WO2010009994A3 - 3-aminomethyl-1-cyclohexylamin und ein verfahren zu dessen herstellung - Google Patents

3-aminomethyl-1-cyclohexylamin und ein verfahren zu dessen herstellung Download PDF

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Publication number
WO2010009994A3
WO2010009994A3 PCT/EP2009/058887 EP2009058887W WO2010009994A3 WO 2010009994 A3 WO2010009994 A3 WO 2010009994A3 EP 2009058887 W EP2009058887 W EP 2009058887W WO 2010009994 A3 WO2010009994 A3 WO 2010009994A3
Authority
WO
WIPO (PCT)
Prior art keywords
cyclohexylamine
aminomethyl
reacting
producing
production
Prior art date
Application number
PCT/EP2009/058887
Other languages
English (en)
French (fr)
Other versions
WO2010009994A2 (de
Inventor
Martin Ernst
Kirsten Dahmen
Alfred Oftring
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Priority to CN2009801291266A priority Critical patent/CN102105434A/zh
Priority to JP2011519115A priority patent/JP2011529027A/ja
Priority to EP09780486A priority patent/EP2310354A2/de
Priority to US13/055,595 priority patent/US20110124919A1/en
Publication of WO2010009994A2 publication Critical patent/WO2010009994A2/de
Publication of WO2010009994A3 publication Critical patent/WO2010009994A3/de

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/33—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings
    • C07C211/34—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings of a saturated carbon skeleton
    • C07C211/36—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings of a saturated carbon skeleton containing at least two amino groups bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/09—Geometrical isomers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)

Abstract

Die vorliegende Erfindung betrifft 3-Aminomethyl-1-cyclohexylamin sowie ein Verfahren zu dessen Herstellung durch a) Umsetzung von Cyclohexenon mit Cyanwasserstoff in Gegenwart eines basischen Katalysators, b) durch Umsetzung des in Stufe a) erhaltenen Cyclohexanonnitrils mit Ammoniak in Gegenwart eines Iminbildungskatalysators, und c) Umsetzung des in Stufe b) erhaltenen 3-Cyanocyclohexylimin-haltigen Reaktionsgemisches mit Wasserstoff und Ammoniak an Hydrierkatalysatoren. Die vorliegende Erfindung betrifft weiterhin die Verwendung von 3-Aminomethyl-1-cyclohexylamin als Härter für Epoxyharze, als Zwischenprodukt bei der Herstellung von Diisocyanaten, als Starter bei der Herstellung von Polyetherolen und/oder als Monomer für die Polyamidherstellung.
PCT/EP2009/058887 2008-07-25 2009-07-13 3-aminomethyl-1-cyclohexylamin und ein verfahren zu dessen herstellung WO2010009994A2 (de)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN2009801291266A CN102105434A (zh) 2008-07-25 2009-07-13 3-氨基甲基-1-环己基胺及其生产方法
JP2011519115A JP2011529027A (ja) 2008-07-25 2009-07-13 ３−アミノメチル−１−シクロヘキシルアミン、及びその製造方法
EP09780486A EP2310354A2 (de) 2008-07-25 2009-07-13 3-aminomethyl-1-cyclohexylamin und ein verfahren zu dessen herstellung
US13/055,595 US20110124919A1 (en) 2008-07-25 2009-07-13 3-aminomethyl-1-cyclohexylamine, and method for the production thereof

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP08161177 2008-07-25
EP08161177.4 2008-07-25

Publications (2)

Publication Number Publication Date
WO2010009994A2 WO2010009994A2 (de) 2010-01-28
WO2010009994A3 true WO2010009994A3 (de) 2010-03-25

Family

ID=41347863

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2009/058887 WO2010009994A2 (de) 2008-07-25 2009-07-13 3-aminomethyl-1-cyclohexylamin und ein verfahren zu dessen herstellung

Country Status (5)

Country Link
US (1) US20110124919A1 (de)
EP (1) EP2310354A2 (de)
JP (1) JP2011529027A (de)
CN (1) CN102105434A (de)
WO (1) WO2010009994A2 (de)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5689078B2 (ja) 2009-03-12 2015-03-25 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ １−アダマンチルトリメチルアンモニウム水酸化物の製造方法
JP5706415B2 (ja) * 2009-07-31 2015-04-22 ダウ グローバル テクノロジーズ エルエルシー 脂肪族シアノアルデヒドの脂肪族ジアミンへの還元的アミノ化のための方法
WO2012007748A1 (en) 2010-07-13 2012-01-19 Astrazeneca Ab New crystalline forms of n-[2-[[(2,3-difluoropheny)methyl)thio]-6-{[(1r,2s)-2,3-dihydroxy-1- methylpropyl]oxy}-4-pyrimidinyl]-1-azetidinesulfonamide
WO2013008002A1 (en) 2011-07-12 2013-01-17 Astrazeneca Ab N- (6- ( (2r,3s) -3,4-dihydroxybutan-2-yloxy) -2- (4 - fluorobenzylthio) pyrimidin- 4 - yl) -3- methylazetidine- 1 - sulfonamide as chemokine receptor modulator
EP2951154B1 (de) * 2013-01-30 2017-04-19 Basf Se 2,6-bis-(aminomethyl)piperidin- (2,6-bamp-), 2,6-bis-(isocyanomethyl)piperidin- (diisocyanat-) und 2,6-dicyanopiperidin-derivate (2,6-dcp-derivate) und ihre verwendung in der herstellung von epoxyharzen, polyurethanen, polyetherolen und polyamiden
ES2864167T3 (es) * 2015-03-09 2021-10-13 Mitsubishi Gas Chemical Co Método de isomerización de diaminodiciclohexilmetano
CN104974045B (zh) * 2015-05-26 2018-03-20 岳阳昌德化工实业有限公司 一种制备胺类化合物的方法
EP3255032B1 (de) 2016-06-10 2018-09-05 Evonik Degussa GmbH 2-(3-(aminomethyl)-3,5,5-trimethylcyclohexyl)propan-1,3-diamin, ein verfahren zur herstellung und verwendung
CN109761855B (zh) 2018-12-20 2020-07-28 万华化学集团股份有限公司 一种制备异佛尔酮二异氰酸酯的方法
CN115073319B (zh) * 2022-06-28 2024-06-25 万华化学集团股份有限公司 一种脂环胺同分异构体的改性分离方法

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0128382A1 (de) * 1983-05-17 1984-12-19 BASF Aktiengesellschaft 1-Alkyl-2-isocyanatomethyl-isocyanato-cyclohexane und/oder 1-Alkyl-4-isocyanatomethyl-isocyanato-cyclohexane sowie die entsprechenden Diamine, Verfahren zu deren Herstellung und Verwendung
EP0394058A1 (de) * 1989-04-21 1990-10-24 MITSUI TOATSU CHEMICALS, Inc. Alicyclische Diamine, alicyclische Diisocyanate und Polyisocyanatisocyanurate sowie Verfahren zu ihrer Herstellung
JPH04145121A (ja) * 1990-10-08 1992-05-19 Mitsui Toatsu Chem Inc エポキシ樹脂組成物
DE4115948A1 (de) * 1991-05-16 1992-11-19 Basf Lacke & Farben Ueberzugsmasse, verfahren zur herstellung von ueberzuegen und beschichtetes substrat
DE4210311A1 (de) * 1992-03-30 1993-10-07 Degussa Verfahren zur Herstellung von Aminen aus Azinen
EP0895984A1 (de) * 1997-01-24 1999-02-10 Daicel Chemical Industries, Ltd. Alizyklische polyamine und verfahren zu ihrer herstellung
DE19836474A1 (de) * 1998-08-12 2000-02-17 Basf Ag Verfahren zur Herstellung von 3-Cyano-3,5,5-trimethyl-cyclohexanon
WO2004056753A1 (de) * 2002-12-19 2004-07-08 Basf Aktiengesellschaft Verbesserte neutralisation von isophoronnitril-syntheseausträgen
US20090192283A1 (en) * 2008-01-25 2009-07-30 Great Eastern Resins Industrial Co., Ltd. Process for preparing high performance waterborne aliphatic-aromatic mixed polyurethanes

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2825603B2 (ja) * 1989-04-21 1998-11-18 三井化学株式会社 アルキルジアミン類およびその製造法
DE4010227A1 (de) * 1990-03-30 1991-10-02 Basf Ag Verfahren zur herstellung von 3-aminomethyl-3,5,5-trimethyl-cyclohexylamin
DE4325847A1 (de) * 1993-07-31 1995-02-02 Basf Ag Kobaltkatalysatoren
DE4428004A1 (de) * 1994-08-08 1996-02-15 Basf Ag Verfahren zur Herstellung von Aminen
ES2169169T3 (es) * 1995-05-09 2002-07-01 Basf Ag Catalizadores de cobalto.
WO2008077852A1 (de) * 2006-12-22 2008-07-03 Basf Se Kontinuierliches verfahren zur hydrierung von 3-cyano-3,5,5-trimethyl-cyclohexylimin

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0128382A1 (de) * 1983-05-17 1984-12-19 BASF Aktiengesellschaft 1-Alkyl-2-isocyanatomethyl-isocyanato-cyclohexane und/oder 1-Alkyl-4-isocyanatomethyl-isocyanato-cyclohexane sowie die entsprechenden Diamine, Verfahren zu deren Herstellung und Verwendung
EP0394058A1 (de) * 1989-04-21 1990-10-24 MITSUI TOATSU CHEMICALS, Inc. Alicyclische Diamine, alicyclische Diisocyanate und Polyisocyanatisocyanurate sowie Verfahren zu ihrer Herstellung
JPH04145121A (ja) * 1990-10-08 1992-05-19 Mitsui Toatsu Chem Inc エポキシ樹脂組成物
DE4115948A1 (de) * 1991-05-16 1992-11-19 Basf Lacke & Farben Ueberzugsmasse, verfahren zur herstellung von ueberzuegen und beschichtetes substrat
DE4210311A1 (de) * 1992-03-30 1993-10-07 Degussa Verfahren zur Herstellung von Aminen aus Azinen
EP0895984A1 (de) * 1997-01-24 1999-02-10 Daicel Chemical Industries, Ltd. Alizyklische polyamine und verfahren zu ihrer herstellung
DE19836474A1 (de) * 1998-08-12 2000-02-17 Basf Ag Verfahren zur Herstellung von 3-Cyano-3,5,5-trimethyl-cyclohexanon
WO2004056753A1 (de) * 2002-12-19 2004-07-08 Basf Aktiengesellschaft Verbesserte neutralisation von isophoronnitril-syntheseausträgen
US20090192283A1 (en) * 2008-01-25 2009-07-30 Great Eastern Resins Industrial Co., Ltd. Process for preparing high performance waterborne aliphatic-aromatic mixed polyurethanes

Also Published As

Publication number Publication date
EP2310354A2 (de) 2011-04-20
WO2010009994A2 (de) 2010-01-28
JP2011529027A (ja) 2011-12-01
CN102105434A (zh) 2011-06-22
US20110124919A1 (en) 2011-05-26

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