WO2004002612A1 - Vorrichtung zur querstromfiltration - Google Patents
Vorrichtung zur querstromfiltration Download PDFInfo
- Publication number
- WO2004002612A1 WO2004002612A1 PCT/CH2003/000391 CH0300391W WO2004002612A1 WO 2004002612 A1 WO2004002612 A1 WO 2004002612A1 CH 0300391 W CH0300391 W CH 0300391W WO 2004002612 A1 WO2004002612 A1 WO 2004002612A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- filtration
- distributor
- flow
- filtration modules
- cross
- Prior art date
Links
- 238000001914 filtration Methods 0.000 title claims abstract description 87
- 230000007423 decrease Effects 0.000 claims description 8
- 238000009295 crossflow filtration Methods 0.000 claims description 7
- 238000005192 partition Methods 0.000 claims 1
- 239000000835 fiber Substances 0.000 description 33
- 239000012528 membrane Substances 0.000 description 24
- 239000000203 mixture Substances 0.000 description 17
- 239000000126 substance Substances 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 5
- 235000013399 edible fruits Nutrition 0.000 description 4
- 238000010276 construction Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 230000000903 blocking effect Effects 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 229940126214 compound 3 Drugs 0.000 description 2
- 235000015203 fruit juice Nutrition 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000012465 retentate Substances 0.000 description 2
- 238000011144 upstream manufacturing Methods 0.000 description 2
- 239000002028 Biomass Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000001427 coherent effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D65/00—Accessories or auxiliary operations, in general, for separation processes or apparatus using semi-permeable membranes
- B01D65/08—Prevention of membrane fouling or of concentration polarisation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/14—Ultrafiltration; Microfiltration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/14—Ultrafiltration; Microfiltration
- B01D61/18—Apparatus therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/14—Ultrafiltration; Microfiltration
- B01D61/20—Accessories; Auxiliary operations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D65/00—Accessories or auxiliary operations, in general, for separation processes or apparatus using semi-permeable membranes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2321/00—Details relating to membrane cleaning, regeneration, sterilization or to the prevention of fouling
- B01D2321/20—By influencing the flow
- B01D2321/2008—By influencing the flow statically
- B01D2321/2025—Tangential inlet
Definitions
- the invention relates to a device for crossflow filtration according to the preamble of claim 1.
- Such systems are used advantageously when it comes to filtering molecularly disperse i or colloidally disperse substance mixtures with proportions of solid or suspended substances.
- mixtures of substances are mixtures of substances which initially arise in the production of fruit and fruit juices. These mixtures of substances are then separated on the one hand by filtration into clear fruit or fruit juice and on the other hand the essentially remaining turbid substances.
- a plant for cross-flow filtration is known from WO-A 1-01 / 51186.
- a solution is shown here how blockages of the filtration module can be removed by fixed retentate portions.
- the problem with systems of this type is that the filter elements can become blocked, so that production must be interrupted in order to first remove the blockages. Production interruptions are undesirable.
- WO-Al-00/03794 is a plant for cross-flow filtration of the type mentioned in the preamble of claim 1, in which a device for mixing fluids is connected upstream of the filter element. This solves the problem that when the filter element is flushed, some of the parallel membrane tubes of the filter element become blocked.
- the filter element is on
- WO-A1-94 / 29007 proposes a method for cleaning filtration modules in order to solve the problem that fibrous constituents of the mixture to be filtered settle on the faces of the individual parallel membrane tubes if the mixture to be filtered has a high fiber content.
- By reversing the direction of flow in the filtration module such deposits of fibers are released again.
- the reversal of the flow direction means an undesirable interference in the continuous production process and reduces the performance of the filtration system.
- Filtration systems are known from US Pat. No. 1-6,221,249 and US Pat. No. 3,387,270, in which the tangential velocity of the medium to be filtered on a membrane remains constant over its length. This is achieved in that the cross section for the passage of the medium to be filtered continuously decreases from the entrance of the membrane module to its exit.
- the invention has for its object to provide a device for cross-flow filtration, which is suitable for processing mixtures with a high fiber content and in which the risk of clogging of membrane tubes by fibers is so significantly reduced that there is an increase in production output.
- FIG. 2 shows a first diagram of a filtration system according to the invention
- FIG. 5 shows a second exemplary embodiment of a distributor
- Fig. 6 shows a third embodiment
- Fig. 1 shows a longitudinal section through a bundle of membrane tubes.
- 1 means a filtration module of a device for cross-flow filtration, in which several membrane tubes 2 are combined to form a bundle, which together form the filtration module 1.
- Such filtration modules 1 are known as linear modules.
- the membrane tubes 2 are fastened on the end face in a module housing 4 by means of a casting compound 3.
- the mixture to be filtered is fed to the filtration module 1 through a connecting pipe 5. With arrows is that Flow direction of the mixture to be filtered is shown. If the mixture to be filtered contains fibers 6 in large numbers, then fiber packs 7 can be built up on the annular end faces of the membrane tubes 2 and the parts of the sealing compound surrounding them, which bundles consist of a large number of fibers 6.
- Reduced membrane tubes 2 increases when a pump delivering the mixture to be filtered works at constant power, the flow rate at the now reduced inlet cross section. If fiber packs 7 have reached a certain size and compactness, it inevitably occurs that individual fiber packs 7 are entrained into the interior of a membrane tube 2. In this way, individual membrane tubes 2 can be blocked by fiber packs 7. This inevitably reduces the filtration performance. In the further course, more or less all membrane tubes 2 can become blocked.
- the actual aim of the invention is therefore to prevent the structure of such fiber packs 7 on the end faces of the filtration modules 1 as far as possible or as far as possible.
- the solution to the problem is to generate a flow transversely to the end face of the filtration modules 1 on the end faces of the filtration modules. This flow across the end face of the filtration modules 1 ensures that there are no areas on these end faces in which there is practically no flow. It has been shown that the construction of fiber bundles 7 can be prevented in an impressively simple manner.
- FIG. 2 shows a first scheme of the solution according to the invention. It shows a filter unit 10, which consists of filtration modules 1 connected in parallel. Each such filtration module 1 can be a single membrane tube 2 (FIG. 1) or a bundle of several parallel membrane tubes 2, as shown in FIG. 1.
- a distributor 20 is connected on the input side to the filter unit 10. There is a connection from this distributor 20 to each filtration module 1.
- the distributor 20 of this exemplary embodiment is a closed circuit which is known per se and to which the mixture to be filtered is fed through a feed pipe 22.
- a discharge pipe 23 is also shown in FIG. 2, in which the retentate leaving the filtration modules 1 is collected and, for example, returned to a batch tank (not shown), as is known.
- a feed pump 24 is arranged in the feed pipe 22 in a known manner, which pumps the mixture to be filtered and generates the pressure required for the filtration.
- Means are present in the distributor 20 by means of which the mixture to be filtered is forced to circulate in the distributor 20.
- These means can be, for example, an injector 25 or a circulation pump 26, as is also known.
- the distributor 20 is designed such that a flow arises transversely to the end face of the filtration modules 1 on the end faces of the individual filtration modules 1. This is achieved by means of the injector 25 or the circulation pump 26. Since these two elements can alternatively be present, they are shown in dashed lines in FIG. 2. , The flow across the end face of the filtration modules 1 reliably prevents the formation of fiber packs 7 (FIG. 1) at the entrances of the individual filtration modules 1.
- the flow transverse to the end face of the filtration modules 1 on all filtration modules 1 is approximately constant. This is achieved in that the cross section Q of the distributor 20 decreases from the branch to the first filtration module 1.1 to the branch to the last filtration module 1.n, as is shown in FIG. 3. At the branch to the first filtration module 1.1, the cross section Q has the value Qi, at the branch to the second filtration module 1.2 the value Q 2 and at the branch to the last filtration module 1.n the value Q n .
- the decrease in the cross section Q of the distributor 20 is advantageously such that the flow velocity v im over the entire length of the distributor 20 from the branch to the first filtration module 1.1 to the branch to the last filtration module 1.n.
- Distributor 20 remains constant. Thus, over the length of the distributor 20 from the branch to the first filtration module 1.1 to the branch to the last filtration module, there is an approximately constant flow transversely to the end face of the filtration modules 1. In this way, the structure of fiber packs 7 (FIG individual filtration modules 1 prevented even more securely.
- the constant flow rate is achieved by reducing the cross-section Q at each branch. If the cross section Q before the branch to the first filtration module 1.1 has the value Q 0 , the cross section Q behind the branch to the first filtration module 1.1 is reduced by a value Q m , for example by 1 cm 2 . Accordingly, the cross-section is reduced by the value Q m after each branch. This ensures that the flow velocity across the end face of the filtration modules 1 remains approximately constant from the first branch to the last branch.
- the size of the value Q m is determined not only by the cross section of the individual filtration modules 1, but also by the ratio of the flow velocity across the filtration modules 1 to the flow velocity through the filtration modules 1.
- the pump 26 is a means for adjusting the flow speed transverse to the end face of the filtration modules 1. If the speed of rotation is increased, this flow speed increases, if it is reduced, the flow speed drops. In this respect, the pump 26 is a more advantageous means than the injector 25.
- FIG. 4 shows a distributor 20 'which does not form a closed circuit with a pump 21, but is a linear distributor. It therefore has a dead end E at which there is no flow across the last branch.
- an additional drain line 30, which leads back, for example, to the batch tank (not shown), ensures that a ln the branch to the last filtration module There is a current across the last branch. The end E is no longer a dead end.
- a throttle valve 31 is advantageously arranged in this drain line 30, by means of which it can be set how large the flow velocity is across the last branch. If this throttle valve 31 is adjustable, it is advantageously possible to vary the size of the flow velocity V E prevailing at the end E of the distributor 20 '. It can therefore be increased or decreased depending on the fiber content of the mixture to be filtered.
- the throttle valve 31 here is the means for setting the flow speed transversely to the end face of the filtration modules 1.
- 5 shows a distributor 20, 20 'in which the clear cross section of the distributor 20, 20' decreases continuously in the direction of flow.
- 5 shows an alternative exemplary embodiment of the distributor 20, 20 ', in which the clear cross section of the distributor 20, 20' decreases in stages.
- the linear distributor 20 ' can also be designed such that its cross section is constant, as is shown for the distributor 20 in FIG. 2. But then it must be ensured that the at the end E of the distributor 20 ', the flow rate V E prevailing is still so great that the build-up of fiber packs 7 (FIG. 1) is prevented.
- FIG. 7 and 8 show an exemplary embodiment for the connection of filtration modules 1 of the type already shown in FIG. 1, in which each filtration module 1 comprises a bundle of membrane tubes 2 arranged in parallel.
- 6 shows a longitudinal section through the distributor 20, 20 '
- FIG. 7 shows a cross section. 7, the central longitudinal axis of the distributor 20, 20 'is designated by M.
- the special feature of this exemplary embodiment is that the end face of the filtration modules 1 is arranged approximately centrally in the cross section of the distributor 20, 20 '.
- a perforated separating plate 40 is arranged in the center of the distributor 20, 20 ′ and lies flush with the end faces of the filtration modules 1. Flanges with which the individual filtration modules 1 are attached to the distributor 20, 20 'are only indicated schematically.
- the separating plate 40 creates two separate flow paths.
- the filtration modules 1 protrude into the upper flow path, which has the consequence that the free flow cross section through the individual filtration modules 1 is reduced. As a result, there is a strongly disturbed flow in this area, which leads to turbulence.
- the lower flow path has an undisturbed semicircular cross section, so that there is an undisturbed linear flow.
- the distributor 20, 20 ' is formed by a tube, ie has a circular cross section. If the filtration modules 1 were inserted into the distributor 20, 20 'in such a way that their end face lies on a dashed line L, this would have the disadvantage that it protrudes in the region of the end faces projecting into the free cross section of the distributor 20, 20' previously mentioned turbulence comes.
Landscapes
- Engineering & Computer Science (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Filtration Of Liquid (AREA)
Abstract
Description
Claims
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/512,508 US20050173318A1 (en) | 2002-06-26 | 2003-06-17 | Device for cross-current filtration |
EP03727122A EP1515793A1 (de) | 2002-06-26 | 2003-06-17 | Vorrichtung zur querstromfiltration |
AU2003233905A AU2003233905B2 (en) | 2002-06-26 | 2003-06-17 | Device for cross-current filtration |
CA002490906A CA2490906C (en) | 2002-06-26 | 2003-06-17 | Device for cross-flow filtration |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH10992002 | 2002-06-26 | ||
CH1099/02 | 2002-06-26 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2004002612A1 true WO2004002612A1 (de) | 2004-01-08 |
Family
ID=29783970
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/CH2003/000391 WO2004002612A1 (de) | 2002-06-26 | 2003-06-17 | Vorrichtung zur querstromfiltration |
Country Status (7)
Country | Link |
---|---|
US (1) | US20050173318A1 (de) |
EP (1) | EP1515793A1 (de) |
CN (1) | CN1331576C (de) |
AU (1) | AU2003233905B2 (de) |
CA (1) | CA2490906C (de) |
PL (1) | PL373075A1 (de) |
WO (1) | WO2004002612A1 (de) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20130034590A1 (en) * | 2009-03-02 | 2013-02-07 | Ijeoma Uchegbu | Delivery of Hydrophilic Drugs |
ITVE20110081A1 (it) * | 2011-12-16 | 2013-06-17 | Della Toffola Spa | Dispositivo di pulizia per moduli di filtrazione tangenziale, particolarmente per l'asportazione di residui di filtrazione.- |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20090152180A1 (en) * | 2005-10-24 | 2009-06-18 | Kazuhisa Nishimori | Large Scale Membrane Separating Device |
WO2009139904A1 (en) * | 2008-05-14 | 2009-11-19 | Proteonomix, Inc. | Methods and devices for isolating embryonic stem cells |
KR20100001493A (ko) * | 2008-06-27 | 2010-01-06 | 주식회사 코오롱 | 여과막 모듈용 헤더 및 그것을 이용한 여과막 모듈 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2046645C1 (ru) * | 1992-04-07 | 1995-10-27 | Юрий Васильевич Тахистов | Мембранный аппарат |
JPH11239719A (ja) * | 1998-02-26 | 1999-09-07 | Asahi Chem Ind Co Ltd | 濾過膜モジュールの配管構造 |
WO2000003794A1 (de) * | 1998-07-13 | 2000-01-27 | Bucher-Guyer Ag | Verfahren und vorrichtung zur vermischung von fluiden in einer leitung |
US6221249B1 (en) * | 1996-01-17 | 2001-04-24 | Genentech, Inc. | Tangential-flow filtration system |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4038191A (en) * | 1975-10-14 | 1977-07-26 | Davis Harold R | Manifold for ultra filtration machine |
US5162101A (en) * | 1989-01-13 | 1992-11-10 | Minntech Corporation | Oxygenator wedge configuration |
EP0447513B1 (de) * | 1989-09-29 | 1997-01-29 | Memtec Limited | Sammelleitung für filterpatronen |
GB9214037D0 (en) * | 1992-07-01 | 1992-08-12 | Ici Plc | Membrane system |
ATE226473T1 (de) * | 1994-06-22 | 2002-11-15 | Fls Miljo As | Vorrichtung zur massenübertragung |
-
2003
- 2003-06-17 CN CNB038147726A patent/CN1331576C/zh not_active Expired - Fee Related
- 2003-06-17 AU AU2003233905A patent/AU2003233905B2/en not_active Ceased
- 2003-06-17 US US10/512,508 patent/US20050173318A1/en not_active Abandoned
- 2003-06-17 EP EP03727122A patent/EP1515793A1/de not_active Withdrawn
- 2003-06-17 PL PL03373075A patent/PL373075A1/xx unknown
- 2003-06-17 CA CA002490906A patent/CA2490906C/en not_active Expired - Fee Related
- 2003-06-17 WO PCT/CH2003/000391 patent/WO2004002612A1/de not_active Application Discontinuation
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2046645C1 (ru) * | 1992-04-07 | 1995-10-27 | Юрий Васильевич Тахистов | Мембранный аппарат |
US6221249B1 (en) * | 1996-01-17 | 2001-04-24 | Genentech, Inc. | Tangential-flow filtration system |
US6387270B1 (en) * | 1996-01-17 | 2002-05-14 | Genentech, Inc. | Tangential-flow filtration system |
JPH11239719A (ja) * | 1998-02-26 | 1999-09-07 | Asahi Chem Ind Co Ltd | 濾過膜モジュールの配管構造 |
WO2000003794A1 (de) * | 1998-07-13 | 2000-01-27 | Bucher-Guyer Ag | Verfahren und vorrichtung zur vermischung von fluiden in einer leitung |
Non-Patent Citations (2)
Title |
---|
DATABASE WPI Section Ch Week 199626, Derwent World Patents Index; Class J01, AN 1996-257849, XP002232983 * |
PATENT ABSTRACTS OF JAPAN vol. 1999, no. 14 22 December 1999 (1999-12-22) * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20130034590A1 (en) * | 2009-03-02 | 2013-02-07 | Ijeoma Uchegbu | Delivery of Hydrophilic Drugs |
US8920819B2 (en) * | 2009-03-02 | 2014-12-30 | University College London | Delivery of hydrophilic drugs |
ITVE20110081A1 (it) * | 2011-12-16 | 2013-06-17 | Della Toffola Spa | Dispositivo di pulizia per moduli di filtrazione tangenziale, particolarmente per l'asportazione di residui di filtrazione.- |
Also Published As
Publication number | Publication date |
---|---|
AU2003233905B2 (en) | 2008-03-20 |
US20050173318A1 (en) | 2005-08-11 |
PL373075A1 (en) | 2005-08-08 |
AU2003233905A2 (en) | 2004-01-19 |
AU2003233905A1 (en) | 2004-01-19 |
CA2490906C (en) | 2009-09-01 |
CN1662294A (zh) | 2005-08-31 |
EP1515793A1 (de) | 2005-03-23 |
CN1331576C (zh) | 2007-08-15 |
CA2490906A1 (en) | 2004-01-08 |
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