WO2006135439A3 - Improved ozonolysis of carbon nanotubes - Google Patents

Improved ozonolysis of carbon nanotubes Download PDF

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Publication number
WO2006135439A3
WO2006135439A3 PCT/US2005/038116 US2005038116W WO2006135439A3 WO 2006135439 A3 WO2006135439 A3 WO 2006135439A3 US 2005038116 W US2005038116 W US 2005038116W WO 2006135439 A3 WO2006135439 A3 WO 2006135439A3
Authority
WO
WIPO (PCT)
Prior art keywords
carbon
carbon nanotubes
ozone
structures
nanotubes
Prior art date
Application number
PCT/US2005/038116
Other languages
French (fr)
Other versions
WO2006135439A2 (en
Inventor
Jun Ma
Asif Chishti
Lein Ngaw
Allen Fischer
Robert Braden
Original Assignee
Hyperion Catalysis Int
Jun Ma
Asif Chishti
Lein Ngaw
Allen Fischer
Robert Braden
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hyperion Catalysis Int, Jun Ma, Asif Chishti, Lein Ngaw, Allen Fischer, Robert Braden filed Critical Hyperion Catalysis Int
Priority to AU2005332975A priority Critical patent/AU2005332975B2/en
Priority to CA002584433A priority patent/CA2584433A1/en
Priority to JP2007538119A priority patent/JP2008517863A/en
Priority to MX2007004684A priority patent/MX2007004684A/en
Priority to EP05858262A priority patent/EP1817447A4/en
Publication of WO2006135439A2 publication Critical patent/WO2006135439A2/en
Publication of WO2006135439A3 publication Critical patent/WO2006135439A3/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82BNANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00Manufacture or treatment of nanostructures
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/158Carbon nanotubes
    • C01B32/168After-treatment
    • C01B32/174Derivatisation; Solubilisation; Dispersion in solvents
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C27/00Processes involving the simultaneous production of more than one class of oxygen-containing compounds
    • C07C27/04Processes involving the simultaneous production of more than one class of oxygen-containing compounds by reduction of oxygen-containing compounds
    • C07C27/06Processes involving the simultaneous production of more than one class of oxygen-containing compounds by reduction of oxygen-containing compounds by hydrogenation of oxides of carbon
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
    • H01G11/00Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/22Electrodes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
    • H01G11/00Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/22Electrodes
    • H01G11/30Electrodes characterised by their material
    • H01G11/32Carbon-based
    • H01G11/34Carbon-based characterised by carbonisation or activation of carbon
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
    • H01G11/00Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/22Electrodes
    • H01G11/30Electrodes characterised by their material
    • H01G11/32Carbon-based
    • H01G11/36Nanostructures, e.g. nanofibres, nanotubes or fullerenes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00Structure or properties of carbon nanotubes
    • C01B2202/02Single-walled nanotubes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00Structure or properties of carbon nanotubes
    • C01B2202/06Multi-walled nanotubes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00Structure or properties of carbon nanotubes
    • C01B2202/20Nanotubes characterized by their properties
    • C01B2202/36Diameter
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/13Energy storage using capacitors

Abstract

Methods of treating single walled and multiwalled carbon nanotubes with ozone are provided. The carbon nanotubes are treated by contacting the carbon nanotubes with ozone at a temperature range between 0°C and 100°C to yield functionalized nanotubes which are greater in weight than the untreated carbon nonotubes. The carbon nonotubes treated according to methods of the invention can be used to prepare complex structures such as three dimensional networks or rigid porous structures which can be utilized to form electordes for fabrication of improved electrochemical capacitors. Useful catalyst supports are prepared by contacting carbon nanotube structures such as carbon nanotube aggregates, three dimensional network or rigid porous structures with ozone in the temperature range between 0°C and 100°C.
PCT/US2005/038116 2004-10-22 2005-10-21 Improved ozonolysis of carbon nanotubes WO2006135439A2 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
AU2005332975A AU2005332975B2 (en) 2004-10-22 2005-10-21 Improved ozonolysis of carbon nanotubes
CA002584433A CA2584433A1 (en) 2004-10-22 2005-10-21 Improved ozonolysis of carbon nanotubes
JP2007538119A JP2008517863A (en) 2004-10-22 2005-10-21 Improved ozonolysis of carbon nanotubes
MX2007004684A MX2007004684A (en) 2004-10-22 2005-10-21 Improved ozonolysis of carbon nanotubes.
EP05858262A EP1817447A4 (en) 2004-10-22 2005-10-21 Improved ozonolysis of carbon nanotubes

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US62113204P 2004-10-22 2004-10-22
US60/621,132 2004-10-22
US72080605P 2005-09-26 2005-09-26
US60/720,806 2005-09-26

Publications (2)

Publication Number Publication Date
WO2006135439A2 WO2006135439A2 (en) 2006-12-21
WO2006135439A3 true WO2006135439A3 (en) 2007-05-24

Family

ID=37532751

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2005/038116 WO2006135439A2 (en) 2004-10-22 2005-10-21 Improved ozonolysis of carbon nanotubes

Country Status (8)

Country Link
US (1) US20080031802A1 (en)
EP (1) EP1817447A4 (en)
JP (1) JP2008517863A (en)
KR (1) KR20070084288A (en)
AU (1) AU2005332975B2 (en)
CA (1) CA2584433A1 (en)
MX (1) MX2007004684A (en)
WO (1) WO2006135439A2 (en)

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US8901024B2 (en) * 2007-08-02 2014-12-02 The Trustees Of Columbia University In The City Of New York Ozone-treated carbon electrodes
EP2062853A1 (en) * 2007-11-23 2009-05-27 Nanoledge Polymer carbon nanotube composites
KR101685210B1 (en) * 2008-03-25 2016-12-09 도레이 카부시키가이샤 Electrically conductive complex and process for production thereof
KR101034579B1 (en) * 2008-03-28 2011-05-12 한화케미칼 주식회사 Continuous methods and apparatus of functionalizing Carbon Nanotube
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CN102171870A (en) * 2008-08-15 2011-08-31 麻省理工学院 Layer-by-layer assemblies of carbon-based nanostructures and their applications in energy storage and generation devices
EP2228343A1 (en) 2009-03-13 2010-09-15 Bayer MaterialScience AG Water vapour assisted ozonolysis of carbon nanotubes
EP2228414A1 (en) * 2009-03-13 2010-09-15 Bayer MaterialScience AG UV-curable, wear resistant and antistatic coating filled with carbon nanotubes
JP6169973B2 (en) * 2010-12-14 2017-07-26 モレキュラー レバー デザイン エルエルシー Improved elastomer formulation
JP6004198B2 (en) * 2011-05-25 2016-10-05 パナソニックIpマネジメント株式会社 Electrode, manufacturing method thereof, energy device including the same, electronic apparatus and transport device
JP6241586B2 (en) 2011-09-30 2017-12-06 三菱マテリアル株式会社 Method for producing carbon nanofiber and method for producing dispersion and composition thereof
CN105829276B (en) 2013-11-05 2018-06-19 加利福尼亚大学董事会 graphene oxide and carbon nanotube ink and preparation method thereof
JP2015188808A (en) * 2014-03-27 2015-11-02 日本ゼオン株式会社 Oxidation-reduction catalyst, electrode material, electrode, solar battery, membrane battery assembly for fuel battery, and fuel battery
JP6340077B2 (en) * 2014-06-26 2018-06-06 国立大学法人 奈良先端科学技術大学院大学 Method for producing nanomaterial-dopant composition composite, nanomaterial-dopant composition composite, and dopant composition
JP6642447B2 (en) 2014-11-14 2020-02-05 戸田工業株式会社 Carbon nanotube, method for producing the same, and lithium ion secondary battery using carbon nanotube
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KR101885249B1 (en) * 2016-07-19 2018-08-03 한국과학기술원 Method of preparing activated carbon
US11019734B1 (en) * 2019-10-30 2021-05-25 Tula Health, Inc. Methods and systems for fabricating miniaturized nanotube sensors
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Also Published As

Publication number Publication date
MX2007004684A (en) 2007-06-14
CA2584433A1 (en) 2006-12-21
JP2008517863A (en) 2008-05-29
EP1817447A2 (en) 2007-08-15
AU2005332975B2 (en) 2010-12-09
KR20070084288A (en) 2007-08-24
AU2005332975A1 (en) 2006-12-21
US20080031802A1 (en) 2008-02-07
EP1817447A4 (en) 2012-01-25
WO2006135439A2 (en) 2006-12-21

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