WO2004038729A1 - Brennstoffpellet für einen kernreaktor und verfahren zu seiner herstellung - Google Patents
Brennstoffpellet für einen kernreaktor und verfahren zu seiner herstellung Download PDFInfo
- Publication number
- WO2004038729A1 WO2004038729A1 PCT/EP2003/011594 EP0311594W WO2004038729A1 WO 2004038729 A1 WO2004038729 A1 WO 2004038729A1 EP 0311594 W EP0311594 W EP 0311594W WO 2004038729 A1 WO2004038729 A1 WO 2004038729A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- fuel
- metallic phase
- green compacts
- pellet
- metal
- Prior art date
Links
Classifications
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21C—NUCLEAR REACTORS
- G21C3/00—Reactor fuel elements and their assemblies; Selection of substances for use as reactor fuel elements
- G21C3/42—Selection of substances for use as reactor fuel
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21C—NUCLEAR REACTORS
- G21C3/00—Reactor fuel elements and their assemblies; Selection of substances for use as reactor fuel elements
- G21C3/42—Selection of substances for use as reactor fuel
- G21C3/58—Solid reactor fuel Pellets made of fissile material
- G21C3/62—Ceramic fuel
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21C—NUCLEAR REACTORS
- G21C3/00—Reactor fuel elements and their assemblies; Selection of substances for use as reactor fuel elements
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E30/00—Energy generation of nuclear origin
- Y02E30/30—Nuclear fission reactors
Definitions
- the invention relates to a fuel pellet for light water reactors and a method for producing fuel pellets.
- a light water reactor be it a pressurized water or boiling water reactor
- the fuel pellets are arranged in cladding tubes. Fission gases are formed during reactor operation, which are initially retained in the fuel pellets, but later diffuse over the outer surface of the pellets into the gap between the pellet and the cladding tube.
- the cladding tubes must therefore be tightly sealed so that the fission gases cannot escape to the outside.
- an increase in rod output and burn-up is aimed for. However, this is associated with an increased release of cracked gas, which can limit combustion.
- the retention capacity for fission gases is increased if the pellets have the largest possible sintered grains.
- the starting materials can be a substance that promotes grain growth, such as Fe 2 0 3 , Cr 2 0 3 , Ti0 2 , JNb 2 0 5 , Al 2 0 3 etc. be added.
- the release of cracked gas can be further reduced with pellets that contain metallic waste.
- the metallic precipitates have a much higher thermal conductivity than the oxidic matrix of the pellets.
- the resulting improved heat dissipation results in a reduction in the temperature gradient between the core of the pellet and its outer surface and a lowering in the central temperature of the fuel pellet. A lower central temperature decreases the mobility of the cracked gases in the fuel and thus reduces their release rate.
- Fuel pellets are known from EP 0 701 734 B1, in whose oxidic matrix a metal is dispersed. The metal is said to serve to trap oxygen generated during nuclear fission.
- the object of the invention is to propose a fuel pellet with increased retention capacity for fission gases and a method for its production.
- this object is achieved in that a preferably radially oriented metallic phase is precipitated or present in the oxidic matrix.
- the excretions preferably extend in the direction of heat flow from the center of the pellet to its outer surface, and less in the axial direction, in which no heat exchange takes place due to the lack of a temperature gradient.
- the heat removal from the pellet is greater in the anisotropy according to the invention than in the case of isotropic distribution.
- a thermal conductivity in the radial direction comparable to a pellet according to the invention in the case of pellets with an isotropic distribution of the metal excretions, it can be achieved by an increased metal content.
- a preferred fuel pellet contains a metallic phase with 0.1 to 6% by weight, preferably with more than 2% by weight.
- the idea according to the invention is applicable to any nuclear fuel, for example based on U0 2 ⁇ x , UPu0 2 ⁇ x , UGd0 2 ⁇ x or U.Th0 2 ⁇ ⁇ .
- At least one metal from the group Ti, Cr, Nb, Mo, Wo and / or an alloy based on at least one of these metals is preferably used as the metallic phase.
- the invention is achieved in that green compacts are produced which, in addition to the oxidic nuclear fuel and possibly further additives, contain a precursor of the metallic phase which has a melting point below the sintering temperature and which, under sintering conditions, contains the metallic phase is convertible, the green compacts being sintered in such a way that they are heated to the sintering temperature so quickly that at least part of the precursor has melted before it has completely converted into the metallic phase, which is solid at the prevailing temperatures.
- pellets are obtained in which a metallic phase is deposited intra and / or intergranularly and is preferably oriented radially.
- This anisotropy of the metallic phase comes about as follows:
- the pressing together of the powdery or granular Ganges are mixed in a conventional manner in a cylindrical die into which a stamp is pressed, ie the starting mixture is practically compressed only in the axial direction.
- cavities and pores contained therein are compressed at least to a certain extent in the axial direction, their original extent in the radial direction being retained or increasing.
- Pellets produced in this way therefore naturally contain pores or cavities which preferably extend in the radial direction.
- the invention is based on the idea of filling these cavities, which are already radially oriented, with a largely coherent metallic phase and thereby increasing the thermal conductivity of the pellet in the direction mentioned.
- the molten phase resulting from a particle of the precursor can flow into cavities in the pellet and combine with the molten phase of neighboring precursor particles to form larger, coherent areas.
- the pellet known from EP 0 701 734 B1 aims to distribute as many uniformly as possible many small metal particles with the largest possible effective surface area in order to enable the reaction with the cracked gas oxygen.
- At least the nuclear fuel is granulated and the precursor of the metallic phase is only added after the granulation step.
- the anisotropy of the metallic phase in the radial direction can be increased further.
- particles of the starting powder are agglomerated in a granulate.
- the cohesion of the powder particles in a granulate is now not so great that it can withstand the pressure when pressing a green compact.
- the granules are therefore compressed and flattened during the pressing process. Accordingly, the grain boundaries between the granules run after the pressing process to a greater extent in the radial direction than in the axial direction.
- the preliminary stage of the metallic phase is not added to the fuel powder but to the granulate produced therefrom, the granules are virtually enveloped by the preliminary stage. Accordingly, the preliminary stage of the metallic phase after the pressing is arranged in the grain boundaries which run predominantly in the radial direction. When the preliminary stage melts during heating, coherent metallic areas are formed in the grain boundaries, which increase the radial thermal conductivity.
- a metal oxide is used as the preliminary stage, the melting point of which is below the sintering temperature, sintering under reducing conditions and the heating being carried out so quickly that at least part of the metal oxide melts before it is reduced to metal.
- Metal oxides that have these properties are, for example, Mo0 2 and Mo0 3 .
- a metal oxide is also used as a precursor, but first sintering at a lower presintering temperature and oxidizing conditions until at least part of the metal oxide has melted, with reducing conditions and a higher temperature, ie at least towards the end of the terns the required sintering temperature. Because of its two stages, this process is associated with a greater technical outlay, but it has the advantage that not just a part but the entire amount of metal oxide added can be melted before the Reduction to metal. In this way, particularly large coherent and radially aligned metallic areas can be produced in a pellet, especially if the precursor is added to the granulate. Mo0 2 and Mo0 3 are also suitable as metal oxide here.
- Example 1 U0 2 78.85% by weight U 3 0 8 15.36% by weight Mo0 2 5.79% by weight
- Example 3 U0 2 92.2% by weight U 3 0 8 5.16% by weight Mo0 2 2.65% by weight
- a homogenized uranium oxide starting mixture is gem.
- Example 1, 2 or 3 provided.
- the next step is granulation, in which the starting mixture is compressed and then pressed through a sieve with a sieve size of, for example, 14 mesh. Granules with an average diameter of about 1 mm result. Mo0 2 or Mo0 3 is now added to the granules. It is also conceivable to add the molybdenum oxide to the fuel powder. If necessary, pressing aids and / or doping agents can be added to this basic mixture before or after the granulation step. The granules obtained in each case are pressed into green compacts and these are sintered.
- the green compacts are sintered in a sintering furnace at temperatures around 1600 ° - 1850 ° C under reducing conditions.
- the heating is controlled in such a way that the melting temperature of Mo0 3 (795 ° C) is reached as quickly as possible so that the proportion (not liquefiable) reduced to molybdenum remains as low as possible. Good results are achieved with heating rates of 10 to 20 ° C / min. receive.
- the reducing conditions will be guaranteed by an atmosphere containing H 2 .
- further gases such as CO 2 , H 2 O (steam), N or argon can be added individually or in any mixture to this H 2 atmosphere.
- disproportionation into metallic molybdenum and Mo0 3 takes place first.
- the green compacts are sintered in a two-stage process.
- the green compacts are treated at a presintering temperature of around 800 to 1300 ° C in an oxidizing atmosphere (for example technical C0 2 ). Since there is no fear of a reduction in the molybdenum oxide, the heat treatment can be carried out until all of the molybdenum oxide has melted.
- reducing conditions are set. For example, a sintering furnace can be used for this purpose, which has different zones with different atmospheres.
- the green compacts are now sintered at a sintering temperature between 1100 ° C - 1850 ° C.
- uranium oxide oxidized in the first process step is reduced again to such an extent that a stoichiometric U / O ratio of 1/2 is established.
- the attached diagram shows the results of measurements made on pellets with a composition according to Examples 1 and 2 above.
- the molybdenum oxide amount of 5.8% and 6.5% contained in the starting mixtures corresponds to a content of 4.4% molybdenum in the pellets.
- the diagram clearly shows that all pellets have a thermal conductivity that is above the calculated thermal conductivity of U0 2 pellets with isotropically distributed, spherical Mo precipitates (lower dashed curve).
- the diagram shows that adding the molybdenum oxide to the granules gives better results than adding it to the powder. The influence of the sintering atmosphere on the thermal conductivity is less pronounced.
Landscapes
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- General Engineering & Computer Science (AREA)
- High Energy & Nuclear Physics (AREA)
- Chemical & Material Sciences (AREA)
- Ceramic Engineering (AREA)
- Powder Metallurgy (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Monitoring And Testing Of Nuclear Reactors (AREA)
- Inert Electrodes (AREA)
- Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
Abstract
Description
Claims
Priority Applications (7)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE50306979T DE50306979D1 (de) | 2002-10-23 | 2003-10-20 | Brennstoffpellet für einen kernreaktor und verfahren zu seiner herstellung |
EP03758024A EP1554733B1 (de) | 2002-10-23 | 2003-10-20 | Brennstoffpellet für einen kernreaktor und verfahren zu seiner herstellung |
JP2004545898A JP4326473B2 (ja) | 2002-10-23 | 2003-10-20 | 原子炉用燃料ペレット及びその製造方法 |
AU2003274046A AU2003274046A1 (en) | 2002-10-23 | 2003-10-20 | Fuel pellet for a nuclear reactor and method for the production thereof |
ZA2005/02296A ZA200502296B (en) | 2002-10-23 | 2005-03-18 | Fuel pellet for a nuclear reactor and method for the production thereof |
US11/113,746 US20050195933A1 (en) | 2002-10-23 | 2005-04-25 | Fuel pellet for a nuclear reactor and method for producing the fuel pellet |
US12/333,723 US20090252279A1 (en) | 2002-10-23 | 2008-12-12 | Fuel Pellet for a Nuclear Reactor and Method for Producing Fuel Pellet |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10249355A DE10249355B4 (de) | 2002-10-23 | 2002-10-23 | Brennstoffpellet für einen Kernreaktor und Verfahren zu seiner Herstellung |
DE10249355.3 | 2002-10-23 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US11/113,746 Continuation US20050195933A1 (en) | 2002-10-23 | 2005-04-25 | Fuel pellet for a nuclear reactor and method for producing the fuel pellet |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2004038729A1 true WO2004038729A1 (de) | 2004-05-06 |
Family
ID=32102902
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2003/011594 WO2004038729A1 (de) | 2002-10-23 | 2003-10-20 | Brennstoffpellet für einen kernreaktor und verfahren zu seiner herstellung |
Country Status (10)
Country | Link |
---|---|
US (2) | US20050195933A1 (de) |
EP (1) | EP1554733B1 (de) |
JP (1) | JP4326473B2 (de) |
KR (1) | KR100783986B1 (de) |
AT (1) | ATE358877T1 (de) |
AU (1) | AU2003274046A1 (de) |
DE (2) | DE10249355B4 (de) |
ES (1) | ES2283816T3 (de) |
WO (1) | WO2004038729A1 (de) |
ZA (1) | ZA200502296B (de) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2014133656A2 (en) * | 2013-01-18 | 2014-09-04 | Westinghouse Electric Company Llc | Laser sintering systems and methods for remote manufacture of high density pellets containing highly radioactive elements |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4674312B2 (ja) * | 2007-08-29 | 2011-04-20 | 独立行政法人 日本原子力研究開発機構 | 核燃料ペレットの製造方法および核燃料ペレット |
US9941025B2 (en) * | 2011-04-08 | 2018-04-10 | Terrapower, Llc | Nuclear fuel and method of fabricating the same |
JP5888781B2 (ja) * | 2011-11-14 | 2016-03-22 | 国立研究開発法人日本原子力研究開発機構 | 放射性モリブデンの作製方法 |
US10790065B2 (en) | 2012-08-15 | 2020-09-29 | University Of Florida Research Foundation, Inc. | High density UO2 and high thermal conductivity UO2 composites by spark plasma sintering (SPS) |
FR2997786B1 (fr) * | 2012-11-08 | 2018-12-07 | Commissariat A L'energie Atomique Et Aux Energies Alternatives | Combustible nucleaire oxyde regulateur des produits de fissions corrosifs additive par au moins un systeme oxydo-reducteur |
CN108028080A (zh) | 2015-07-25 | 2018-05-11 | 奥卓安全核能公司 | 全陶瓷微封装核燃料的制造方法 |
CA3017939A1 (en) | 2016-03-29 | 2017-10-05 | Ultra Safe Nuclear Corporation | Fully ceramic microencapsulated fuel fabricated with burnable poison as sintering aid |
EP3437106B1 (de) | 2016-03-29 | 2021-03-17 | Ultra Safe Nuclear Corporation | Zähigkeitsverbesserung bei mikroverkapseltem kernbrennstoff |
KR102626243B1 (ko) | 2016-03-29 | 2024-01-18 | 울트라 세이프 뉴클리어 코포레이션 | SiC 및 흑연 매트릭스 TRISO-포함 페블 연료의 신속한 처리를 위한 공정 |
KR102084466B1 (ko) | 2018-02-13 | 2020-03-04 | 한국원자력연구원 | 열전도도가 향상된 핵연료 소결체 및 이의 제조방법 |
KR102148779B1 (ko) * | 2019-12-30 | 2020-08-27 | 한전원자력연료 주식회사 | 미세한 석출물이 원주방향으로 분산된 산화물 핵연료 소결체 및 이의 제조방법 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1511075A (fr) * | 1966-12-14 | 1968-01-26 | Commissariat Energie Atomique | élément combustible et son procédé de fabrication |
US3409504A (en) * | 1966-02-02 | 1968-11-05 | Commissariat Energie Atomique | Nuclear fuel element |
US3845177A (en) * | 1971-12-13 | 1974-10-29 | Atomic Energy Authority Uk | Coated particle oxide fuel for nuclear reactors |
US4460522A (en) * | 1982-09-14 | 1984-07-17 | Doryokuro Kakunenryo Kaihatsu Jigyodan | Method of producing low density oxide fuel pellet |
US5999585A (en) * | 1993-06-04 | 1999-12-07 | Commissariat A L'energie Atomique | Nuclear fuel having improved fission product retention properties |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
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US2236943A (en) * | 1939-12-14 | 1941-04-01 | Robert O Friend | Fluid distributor |
GB933984A (en) * | 1961-05-25 | 1963-08-14 | Atomic Energy Authority Uk | Improvements in or relating to nuclear fuels |
US3365371A (en) * | 1966-10-14 | 1968-01-23 | Gen Electric | Nuclear reactor fuel pellet |
US4111748A (en) * | 1975-06-18 | 1978-09-05 | Doryokuro Kakunenryo Kaihatsu Jigyodan | Nuclear fuel rod with stress relieving device |
US4236943A (en) * | 1978-06-22 | 1980-12-02 | The United States Of America As Represented By The United States Department Of Energy | Precipitation hardenable iron-nickel-chromium alloy having good swelling resistance and low neutron absorbence |
US5180527A (en) * | 1990-04-03 | 1993-01-19 | Nippon Nuclear Fuel Development Co., Ltd. | Nuclear fuel pellets |
DE19627806A1 (de) * | 1996-07-11 | 1998-01-15 | Siemens Ag | Kernbrennstoffsinterkörper und Verfahren zum Herstellen eines Kernbrennstoffsinterkörpers |
DE19934516A1 (de) * | 1999-07-22 | 2001-01-25 | Siemens Ag | Sinterkörper und seine Verwendung in einem Brennstab, Brutstab oder Absorberstab für einen Kernreaktor |
FR2817385B1 (fr) * | 2000-11-30 | 2005-10-07 | Framatome Anp | Pastille de combustible nucleaire oxyde et crayon comportant un empilement de telles pastilles |
-
2002
- 2002-10-23 DE DE10249355A patent/DE10249355B4/de not_active Expired - Fee Related
-
2003
- 2003-10-20 ES ES03758024T patent/ES2283816T3/es not_active Expired - Lifetime
- 2003-10-20 JP JP2004545898A patent/JP4326473B2/ja not_active Expired - Fee Related
- 2003-10-20 KR KR1020057006859A patent/KR100783986B1/ko not_active IP Right Cessation
- 2003-10-20 WO PCT/EP2003/011594 patent/WO2004038729A1/de active IP Right Grant
- 2003-10-20 AU AU2003274046A patent/AU2003274046A1/en not_active Abandoned
- 2003-10-20 DE DE50306979T patent/DE50306979D1/de not_active Expired - Lifetime
- 2003-10-20 EP EP03758024A patent/EP1554733B1/de not_active Expired - Lifetime
- 2003-10-20 AT AT03758024T patent/ATE358877T1/de not_active IP Right Cessation
-
2005
- 2005-03-18 ZA ZA2005/02296A patent/ZA200502296B/en unknown
- 2005-04-25 US US11/113,746 patent/US20050195933A1/en not_active Abandoned
-
2008
- 2008-12-12 US US12/333,723 patent/US20090252279A1/en not_active Abandoned
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3409504A (en) * | 1966-02-02 | 1968-11-05 | Commissariat Energie Atomique | Nuclear fuel element |
FR1511075A (fr) * | 1966-12-14 | 1968-01-26 | Commissariat Energie Atomique | élément combustible et son procédé de fabrication |
US3845177A (en) * | 1971-12-13 | 1974-10-29 | Atomic Energy Authority Uk | Coated particle oxide fuel for nuclear reactors |
US4460522A (en) * | 1982-09-14 | 1984-07-17 | Doryokuro Kakunenryo Kaihatsu Jigyodan | Method of producing low density oxide fuel pellet |
US5999585A (en) * | 1993-06-04 | 1999-12-07 | Commissariat A L'energie Atomique | Nuclear fuel having improved fission product retention properties |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2014133656A2 (en) * | 2013-01-18 | 2014-09-04 | Westinghouse Electric Company Llc | Laser sintering systems and methods for remote manufacture of high density pellets containing highly radioactive elements |
WO2014133656A3 (en) * | 2013-01-18 | 2014-11-27 | Westinghouse Electric Company Llc | Laser sintering systems and methods for remote manufacture of high density pellets containing highly radioactive elements |
CN104919536A (zh) * | 2013-01-18 | 2015-09-16 | 西屋电气有限责任公司 | 用于远程制造含有高度放射性元素的高密度芯块的激光烧结***和方法 |
US9646729B2 (en) | 2013-01-18 | 2017-05-09 | Westinghouse Electric Company Llc | Laser sintering systems and methods for remote manufacture of high density pellets containing highly radioactive elements |
Also Published As
Publication number | Publication date |
---|---|
JP2006504086A (ja) | 2006-02-02 |
DE10249355A1 (de) | 2004-05-13 |
ZA200502296B (en) | 2005-10-26 |
US20090252279A1 (en) | 2009-10-08 |
KR20050059282A (ko) | 2005-06-17 |
DE50306979D1 (de) | 2007-05-16 |
DE10249355B4 (de) | 2005-08-04 |
EP1554733B1 (de) | 2007-04-04 |
US20050195933A1 (en) | 2005-09-08 |
KR100783986B1 (ko) | 2007-12-11 |
EP1554733A1 (de) | 2005-07-20 |
JP4326473B2 (ja) | 2009-09-09 |
ATE358877T1 (de) | 2007-04-15 |
ES2283816T3 (es) | 2007-11-01 |
AU2003274046A1 (en) | 2004-05-13 |
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