合物
成分C:粘土鉱物
成分D:多糖系化合物 - 前記成分Cと前記成分Dとの合計の含有量が、0.3質量%以上、5質量%以下である、請求項1に記載の整髪剤組成物。
- さらに、下記成分Eを含む、請求項1又は2に記載の整髪剤組成物。
成分E:ポリエチレングリコール - さらに、下記成分Fを含む、請求項1~3のいずれか1項に記載の整髪剤組成物。
成分F:ポリオキシアルキレンアルキルグルコシド及びポリオキシアルキレングリセリン脂肪酸エステルからなる群より選ばれた化合物
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KR1020167010515A KR20160058178A (ko) | 2014-03-28 | 2014-09-22 | 정발제 조성물 |
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WO2017163656A1 (ja) * | 2016-03-25 | 2017-09-28 | 株式会社マンダム | 整髪剤組成物 |
WO2020175606A1 (ja) * | 2019-02-27 | 2020-09-03 | 株式会社 資生堂 | 皮膚外用剤組成物 |
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CN112569166B (zh) * | 2020-12-15 | 2023-12-15 | 金发拉比妇婴童用品股份有限公司 | 一种温和的洗发水 |
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WO2014157562A1 (ja) * | 2013-03-29 | 2014-10-02 | 株式会社マンダム | 整髪剤組成物 |
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JP5972025B2 (ja) * | 2012-04-25 | 2016-08-17 | 株式会社マンダム | 頭髪用組成物 |
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JP2012025744A (ja) * | 2010-06-25 | 2012-02-09 | Shiseido Co Ltd | 整髪用化粧料 |
JP2012102056A (ja) * | 2010-11-11 | 2012-05-31 | Mandom Corp | ジェル状整髪剤用組成物 |
WO2014157562A1 (ja) * | 2013-03-29 | 2014-10-02 | 株式会社マンダム | 整髪剤組成物 |
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WO2017163656A1 (ja) * | 2016-03-25 | 2017-09-28 | 株式会社マンダム | 整髪剤組成物 |
KR20180026772A (ko) * | 2016-03-25 | 2018-03-13 | 가부시키가이샤 만다무 | 정발제 조성물 |
CN108024918A (zh) * | 2016-03-25 | 2018-05-11 | 株式会社漫丹 | 整发剂组合物 |
JPWO2017163656A1 (ja) * | 2016-03-25 | 2018-06-07 | 株式会社マンダム | 整髪剤組成物 |
KR102033023B1 (ko) | 2016-03-25 | 2019-10-16 | 가부시키가이샤 만다무 | 정발제 조성물 |
WO2020175606A1 (ja) * | 2019-02-27 | 2020-09-03 | 株式会社 資生堂 | 皮膚外用剤組成物 |
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CN105792802A (zh) | 2016-07-20 |
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